#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210970.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210970_Fobs loop_ _publ_author_name 'Boufas, Sihem' 'Merazig, Hocine' 'Bendjeddou, Lamia' 'Beghidja, Adel' 'D\'en\'es, Georges' _publ_section_title ; Naphthalene-1,5-diammonium dichloride ; _journal_coeditor_code DN2077 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5268 _journal_page_last o5270 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.394 _cell_angle_gamma 90.000 _cell_length_a 8.5766 _cell_length_b 5.1650 _cell_length_c 12.2001 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7119 _[local]_cod_data_source_file dn2077Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lch8 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 76.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1.32 0.81 1.04 o 2 0 0 1881.97 2021.46 75.84 o 3 0 0 1302.64 1491.65 64.96 o 4 0 0 1151.54 1348.21 53.62 o 5 0 0 131.14 169.49 10.47 o 6 0 0 41.99 45.98 3.57 o 7 0 0 26.23 33.49 1.79 o 8 0 0 634.56 586.56 33.34 o 9 0 0 162.14 184.50 16.06 o 10 0 0 377.31 383.10 30.31 o 11 0 0 300.51 299.80 38.73 o 1 1 0 2008.85 1852.35 37.06 o 2 1 0 2770.76 2604.52 48.71 o 3 1 0 1569.05 1587.58 35.02 o 4 1 0 1157.53 1201.65 28.07 o 5 1 0 165.20 145.16 4.37 o 6 1 0 513.19 485.60 19.52 o 7 1 0 318.30 320.77 12.32 o 8 1 0 383.16 365.58 15.69 o 9 1 0 3.84 2.10 4.22 o 10 1 0 8.10 12.00 4.63 o 11 1 0 15.58 9.54 9.56 o 0 2 0 4567.48 4246.14 202.60 o 1 2 0 2097.24 2019.02 42.61 o 2 2 0 215.19 205.39 4.19 o 3 2 0 263.72 264.88 5.40 o 4 2 0 0.94 3.43 0.88 o 5 2 0 57.51 54.98 2.39 o 6 2 0 79.33 81.44 3.67 o 7 2 0 184.55 181.02 5.41 o 8 2 0 235.79 224.15 11.41 o 9 2 0 139.93 131.60 9.82 o 10 2 0 369.94 410.67 34.97 o 11 2 0 63.33 60.55 6.45 o 1 3 0 305.47 299.72 6.18 o 2 3 0 457.92 460.22 8.10 o 3 3 0 299.41 283.30 8.62 o 4 3 0 359.67 357.54 8.53 o 5 3 0 138.11 136.93 4.29 o 6 3 0 140.70 134.16 5.01 o 7 3 0 340.61 349.29 12.39 o 8 3 0 47.28 45.64 8.33 o 9 3 0 24.80 28.92 5.80 o 10 3 0 0.10 6.69 5.68 o 0 4 0 233.71 217.61 10.47 o 1 4 0 463.37 459.19 11.97 o 2 4 0 103.76 100.69 3.75 o 3 4 0 9.42 8.91 0.77 o 4 4 0 14.98 20.03 1.63 o 5 4 0 0.01 0.67 1.20 o 6 4 0 2.21 1.78 1.19 o 7 4 0 3.44 5.10 2.25 o 8 4 0 