#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/10/2211020.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211020_Fobs loop_ _publ_author_name 'Oliveira-Campos, Ana Maria Ferreira' 'Rodrigues, Ligia M.' 'Kaja, Martin' 'Guilardi, Silvana' 'de Franca, Eduardo' 'Ellena, Javier' _publ_section_title ; 7-Amino-1-(3-bromophenyl)-3-cyanopyrazolo[4,3-d]pyrimidine ; _journal_coeditor_code HB2161 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5246 _journal_page_last o5248 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.560 _cell_angle_gamma 90.000 _cell_length_a 7.7153 _cell_length_b 7.6270 _cell_length_c 20.3497 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8089 _[local]_cod_data_source_file hb2161IIIasup2.hkl _[local]_cod_data_source_block IIIa #BEGIN Tags that were not found in dictionaries: _shelx_title ' silvana amostra 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 187.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28696.20 27671.21 1036.97 o 4 0 0 1713.88 1941.09 52.18 o 6 0 0 74.14 49.90 8.23 o 8 0 0 561.48 623.40 22.14 o 1 1 0 4893.77 354.52 2330.52 o 2 1 0 10071.39 9973.55 218.44 o 3 1 0 554.29 480.50 14.99 o 4 1 0 16284.62 17171.32 297.64 o 5 1 0 579.36 546.30 16.57 o 6 1 0 3328.90 3586.68 132.10 o 7 1 0 241.41 252.41 20.58 o 8 1 0 23.09 17.80 6.55 o 9 1 0 4.10 4.14 6.76 o 0 2 0 22659.73 24335.72 900.67 o 1 2 0 14026.76 9218.18 4818.46 o 2 2 0 13160.63 13686.33 310.11 o 3 2 0 238.29 248.55 8.92 o 4 2 0 60.51 51.78 6.47 o 5 2 0 670.50 618.31 18.03 o 6 2 0 872.90 851.47 21.88 o 7 2 0 15.23 6.60 5.76 o 8 2 0 548.61 565.48 17.98 o 9 2 0 1.27 7.96 17.60 o 1 3 0 1068.05 978.60 25.45 o 2 3 0 3424.08 3434.07 75.53 o 3 3 0 114.01 125.39 6.46 o 4 3 0 2780.99 2836.00 62.84 o 5 3 0 23.11 22.29 6.87 o 6 3 0 614.18 614.80 36.28 o 7 3 0 19.48 20.15 8.75 o 8 3 0 36.06 38.97 7.27 o 9 3 0 91.45 70.71 21.09 o 0 4 0 611.92 647.08 26.79 o 1 4 0 418.94 390.61 11.38 o 2 4 0 6697.87 7377.00 139.34 o 3 4 0 294.81 264.44 12.72 o 4 4 0 526.80 536.19 17.16 o 5 4 0 495.28 560.84 30.89 o 6 4 0 118.70 135.10 11.59 o 7 4 0 148.45 120.33 16.87 o 8 4 0 66.07 70.61 9.98 o 1 5 0 3064.92 3178.71 87.40 o 2 5 0 1160.71 1227.36 26.06 o 3 5 0 997.65 1069.77 23.75 o 4 5 0 230.37 245.83 11.95 o 5 5 0 159.04 160.78 15.22 o 6 5 0 20.10 26.66 8.40 o 7 5 0 29.61 