#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210974.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210974_Fobs loop_ _publ_author_name 'Naveen, S.' 'Sadashiva, M. P.' 'Rangappa, K. S.' 'Sridhar, M. A.' 'Shashidhara Prasad, J.' _publ_section_title ; 2-Methyl-N-(3,4,5-trimethoxybenzylidene)aniline N-oxide ; _journal_coeditor_code DN3023 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4793 _journal_page_last o4795 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.283 _cell_angle_gamma 90.000 _cell_length_a 7.5320 _cell_length_b 8.2560 _cell_length_c 12.8720 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8401 _[local]_cod_data_source_file dn3023Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sr1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 71.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10.49 9.11 0.32 o 3 0 0 22.03 19.80 0.57 o 4 0 0 409.42 405.85 9.16 o 5 0 0 12.12 12.57 0.38 o 6 0 0 45.84 49.37 0.98 o 7 0 0 0.00 0.70 0.16 o 8 0 0 0.06 0.47 0.16 o 2 1 0 331.49 340.61 5.41 o 4 1 0 73.27 67.83 1.37 o 5 1 0 123.81 124.79 1.88 o 6 1 0 160.82 184.07 3.02 o 7 1 0 58.67 64.57 3.03 o 8 1 0 5.59 5.73 0.66 o 0 2 0 262.22 282.18 8.37 o 2 2 0 223.53 224.72 7.65 o 3 2 0 501.95 491.84 7.62 o 4 2 0 138.15 138.52 4.90 o 5 2 0 0.84 0.86 0.08 o 6 2 0 7.17 7.12 0.71 o 7 2 0 18.90 19.98 2.28 o 8 2 0 0.46 0.26 0.10 o 1 3 0 220.42 212.88 2.45 o 2 3 0 668.18 603.63 13.15 o 3 3 0 198.17 187.41 8.50 o 4 3 0 17.71 18.72 0.79 o 5 3 0 64.11 63.44 1.27 o 6 3 0 209.65 208.55 9.07 o 7 3 0 5.48 6.25 0.41 o 8 3 0 3.09 2.57 0.38 o 0 4 0 152.19 150.07 2.86 o 1 4 0 72.82 69.61 1.64 o 2 4 0 142.55 138.33 6.43 o 3 4 0 80.13 85.15 3.09 o 4 4 0 10.02 8.36 0.77 o 5 4 0 99.20 98.84 3.14 o 6 4 0 62.04 64.72 4.48 o 7 4 0 16.85 17.29 0.96 o 8 4 0 6.98 8.20 1.01 o 1 5 0 39.98 39.35 0.79 o 2 5 0 15.67 17.09 0.73 o 3 5 0 19.35 20.22 1.68 o 4 5 0 191.57 207.14 3.81 o 5 5 0 27.37 31.46 0.93 o 6 5 0 22.45 21.06 0.76 o 7 5 0 16.10 16.15 0.99 o 0 6 0 33.48 39.78 0.86 o 1 6 0 6.80 6.90 0.29 o 2 6 0 20.15 20.80 1.05 o 3 6 0 245.72 261.79 12.34 o 4 6 0 47.79 49.15 1.69 o 5 6 0 11.49 11.94 1.66 o 7 6 0 