#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/10/2211000.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211000_Fobs loop_ _publ_author_name 'Xie, Hui-Dong' 'Xie, Cheng-Zhi' 'Wang, Xiao-Qing' 'Shen, Guang-Qiu' 'Shen, De-Zhong' _publ_section_title ; Tetraaqua(pyrazole-3,5-dicarboxylato)zinc(II) ; _journal_coeditor_code GA2003 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3119 _journal_page_last m3121 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 87.169 _cell_angle_beta 80.707 _cell_angle_gamma 77.899 _cell_length_a 6.1483 _cell_length_b 7.7259 _cell_length_c 10.8517 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.7998 _[local]_cod_data_source_file ga2003Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030927H in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1693.93 1686.35 42.14 o 2 0 0 5645.07 5163.78 128.17 o 3 0 0 1173.24 1229.57 31.43 o 4 0 0 173.98 158.59 5.47 o 5 0 0 546.12 525.05 21.26 o 6 0 0 366.16 348.52 14.99 o 7 0 0 191.50 197.35 10.83 o -7 1 0 25.21 14.38 4.96 o -6 1 0 703.04 714.26 27.24 o -5 1 0 395.15 405.15 12.07 o -4 1 0 471.63 461.77 45.67 o -3 1 0 2479.06 2496.09 62.64 o -2 1 0 1331.77 1306.02 33.04 o -1 1 0 5054.73 4207.21 104.58 o 0 1 0 11.61 13.37 1.11 o 1 1 0 5303.16 4428.65 166.97 o 2 1 0 730.97 754.36 19.29 o 3 1 0 2593.07 2575.45 97.81 o 4 1 0 185.47 197.89 6.36 o 5 1 0 126.38 123.54 5.05 o 6 1 0 271.55 260.43 12.05 o 7 1 0 0.65 3.24 4.66 o -6 2 0 184.01 179.22 10.13 o -5 2 0 314.68 345.20 10.78 o -4 2 0 251.99 288.22 8.95 o -3 2 0 1792.95 2048.26 60.30 o -2 2 0 2678.81 2729.14 68.45 o -1 2 0 520.98 579.95 15.14 o 0 2 0 4249.27 3787.77 94.23 o 1 2 0 8471.73 8007.14 301.24 o 2 2 0 116.47 162.31 4.94 o 3 2 0 371.87 349.57 12.45 o 4 2 0 836.55 779.00 20.77 o 5 2 0 38.26 36.33 4.71 o 6 2 0 242.51 252.13 11.75 o 7 2 0 280.37 244.64 12.15 o -6 3 0 117.34 118.57 8.40 o -5 3 0 277.71 274.02 15.90 o -4 3 0 550.10 609.51 22.78 o -3 3 0 175.68 189.23 6.41 o -2 3 0 1665.49 1672.48 44.30 o -1 3 0 1470.24 1533.81 63.54 o 0 3 0 7.07 10.88 1.27 o 1 3 0 6157.88 5797.73 218.61 o 2 3 0 8.20 7.59 2.13 o 3 3 0 1429.05 1380.12 35.44 o 4 3 0 422.20 410.37 11.80 o 5 3 0 422.86 405.52 12.00 o 6 3 0 221.77 226.31 11.04 o 7 3 0 249.03 246.96 12.35 o -5 4 0 92.17 107.17 5.40 o -4 4 0 1.35 -1.78 2.50 o -3 4 0 287.36 293.48 9.31 o -2 4 0 2948.08 2935.98 73.94 o -1 4 0 335.41 320.83 9.37 o 0 4 0 2214.23 2131.87 57.41 o 1 4 0 3.48 9.62 2.43 o 2 4 0 13.61 10.23 2.73 o 3 4 