#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:21:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181030 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/10/2211010.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211010_Fobs loop_ _publ_author_name 'Lu, Ji-Lin' 'Zhang, Da-Shun' 'Li, Lin' 'Liu, Bei-Ping' _publ_section_title ; 1,4-Dihydro-3,6-dipyrazin-2-yl-1,2,4,5-tetrazine--benzene-1,3-dicarboxylic acid (1/1) ; _journal_coeditor_code GG2015 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4855 _journal_page_last o4857 _journal_volume 62 _journal_year 2006 _space_group_IT_number 52 _symmetry_space_group_name_Hall '-P 2a 2bc' _symmetry_space_group_name_H-M 'P n n a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5457 _cell_length_b 33.6545 _cell_length_c 3.7035 _exptl_crystal_F_000 840.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file gg2015Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50608D in Pnna' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6443.88 6050.55 240.04 o 4 0 0 673.63 602.65 26.52 o 6 0 0 8800.66 8948.24 355.89 o 8 0 0 2013.36 1924.20 80.21 o 10 0 0 302.07 348.33 22.77 o 12 0 0 206.24 165.81 26.97 o 14 0 0 166.36 85.28 27.77 o 16 0 0 296.44 288.44 60.02 o 2 1 0 44.88 49.91 4.58 o 4 1 0 1.16 -7.23 4.82 o 6 1 0 8928.54 9144.98 257.47 o 8 1 0 1175.78 1169.12 36.01 o 10 1 0 296.74 318.12 17.95 o 12 1 0 1.83 3.55 16.64 o 14 1 0 6.38 3.33 18.95 o 16 1 0 1.10 -0.54 28.77 o 2 2 0 1235.66 1127.14 35.61 o 4 2 0 348.94 301.26 16.55 o 6 2 0 1505.52 1573.09 45.98 o 8 2 0 700.13 791.93 25.85 o 10 2 0 0.20 -7.53 11.09 o 12 2 0 1204.33 1067.74 45.82 o 14 2 0 150.61 194.49 22.75 o 16 2 0 212.23 177.82 27.01 o 2 3 0 16522.80 16421.63 507.66 o 4 3 0 588.27 608.53 18.99 o 6 3 0 543.23 527.38 17.66 o 8 3 0 51.53 60.22 8.02 o 10 3 0 0.89 2.59 11.06 o 12 3 0 15.34 -7.96 16.56 o 14 3 0 133.27 86.51 21.38 o 16 3 0 16.62 31.95 24.66 o 0 4 0 840.85 751.13 38.01 o 2 4 0 7438.74 6764.86 233.66 o 4 4 0 20.11 31.18 4.81 o 6 4 0 42.79 66.91 12.07 o 8 4 0 496.99 589.17 20.12 o 10 4 0 347.99 358.73 18.73 o 12 4 0 59.66 11.98 16.70 o 14 4 0 15.32 15.16 18.74 o 16 4 0 21.13 26.87 27.23 o 2 5 0 110.46 97.91 6.53 o 4 5 0 1224.33 1116.36 33.11 o 6 