71.70 70.18 5.54 o 9 4 0 86.65 112.67 14.84 o 1 5 0 40.95 42.40 2.93 o 2 5 0 19.30 18.17 1.67 o 3 5 0 62.18 61.00 3.38 o 4 5 0 22.80 24.26 2.92 o 5 5 0 47.98 46.28 3.52 o 6 5 0 7.51 11.31 3.53 o 7 5 0 110.30 122.34 11.86 o 8 5 0 0.01 -0.60 3.07 o 0 6 0 147.89 144.67 10.16 o 1 6 0 235.59 225.27 14.97 o 2 6 0 0.08 1.17 1.99 o 3 6 0 11.58 9.51 6.09 o 4 6 0 69.09 62.07 6.11 o 5 6 0 12.03 9.55 5.33 o 6 6 0 7.91 12.00 5.05 o 1 7 0 0.19 3.25 2.83 o 2 7 0 1.73 5.32 5.72 o 3 7 0 1.10 16.60 6.85 o -11 1 1 1.09 0.27 7.76 o -10 1 1 0.00 5.08 7.00 o -9 1 1 20.78 19.02 2.54 o -8 1 1 0.74 0.85 1.73 o -7 1 1 7.37 8.05 1.78 o -6 1 1 27.68 25.54 3.29 o -5 1 1 57.95 49.18 2.39 o -4 1 1 135.74 152.71 4.70 o -3 1 1 37.54 37.31 1.20 o -2 1 1 545.97 540.59 13.85 o -1 1 1 243.04 256.21 5.72 o 0 1 1 293.77 290.63 6.60 o 1 1 1 125.30 140.88 2.43 o 2 1 1 0.06 0.31 0.30 o 3 1 1 86.89 97.25 2.35 o 4 1 1 33.30 39.95 1.59 o 5 1 1 89.82 96.75 2.74 o 6 1 1 13.42 13.41 0.90 o 7 1 1 89.99 79.45 6.21 o 8 1 1 1.23 1.66 3.81 o 9 1 1 18.87 14.20 2.52 o 10 1 1 1.95 5.97 4.27 o 11 1 1 25.65 47.79 12.09 o -11 2 1 19.31 18.04 4.49 o -10 2 1 14.63 13.00 4.43 o -9 2 1 37.12 37.81 4.63 o -8 2 1 25.36 22.03 3.45 o -7 2 1 56.92 60.64 3.21 o -6 2 1 65.78 64.81 5.93 o -5 2 1 214.39 216.73 6.29 o -4 2 1 105.52 106.34 2.98 o -3 2 1 3.80 3.93 0.49 o -2 2 1 0.34 0.21 0.20 o -1 2 1 687.42 693.19 14.66 o 0 2 1 60.75 60.53 1.26 o 1 2 1 1013.68 1006.71 20.01 o 2 2 1 22.40 30.47 0.85 o 3 2 1 271.79 288.22 6.31 o 4 2 1 298.20 291.81 7.29 o 5 2 1 26.09 24.72 1.80 o 6 2 1 489.40 481.92 16.63 o 7 2 1 144.42 136.97 5.99 o 8 2 1 25.75 20.69 3.05 o 9 2 1 1.43 3.93 3.75 o 10 2 1 118.59 126.63 12.10 o 11 2 1 3.37 1.96 3.76 o -10 3 1 21.44 21.38 5.34 o -9 3 1 80.53 90.94 6.52 o -8 3 1 19.29 17.27 2.03 o -7 3 1 314.53 302.59 11.93 o -6 3 1 544.39 535.47 20.36 o -5 3 1 677.51 699.89 23.35 o -4 3 1 222.80 236.72 7.31 o -3 3 1 92.62 75.75 2.37 o -2 3 1 1791.44 1847.97 41.28 o -1 3 1 45.89 38.51 1.49 o 0 3 1 106.91 108.72 3.57 o 1 3 1 50.57 63.35 1.58 o 2 3 1 209.66 234.40 4.77 o 3 3 1 173.97 179.74 4.21 o 4 3 1 30.46 31.03 1.45 o 5 3 1 3.17 4.52 0.93 o 6 3 1 721.98 735.91 22.45 o 7 3 1 72.46 76.94 3.72 o 8 3 1 96.06 92.73 6.51 o 9 3 1 78.70 78.26 6.55 o 10 3 1 4.14 