0 235.64 269.75 12.66 o 4 4 0 1175.05 1167.43 30.78 o 5 4 0 49.03 45.25 6.89 o 6 4 0 151.88 147.33 8.71 o 7 4 0 154.69 143.99 8.91 o -5 5 0 22.36 23.29 5.47 o -4 5 0 294.30 310.11 10.44 o -3 5 0 107.95 124.30 5.33 o -2 5 0 488.32 461.13 13.40 o -1 5 0 1499.11 1502.34 38.82 o 0 5 0 25.11 20.94 2.23 o 1 5 0 627.16 628.19 26.12 o 2 5 0 2.74 -3.24 3.24 o 3 5 0 43.01 46.78 4.96 o 4 5 0 46.45 48.35 3.50 o 5 5 0 55.26 52.91 5.21 o 6 5 0 34.42 29.97 4.46 o 7 5 0 37.44 31.69 5.16 o -4 6 0 7.74 5.77 5.06 o -3 6 0 991.94 1016.29 27.69 o -2 6 0 63.35 69.52 4.05 o -1 6 0 117.81 121.97 5.11 o 0 6 0 6.84 3.95 3.34 o 1 6 0 7.45 11.75 3.34 o 2 6 0 300.10 304.38 15.09 o 3 6 0 280.74 295.67 14.88 o 4 6 0 625.91 620.77 17.93 o 5 6 0 83.39 79.08 5.97 o 6 6 0 70.61 77.16 6.78 o -3 7 0 7.63 3.54 5.16 o -2 7 0 204.10 189.79 7.27 o -1 7 0 211.81 237.95 13.26 o 0 7 0 92.50 104.19 7.90 o 1 7 0 82.68 82.83 6.58 o 2 7 0 62.50 58.63 6.68 o 3 7 0 245.04 262.96 14.18 o 4 7 0 2.42 10.13 4.86 o 5 7 0 379.84 372.02 16.30 o 6 7 0 1.83 2.03 4.15 o -2 8 0 328.47 341.44 18.12 o -1 8 0 114.38 106.12 8.81 o 0 8 0 220.00 237.34 13.26 o 1 8 0 138.57 148.14 9.62 o 2 8 0 400.66 374.24 18.83 o 3 8 0 18.16 20.05 4.96 o 4 8 0 276.00 271.87 15.59 o 5 8 0 108.20 95.18 7.70 o -1 9 0 143.39 151.78 11.24 o 0 9 0 105.44 112.09 8.91 o 1 9 0 55.30 55.41 4.74 o 2 9 0 20.39 18.73 5.27 o 3 9 0 147.95 148.75 11.14 o 4 9 0 0.05 -3.24 5.87 o -3 -9 1 53.23 51.74 6.89 o -2 -9 1 57.28 65.01 7.90 o -1 -9 1 33.06 34.63 5.97 o 0 -9 1 35.98 21.47 5.47 o 1 -9 1 95.43 113.51 9.52 o -5 -8 1 194.55 213.65 11.44 o -4 -8 1 97.59 99.57 8.00 o -3 -8 1 123.15 137.30 10.02 o -2 -8 1 309.30 305.29 16.30 o -1 -8 1 157.80 162.52 10.33 o 0 -8 1 520.38 535.34 24.71 o 1 -8 1 0.08 -0.61 4.96 o 2 -8 1 21.53 28.35 5.77 o -6 -7 1 146.17 149.25 9.32 o -5 -7 1 71.10 82.22 6.48 o -4 -7 1 221.76 212.70 8.13 o -3 -7 1 208.23 222.56 12.56 o -2 -7 1 399.28 450.08 21.06 o -1 -7 1 135.31 146.52 9.21 o 0 -7 1 143.20 147.02 9.42 o 1 -7 1 472.35 496.76 22.88 o 2 -7 1 27.78 29.16 5.47 o 3 -7 1 237.18 251.12 14.58 o 4 -7 1 5.89 2.94 4.96 o -6 -6 1 8.21 14.38 4.15 o -5 -6 1 192.31 186.62 9.92 o -4 -6 1 0.72 1.01 2.41 o -3 -6 1 39.85 40.81 5.27 o -2 -6 1 44.16 44.15 4.96 o -1 -6 1 67.12 69.44 3.81 o 0 -6 1 390.09 406.44 18.63 o 1 -6 1 1.19 -0.81 3.65 o 2 -6 1 79.57 74.07 4.03 o 3 -6 1 66.16 62.88 6.38 o 4 -6 1 574.43 543.04 25.42 o -7 -5 1 18.28 14.78 4.35 o -6 -5 1 154.21 152.39 8.81 o -5 -5 1 5.51 7.09 3.34 o -4 -5 1 374.89 383.08 11.65 o -3 -5 1 12.07 12.45 3.85 o -2 -5 1 215.75 230.66 11.44 o -1 -5 1 782.95 775.72 31.69 o 0 -5 1 27.44 25.78 2.33 o 1 -5 1 1699.66 1702.57 43.64 o 2 -5 1 1.65 2.47 2.33 o 3 -5 1 840.47 796.78 21.91 o 4 -5 1 72.28 71.49 6.78 o 5 -5 1 500.14 452.11 21.87 o -7 -4 1 158.09 165.45 9.92 o -6 -4 1 8.59 6.89 3.54 o -5 -4 1 145.33 154.31 8.20 o -4 -4 1 103.25 101.95 4.46 o -3 -4 1 1084.83 1094.54 28.70 o -2 -4 1 1070.26 1096.40 43.24 o -1 -4 1 2251.84 2469.94 94.57 o 0 -4 1 823.46 805.15 22.55 o 2 -4 1 1292.90 1270.23 36.50 o 3 -4 1 43.92 40.79 3.03 o 4 -4 1 1863.87 1840.61 47.59 o 5 -4 1 151.30 148.54 9.72 o -7 -3 1 43.88 46.48 5.57 o -6 -3 1 368.07 346.20 15.09 o -5 -3 1 202.95 208.08 10.02 o -4 -3 1 762.90 702.93 19.00 o -3 -3 1 317.07 321.18 9.31 o -2 -3 1 307.66 270.56 11.75 o -1 -3 1 1375.29 1398.25 53.87 o 1 -3 1 363.29 312.08 8.46 o 2 -3 1 14.77 9.27 1.75 o 3 -3 1 60.73 59.68 4.96 o 4 -3 1 276.92 272.71 8.78 o 5 -3 1 308.16 345.15 11.03 o -7 -2 1 222.60 209.09 11.04 o -6 -2 1 38.57 38.17 4.66 o -5 -2 1 308.64 309.34 13.16 o -4 -2 1 24.96 25.48 2.31 o -3 -2 1 744.62 746.53 19.50 o -2 -2 1 728.84 777.78 20.01 o -1 -2 1 222.37 251.32 10.33 o 0 -2 1 1543.12 1538.12 41.35 o 1 -2 1 93.60 88.27 2.43 o 2 -2 1 464.25 410.02 11.14 o 3 -2 1 91.53 101.73 7.44 o 4 -2 1 975.72 1030.64 27.13 o 5 -2 1 768.74 742.51 20.53 o 6 -2 1 123.09 136.80 8.51 o -7 -1 1 81.63 62.78 6.48 o -6 -1 1 696.84 658.87 25.21 o -5 -1 1 57.23 56.30 4.76 o -4 -1 1 26.28 27.47 5.01 o -3 -1 1 22.22 31.98 2.00 o -2 -1 1 225.95 219.31 6.11 o -1 -1 1 1019.04 1045.31 26.30 o 0 -1 1 2799.28 2794.88 105.51 o 1 -1 1 551.29 596.80 23.29 o 2 -1 1 707.34 813.55 20.79 o 3 -1 1 4191.76 4259.07 106.21 o 4 -1 1 154.21 178.09 6.01 o 5 -1 1 1040.69 1074.63 28.47 o 6 -1 1 0.56 4.46 4.15 o -7 0 1 57.23 64.70 6.78 o -6 0 1 15.76 16.91 3.95 o -5 0 1 620.91 646.82 24.30 o -4 0 1 193.45 201.89 6.44 o -3 0 1 4955.55 4906.52 121.92 o -2 0 1 689.34 749.24 19.17 o -1 0 1 8.80 15.49 1.42 o 1 0 1 971.81 909.08 34.83 o 2 0 1 3731.91 3712.65 92.14 o 3 0 1 1991.29 2235.20 56.12 o 4 0 1 1609.36 1599.01 81.61 o 5 0 1 91.21 96.44 4.32 o 6 0 1 64.89 69.66 5.87 o 7 0 1 0.48 -3.85 3.85 o -7 1 1 5.90 4.96 5.27 o -6 1 1 446.10 456.67 19.04 o -5 1 1 29.91 30.78 4.46 o -4 1 1 916.87 933.17 24.66 o -3 1 1 6.42 -0.38 1.62 o -2 1 1 6866.96 6373.78 158.02 o -1 1 1 621.32 604.59 15.55 o 0 1 1 4635.33 3768.14 114.32 o 1 1 1 829.61 834.35 32.20 o 2 1 1 474.23 517.20 13.54 o 3 