37.62 7.05 o 8 5 0 2.32 10.73 12.59 o 0 6 0 51.64 55.04 7.20 o 1 6 0 593.14 603.95 16.77 o 2 6 0 23.38 8.69 10.29 o 3 6 0 468.47 491.90 17.18 o 4 6 0 59.44 60.50 16.90 o 5 6 0 336.97 328.39 14.04 o 6 6 0 129.09 130.49 15.33 o 7 6 0 57.68 50.38 11.27 o 1 7 0 412.51 412.36 23.68 o 2 7 0 51.42 47.80 13.31 o 3 7 0 289.85 271.16 13.73 o 4 7 0 2.14 -10.20 30.35 o 5 7 0 11.86 15.33 19.03 o 6 7 0 39.61 34.47 11.83 o 0 8 0 29.81 25.21 3.09 o 1 8 0 158.40 155.44 9.39 o 2 8 0 2.51 -10.53 11.63 o 3 8 0 596.55 614.81 34.14 o 4 8 0 25.16 14.93 13.37 o 5 8 0 489.26 418.44 60.22 o 1 9 0 741.64 757.14 59.80 o 2 9 0 73.15 67.64 24.95 o -9 0 1 0.66 -10.80 19.03 o -7 0 1 2376.97 2596.30 57.82 o -5 0 1 5212.71 5313.16 117.00 o -3 0 1 7140.71 6582.33 365.90 o 1 0 1 1687.01 1534.17 406.63 o 3 0 1 74.59 90.55 8.75 o 5 0 1 801.16 716.70 22.67 o 7 0 1 75.77 77.68 10.80 o 9 0 1 3.31 11.32 12.35 o -9 1 1 233.93 251.74 13.92 o -8 1 1 33.04 23.15 6.18 o -7 1 1 150.87 168.45 10.12 o -6 1 1 268.14 265.72 14.64 o -5 1 1 310.47 336.21 23.92 o -4 1 1 70.92 61.63 9.07 o -3 1 1 1103.97 936.76 38.62 o -2 1 1 2333.25 2363.17 69.84 o -1 1 1 1586.16 1604.60 41.35 o 1 1 1 2418.80 1059.35 634.05 o 2 1 1 40.66 71.68 16.41 o 3 1 1 127.05 146.12 7.24 o 4 1 1 817.81 821.71 32.95 o 5 1 1 66.77 67.70 5.88 o 6 1 1 8.40 12.99 7.50 o 7 1 1 1197.19 1270.92 59.52 o 8 1 1 28.90 16.98 14.77 o 9 1 1 315.83 326.51 34.73 o -9 2 1 30.20 20.42 14.15 o -8 2 1 6.09 6.49 8.37 o -7 2 1 527.76 535.57 19.58 o -6 2 1 254.97 246.08 9.43 o -5 2 1 2530.12 2612.55 62.88 o -4 2 1 26.40 28.98 6.01 o -3 2 1 3593.64 3472.63 100.03 o -2 2 1 379.87 354.15 25.50 o -1 2 1 3503.86 3776.94 602.92 o 0 2 1 718.01 683.84 17.85 o 1 2 1 685.27 696.30 450.62 o 2 2 1 3.94 36.07 6.77 o 3 2 1 2864.83 2675.16 55.49 o 4 2 1 1280.31 1358.61 29.17 o 5 2 1 902.41 851.61 22.68 o 6 2 1 977.78 988.94 20.29 o 7 2 1 22.82 28.02 11.26 o 8 2 1 354.79 352.63 19.56 o 9 2 1 50.36 39.70 23.15 o -9 3 1 140.91 132.09 18.52 o -8 3 1 30.66 46.77 11.25 o -7 3 1 99.75 113.26 9.10 o -6 3 1 1103.06 1100.77 29.89 o -5 3 1 13.39 19.52 8.61 o -4 3 1 715.48 707.15 15.15 o -3 3 1 447.60 392.85 9.70 o -2 3 1 44.16 35.51 7.28 o -1 3 1 8619.48 8676.39 152.37 o 0 3 1 236.07 230.48 7.08 o 1 3 1 3640.09 3698.75 107.51 o 2 3 1 3038.43 3156.95 77.77 o 3 3 1 1414.74 1465.38 46.98 o 4 