8.43 11.51 1.49 o 1 7 0 3.50 4.14 0.22 o 2 7 0 3.69 3.59 0.59 o 3 7 0 90.34 99.45 2.24 o 4 7 0 5.70 6.50 0.70 o 5 7 0 2.90 5.51 0.65 o 6 7 0 0.31 0.89 0.34 o 0 8 0 20.16 21.01 1.46 o 1 8 0 2.11 1.82 0.16 o 2 8 0 64.99 71.36 1.45 o 3 8 0 0.72 0.30 0.07 o 4 8 0 9.65 11.62 0.86 o 1 9 0 0.48 0.31 0.13 o 2 9 0 19.62 18.87 0.82 o 3 9 0 8.00 7.76 0.78 o -8 0 1 55.27 53.67 1.14 o -7 0 1 34.61 36.50 0.87 o -6 0 1 235.53 242.60 6.67 o -5 0 1 112.30 112.45 2.21 o -4 0 1 43.95 45.32 1.40 o -3 0 1 29.14 27.09 0.72 o 1 0 1 4.74 4.28 0.17 o 3 0 1 136.64 146.99 3.18 o 4 0 1 186.21 188.72 2.94 o 5 0 1 147.77 154.81 2.66 o 6 0 1 0.18 0.41 0.16 o 7 0 1 2.12 1.83 0.30 o 8 0 1 0.97 0.68 0.23 o -8 1 1 0.04 0.27 0.10 o -7 1 1 35.62 37.03 0.70 o -6 1 1 133.96 127.31 4.03 o -5 1 1 76.97 82.88 1.35 o -4 1 1 67.04 70.87 1.78 o -3 1 1 121.23 138.27 1.66 o -2 1 1 1234.47 1183.25 22.69 o 0 1 1 1062.90 581.61 26.72 o 1 1 1 139.15 136.50 1.74 o 2 1 1 365.89 344.59 8.38 o 3 1 1 7.91 6.43 0.14 o 4 1 1 131.46 135.67 1.70 o 5 1 1 134.53 134.62 1.60 o 6 1 1 62.29 61.21 1.34 o 7 1 1 30.49 31.57 0.56 o 8 1 1 0.66 0.33 0.09 o -8 2 1 13.99 13.99 0.56 o -7 2 1 101.33 101.92 3.15 o -6 2 1 112.31 106.07 1.87 o -5 2 1 74.28 76.20 0.97 o -4 2 1 25.23 27.80 0.97 o -3 2 1 249.31 253.07 3.85 o -2 2 1 1680.02 1584.45 56.27 o 0 2 1 678.36 663.14 7.77 o 1 2 1 116.64 103.41 1.47 o 2 2 1 103.11 94.69 5.16 o 3 2 1 106.19 112.63 2.33 o 4 2 1 74.53 75.74 1.26 o 5 2 1 43.16 46.32 0.78 o 6 2 1 27.23 30.50 1.95 o 7 2 1 2.75 2.38 0.18 o 8 2 1 3.36 2.27 0.15 o -8 3 1 0.21 -0.08 0.25 o -7 3 1 0.25 0.02 0.42 o -6 3 1 5.56 9.31 0.59 o -5 3 1 170.30 172.00 4.77 o -4 3 1 115.54 112.75 6.80 o -3 3 1 307.39 308.35 13.07 o -2 3 1 1208.74 1139.12 17.23 o -1 3 1 413.67 392.40 4.90 o 0 3 1 137.96 132.72 2.16 o 1 3 1 8.70 7.58 0.29 o 2 3 1 260.62 256.07 11.93 o 3 3 1 573.16 601.23 30.44 o 4 3 1 86.07 89.89 1.42 o 5 3 1 1.05 0.86 0.51 o 6 3 1 58.41 42.84 2.66 o 7 3 1 2.34 2.80 0.90 o 8 3 1 0.01 0.06 0.22 o -8 4 1 1.34 1.46 0.33 o -7 4 1 6.32 5.89 0.73 o -6 4 1 16.01 16.98 0.94 o -5 4 1 165.67 185.79 4.38 o -4 4 1 118.31 126.84 2.17 o -3 4 1 582.98 581.32 30.65 o -2 4 1 