1 1 2637.54 2640.07 66.22 o 4 1 1 25.51 26.56 4.00 o 5 1 1 803.20 806.34 21.78 o 6 1 1 51.00 47.39 4.96 o 7 1 1 259.23 247.27 12.25 o -6 2 1 101.30 108.85 7.80 o -5 2 1 731.31 759.12 28.45 o -4 2 1 103.90 89.77 12.76 o -3 2 1 328.55 314.00 14.78 o -2 2 1 267.51 287.66 8.30 o -1 2 1 550.45 504.16 13.35 o 0 2 1 411.39 503.45 14.63 o 1 2 1 13402.43 10125.63 380.72 o 2 2 1 290.24 294.86 12.66 o 3 2 1 615.57 630.37 16.82 o 4 2 1 2899.98 2846.39 71.71 o 5 2 1 26.40 28.83 2.89 o 6 2 1 538.46 479.45 19.14 o 7 2 1 59.74 61.26 5.77 o -6 3 1 30.07 33.52 5.87 o -5 3 1 183.00 191.07 10.13 o -4 3 1 180.57 187.18 6.78 o -3 3 1 13.23 18.03 2.29 o -2 3 1 3564.69 3464.36 86.72 o -1 3 1 428.98 485.46 15.54 o 0 3 1 2062.12 2052.50 51.57 o 1 3 1 3100.29 3088.82 117.46 o 2 3 1 3092.95 2925.70 111.58 o 3 3 1 3324.19 3223.70 123.03 o 4 3 1 678.74 702.57 19.00 o 5 3 1 467.21 473.38 13.75 o 6 3 1 0.41 2.73 3.85 o 7 3 1 289.38 282.81 13.37 o -5 4 1 550.60 558.73 22.68 o -4 4 1 49.06 51.10 3.79 o -3 4 1 1013.56 1009.34 26.97 o -2 4 1 18.16 25.49 5.62 o -1 4 1 2944.13 2981.78 75.04 o 0 4 1 386.67 384.13 14.02 o 1 4 1 8345.19 7748.84 206.74 o 2 4 1 5667.99 5414.27 205.25 o 3 4 1 511.37 498.59 21.47 o 4 4 1 1646.50 1638.54 42.33 o 5 4 1 0.47 3.77 5.57 o 6 4 1 108.23 107.43 6.99 o 7 4 1 2.19 3.65 4.35 o -4 5 1 1072.33 1082.80 29.57 o -3 5 1 103.52 103.79 4.80 o -2 5 1 1426.11 1460.67 38.12 o -1 5 1 45.95 51.70 3.21 o 0 5 1 639.00 653.10 27.14 o 1 5 1 187.02 202.92 10.13 o 2 5 1 818.59 841.64 34.43 o 3 5 1 376.86 397.23 18.23 o 4 5 1 5.09 6.68 4.15 o 5 5 1 328.40 351.51 11.30 o 6 5 1 0.38 -3.14 3.34 o 7 5 1 143.53 158.87 9.62 o -4 6 1 29.00 35.03 6.38 o -3 6 1 193.03 202.76 7.79 o -2 6 1 4.98 8.34 5.37 o -1 6 1 1397.82 1453.78 38.15 o 0 6 1 0.28 4.96 3.34 o 1 6 1 492.50 510.64 22.28 o 2 6 1 1090.27 1085.87 44.25 o 3 6 1 87.45 89.00 7.39 o 4 6 1 168.38 174.77 10.83 o 5 6 1 45.09 40.45 3.93 o 6 6 1 42.14 42.22 5.27 o -3 7 1 14.32 9.62 5.57 o -2 7 1 189.78 191.28 7.49 o -1 7 1 2.18 2.53 3.85 o 0 7 1 619.34 613.41 26.93 o 1 7 1 47.68 51.54 5.27 o 2 7 1 913.93 890.55 37.57 o 3 7 1 234.86 214.46 12.35 o 4 7 1 93.54 98.83 8.40 o 5 7 1 180.34 183.41 7.76 o 6 7 1 38.27 34.02 5.16 o -2 8 1 61.37 58.93 6.89 o -1 8 1 400.42 415.25 20.35 o 0 8 1 37.25 41.11 5.77 o 1 8 1 262.09 265.29 14.58 o 2 8 1 133.25 132.24 9.62 o 3 8 1 46.50 47.89 6.28 o 4 8 1 30.64 31.29 6.38 o 5 8 1 110.08 104.01 12.05 o -1 9 1 15.78 17.01 6.08 o 0 9 1 225.52 232.79 13.67 o 1 9 1 