5 0 39.41 43.10 7.62 o 8 5 0 577.61 680.90 22.88 o 10 5 0 331.66 361.46 18.94 o 12 5 0 427.22 408.58 33.26 o 14 5 0 624.30 573.38 33.94 o 16 5 0 37.40 59.47 28.28 o 0 6 0 383.11 314.41 17.86 o 2 6 0 27495.77 28126.45 970.83 o 4 6 0 1008.97 964.61 28.72 o 6 6 0 868.80 813.33 25.65 o 8 6 0 1870.85 1862.78 55.43 o 10 6 0 88.34 92.52 12.77 o 12 6 0 468.53 548.31 28.63 o 14 6 0 15.48 32.50 19.54 o 2 7 0 16.47 2.40 6.00 o 4 7 0 817.72 788.24 26.97 o 6 7 0 345.22 393.78 21.80 o 8 7 0 4446.30 4658.57 133.09 o 10 7 0 7.27 12.64 12.14 o 12 7 0 1302.86 1287.15 46.85 o 14 7 0 75.47 31.48 21.55 o 0 8 0 752.97 652.16 35.21 o 2 8 0 1592.58 1362.78 56.60 o 4 8 0 205.60 185.56 11.24 o 6 8 0 125.85 164.02 9.81 o 8 8 0 0.22 0.46 8.14 o 10 8 0 315.99 300.20 17.78 o 12 8 0 927.77 899.75 35.84 o 14 8 0 396.62 352.46 29.96 o 2 9 0 2282.59 2136.65 88.48 o 4 9 0 11811.57 11598.15 401.66 o 6 9 0 9.83 11.23 6.43 o 8 9 0 592.91 621.85 24.64 o 10 9 0 18.28 7.43 17.49 o 12 9 0 222.04 236.64 18.52 o 14 9 0 48.11 23.83 25.29 o 0 10 0 7.94 2.71 9.56 o 2 10 0 1.91 7.81 7.83 o 4 10 0 5524.09 5432.11 189.14 o 6 10 0 1179.35 1250.57 37.86 o 8 10 0 0.87 -10.75 11.45 o 10 10 0 1506.45 1498.63 51.98 o 12 10 0 3149.66 2993.12 127.86 o 14 10 0 39.93 66.21 24.40 o 2 11 0 436.65 466.93 23.06 o 4 11 0 1305.66 1302.27 49.38 o 6 11 0 1285.72 1401.65 52.61 o 8 11 0 46.44 63.71 11.80 o 10 11 0 439.03 445.17 22.51 o 12 11 0 136.70 138.06 19.67 o 14 11 0 0.15 4.96 23.92 o 0 12 0 1455.89 1607.11 82.63 o 2 12 0 843.32 756.66 29.64 o 4 12 0 187.91 201.61 14.56 o 6 12 0 1017.45 1018.29 39.40 o 8 12 0 291.81 307.95 16.68 o 10 12 0 3739.50 3612.56 116.40 o 12 12 0 15.07 -1.25 16.57 o 14 12 0 183.50 164.84 28.10 o 2 13 0 61.92 53.83 8.12 o 4 13 0 4704.97 4783.18 196.68 o 6 13 0 0.71 5.12 10.14 o 8 13 0 5.26 -8.62 12.21 o 10 13 0 3461.63 3516.21 128.29 o 12 13 0 5.80 -25.89 18.30 o 14 13 0 153.40 172.51 33.80 o 0 14 0 942.29 810.75 45.06 o 2 14 0 2799.96 2658.85 95.16 o 4 14 0 6381.75 6718.81 273.89 o 6 14 0 0.24 3.76 12.31 o 8 14 0 569.49 550.97 30.94 o 10 14 0 19.74 -10.97 23.70 o 12 14 0 0.30 10.08 38.94 o 14 14 0 120.06 51.91 31.06 o 2 15 0 16020.11 16051.35 562.26 o 4 15 0 2.07 -3.95 13.13 o 6 15 0 280.60 312.99 21.65 o 8 15 