3 1 932.26 927.17 38.02 o 5 3 1 405.53 393.70 13.38 o 6 3 1 110.77 93.11 11.77 o 7 3 1 854.46 884.77 28.64 o 8 3 1 47.61 25.55 8.12 o -8 4 1 370.45 368.06 31.68 o -7 4 1 381.54 385.36 21.62 o -6 4 1 251.93 254.46 9.45 o -5 4 1 1987.51 2199.97 34.56 o -4 4 1 88.13 90.04 6.79 o -3 4 1 2827.36 2917.74 56.92 o -2 4 1 3449.10 3638.30 62.42 o -1 4 1 1089.26 1115.33 25.64 o 0 4 1 3209.21 3180.51 67.78 o 1 4 1 415.21 400.48 18.87 o 2 4 1 129.67 187.41 24.35 o 3 4 1 2371.00 2441.18 63.69 o 4 4 1 315.70 331.17 13.64 o 5 4 1 1601.31 1674.66 59.58 o 6 4 1 961.06 1099.77 25.87 o 7 4 1 190.30 199.14 25.47 o 8 4 1 491.97 423.85 27.24 o -8 5 1 100.68 80.30 12.86 o -7 5 1 293.51 299.11 30.35 o -6 5 1 1642.41 1791.61 71.46 o -5 5 1 323.80 324.41 13.66 o -4 5 1 3332.81 3591.36 80.36 o -3 5 1 1369.10 1401.49 29.06 o -2 5 1 939.70 955.37 37.24 o -1 5 1 1471.99 1518.66 51.52 o 0 5 1 64.16 65.69 4.43 o 1 5 1 2886.47 3089.74 74.18 o 2 5 1 2858.19 2980.01 67.49 o 3 5 1 65.82 88.89 17.80 o 4 5 1 1562.14 1622.49 50.55 o 5 5 1 298.63 281.36 8.28 o 6 5 1 129.77 146.84 7.44 o 7 5 1 87.47 86.10 8.83 o 8 5 1 9.33 37.98 26.06 o -7 6 1 59.54 54.26 7.33 o -6 6 1 289.59 250.68 21.39 o -5 6 1 232.20 251.86 19.83 o -4 6 1 88.47 77.17 9.39 o -3 6 1 293.50 309.94 18.94 o -2 6 1 2499.35 2648.69 57.08 o -1 6 1 36.76 34.52 6.03 o 0 6 1 2817.06 2890.49 82.45 o 1 6 1 1024.61 1051.65 37.29 o 2 6 1 592.72 596.94 34.50 o 3 6 1 448.46 488.80 24.70 o 4 6 1 288.73 283.85 17.10 o 5 6 1 467.24 463.77 21.12 o 6 6 1 679.20 698.27 26.30 o 7 6 1 76.65 60.41 15.09 o -6 7 1 184.29 148.18 23.67 o -5 7 1 126.02 115.42 20.64 o -4 7 1 1712.76 1712.29 58.18 o -3 7 1 341.20 356.20 26.50 o -2 7 1 1020.59 1005.66 26.05 o -1 7 1 696.63 754.12 30.19 o 0 7 1 357.84 348.69 8.01 o 1 7 1 539.72 544.72 17.93 o 2 7 1 1280.28 1298.44 32.91 o 3 7 1 122.68 115.06 30.61 o 4 7 1 1498.75 1558.18 37.00 o 5 7 1 23.63 31.74 13.02 o 6 7 1 457.59 450.30 30.03 o -5 8 1 15.58 12.00 11.68 o -4 8 1 100.73 75.64 33.18 o -3 8 1 48.04 23.56 20.06 o -2 8 1 1278.28 1360.25 54.87 o -1 8 1 17.64 19.90 11.71 o 0 8 1 1889.60 1985.51 25.61 o 1 8 1 43.10 32.66 6.94 o 2 8 1 827.93 782.87 49.22 o 3 8 1 120.75 88.71 20.32 o 4 8 1 4.88 2.33 18.78 o -2 9 1 110.97 82.42 23.08 o -1 9 1 15.80 0.00 25.93 o 0 9 1 47.61 48.16 20.45 o 1 9 1 0.17 9.39 29.32 o 2 9 1 773.67 