0.24 5.77 4.76 o 2 9 1 45.05 43.64 6.18 o 3 9 1 53.07 34.22 6.38 o 4 9 1 1.10 10.53 5.87 o -3 -9 2 18.20 18.33 6.38 o -2 -9 2 339.88 365.64 19.14 o -1 -9 2 28.85 17.42 5.06 o 0 -9 2 348.63 349.54 18.43 o -5 -8 2 172.70 171.33 9.82 o -4 -8 2 66.27 69.87 6.38 o -3 -8 2 347.34 352.07 18.12 o -2 -8 2 4.48 6.37 3.06 o -1 -8 2 253.62 252.13 13.77 o 0 -8 2 35.37 36.35 5.47 o 1 -8 2 518.71 518.23 24.50 o 2 -8 2 17.26 7.09 5.47 o -5 -7 2 140.14 133.56 8.30 o -4 -7 2 348.13 340.02 14.78 o -3 -7 2 37.87 41.10 3.66 o -2 -7 2 922.15 963.05 39.79 o -1 -7 2 33.99 38.78 5.16 o 0 -7 2 119.85 114.82 8.30 o 1 -7 2 54.02 49.92 6.18 o 2 -7 2 12.28 12.05 4.46 o 3 -7 2 71.18 75.54 7.80 o -6 -6 2 138.61 133.35 8.51 o -5 -6 2 217.05 214.97 10.73 o -4 -6 2 252.33 255.37 11.54 o -3 -6 2 378.11 384.32 11.72 o -2 -6 2 139.99 135.89 8.00 o -1 -6 2 474.62 489.39 15.00 o 0 -6 2 23.22 20.25 3.95 o 1 -6 2 494.02 481.17 21.87 o 2 -6 2 220.99 231.78 12.86 o 3 -6 2 104.54 110.17 8.61 o 4 -6 2 381.39 398.34 20.15 o -6 -5 2 23.44 20.96 4.15 o -5 -5 2 144.79 143.58 8.10 o -4 -5 2 425.03 394.39 15.90 o -3 -5 2 110.22 126.11 13.01 o -2 -5 2 1097.33 1110.58 44.05 o -1 -5 2 0.56 2.55 2.06 o 0 -5 2 165.80 158.48 9.16 o 1 -5 2 4.54 10.97 5.57 o 2 -5 2 1116.36 1077.67 43.95 o 3 -5 2 4.47 1.11 3.24 o 4 -5 2 395.40 384.88 18.93 o 5 -5 2 158.45 168.59 11.14 o -7 -4 2 114.50 117.36 8.40 o -6 -4 2 195.99 185.91 9.92 o -5 -4 2 345.05 338.60 14.48 o -4 -4 2 392.42 363.61 14.68 o -3 -4 2 1049.61 1024.54 26.87 o -2 -4 2 153.44 171.08 8.00 o -1 -4 2 3696.26 3632.06 138.11 o 0 -4 2 67.87 67.10 3.33 o 1 -4 2 2482.61 2508.53 67.61 o 2 -4 2 71.33 71.67 3.38 o 3 -4 2 55.08 56.50 5.37 o 4 -4 2 113.08 120.29 8.30 o 5 -4 2 97.98 84.65 7.59 o 6 -4 2 57.97 46.88 6.68 o -7 -3 2 257.20 240.48 12.45 o -6 -3 2 305.43 299.62 13.77 o -5 -3 2 232.30 229.04 10.73 o -4 -3 2 820.76 793.14 28.66 o -3 -3 2 194.05 197.31 6.26 o -2 -3 2 711.21 667.04 23.44 o -1 -3 2 0.58 2.43 2.03 o 0 -3 2 225.80 185.79 6.12 o 1 -3 2 80.28 91.19 2.70 o 2 -3 2 2284.88 2294.73 57.75 o 3 -3 2 353.71 350.93 10.21 o 4 -3 2 461.99 476.51 13.68 o 5 -3 2 425.38 407.15 19.24 o 6 -3 2 25.91 29.67 5.47 o -7 -2 2 30.27 22.38 5.16 o -6 -2 2 191.37 173.96 9.62 o -5 -2 2 50.17 50.63 4.66 o -4 -2 2 173.20 158.67 7.70 o -3 -2 2 646.72 595.03 15.82 o -2 -2 2 108.77 119.27 3.83 o -1 -2 2 146.16 173.20 4.99 o 0 -2 2 48.07 54.68 2.43 o 1 -2 2 224.92 273.85 8.20 o 2 -2 2 1303.49 1476.12 37.45 o 3 -2 2 859.11 875.24 22.86 o 4 -2 2 