462.04 485.65 8.14 o -1 4 1 23.46 22.22 1.40 o 0 4 1 130.31 130.31 4.67 o 1 4 1 146.15 136.79 2.19 o 2 4 1 100.21 99.37 1.64 o 3 4 1 6.92 5.83 0.31 o 4 4 1 52.34 54.18 1.71 o 5 4 1 22.26 24.22 0.97 o 6 4 1 0.30 0.66 0.30 o 7 4 1 6.03 7.06 0.65 o -7 5 1 1.63 2.08 0.50 o -6 5 1 1.09 1.37 0.41 o -5 5 1 18.50 18.98 2.03 o -4 5 1 280.47 282.40 17.12 o -3 5 1 144.95 145.52 8.11 o -2 5 1 67.66 73.03 2.09 o -1 5 1 29.45 30.80 0.52 o 0 5 1 56.85 60.82 0.97 o 1 5 1 97.90 104.75 1.33 o 2 5 1 91.70 86.12 3.33 o 3 5 1 57.67 58.17 1.93 o 4 5 1 84.85 91.61 2.46 o 5 5 1 52.23 53.86 3.85 o 6 5 1 1.62 2.26 0.49 o 7 5 1 4.48 5.28 0.53 o -7 6 1 0.81 0.07 0.46 o -5 6 1 4.42 4.66 0.94 o -4 6 1 19.42 21.35 1.04 o -3 6 1 70.04 70.60 3.37 o -2 6 1 43.14 46.31 1.09 o -1 6 1 25.04 26.86 1.20 o 0 6 1 7.08 7.29 0.26 o 1 6 1 128.96 140.22 7.10 o 2 6 1 3.78 2.98 0.62 o 3 6 1 103.05 107.23 3.42 o 4 6 1 44.49 44.64 1.57 o 5 6 1 13.25 12.57 0.85 o 6 6 1 3.42 2.79 0.54 o -6 7 1 0.10 0.48 0.34 o -4 7 1 89.70 99.99 2.84 o -3 7 1 49.05 48.07 1.04 o -2 7 1 2.89 2.54 0.26 o -1 7 1 4.83 4.98 0.30 o 0 7 1 13.30 15.01 0.48 o 1 7 1 22.26 22.51 0.61 o 2 7 1 25.71 27.66 3.02 o 3 7 1 50.69 52.00 1.77 o 4 7 1 16.38 17.01 1.47 o 5 7 1 1.05 1.40 0.58 o -5 8 1 2.42 3.75 0.46 o -4 8 1 4.63 5.56 0.67 o -3 8 1 14.99 15.98 0.68 o -2 8 1 2.25 2.53 0.23 o -1 8 1 2.24 2.43 0.65 o 0 8 1 6.31 6.26 0.60 o 1 8 1 6.94 7.45 0.72 o 2 8 1 170.41 191.52 3.18 o 3 8 1 17.91 16.35 2.45 o 4 8 1 8.82 10.22 0.86 o -3 9 1 4.30 3.77 0.42 o -2 9 1 10.11 9.05 1.03 o -1 9 1 2.71 2.12 0.58 o 0 9 1 1.49 1.59 0.36 o 1 9 1 28.58 28.81 2.99 o 2 9 1 0.45 0.17 0.14 o 3 9 1 16.02 13.60 1.01 o -8 0 2 80.08 86.71 1.74 o -7 0 2 39.34 46.74 1.39 o -6 0 2 12.33 12.88 0.40 o -5 0 2 1.97 2.44 0.18 o -4 0 2 26.37 36.05 0.80 o -3 0 2 2.93 3.30 0.15 o -2 0 2 13.57 15.01 0.39 o -1 0 2 1068.75 1005.38 22.57 o 1 0 2 2.04 11.80 1.10 o 2 0 2 39.69 36.80 0.68 o 3 0 2 838.71 857.99 13.64 o 4 0 2 430.86 433.92 7.13 o 5 0 2 0.57 0.91 0.19 o 6 0 2 61.82 62.52 1.23 o 7 0 2 21.23 20.86 0.86 o 8 0 2 0.51 0.38 0.16 o -8 1 2 3.07 4.03 0.33 o -7 1 2 102.13 107.79 4.20 o -6 1 2 3.87 3.96 0.56 o -5 1 2 0.23 