673.42 28.56 o -8 0 2 919.70 1002.77 37.60 o -6 0 2 448.36 456.11 15.44 o -4 0 2 3516.51 3573.52 284.18 o -2 0 2 17823.10 18859.72 435.07 o 2 0 2 35245.26 35419.16 1747.25 o 4 0 2 297.68 246.57 42.73 o 6 0 2 2261.57 2343.92 60.42 o 8 0 2 496.68 505.47 24.71 o -9 1 2 17.10 12.29 10.29 o -8 1 2 392.99 389.77 12.19 o -7 1 2 17.87 19.08 9.08 o -6 1 2 1703.03 1734.10 43.19 o -5 1 2 123.68 132.24 5.82 o -4 1 2 4105.64 3976.73 75.28 o -3 1 2 1718.58 1821.28 42.25 o -2 1 2 2438.57 2518.72 136.56 o -1 1 2 4282.80 370.38 1468.93 o 0 1 2 7227.32 691.89 2091.26 o 1 1 2 811.48 538.39 181.10 o 2 1 2 24623.51 24291.50 348.01 o 3 1 2 3240.50 3256.60 66.03 o 4 1 2 5196.51 4968.38 176.30 o 5 1 2 1.90 7.43 5.19 o 6 1 2 1145.46 1148.33 27.36 o 7 1 2 17.37 20.85 21.86 o 8 1 2 168.55 133.00 12.72 o 9 1 2 95.40 77.26 17.75 o -9 2 2 2.56 10.36 9.88 o -8 2 2 953.65 992.45 21.02 o -7 2 2 50.08 52.36 7.37 o -6 2 2 400.25 394.63 13.11 o -5 2 2 18.47 20.00 6.32 o -4 2 2 585.56 564.80 16.03 o -3 2 2 574.68 552.28 21.63 o -2 2 2 4036.21 3872.86 66.30 o -1 2 2 868.89 905.63 25.79 o 0 2 2 3708.51 3250.01 420.76 o 1 2 2 29044.68 30787.44 1266.62 o 2 2 2 231.66 239.53 6.23 o 3 2 2 187.74 158.18 7.67 o 4 2 2 1975.50 1991.08 42.33 o 5 2 2 575.96 548.32 32.19 o 6 2 2 2585.10 2740.22 74.71 o 7 2 2 314.16 264.46 17.36 o 8 2 2 1152.12 1090.89 86.55 o 9 2 2 20.78 2.77 17.75 o -9 3 2 48.05 41.38 13.10 o -8 3 2 285.14 274.17 23.14 o -7 3 2 266.51 281.43 10.36 o -6 3 2 1809.38 1890.41 42.13 o -5 3 2 149.73 145.74 9.18 o -4 3 2 2248.98 2247.75 38.66 o -3 3 2 1340.27 1409.60 27.19 o -2 3 2 137.65 122.82 5.51 o -1 3 2 31.38 28.74 2.29 o 0 3 2 4936.98 5002.70 168.16 o 1 3 2 623.65 529.33 17.79 o 2 3 2 3639.29 3585.67 91.26 o 3 3 2 50.53 50.06 5.62 o 4 3 2 3974.46 4006.76 75.77 o 5 3 2 796.74 833.94 25.26 o 6 3 2 287.60 243.13 10.03 o 7 3 2 1008.49 1062.38 31.37 o 8 3 2 83.57 69.81 10.26 o -8 4 2 66.32 84.52 7.79 o -7 4 2 84.10 95.74 8.60 o -6 4 2 6.44 -0.16 9.54 o -5 4 2 259.13 256.40 10.04 o -4 4 2 423.09 473.13 24.52 o -3 4 2 156.18 140.79 16.57 o -2 4 2 3561.26 3567.43 110.58 o -1 4 2 499.43 536.71 12.49 o 0 4 2 8817.42 9237.29 161.61 o 1 4 2 2203.40 2298.79 68.15 o 2 4 2 603.94 664.47 24.87 o 3 4 2 3998.20 4123.52 111.73 o 4 4 2 38.78 31.50 5.17 o 5 4 2 1086.44 1098.48 40.54 o 6 4 2 249.77 245.63 19.92 