#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211108.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211108_Fobs loop_ _publ_author_name 'Yathirajan, H. S.' 'Narayana, B.' 'Ashalatha, B. V.' 'Sarojini, B. K.' 'Bolte, Michael' _publ_section_title ; (2E)-1-(3-Bromo-2-thienyl)-3-(4-methoxy-2,3,6-trimethylphenyl)prop-2-en-1-one ; _journal_coeditor_code LH2201 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5010 _journal_page_last o5012 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.953 _cell_angle_gamma 90.000 _cell_length_a 8.1973 _cell_length_b 12.3023 _cell_length_c 16.0999 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.7676 _[local]_cod_data_source_file lh2201Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat45 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8264.56 8414.28 140.04 o 3 0 0 172.04 168.08 24.16 o 4 0 0 684.50 619.57 34.18 o 5 0 0 988.44 1040.02 36.83 o 6 0 0 2705.11 2697.11 65.52 o 7 0 0 1291.39 1222.10 42.19 o 8 0 0 2.00 10.01 27.79 o 9 0 0 1487.70 1703.80 166.70 o 10 0 0 50.18 58.67 32.18 o 2 1 0 7535.22 7075.62 74.83 o 3 1 0 2201.37 2352.29 114.82 o 4 1 0 716.19 737.79 65.07 o 5 1 0 55.39 38.66 20.07 o 6 1 0 330.23 384.41 75.40 o 7 1 0 87.36 94.61 22.94 o 8 1 0 8.30 25.23 19.10 o 9 1 0 22.28 23.22 22.04 o 10 1 0 26.45 33.20 23.90 o 1 2 0 665.45 573.63 14.50 o 2 2 0 22296.73 22999.65 657.32 o 3 2 0 5675.25 5492.02 50.08 o 4 2 0 3653.86 3395.15 120.43 o 5 2 0 3430.11 3549.27 45.65 o 6 2 0 1627.60 1628.83 109.22 o 7 2 0 382.92 381.29 23.72 o 8 2 0 5.87 0.59 22.44 o 9 2 0 946.12 1114.46 197.35 o 10 2 0 3.29 44.69 32.21 o 1 3 0 3978.92 3407.09 54.22 o 2 3 0 1333.59 1156.98 45.71 o 3 3 0 4547.04 4789.16 128.74 o 4 3 0 179.61 206.58 13.25 o 5 3 0 710.79 697.56 29.51 o 6 3 0 2328.90 2530.77 252.26 o 7 3 0 757.02 806.04 123.65 o 8 3 0 253.20 363.05 32.11 o 9 3 0 1.36 12.47 20.90 o 10 3 0 14.11 39.23 33.03 o 0 4 0 12056.73 10562.59 985.70 o 1 4 0 1296.16 1159.62 31.97 o 2 4 0 1871.44 1755.13 93.26 o 3 4 0 1462.12 1429.07 88.64 o 4 4 0 2080.71 2002.92 168.68 o 5 4 0 347.44 312.04 15.96 o 6 4 0 199.25 189.96 28.43 o 7 4 0 355.50 386.40 29.81 o 8 4 0 18.38 33.64 20.74 o 9 4 0 504.61 395.15 25.53 o 10 4 0 36.19 26.15 31.84 o 1 5 0 6453.52 6522.09 122.67 o 2 5 0 562.83 501.18 13.45 o 3 5 0 11203.65 10879.78 676.40 o 4 5 0 28.44 38.98 14.28 o 5 5 0 125.21 91.14 14.50 o 6 5 0 2718.55 2917.07 64.63 o 7 5 0 334.48 419.75 31.56 o 8 5 0 1093.50 1307.54 43.03 o 9 5 0 66.36 81.40 30.28 o 0 6 0 1371.34 1455.74 23.78 o 1 6 0 533.44 558.29 11.67 o 2 6 0 44.37 54.13 9.68 o 3 6 0 18.32 24.70 11.48 o 4 6 0 0.46 9.37 10.59 o 5 6 0 12.60 10.86 13.87 o 6 6 0 62.61 137.99 40.58 o 7 6 0 34.82 -7.58 18.31 o 8 6 0 25.73 19.01 29.42 o 9 