4.16 4.52 o -9 4 1 67.60 70.01 11.16 o -8 4 1 66.81 64.71 7.78 o -7 4 1 75.59 77.99 4.08 o -6 4 1 117.88 119.15 5.81 o -5 4 1 268.64 269.90 12.44 o -4 4 1 140.89 139.32 4.04 o -3 4 1 0.23 2.80 1.03 o -2 4 1 8.25 8.08 1.09 o -1 4 1 345.58 341.56 9.34 o 0 4 1 357.26 344.98 8.74 o 1 4 1 320.68 326.39 6.95 o 2 4 1 68.96 64.71 2.15 o 3 4 1 397.96 418.74 10.23 o 4 4 1 171.36 174.29 4.86 o 5 4 1 33.93 34.84 2.27 o 6 4 1 283.27 280.80 11.84 o 7 4 1 90.72 84.10 5.05 o 8 4 1 48.05 48.47 4.04 o 9 4 1 21.28 24.47 4.54 o -8 5 1 8.13 17.54 9.95 o -7 5 1 0.00 6.27 2.15 o -6 5 1 0.66 -0.35 1.59 o -5 5 1 44.22 46.19 3.79 o -4 5 1 429.39 420.68 21.59 o -3 5 1 257.85 253.51 9.33 o -2 5 1 371.87 367.59 12.20 o -1 5 1 570.68 561.65 17.28 o 0 5 1 21.51 24.90 2.51 o 1 5 1 45.37 46.12 9.00 o 2 5 1 5.10 7.96 8.72 o 3 5 1 87.92 76.68 5.00 o 4 5 1 0.12 1.80 1.27 o 5 5 1 145.41 140.60 7.74 o 6 5 1 209.17 205.92 10.42 o 7 5 1 253.80 276.17 18.78 o 8 5 1 59.39 63.90 17.90 o -6 6 1 77.73 79.82 7.40 o -5 6 1 140.90 137.92 18.34 o -4 6 1 79.50 70.02 5.23 o -3 6 1 0.77 5.10 8.77 o -2 6 1 5.12 6.73 2.46 o -1 6 1 162.48 163.37 23.43 o 0 6 1 336.58 354.95 45.18 o 1 6 1 25.19 27.37 3.39 o 2 6 1 238.59 243.22 10.98 o 3 6 1 107.35 115.22 9.79 o 4 6 1 52.33 59.41 6.66 o 5 6 1 166.53 178.06 17.81 o 6 6 1 10.57 10.20 4.05 o -3 7 1 176.47 160.24 12.52 o -2 7 1 116.01 124.66 30.77 o -1 7 1 127.02 139.75 9.58 o 0 7 1 13.85 19.13 5.67 o 1 7 1 0.76 3.30 7.24 o 2 7 1 4.47 12.90 5.53 o -11 0 2 80.44 98.96 11.77 o -10 0 2 0.04 4.95 6.94 o -9 0 2 142.83 118.69 9.37 o -8 0 2 0.45 3.23 2.31 o -7 0 2 695.02 705.05 41.69 o -6 0 2 1185.96 1145.43 59.69 o -5 0 2 3104.77 3099.78 147.29 o -4 0 2 250.60 186.91 13.69 o -3 0 2 1030.95 1094.31 41.91 o -2 0 2 53.57 30.40 1.45 o -1 0 2 1443.24 1326.42 52.88 o 0 0 2 1709.19 1520.29 66.06 o 1 0 2 369.08 447.28 13.38 o 2 0 2 1066.30 1119.14 36.48 o 3 0 2 1174.51 1185.36 47.48 o 4 0 2 2507.36 2539.23 134.71 o 5 0 2 1973.32 1935.68 95.58 o 6 0 2 195.08 198.78 19.11 o 7 0 2 105.27 120.33 10.85 o 8 0 2 0.18 -1.72 3.59 o 9 0 2 8.46 10.62 4.97 o 10 0 2 0.32 -0.12 4.45 o 11 0 2 24.64 30.80 10.74 o -11 1 2 46.02 50.21 7.03 o -10 1 2 87.85 114.13 17.92 o -9 1 2 270.20 287.32 15.14 o -8 1 2 181.66 206.59 8.86 o -7 1 