0 889.47 853.12 43.21 o 10 15 0 1654.45 1649.65 75.17 o 12 15 0 1260.49 1298.90 79.40 o 14 15 0 2.21 2.95 34.06 o 0 16 0 1517.28 1451.36 76.76 o 2 16 0 3892.69 3716.39 132.27 o 4 16 0 39.38 51.64 11.96 o 6 16 0 71.24 116.07 21.72 o 8 16 0 3965.57 3822.18 160.45 o 10 16 0 800.03 833.39 64.68 o 12 16 0 386.79 467.06 44.80 o 14 16 0 141.48 120.29 69.36 o 2 17 0 1618.07 1608.64 59.53 o 4 17 0 1701.13 1682.43 73.44 o 6 17 0 13.24 27.65 18.49 o 8 17 0 1550.10 1514.38 68.61 o 10 17 0 1772.92 1657.93 76.60 o 12 17 0 389.04 384.21 42.18 o 14 17 0 136.23 246.43 87.57 o 0 18 0 172.44 187.32 18.55 o 2 18 0 2389.55 2243.48 81.45 o 4 18 0 1132.90 1223.97 49.27 o 6 18 0 108.70 125.73 28.81 o 8 18 0 419.91 463.92 30.39 o 10 18 0 48.63 37.70 29.29 o 12 18 0 355.66 386.56 147.87 o 14 18 0 94.93 108.87 39.55 o 2 19 0 34.74 53.52 14.80 o 4 19 0 762.78 826.91 53.00 o 6 19 0 289.79 271.39 22.04 o 8 19 0 1467.03 1387.72 65.19 o 10 19 0 1781.20 1747.98 99.47 o 12 19 0 21.68 37.56 77.08 o 14 19 0 115.40 155.02 46.98 o 0 20 0 483.66 445.75 30.42 o 2 20 0 565.03 588.16 26.40 o 4 20 0 27.43 37.01 12.04 o 6 20 0 2310.08 2211.34 95.55 o 8 20 0 20.36 38.52 22.77 o 10 20 0 576.17 582.37 47.14 o 12 20 0 68.83 120.56 55.63 o 2 21 0 28.06 6.92 13.02 o 4 21 0 1078.15 1202.48 47.62 o 6 21 0 39.32 24.75 17.70 o 8 21 0 10.63 3.83 20.01 o 10 21 0 1268.62 1254.00 106.20 o 12 21 0 131.70 151.60 34.98 o 0 22 0 478.71 522.41 35.32 o 2 22 0 819.54 869.36 35.91 o 4 22 0 125.74 153.69 18.67 o 6 22 0 48.85 61.39 18.22 o 8 22 0 111.16 109.85 22.11 o 10 22 0 822.12 989.49 66.97 o 12 22 0 108.26 135.67 39.62 o 2 23 0 280.22 302.94 20.86 o 4 23 0 0.63 -8.29 12.97 o 6 23 0 290.08 324.65 21.46 o 8 23 0 1501.54 1423.60 67.58 o 10 23 0 660.37 599.27 50.74 o 12 23 0 20.31 -18.91 33.80 o 0 24 0 164.94 173.67 27.57 o 2 24 0 804.08 805.43 34.69 o 4 24 0 303.25 287.98 20.13 o 6 24 0 367.86 383.85 24.09 o 8 24 0 21.96 -38.29 25.53 o 10 24 0 40.45 13.40 31.61 o 12 24 0 0.11 -9.21 34.74 o 2 25 0 210.30 239.47 34.10 o 4 25 0 457.67 475.39 39.12 o 6 25 0 39.62 47.27 15.99 o 8 25 0 171.49 159.93 33.18 o 10 25 0 293.06 306.57 53.68 o 12 25 0 1.57 -23.22 35.59 o 0 26 0 645.00 672.27 44.84 o 2 26 0 593.63 578.56 28.97 o 4 26 0 268.76 250.57 