6 0 4.89 14.40 22.38 o 1 7 0 5830.66 6137.84 142.72 o 2 7 0 2365.34 2458.85 92.58 o 3 7 0 3797.86 3463.98 243.06 o 4 7 0 89.73 92.43 12.96 o 5 7 0 798.95 774.35 43.19 o 6 7 0 1542.12 1514.97 25.44 o 7 7 0 421.20 452.51 27.52 o 8 7 0 681.93 525.96 22.12 o 9 7 0 1.71 -8.23 30.59 o 0 8 0 495.98 476.19 19.75 o 1 8 0 270.58 263.56 9.38 o 2 8 0 117.51 130.02 10.89 o 3 8 0 406.07 344.18 23.29 o 4 8 0 2691.22 2536.02 176.13 o 5 8 0 1642.45 1757.34 80.68 o 6 8 0 439.03 424.98 14.28 o 7 8 0 169.95 147.72 21.60 o 8 8 0 46.99 31.83 19.97 o 1 9 0 1003.36 1021.53 20.89 o 2 9 0 79.30 97.66 8.71 o 3 9 0 3762.03 3747.12 217.43 o 4 9 0 16.23 12.61 13.63 o 5 9 0 80.48 102.27 15.43 o 6 9 0 1712.43 1586.91 33.66 o 7 9 0 96.25 98.82 14.12 o 8 9 0 298.61 329.61 28.72 o 0 10 0 5477.16 5657.29 56.01 o 1 10 0 699.10 691.16 13.94 o 2 10 0 3385.23 3541.43 27.97 o 3 10 0 89.74 95.45 13.81 o 4 10 0 351.42 329.92 24.20 o 5 10 0 1118.53 1192.47 78.04 o 6 10 0 405.85 395.20 18.84 o 7 10 0 192.93 179.43 12.70 o 8 10 0 39.37 25.20 18.83 o 1 11 0 27.03 44.66 14.09 o 2 11 0 18.17 32.47 10.67 o 3 11 0 498.27 481.01 27.11 o 4 11 0 423.76 413.70 25.96 o 5 11 0 83.51 94.87 11.82 o 6 11 0 494.22 410.46 18.44 o 7 11 0 55.04 40.10 14.87 o 0 12 0 5244.05 5929.96 284.37 o 1 12 0 0.61 23.01 12.17 o 2 12 0 714.48 796.22 31.26 o 3 12 0 456.00 419.49 29.98 o 4 12 0 853.30 754.48 45.29 o 5 12 0 603.82 633.87 36.45 o 6 12 0 512.81 513.37 29.31 o 1 13 0 22.13 36.50 11.11 o 2 13 0 5.14 21.37 11.66 o 3 13 0 58.29 84.53 10.89 o 4 13 0 1.67 1.34 9.21 o 5 13 0 0.27 3.40 13.35 o 6 13 0 35.39 6.14 9.82 o 0 14 0 1676.74 1867.31 29.91 o 1 14 0 66.11 69.30 11.46 o 2 14 0 343.91 329.40 19.87 o 3 14 0 362.27 341.13 27.31 o 4 14 0 222.05 173.77 14.82 o 5 14 0 336.70 306.21 23.92 o 1 15 0 375.00 377.64 16.48 o 2 15 0 3.90 21.07 13.02 o 3 15 0 63.43 79.95 21.98 o 0 16 0 97.31 107.04 18.70 o -10 1 1 45.31 48.31 29.46 o -9 1 1 1148.49 1334.54 192.96 o -8 1 1 90.68 115.45 20.04 o -7 1 1 3198.41 3338.82 55.24 o -6 1 1 158.27 139.95 19.72 o -5 1 1 1922.32 1923.79 146.54 o -4 1 1 7619.58 7186.58 150.11 o -3 1 1 5093.89 4828.22 49.33 o -2 1 1 1683.78 1677.86 54.89 o 2 1 1 34067.71 40734.41 2038.51 o 3 1 1 335.16 364.70 19.38 o 4 1 1 275.67 259.32 19.69 o 5 1 1 6480.70 7647.57 135.27 o 6 1 1 207.89 196.07 18.22 o 7 1 1 1129.96 1469.37 102.15 o 8 1 1 0.79 14.83 19.56 o 9 1 1 669.44 750.09 97.55 o 10 1 1 79.93 91.12 22.57 o -10 2 1 143.89 179.01 42.72 o -9 2 1 28.97 31.15 25.93 o -8 2 1 290.78 285.14 38.40 o -7 2 1 600.45 630.68 61.52 o -6 2 1 920.36 1031.27 96.74 o -5 2 1 642.23 600.62 16.40 o -4 2 1 1627.60 1816.05 29.11 o -3 2 1 880.83 738.26 17.65 o -2 2 1 20301.43 19816.36 949.57 o -1 2 1 4271.05 3863.67 62.39 o 0 2 1 1.00 5.71 