67.30 73.35 3.62 o 5 -2 2 823.98 833.25 39.44 o 6 -2 2 329.11 304.28 15.39 o -7 -1 2 13.40 10.73 4.25 o -6 -1 2 15.23 5.67 3.75 o -5 -1 2 123.55 125.25 7.39 o -4 -1 2 355.54 363.21 14.48 o -3 -1 2 477.61 505.81 13.51 o -2 -1 2 163.74 153.80 4.51 o -1 -1 2 191.03 186.01 6.23 o 0 -1 2 4032.26 3584.97 135.33 o 1 -1 2 8.82 16.00 5.72 o 2 -1 2 4783.53 4621.67 114.96 o 3 -1 2 1210.40 1416.11 36.03 o 4 -1 2 95.68 103.54 4.21 o 5 -1 2 1175.16 1195.16 31.33 o 6 -1 2 201.62 197.71 8.05 o -7 0 2 0.36 -0.41 4.86 o -6 0 2 325.23 305.69 13.97 o -5 0 2 19.89 24.10 3.95 o -4 0 2 140.23 133.56 9.01 o -3 0 2 1388.84 1397.68 35.63 o -2 0 2 6.83 6.58 1.01 o -1 0 2 4601.63 4309.97 142.16 o 0 0 2 783.62 820.86 22.20 o 1 0 2 4118.70 3728.85 107.53 o 2 0 2 108.95 86.13 3.65 o 3 0 2 1110.62 1069.71 27.39 o 4 0 2 257.90 262.86 7.99 o 5 0 2 547.62 573.78 16.03 o 6 0 2 888.06 873.76 28.35 o 7 0 2 1.42 -2.03 4.46 o -6 1 2 0.18 4.86 4.46 o -5 1 2 864.36 894.80 32.81 o -4 1 2 185.29 188.73 6.37 o -3 1 2 29.15 20.08 1.87 o -2 1 2 1144.17 1179.02 30.00 o -1 1 2 30.14 32.46 1.63 o 0 1 2 888.64 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6.68 o 1 -1 12 48.27 40.10 6.68 o 2 -1 12 4.67 3.95 5.57 o 3 -1 12 265.68 243.72 18.12 o 4 -1 12 26.00 16.50 5.77 o -2 0 12 0.29 6.48 5.06 o -1 0 12 150.94 149.25 10.43 o 0 0 12 7.51 12.96 4.96 o 1 0 12 155.83 146.92 10.43 o 2 0 12 166.30 177.40 11.95 o 3 0 12 31.50 35.56 4.61 o 4 0 12 518.94 546.89 26.12 o -2 1 12 244.96 261.44 13.47 o -1 1 12 0.33 -3.04 4.76 o 0 1 12 112.69 103.48 8.40 o 1 1 12 23.55 16.10 5.06 o 2 1 12 370.85 422.85 21.26 o 3 1 12 236.05 269.85 14.99 o 4 1 12 132.95 153.20 11.04 o -1 2 12 326.21 356.32 16.40 o 0 2 12 145.68 138.92 10.13 o 1 2 12 731.70 716.69 31.59 o 2 2 12 167.44 175.27 11.75 o 3 2 12 93.33 108.45 9.01 o 4 2 12 301.40 302.76 17.01 o -1 3 12 0.64 2.23 5.47 o 0 3 12 325.49 342.95 16.00 o 3 3 12 344.25 341.13 17.82 o 4 3 12 172.83 179.22 12.25 o 0 4 12 19.88 20.76 5.97 o 1 4 12 202.17 205.85 11.54 o 3 4 12 172.36 169.40 11.95 o 0 -2 13 119.42 130.72 10.53 o 1 -2 13 211.92 200.79 13.67 o 0 -1 13 447.98 472.46 23.59 o 1 -1 13 30.46 22.07 6.38 o 2 -1 13 286.29 295.57 17.52 o 0 0 13 12.06 15.39 5.97 o 1 0 13 447.96 452.82 22.78 o 2 0 13 4.51 -5.87 5.97 o 3 0 13 75.21 74.97 6.08 o 0 1 13 204.64 212.84 13.47 o 1 1 13 4.26 11.44 5.77 o 2 1 13 205.72 212.03 13.57 o 3 1 13 180.40 170.11 11.24 o 1 2 13 354.11 377.18 19.64 o 2 2 13 22.25 28.35 7.09 o 3 2 13 224.78 235.12 14.18 o