19.77 o 6 26 0 438.31 396.04 29.67 o 8 26 0 524.64 427.11 87.80 o 10 26 0 372.33 431.91 117.79 o 12 26 0 12.34 -26.43 38.21 o 2 27 0 182.31 223.08 19.91 o 4 27 0 728.05 754.99 41.30 o 6 27 0 8.73 9.99 19.83 o 8 27 0 407.07 379.17 41.73 o 10 27 0 87.28 90.20 47.22 o 0 28 0 723.23 738.66 53.26 o 2 28 0 2079.21 2143.68 80.81 o 4 28 0 259.48 260.48 31.50 o 6 28 0 3.26 -1.91 25.73 o 8 28 0 126.29 66.73 37.87 o 10 28 0 4.68 -14.97 35.37 o 2 29 0 4697.03 4642.59 166.91 o 4 29 0 371.11 359.87 41.72 o 6 29 0 522.46 536.06 130.17 o 8 29 0 0.07 -24.48 31.69 o 10 29 0 125.75 104.08 40.34 o 0 30 0 2318.48 2485.74 136.19 o 2 30 0 420.42 522.08 28.74 o 4 30 0 1208.45 1209.45 60.18 o 6 30 0 0.45 -3.65 28.48 o 8 30 0 23.73 35.55 34.35 o 10 30 0 39.96 56.38 39.67 o 2 31 0 249.21 326.10 34.13 o 4 31 0 3.98 21.64 20.36 o 6 31 0 207.20 205.79 50.82 o 8 31 0 126.22 142.87 36.45 o 10 31 0 22.54 -11.22 41.91 o 0 32 0 6821.93 6922.71 349.62 o 2 32 0 1414.50 1458.55 68.92 o 4 32 0 597.92 451.63 43.80 o 6 32 0 94.97 65.15 34.07 o 8 32 0 281.06 304.04 43.79 o 2 33 0 33.98 73.97 24.08 o 4 33 0 29.17 66.06 44.47 o 6 33 0 391.85 385.82 61.69 o 8 33 0 112.00 164.99 79.02 o 0 34 0 28.31 -13.35 41.76 o 2 34 0 83.42 99.28 30.98 o 4 34 0 9.10 -27.78 31.33 o 6 34 0 41.12 70.57 37.08 o 8 34 0 192.02 173.15 42.97 o 2 35 0 125.81 197.30 28.80 o 4 35 0 610.06 652.14 66.02 o 6 35 0 117.41 98.77 57.12 o 0 36 0 42.26 31.25 37.29 o 2 36 0 619.14 708.15 75.52 o 4 36 0 151.31 162.41 38.95 o 6 36 0 198.24 204.67 52.38 o 2 37 0 29.22 37.56 42.57 o 4 37 0 41.00 33.95 38.12 o 6 37 0 4.40 -18.84 62.53 o 0 38 0 2.24 26.30 44.54 o 2 38 0 0.19 49.69 44.33 o 4 38 0 14.53 43.99 56.47 o 2 39 0 26.74 64.26 44.40 o 1 0 1 6933.31 6575.04 266.75 o 3 0 1 19.85 22.68 5.43 o 5 0 1 286.12 251.48 12.17 o 7 0 1 6.68 10.12 8.43 o 9 0 1 204.44 201.19 21.20 o 11 0 1 491.39 479.75 28.20 o 13 0 1 67.19 31.27 21.53 o 15 0 1 98.80 81.88 26.95 o 0 1 1 1380.73 1282.83 65.79 o 1 1 1 491.37 454.68 13.57 o 2 1 1 12274.08 11900.43 292.92 o 3 1 1 166.95 175.86 6.89 o 4 1 1 0.16 -6.16 4.11 o 5 1 1 49.05 57.68 5.60 o 6 1 1 554.27 549.66 15.32 o 7 1 1 195.86 246.72 9.44 o 8 1 1 1156.77 1141.17 28.11 o 9 1 1 90.25 87.10 8.65 o 10 1 1 8.56 7.47 8.73 o 11 1 1 