0.19 0.08 o -4 1 2 43.21 45.45 0.65 o -3 1 2 275.68 296.75 4.98 o -2 1 2 461.71 420.76 14.60 o -1 1 2 1092.66 1003.86 13.89 o 1 1 2 361.89 321.89 3.53 o 2 1 2 348.27 329.68 4.74 o 3 1 2 358.21 374.96 4.45 o 4 1 2 55.86 54.93 0.75 o 5 1 2 135.40 132.85 1.99 o 6 1 2 189.47 198.66 2.64 o 7 1 2 16.17 14.50 0.75 o 8 1 2 2.31 1.60 0.31 o -8 2 2 0.92 0.29 0.10 o -7 2 2 35.82 35.80 0.72 o -6 2 2 211.89 220.10 5.74 o -5 2 2 35.41 36.24 2.23 o -4 2 2 93.79 88.11 2.15 o -3 2 2 212.68 201.10 3.14 o -2 2 2 223.82 222.37 3.65 o -1 2 2 1603.66 1511.02 44.70 o 0 2 2 5130.22 4655.23 129.99 o 1 2 2 320.29 300.28 7.78 o 2 2 2 118.37 112.59 3.51 o 3 2 2 651.28 642.96 16.70 o 4 2 2 56.08 45.83 2.18 o 5 2 2 43.47 40.06 0.71 o 6 2 2 7.78 6.63 0.20 o 7 2 2 13.53 12.11 0.31 o 8 2 2 7.26 7.26 0.64 o -8 3 2 2.29 1.99 0.60 o -7 3 2 12.72 12.04 1.54 o -6 3 2 148.10 154.61 5.05 o -5 3 2 37.71 39.95 0.94 o -4 3 2 9.62 11.74 0.55 o -3 3 2 291.64 294.72 18.20 o -2 3 2 619.87 642.00 24.51 o -1 3 2 188.67 178.42 2.64 o 0 3 2 281.99 266.61 8.91 o 1 3 2 162.77 148.09 4.27 o 2 3 2 294.87 302.68 14.29 o 3 3 2 74.40 74.32 3.59 o 4 3 2 1.00 0.86 0.12 o 5 3 2 30.42 29.75 0.59 o 6 3 2 8.58 7.20 0.50 o 7 3 2 7.39 5.20 1.11 o 8 3 2 0.93 0.73 0.27 o -8 4 2 3.79 4.40 1.09 o -7 4 2 6.13 6.04 0.50 o -6 4 2 4.10 4.81 0.96 o -5 4 2 51.56 51.03 3.15 o -4 4 2 43.36 46.46 1.31 o -3 4 2 792.28 739.35 15.86 o -2 4 2 39.68 40.19 1.12 o -1 4 2 632.06 630.30 17.94 o 0 4 2 276.35 293.85 8.98 o 1 4 2 17.43 17.03 0.67 o 2 4 2 92.11 99.15 2.02 o 3 4 2 2.88 2.02 0.23 o 4 4 2 29.64 27.99 0.61 o 5 4 2 4.28 5.26 0.36 o 6 4 2 13.13 12.86 0.69 o 7 4 2 0.60 0.57 0.30 o -6 5 2 6.07 5.67 0.60 o -5 5 2 6.77 6.88 0.54 o -4 5 2 99.14 107.69 5.94 o -3 5 2 47.21 45.80 2.29 o -1 5 2 32.77 35.89 0.95 o 0 5 2 156.47 156.53 4.35 o 1 5 2 1.86 1.67 0.22 o 2 5 2 80.97 77.52 2.23 o 3 5 2 0.45 0.55 0.10 o 4 5 2 20.52 21.75 1.05 o 5 5 2 15.69 14.41 1.13 o 6 5 2 17.66 18.03 1.00 o 7 5 2 3.07 4.84 0.58 o -6 6 2 11.20 12.36 1.04 o -5 6 2 44.95 44.00 2.63 o -4 6 2 135.38 135.42 3.49 o -3 6 2 36.12 35.72 1.99 o -2 6 2 10.77 11.17 0.69 o -1 6 2 9.84 8.98 0.24 o 0 6 2 61.06 66.85 1.20 o 1 6 