2 407.57 387.28 13.12 o -6 1 2 26.84 27.48 1.68 o -5 1 2 26.54 23.74 1.24 o -4 1 2 2250.99 2338.82 59.24 o -3 1 2 822.03 798.67 17.94 o -2 1 2 1393.95 1428.22 38.17 o -1 1 2 4916.62 4781.04 152.93 o 0 1 2 728.74 657.34 14.84 o 1 1 2 5565.82 5237.76 109.11 o 2 1 2 2086.35 1999.32 37.46 o 3 1 2 139.00 134.51 3.00 o 4 1 2 314.67 372.90 9.89 o 5 1 2 316.27 331.55 14.57 o 6 1 2 759.37 754.69 25.26 o 7 1 2 353.91 342.18 13.21 o 8 1 2 95.61 101.81 5.67 o 9 1 2 344.18 344.78 18.04 o 10 1 2 32.36 33.56 8.15 o 11 1 2 42.46 37.52 6.13 o -11 2 2 1.46 6.06 12.82 o -10 2 2 8.52 9.64 6.40 o -9 2 2 50.27 47.91 3.68 o -8 2 2 74.80 78.03 4.56 o -7 2 2 89.64 100.77 6.98 o -6 2 2 1483.48 1483.96 48.29 o -5 2 2 764.49 787.11 22.32 o -4 2 2 531.70 510.94 12.64 o -3 2 2 602.63 622.14 14.04 o -2 2 2 85.07 104.36 2.66 o -1 2 2 1.15 3.31 0.59 o 0 2 2 5.48 7.97 0.46 o 1 2 2 1.09 5.38 0.47 o 2 2 2 1053.17 1076.22 20.12 o 3 2 2 801.74 765.51 15.05 o 4 2 2 1007.05 1009.06 21.51 o 5 2 2 1637.23 1602.46 39.12 o 6 2 2 17.44 19.53 1.53 o 7 2 2 137.69 131.86 6.11 o 8 2 2 0.72 2.29 1.60 o 9 2 2 6.85 8.81 3.45 o 10 2 2 2.76 5.18 5.38 o -10 3 2 35.99 28.60 3.86 o -9 3 2 104.35 97.27 8.52 o -8 3 2 66.77 71.84 5.26 o -7 3 2 95.39 101.84 6.21 o -6 3 2 81.51 81.09 3.95 o -5 3 2 143.20 149.58 6.82 o -4 3 2 161.34 163.04 6.23 o -3 3 2 444.74 453.38 15.35 o -2 3 2 711.47 698.48 18.77 o -1 3 2 164.87 164.00 4.89 o 0 3 2 481.62 447.27 8.79 o 1 3 2 433.00 419.88 8.95 o 2 3 2 566.13 571.97 12.02 o 3 3 2 116.99 112.00 2.69 o 4 3 2 4.14 5.01 0.89 o 5 3 2 46.54 45.41 1.73 o 6 3 2 327.31 334.76 11.89 o 7 3 2 94.42 95.52 4.73 o 8 3 2 88.59 93.97 5.25 o 9 3 2 82.88 82.90 6.17 o 10 3 2 23.61 14.89 3.63 o -10 4 2 4.88 14.33 13.18 o -9 4 2 0.01 3.46 4.85 o -8 4 2 51.93 51.68 7.38 o -7 4 2 73.20 73.13 4.06 o -6 4 2 115.58 119.65 5.94 o -5 4 2 374.96 383.13 14.11 o -4 4 2 84.76 88.76 4.03 o -3 4 2 35.39 37.35 2.87 o -2 4 2 48.63 48.42 2.26 o -1 4 2 52.70 51.99 2.24 o 0 4 2 15.41 18.45 1.34 o 1 4 2 67.37 69.17 2.08 o 2 4 2 35.09 34.29 1.34 o 3 4 2 302.90 318.92 7.78 o 4 4 2 324.10 323.07 9.27 o 5 4 2 56.27 56.50 2.87 o 6 4 2 325.01 325.86 11.53 o 7 4 2 45.72 46.63 3.68 o 8 4 2 56.93 58.36 4.13 o 9 4 2 0.13 1.69 2.42 o -8 5 2 17.43 13.53 5.22 o -7 5 2 