147.96 157.15 11.87 o 12 1 1 8.70 -1.20 10.92 o 13 1 1 226.77 245.24 18.66 o 14 1 1 8.08 18.03 16.67 o 15 1 1 48.21 37.18 18.51 o 1 2 1 5498.02 5165.08 135.96 o 2 2 1 5088.12 5142.06 127.18 o 3 2 1 550.07 520.73 13.80 o 4 2 1 546.03 513.71 13.23 o 5 2 1 1270.71 1214.25 28.42 o 6 2 1 1.04 8.59 5.44 o 7 2 1 404.22 406.46 12.35 o 8 2 1 1785.52 1795.86 41.83 o 9 2 1 0.13 -3.38 7.60 o 10 2 1 43.76 51.97 9.22 o 11 2 1 363.32 360.88 14.41 o 12 2 1 85.38 107.46 12.63 o 13 2 1 81.34 71.78 15.21 o 14 2 1 53.81 29.76 16.73 o 15 2 1 3.87 -7.59 18.62 o 0 3 1 16.15 1.59 6.49 o 1 3 1 17113.94 17047.90 392.35 o 2 3 1 3598.17 3460.42 91.26 o 3 3 1 0.29 -0.33 4.16 o 4 3 1 322.29 297.32 8.73 o 5 3 1 950.38 921.56 22.15 o 6 3 1 22.75 23.12 5.43 o 7 3 1 376.92 422.47 12.73 o 8 3 1 400.68 411.86 13.65 o 9 3 1 183.57 216.60 13.27 o 10 3 1 18.33 23.16 8.90 o 11 3 1 32.91 31.70 10.35 o 12 3 1 3.12 1.32 11.64 o 13 3 1 426.05 448.11 20.00 o 14 3 1 234.33 215.30 20.23 o 15 3 1 131.46 160.10 23.58 o 1 4 1 14362.06 14300.75 348.74 o 2 4 1 36.67 29.13 4.09 o 3 4 1 33.97 46.80 4.43 o 4 4 1 1004.08 945.98 25.07 o 5 4 1 807.45 797.52 19.72 o 6 4 1 2009.01 2100.84 50.47 o 7 4 1 741.84 743.81 19.25 o 8 4 1 562.56 544.66 18.29 o 9 4 1 312.97 338.63 12.60 o 10 4 1 78.07 108.47 11.91 o 11 4 1 295.03 282.80 14.06 o 12 4 1 126.95 93.60 13.32 o 13 4 1 38.87 28.22 14.21 o 14 4 1 26.96 34.32 16.23 o 15 4 1 7.60 11.17 18.41 o 0 5 1 77762.57 86584.71 2973.54 o 1 5 1 2200.11 2142.81 56.88 o 2 5 1 1034.73 978.43 26.91 o 3 5 1 1337.75 1310.30 35.85 o 4 5 1 467.40 457.61 13.57 o 5 5 1 1354.75 1395.35 32.22 o 6 5 1 2072.95 2114.32 48.09 o 7 5 1 2022.57 2069.28 47.46 o 8 5 1 207.86 194.83 9.40 o 9 5 1 56.01 67.36 8.57 o 10 5 1 44.00 34.73 9.59 o 11 5 1 3.04 8.74 10.39 o 12 5 1 1247.30 1245.81 36.41 o 13 5 1 331.42 312.06 17.51 o 14 5 1 0.56 -11.99 15.93 o 15 5 1 2.59 9.24 21.36 o 1 6 1 5196.92 5136.92 144.76 o 2 6 1 629.72 621.08 18.17 o 3 6 1 228.66 206.08 8.54 o 4 6 1 210.45 191.15 6.84 o 5 6 1 145.59 158.56 7.59 o 6 6 1 216.26 221.85 8.51 o 7 6 1 36.28 25.18 6.35 o 8 6 1 69.53 81.18 7.81 o 9 6 1 11.96 15.53 9.79 o 10 6 1 310.16 318.39 13.98 o 11 6 1 5.92 3.30 11.08 o 12 6 1 123.65 129.37 16.37 o 13 6 1 59.14 71.59 14.06 o 14 