2 77.70 79.95 5.28 o 2 6 2 17.94 17.97 0.68 o 3 6 2 3.72 3.60 0.14 o 4 6 2 2.04 1.35 0.42 o 5 6 2 1.09 1.31 0.46 o 6 6 2 2.73 3.53 0.41 o -4 7 2 32.96 32.09 1.39 o -3 7 2 6.07 4.84 0.17 o -2 7 2 22.34 22.93 0.92 o -1 7 2 1.74 1.66 0.17 o 0 7 2 15.48 15.59 0.89 o 1 7 2 10.44 12.00 0.57 o 2 7 2 40.72 44.58 1.59 o 3 7 2 44.66 38.54 0.80 o 4 7 2 6.01 5.27 0.76 o 5 7 2 8.63 9.06 0.81 o -5 8 2 1.97 1.55 0.55 o -4 8 2 3.24 3.70 0.59 o -3 8 2 2.08 1.19 0.15 o -2 8 2 1.79 1.37 0.15 o -1 8 2 1.33 1.21 0.24 o 0 8 2 1.73 1.41 0.36 o 1 8 2 17.49 17.81 1.00 o 2 8 2 17.72 18.27 0.60 o 3 8 2 14.84 14.27 0.47 o 4 8 2 2.45 2.97 0.58 o -3 9 2 2.44 2.17 0.54 o -2 9 2 5.31 4.14 0.69 o -1 9 2 2.25 1.99 0.24 o 0 9 2 5.99 6.53 0.93 o 1 9 2 31.30 31.58 2.76 o 2 9 2 5.68 5.18 0.30 o -8 0 3 55.58 58.56 1.35 o -7 0 3 68.35 75.90 1.59 o -6 0 3 0.34 0.44 0.14 o -5 0 3 2.67 2.83 0.25 o -4 0 3 103.70 103.06 2.01 o -3 0 3 239.00 241.52 8.98 o -2 0 3 32.39 27.25 0.84 o -1 0 3 315.58 301.85 7.72 o 0 0 3 52.98 47.99 0.82 o 1 0 3 715.03 693.10 10.85 o 2 0 3 2.75 3.18 0.21 o 3 0 3 195.08 202.41 3.81 o 4 0 3 22.58 24.66 0.80 o 5 0 3 43.35 43.50 0.88 o 6 0 3 106.95 105.02 3.84 o 7 0 3 61.04 66.12 1.31 o 8 0 3 4.63 3.98 0.29 o -8 1 3 10.45 9.89 0.30 o -7 1 3 34.83 36.18 0.95 o -6 1 3 0.66 0.49 0.10 o -5 1 3 25.10 24.01 1.62 o -4 1 3 207.53 228.48 3.16 o -3 1 3 388.79 405.89 5.21 o -2 1 3 45.92 49.94 1.06 o -1 1 3 254.52 240.49 4.22 o 0 1 3 2457.61 2258.80 47.31 o 1 1 3 1969.41 1839.24 37.28 o 2 1 3 498.26 459.15 7.21 o 3 1 3 407.90 446.58 11.76 o 4 1 3 46.83 46.70 0.62 o 5 1 3 28.48 32.04 1.39 o 6 1 3 22.15 21.94 0.61 o 7 1 3 11.83 11.24 0.47 o 8 1 3 1.03 0.85 0.13 o -8 2 3 17.00 16.73 0.94 o -7 2 3 33.85 37.34 0.98 o -6 2 3 91.85 94.02 1.74 o -5 2 3 6.15 6.33 0.18 o -4 2 3 229.66 245.90 3.26 o -3 2 3 360.85 390.18 4.95 o -2 2 3 767.14 737.26 10.20 o -1 2 3 318.81 308.95 5.27 o 0 2 3 471.02 464.61 13.04 o 1 2 3 108.19 99.21 5.07 o 2 2 3 671.88 657.72 15.46 o 3 2 3 11.54 11.92 0.39 o 4 2 3 19.01 20.54 0.39 o 5 2 3 6.28 8.27 0.27 o 6 2 3 30.18 29.17 1.83 o 7 2 3 11.52 11.76 0.81 o 8 2 3 0.69 0.31 0.25 o -8 3 3 2.90 3.41 0.43 o -7 3 3 11.59 