o 7 4 2 109.46 110.09 19.89 o 8 4 2 116.18 107.51 12.40 o -8 5 2 60.96 40.79 17.43 o -7 5 2 3.12 14.82 18.41 o -6 5 2 961.00 1013.52 20.68 o -5 5 2 67.24 70.21 9.28 o -4 5 2 279.67 302.02 11.99 o -3 5 2 1835.07 2008.24 58.38 o -2 5 2 283.02 294.22 14.98 o -1 5 2 2665.46 2730.55 67.97 o 0 5 2 14.70 14.17 2.84 o 1 5 2 2351.09 2444.36 53.07 o 2 5 2 930.00 972.79 33.83 o 3 5 2 96.51 76.13 14.04 o 4 5 2 783.74 838.55 29.63 o 5 5 2 75.83 78.03 14.59 o 6 5 2 124.11 115.10 29.14 o 7 5 2 79.20 83.43 8.63 o -7 6 2 122.08 119.94 17.08 o -6 6 2 1.68 -5.27 11.61 o -5 6 2 373.85 376.17 18.17 o -4 6 2 24.92 30.58 8.13 o -3 6 2 32.73 25.76 6.90 o -2 6 2 74.54 71.40 7.72 o -1 6 2 406.10 422.40 37.58 o 0 6 2 42.32 50.00 4.19 o 1 6 2 701.75 702.87 17.95 o 2 6 2 9.36 15.80 12.16 o 3 6 2 3392.62 3689.95 71.86 o 4 6 2 287.08 285.48 19.43 o 5 6 2 570.71 522.69 31.63 o 6 6 2 194.37 176.01 14.18 o 7 6 2 28.97 26.27 4.02 o -6 7 2 55.57 34.42 16.20 o -5 7 2 52.26 41.76 19.29 o -4 7 2 322.56 324.15 23.16 o -3 7 2 282.46 297.04 35.51 o -2 7 2 29.93 24.12 8.69 o -1 7 2 2268.12 2397.87 100.13 o 0 7 2 26.86 29.76 5.66 o 1 7 2 213.55 212.58 21.61 o 2 7 2 25.12 36.66 7.79 o 3 7 2 52.22 49.59 9.66 o 4 7 2 7.38 3.06 16.63 o 5 7 2 416.45 428.80 28.29 o 6 7 2 0.93 20.69 24.64 o -5 8 2 455.18 397.22 47.09 o -4 8 2 55.65 63.97 43.21 o -3 8 2 514.63 479.21 23.16 o -2 8 2 7.84 11.37 7.97 o -1 8 2 9.70 -0.87 9.00 o 0 8 2 15.15 14.94 2.18 o 1 8 2 462.74 455.93 20.51 o 2 8 2 208.56 212.68 22.31 o 3 8 2 856.90 902.68 42.03 o 4 8 2 14.95 13.68 11.93 o -2 9 2 57.37 44.84 17.75 o -1 9 2 1271.86 1283.23 87.57 o 0 9 2 0.35 -28.69 34.98 o 1 9 2 1069.63 1062.85 70.89 o 2 9 2 107.67 64.41 16.73 o -9 0 3 404.22 385.98 28.31 o -7 0 3 60.38 59.67 8.23 o -5 0 3 3172.34 3190.87 323.87 o -3 0 3 1854.61 1827.41 56.41 o -1 0 3 1566.94 561.71 743.16 o 1 0 3 5701.03 4718.79 201.43 o 3 0 3 5419.19 4887.54 147.63 o 5 0 3 52.52 47.33 8.75 o 7 0 3 204.18 189.87 33.45 o 9 0 3 163.74 150.75 18.52 o -9 1 3 142.98 162.59 34.47 o -8 1 3 176.99 174.62 13.89 o -7 1 3 190.11 181.44 10.39 o -6 1 3 190.80 181.64 11.64 o -5 1 3 1944.00 2104.83 54.68 o -4 1 3 1409.70 1463.48 30.95 o -3 1 3 4694.94 4508.51 89.07 o -2 1 3 9.16 7.23 6.17 o -1 1 3 7759.72 2164.76 2690.52 o 0 1 3 24.35 12.54 6.26 o 1 1 3 1852.75 1177.22 351.86 o 2 1 3 25.45 