6 1 0.11 -1.62 16.28 o 15 6 1 10.08 12.77 21.43 o 0 7 1 27.33 47.33 4.99 o 1 7 1 1658.13 1744.34 43.89 o 2 7 1 1448.57 1421.05 41.55 o 3 7 1 1016.59 987.20 25.78 o 4 7 1 164.81 167.55 6.44 o 5 7 1 15.19 15.49 5.75 o 6 7 1 1564.47 1608.92 39.29 o 7 7 1 28.43 49.68 7.89 o 8 7 1 14.60 1.95 7.06 o 9 7 1 126.13 120.67 9.87 o 10 7 1 468.47 443.28 16.52 o 11 7 1 16.51 2.19 11.55 o 12 7 1 251.97 251.86 15.83 o 13 7 1 187.43 173.29 15.85 o 14 7 1 0.00 -22.99 15.82 o 15 7 1 0.01 -5.95 19.79 o 1 8 1 256.30 215.07 7.55 o 2 8 1 874.55 829.38 23.69 o 3 8 1 1226.17 1257.51 34.78 o 4 8 1 24.56 12.71 4.52 o 5 8 1 6.69 6.21 5.47 o 6 8 1 383.45 353.15 11.60 o 7 8 1 295.11 315.71 11.57 o 8 8 1 35.33 44.02 7.56 o 9 8 1 15.80 13.43 8.75 o 10 8 1 549.63 568.27 18.83 o 11 8 1 631.44 614.61 22.28 o 12 8 1 5.77 -6.98 12.28 o 13 8 1 86.47 85.52 15.83 o 14 8 1 7.75 14.69 16.17 o 15 8 1 2.13 -2.89 20.14 o 0 9 1 2789.82 2582.55 81.41 o 1 9 1 1036.01 1002.43 24.73 o 2 9 1 5.51 -0.80 4.96 o 3 9 1 2143.33 2090.50 56.25 o 4 9 1 2036.81 2200.06 54.92 o 5 9 1 345.93 393.72 12.94 o 6 9 1 3.13 3.90 8.10 o 7 9 1 5.55 0.18 6.88 o 8 9 1 290.95 304.40 17.39 o 9 9 1 541.68 531.37 17.53 o 10 9 1 292.02 307.75 15.13 o 11 9 1 1308.36 1307.28 47.82 o 12 9 1 3.80 -9.73 13.37 o 13 9 1 81.62 91.02 16.53 o 14 9 1 35.79 16.64 16.78 o 15 9 1 195.69 164.56 23.03 o 1 10 1 1102.87 1164.50 28.35 o 2 10 1 4697.76 4569.01 129.44 o 3 10 1 31.12 37.68 5.81 o 4 10 1 196.10 221.39 9.73 o 5 10 1 1801.07 1890.15 48.23 o 6 10 1 0.17 -5.06 6.37 o 7 10 1 52.11 65.94 8.29 o 8 10 1 0.07 -5.06 8.41 o 9 10 1 1065.36 1085.26 30.91 o 10 10 1 766.30 801.85 35.47 o 11 10 1 672.69 675.37 23.64 o 12 10 1 82.70 84.15 14.93 o 13 10 1 7.76 26.67 15.72 o 14 10 1 97.70 49.10 17.23 o 15 10 1 1.17 10.93 20.51 o 0 11 1 152.17 151.11 8.41 o 1 11 1 3890.41 3821.35 100.91 o 2 11 1 27.50 14.55 5.13 o 3 11 1 854.90 837.90 26.47 o 4 11 1 235.14 230.91 13.64 o 5 11 1 0.58 -11.65 7.77 o 6 11 1 16.18 12.69 10.46 o 7 11 1 9.24 27.13 8.03 o 8 11 1 415.04 418.31 15.84 o 9 11 1 0.00 -2.56 9.89 o 10 11 1 217.19 221.44 16.40 o 11 11 1 30.62 53.34 15.14 o 12 11 1 504.49 509.15 25.76 o 13 11 1 86.78 69.33 22.25 o 14 11 1 25.98 29.15 19.56 o 15 11 1 0.01 -7.30 21.94 o 1 12 1 