9.93 0.82 o -6 3 3 35.42 39.12 0.98 o -5 3 3 49.04 46.91 1.04 o -4 3 3 62.31 63.64 3.47 o -3 3 3 11.60 11.77 1.09 o -2 3 3 267.74 298.30 10.15 o -1 3 3 53.81 49.79 1.35 o 0 3 3 324.65 305.62 16.74 o 1 3 3 217.25 196.31 5.18 o 2 3 3 427.86 428.69 17.51 o 3 3 3 12.80 15.83 0.62 o 4 3 3 9.16 8.93 0.26 o 5 3 3 0.37 0.69 0.51 o 6 3 3 9.25 8.35 1.07 o 7 3 3 8.28 6.24 0.23 o 8 3 3 1.84 1.67 0.36 o -7 4 3 3.74 2.79 0.52 o -6 4 3 52.46 55.85 2.38 o -5 4 3 70.34 72.16 1.48 o -4 4 3 77.22 78.63 1.51 o -3 4 3 82.55 83.31 2.97 o -2 4 3 5.94 6.74 0.24 o -1 4 3 509.53 513.43 14.02 o 0 4 3 15.43 17.42 0.58 o 1 4 3 252.17 264.98 5.79 o 2 4 3 58.93 61.21 0.92 o 3 4 3 46.38 47.17 0.81 o 4 4 3 19.72 17.98 0.48 o 5 4 3 7.40 6.70 0.31 o 6 4 3 0.47 0.23 0.06 o 7 4 3 2.57 1.98 0.33 o -7 5 3 2.67 3.64 0.55 o -6 5 3 3.30 3.19 0.35 o -5 5 3 19.17 21.34 2.25 o -4 5 3 176.39 175.12 2.95 o -3 5 3 3.54 4.07 0.35 o -2 5 3 40.64 43.74 1.45 o -1 5 3 83.42 94.34 3.58 o 0 5 3 50.48 54.76 0.78 o 1 5 3 46.03 53.84 2.65 o 2 5 3 22.55 22.93 0.52 o 3 5 3 14.72 13.78 0.36 o 4 5 3 20.36 18.60 1.57 o 5 5 3 5.69 5.58 0.42 o 6 5 3 1.37 1.69 0.35 o 7 5 3 1.47 1.04 0.67 o -7 6 3 5.96 9.29 0.90 o -6 6 3 2.80 3.27 0.44 o -5 6 3 30.62 28.21 1.28 o -4 6 3 70.47 69.20 2.14 o -3 6 3 70.01 74.00 2.09 o -2 6 3 63.56 66.35 2.21 o -1 6 3 6.37 6.08 0.29 o 0 6 3 19.41 19.02 0.38 o 1 6 3 55.00 59.35 0.93 o 2 6 3 51.14 52.01 0.90 o 3 6 3 24.06 24.42 0.49 o 4 6 3 16.91 16.38 1.23 o 5 6 3 2.03 2.43 0.79 o 6 6 3 1.08 0.98 0.32 o -5 7 3 25.96 30.65 1.42 o -4 7 3 0.86 0.94 0.51 o -3 7 3 7.22 7.89 0.68 o -2 7 3 1.96 1.82 0.14 o -1 7 3 3.04 3.30 0.39 o 0 7 3 41.58 43.57 1.68 o 1 7 3 22.41 25.32 1.70 o 2 7 3 20.95 20.39 1.25 o 3 7 3 16.39 14.98 1.19 o 4 7 3 2.42 2.45 0.36 o 5 7 3 2.09 2.42 0.54 o -4 8 3 4.85 5.41 0.66 o -3 8 3 1.53 0.77 0.38 o -2 8 3 0.27 0.29 0.13 o -1 8 3 1.97 1.56 0.16 o 0 8 3 4.61 4.72 0.43 o 1 8 3 18.52 19.77 1.51 o 2 8 3 19.26 19.20 1.10 o 3 8 3 1.83 1.44 0.14 o 4 8 3 1.04 1.05 0.35 o -2 9 3 4.65 5.63 0.43 o -1 9 3 5.94 4.63 0.79 o 0 9 3 2.41 1.66 0.18 o 1 9 3 5.43 3.59 0.21 o 2 9 3 11.24 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