0.46 5.82 4.06 o -6 5 2 26.28 26.04 4.05 o -5 5 2 76.22 72.84 4.81 o -4 5 2 0.24 1.75 1.79 o -3 5 2 81.16 83.09 4.06 o -2 5 2 182.96 183.44 5.93 o -1 5 2 31.89 32.99 2.20 o 0 5 2 379.38 385.36 15.11 o 1 5 2 0.34 5.83 2.94 o 2 5 2 42.89 45.07 2.63 o 3 5 2 94.22 96.36 4.42 o 4 5 2 14.85 10.77 1.85 o 5 5 2 0.06 2.08 2.11 o 6 5 2 20.56 33.60 4.60 o 7 5 2 10.17 6.72 4.74 o 8 5 2 29.22 32.49 10.05 o -6 6 2 22.44 26.48 10.07 o -5 6 2 0.27 4.74 6.78 o -4 6 2 62.50 63.09 12.32 o -3 6 2 13.37 14.79 3.53 o -2 6 2 1.96 7.90 4.57 o -1 6 2 17.35 15.95 2.40 o 0 6 2 55.74 60.62 4.75 o 1 6 2 16.69 16.66 7.36 o 2 6 2 8.78 13.80 4.08 o 3 6 2 24.45 29.63 4.22 o 4 6 2 3.53 7.76 4.08 o 5 6 2 6.46 11.75 4.40 o 6 6 2 14.05 17.68 5.88 o -3 7 2 14.07 -0.57 14.01 o -2 7 2 0.63 -0.46 4.22 o -1 7 2 8.66 8.95 3.71 o 0 7 2 36.28 38.75 5.69 o 1 7 2 12.90 22.15 6.44 o 2 7 2 0.00 15.01 5.44 o -11 1 3 13.23 11.08 3.59 o -10 1 3 5.08 10.32 3.87 o -9 1 3 3.01 5.29 3.27 o -8 1 3 89.05 81.49 6.40 o -7 1 3 4.26 7.92 1.67 o -6 1 3 68.63 65.48 3.12 o -5 1 3 72.36 80.49 3.37 o -4 1 3 132.81 161.22 4.86 o -3 1 3 32.19 38.14 1.39 o -2 1 3 88.55 99.09 2.47 o -1 1 3 679.65 713.50 17.88 o 0 1 3 2703.11 2682.56 62.99 o 1 1 3 289.21 317.95 7.19 o 2 1 3 633.26 626.99 13.98 o 3 1 3 156.43 160.53 4.22 o 4 1 3 87.76 95.48 3.41 o 5 1 3 195.13 210.14 7.28 o 6 1 3 212.29 210.20 7.96 o 7 1 3 55.65 54.54 3.35 o 8 1 3 20.75 15.52 5.93 o 9 1 3 15.07 17.54 4.02 o 10 1 3 0.72 2.71 12.77 o 11 1 3 50.85 43.25 6.24 o -11 2 3 1.43 -0.42 3.99 o -10 2 3 114.59 139.03 9.95 o -9 2 3 0.06 3.32 2.33 o -8 2 3 23.61 20.88 4.92 o -7 2 3 59.85 61.30 5.90 o -6 2 3 755.66 754.43 26.49 o -5 2 3 1.30 3.03 2.32 o -4 2 3 67.38 63.25 2.51 o -3 2 3 629.72 674.58 17.31 o -2 2 3 3.59 11.56 1.16 o -1 2 3 324.77 332.41 6.71 o 0 2 3 435.35 455.05 9.12 o 1 2 3 29.30 31.71 0.89 o 2 2 3 350.20 373.73 6.51 o 3 2 3 3.75 3.35 0.55 o 4 2 3 294.24 304.54 7.57 o 5 2 3 216.04 211.57 7.17 o 6 2 3 0.05 2.41 1.24 o 7 2 3 51.67 54.50 4.72 o 8 2 3 99.47 97.56 5.84 o 9 2 3 4.01 7.36 3.03 o 10 2 3 16.34 13.59 3.54 o -10 3 3 128.56 139.61 11.61 o -9 3 3 23.44 22.84 2.50 o -8 3 3 171.79 178.87 9.44 o -7 3 3 389.40 392.68 19.12 o -6 3 3 0.13 2.22 1.17 o -5 3 3 55.25 59.03 3.15 o -4 3 3 1.32 1.68 