2266.92 2303.94 52.04 o 2 12 1 640.34 661.81 18.51 o 3 12 1 31.87 38.92 6.51 o 4 12 1 796.04 816.97 24.69 o 5 12 1 412.42 429.69 18.85 o 6 12 1 237.48 225.50 13.68 o 7 12 1 1246.97 1244.66 36.85 o 8 12 1 0.07 21.34 12.93 o 9 12 1 209.23 228.42 16.31 o 10 12 1 619.49 623.71 25.78 o 11 12 1 655.79 633.36 26.56 o 12 12 1 791.37 850.64 36.13 o 13 12 1 26.40 20.25 17.28 o 14 12 1 189.14 205.09 27.51 o 0 13 1 837.41 811.13 27.84 o 1 13 1 511.46 475.27 12.60 o 2 13 1 1160.25 1108.25 25.87 o 3 13 1 722.36 772.92 20.05 o 4 13 1 572.77 590.79 19.14 o 5 13 1 7.46 -1.66 9.88 o 6 13 1 148.98 146.78 11.54 o 7 13 1 721.01 771.06 30.06 o 8 13 1 0.56 -3.12 9.08 o 9 13 1 265.49 284.75 16.14 o 10 13 1 333.70 417.36 21.13 o 11 13 1 533.72 523.38 24.42 o 12 13 1 493.86 521.59 27.62 o 13 13 1 47.35 18.68 17.59 o 14 13 1 96.53 61.87 22.03 o 1 14 1 476.74 514.33 13.59 o 2 14 1 629.36 677.81 17.10 o 3 14 1 1805.70 1847.50 44.52 o 4 14 1 2885.24 2855.84 72.28 o 5 14 1 1043.37 1059.51 31.61 o 6 14 1 3.66 2.13 11.99 o 7 14 1 369.27 379.91 18.33 o 8 14 1 1254.33 1187.50 38.55 o 9 14 1 1.95 -19.07 12.71 o 10 14 1 295.89 335.02 24.95 o 11 14 1 550.15 573.11 25.82 o 12 14 1 14.35 24.92 16.15 o 13 14 1 76.78 54.26 19.02 o 14 14 1 20.66 23.71 20.13 o 0 15 1 34.07 31.24 7.57 o 1 15 1 16.39 3.97 5.18 o 2 15 1 46.41 55.98 5.58 o 3 15 1 418.07 381.13 15.02 o 4 15 1 382.18 371.28 12.86 o 5 15 1 858.15 892.81 30.23 o 6 15 1 1489.14 1498.27 46.79 o 7 15 1 257.94 247.88 15.70 o 8 15 1 31.86 37.77 17.19 o 9 15 1 3.03 -10.80 20.41 o 10 15 1 864.51 843.55 34.95 o 11 15 1 5.34 -3.79 15.23 o 12 15 1 259.69 293.21 32.33 o 13 15 1 17.68 12.42 19.17 o 14 15 1 3.68 -8.42 19.58 o 1 16 1 570.83 582.74 15.39 o 2 16 1 18.71 8.01 5.49 o 3 16 1 359.23 409.43 14.72 o 4 16 1 70.42 76.05 8.36 o 5 16 1 129.04 112.06 11.75 o 6 16 1 56.75 63.52 11.74 o 7 16 1 11.58 13.06 11.57 o 8 16 1 81.35 71.94 13.68 o 9 16 1 1808.57 1784.13 57.71 o 10 16 1 74.14 48.75 15.62 o 11 16 1 313.69 345.30 30.61 o 12 16 1 42.96 25.90 19.11 o 13 16 1 2.53 0.44 18.93 o 14 16 1 0.44 -10.21 20.47 o 0 17 1 315.97 325.61 14.91 o 1 17 1 122.60 147.42 7.45 o 2 17 1 293.54 312.64 10.89 o 3 17 1 2.12 0.22 8.18 o 4 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