13.12 6.76 o 3 1 3 341.66 309.14 10.25 o 4 1 3 1.29 12.00 6.35 o 5 1 3 1833.67 1828.55 32.29 o 6 1 3 0.17 8.65 7.08 o 7 1 3 305.84 351.88 16.78 o 8 1 3 34.00 43.93 11.87 o 9 1 3 30.02 21.20 11.70 o -9 2 3 9.41 -11.02 18.09 o -8 2 3 366.14 366.43 15.05 o -7 2 3 670.75 694.89 25.07 o -6 2 3 674.99 701.21 13.97 o -5 2 3 893.44 905.81 25.15 o -4 2 3 1542.58 1590.18 34.19 o -3 2 3 37.30 32.44 3.68 o -2 2 3 3177.24 3253.60 55.48 o -1 2 3 4043.25 3981.19 108.90 o 0 2 3 2557.93 2291.87 214.51 o 1 2 3 16667.04 16617.16 345.71 o 2 2 3 86.61 99.25 5.03 o 3 2 3 2697.59 2470.01 44.17 o 4 2 3 10.15 -3.77 8.93 o 5 2 3 1026.50 1029.16 35.22 o 6 2 3 239.08 242.51 15.56 o 7 2 3 0.77 8.68 7.01 o 8 2 3 81.61 72.97 11.49 o 9 2 3 151.31 137.62 16.72 o -9 3 3 277.86 259.14 23.72 o -8 3 3 268.95 271.66 41.61 o -7 3 3 83.56 84.59 4.70 o -6 3 3 117.41 117.57 7.95 o -5 3 3 363.86 397.92 16.75 o -4 3 3 1671.58 1800.02 34.42 o -3 3 3 6456.39 6817.09 98.65 o -2 3 3 59.99 55.73 4.51 o -1 3 3 5372.52 5268.01 161.66 o 0 3 3 3135.20 3110.41 102.20 o 1 3 3 2377.52 2262.83 77.30 o 2 3 3 3332.44 3244.56 57.63 o 3 3 3 32.11 29.75 5.52 o 4 3 3 866.27 854.59 21.41 o 5 3 3 692.95 674.50 22.13 o 6 3 3 73.08 49.27 7.33 o 7 3 3 383.59 423.17 14.64 o 8 3 3 311.84 326.79 20.36 o -8 4 3 43.74 36.52 15.40 o -7 4 3 1355.28 1435.66 34.14 o -6 4 3 0.03 2.99 4.56 o -5 4 3 1336.07 1374.81 24.24 o -4 4 3 1841.56 1925.31 33.31 o -3 4 3 821.72 833.16 33.03 o -2 4 3 5722.80 5855.17 245.35 o -1 4 3 520.62 494.80 14.90 o 0 4 3 4293.47 4395.90 63.21 o 1 4 3 2827.06 2727.30 63.53 o 2 4 3 3423.42 3653.75 85.73 o 3 4 3 3154.10 3214.53 90.20 o 4 4 3 652.68 673.62 27.31 o 5 4 3 732.29 695.23 26.13 o 6 4 3 454.33 438.96 27.03 o 7 4 3 39.67 18.06 9.81 o 8 4 3 37.35 41.95 18.25 o -8 5 3 214.84 160.19 29.15 o -7 5 3 0.31 10.37 5.19 o -6 5 3 1124.24 1210.58 28.99 o -5 5 3 13.42 10.80 10.67 o -4 5 3 1839.95 1993.88 36.93 o -3 5 3 1759.02 1796.62 49.77 o -2 5 3 884.77 920.36 26.08 o -1 5 3 4088.86 4205.73 51.45 o 0 5 3 575.75 548.92 12.41 o 1 5 3 687.10 651.00 22.93 o 2 5 3 1910.97 1906.74 56.63 o 3 5 3 52.19 31.89 12.05 o 4 5 3 864.47 883.32 20.99 o 5 5 3 520.30 536.34 28.29 o 6 5 3 25.27 23.67 10.43 o 7 5 3 713.67 747.30 48.48 o -7 6 3 65.92 53.20 7.59 o -6 6 3 0.71 4.04 6.58 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