1.20 o -3 3 3 23.34 26.97 1.25 o -2 3 3 7.02 6.85 0.36 o -1 3 3 45.64 44.71 1.62 o 0 3 3 726.73 718.32 15.58 o 1 3 3 346.03 337.16 6.63 o 2 3 3 593.72 596.96 11.23 o 3 3 3 239.97 230.96 5.20 o 4 3 3 5.99 6.44 0.90 o 5 3 3 11.93 13.24 3.04 o 6 3 3 48.91 45.08 2.24 o 7 3 3 0.22 0.11 1.50 o 8 3 3 10.58 10.65 2.93 o 9 3 3 48.93 54.13 4.95 o 10 3 3 34.74 32.45 5.19 o -10 4 3 133.99 118.45 19.89 o -9 4 3 0.01 -2.53 2.53 o -8 4 3 0.57 2.78 6.13 o -7 4 3 0.01 0.58 4.38 o -6 4 3 613.59 631.46 37.58 o -5 4 3 39.77 42.78 8.55 o -4 4 3 143.89 155.79 7.36 o -3 4 3 450.94 443.89 28.38 o -2 4 3 87.30 80.77 4.84 o -1 4 3 177.59 182.60 4.75 o 0 4 3 386.72 383.43 10.41 o 1 4 3 8.83 10.60 0.88 o 2 4 3 264.40 272.89 7.99 o 3 4 3 14.51 18.02 1.20 o 4 4 3 453.74 430.36 13.86 o 5 4 3 261.72 269.34 9.22 o 6 4 3 6.32 7.82 1.26 o 7 4 3 113.05 106.36 13.27 o 8 4 3 96.03 102.61 7.89 o 9 4 3 3.28 3.31 4.64 o -8 5 3 233.10 213.61 28.93 o -7 5 3 139.43 134.90 14.48 o -6 5 3 87.60 90.17 8.09 o -5 5 3 0.88 5.45 4.29 o -4 5 3 17.43 18.05 6.56 o -3 5 3 6.28 9.86 2.63 o -2 5 3 82.57 80.95 3.58 o -1 5 3 0.88 3.58 2.35 o 0 5 3 532.18 532.88 17.16 o 1 5 3 364.53 376.59 11.76 o 2 5 3 359.34 357.80 12.58 o 3 5 3 229.36 219.27 8.69 o 4 5 3 22.21 29.38 3.61 o 5 5 3 4.64 9.91 8.64 o 6 5 3 36.25 29.01 9.29 o 7 5 3 6.12 10.62 19.27 o -6 6 3 88.09 87.18 10.65 o -5 6 3 134.47 172.18 15.99 o -4 6 3 65.39 74.08 6.90 o -3 6 3 146.69 163.22 16.33 o -2 6 3 123.08 139.35 22.44 o -1 6 3 62.43 68.36 5.97 o 0 6 3 224.11 228.40 10.34 o 1 6 3 0.04 8.45 9.51 o 2 6 3 39.62 39.12 3.04 o 3 6 3 48.89 49.92 3.82 o 4 6 3 209.11 202.31 14.68 o 5 6 3 121.32 122.88 7.76 o -2 7 3 4.74 14.98 8.01 o -1 7 3 90.01 85.91 12.07 o 0 7 3 4.22 6.84 3.09 o 1 7 3 511.38 485.46 25.96 o -12 0 4 217.03 204.90 29.56 o -11 0 4 199.45 208.60 22.06 o -10 0 4 228.20 209.85 16.20 o -9 0 4 223.25 197.57 13.90 o -8 0 4 26.00 30.56 13.56 o -7 0 4 32.59 30.20 4.37 o -6 0 4 13.74 10.27 1.58 o -5 0 4 88.62 84.63 4.13 o -4 0 4 57.90 58.53 2.64 o -3 0 4 1349.18 1398.74 52.10 o -2 0 4 4753.42 4589.81 162.96 o -1 0 4 2782.72 2641.37 111.37 o 0 0 4 5812.04 5335.24 185.71 o 1 0 4 193.22 189.55 10.75 o 2 0 4 0.40 1.95 0.83 o 3 0 4 1.83 1.87 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