13.15 o 1 2 1 79.16 106.54 14.57 o 2 2 1 2474.01 2484.04 83.15 o 3 2 1 35.23 57.59 25.54 o 4 2 1 775.68 847.61 65.63 o 5 2 1 326.22 340.74 30.52 o 6 2 1 680.70 815.28 31.29 o 7 2 1 137.79 136.47 21.03 o 8 2 1 1140.68 1452.50 140.90 o 9 2 1 149.73 176.24 25.09 o 10 2 1 33.90 62.95 31.88 o -10 3 1 12.70 29.48 32.10 o -9 3 1 1168.13 1144.71 42.31 o -8 3 1 0.26 -7.74 28.36 o -7 3 1 2044.67 1771.60 43.99 o -6 3 1 73.08 56.32 14.34 o -5 3 1 516.14 524.09 17.18 o -4 3 1 822.21 598.40 19.06 o -3 3 1 58.41 77.11 28.85 o -2 3 1 52.35 41.62 11.26 o -1 3 1 4243.89 3947.78 82.79 o 0 3 1 12904.64 12111.85 357.62 o 1 3 1 197.35 172.04 15.18 o 2 3 1 4001.57 3700.94 33.85 o 3 3 1 1248.30 1253.86 35.51 o 4 3 1 683.76 648.86 39.50 o 5 3 1 1207.33 1403.12 177.95 o 6 3 1 787.45 819.28 42.41 o 7 3 1 550.65 641.75 25.03 o 8 3 1 97.15 93.55 18.93 o 9 3 1 221.99 245.48 33.99 o 10 3 1 64.53 43.38 32.72 o -10 4 1 606.55 715.63 38.67 o -9 4 1 8.47 37.18 29.89 o -8 4 1 740.28 764.72 34.85 o -7 4 1 470.13 580.35 30.28 o -6 4 1 4529.15 4912.65 112.93 o -5 4 1 36.73 25.06 16.29 o -4 4 1 6254.37 6645.25 132.84 o -3 4 1 2691.53 2448.83 100.04 o -2 4 1 42.10 44.60 11.99 o -1 4 1 14928.35 14373.58 280.10 o 0 4 1 3311.48 2901.56 149.06 o 1 4 1 1394.93 1307.08 16.71 o 2 4 1 4750.78 4576.48 284.78 o 3 4 1 8260.81 7835.74 308.44 o 4 4 1 213.26 193.17 13.35 o 5 4 1 666.60 742.40 85.17 o 6 4 1 1267.89 1525.87 116.07 o 7 4 1 2.49 6.87 18.31 o 8 4 1 1613.42 1802.03 48.89 o 9 4 1 102.77 135.86 31.18 o -9 5 1 105.72 78.83 29.91 o -8 5 1 50.29 121.46 28.44 o -7 5 1 414.50 380.94 15.11 o -6 5 1 39.66 27.54 19.00 o -5 5 1 21.03 31.97 14.19 o -4 5 1 173.65 124.52 17.83 o -3 5 1 1499.31 1432.94 120.74 o -2 5 1 148.90 146.31 11.53 o -1 5 1 1596.10 1453.49 28.06 o 0 5 1 1919.52 1791.40 82.20 o 1 5 1 334.13 325.25 10.51 o 2 5 1 2725.71 2485.23 120.57 o 3 5 1 1.85 11.37 10.54 o 4 5 1 16.72 9.59 10.68 o 5 5 1 1269.33 1170.05 73.78 o 6 5 1 206.38 162.79 27.66 o 7 5 1 3.78 23.56 27.87 o 8 5 1 0.13 -22.62 22.62 o 9 5 1 150.13 90.32 22.78 o -9 6 1 94.98 148.63 28.21 o -8 6 1 761.19 810.20 35.30 o -7 6 1 311.58 313.92 46.01 o -6 6 1 7856.24 8189.13 468.82 o -5 6 1 414.08 411.04 20.95 o -4 6 1 2043.56 2124.86 156.78 o -3 6 1 1072.80 934.23 79.08 o -2 6 1 184.95 149.09 14.60 o -1 6 1 12182.85 11832.02 133.18 o 0 6 1 50.80 60.52 8.48 o 1 6 1 6618.58 6782.29 96.38 o 2 6 1 496.43 450.44 24.23 o 3 6 1 4807.53 4440.16 329.85 o 4 6 1 1260.68 1303.87 39.00 o 5 6 1 1134.23 1101.13 42.07 o 6 6 1 922.54 989.46 32.13 o 7 6 1 16.37 46.58 18.47 o 8 6 1 1733.81 2005.00 53.75 o 9 6 1 42.82 66.44 29.26 o -9 7 1 9.12 12.33 21.60 o -8 7 1 75.53 72.10 28.71 o -7 7 1 11.55 11.54 24.05 o -6 7 1 88.94 102.88 15.00 o -5 7 1 59.34 81.05 13.87 o -4 7 1 77.76 47.19 25.39 o -3 7 1 1199.06 1193.50 69.93 o -2 7 1 336.37 371.85 10.33 o -1 7 1 272.91 281.71 10.17 o 0 7 1 129.17 148.31 8.81 o 1 7 1 17.12 23.35 10.00 o 2 7 1 107.86 145.81 19.61 o 3 7 1 14.00 15.16 10.73 o 4 7 1 37.80 42.05 11.72 o 5 7 1 98.08 147.77 22.40 o 6 7 1 7.23 83.10 25.37 o 7 7 1 11.07 9.98 26.88 o 8 7 1 16.85 48.68 27.53 o 9 7 1 24.83 51.32 21.20 o -9 8 1 11.37 2.63 29.17 o -8 8 1 115.72 154.02 27.39 o -7 8 1 360.97 390.14 18.98 o -6 8 1 2300.51 2377.69 82.51 o -5 8 1 238.24 241.54 25.70 o -4 8 1 4552.45 4209.37 429.57 o -3 8 1 3344.38 3153.09 174.32 o -2 8 1 141.06 130.41 8.85 o -1 8 1 5152.52 5258.71 117.79 o 0 8 1 800.41 898.05 24.83 o 1 8 1 284.98 292.45 10.01 o 2 8 1 1013.49 1017.83 71.96 o 3 8 1 2482.11 2150.23 176.59 o 4 8 1 1571.67 1441.01 68.51 o 5 8 1 325.06 323.11 13.51 o 6 8 1 1213.26 1167.40 60.32 o 7 8 1 121.28 166.20 26.95 o 8 8 1 1022.49 941.08 29.04 o -8 9 1 17.60 33.63 25.72 o -7 9 1 194.54 201.42 18.88 o -6 9 1 527.28 493.86 19.43 o -5 9 1 481.33 515.09 26.25 o -4 9 1 67.69 48.30 11.90 o -3 9 1 2817.54 2683.00 107.32 o -2 9 1 88.74 87.20 13.08 o -1 9 1 80.10 114.60 11.88 o 0 9 1 2557.46 2704.97 23.42 o 1 9 1 535.76 577.00 12.00 o 2 9 1 54.57 70.45 14.48 o 3 9 1 65.08 42.44 10.36 o 4 9 1 373.91 368.30 19.89 o 5 9 1 819.40 854.78 16.09 o 6 9 1 297.83 330.19 32.08 o 7 9 1 638.45 669.86 29.51 o 8 9 1 59.82 -28.09 28.09 o -8 10 1 106.53 63.92 26.82 o -7 10 1 174.51 161.40 14.81 o -6 10 1 401.95 392.71 17.95 o -5 10 1 157.65 156.94 11.37 o -4 10 1 380.49 383.68 28.41 o -3 10 1 223.00 233.23 9.92 o -2 10 1 1108.52 1185.37 32.83 o -1 10 1 3173.48 3482.23 50.58 o 0 10 1 264.32 321.39 21.97 o 1 10 1 144.06 159.79 12.23 o 2 10 1 2891.32 2974.51 169.19 o 3 10 1 219.89 212.71 18.05 o 4 10 1 29.82 22.99 10.98 o 5 10 1 186.81 194.66 14.56 o 6 10 1 221.05 186.01 38.13 o 7 10 1 31.59 21.81 16.72 o -7 11 1 270.30 252.77 26.22 o -6 11 1 12.51 68.25 33.43 o -5 11 1 992.56 964.22 38.78 o -4 11 1 907.24 846.47 51.38 o -3 11 1 1339.48 1277.62 62.01 o -2 11 1 326.14 362.42 12.21 o -1 11 1 87.94 111.74 12.07 o 0 11 1 493.30 503.47 17.94 o 1 11 1 19.23 25.48 10.34 o 2 11 1 1184.93 1209.16 30.34 o 3 11 1 14.89 29.53 10.52 o 4 11 1 114.56 126.72 8.41 o 5 11 1 1012.62 1025.47 66.58 o 6 11 1 59.96 64.81 13.71 o 7 11 1 571.69 496.46 21.12 o -6 12 1 0.63 6.79 15.83 o -5 12 1 8.61 6.00 10.56 o -4 12 1 96.05 88.46 9.33 o -3 12 1 102.48 130.45 10.26 o -2 12 1 4.75 24.20 12.17 o -1 12 1 187.91 228.57 11.65 o 0 12 1 371.17 375.31 11.73 o 1 12 1 2.75 22.80 16.70 o 2 12 1 2.74 9.72 8.87 o 3 12 1 57.21 74.82 16.19 o 4 12 1 10.34 25.15 11.57 o 5 12 1 9.69 25.08 11.10 o 6 12 1 5.24 22.70 14.17 o -6 13 1 2.03 13.51 11.91 o -5 13 1 51.94 71.51 12.83 o -4 13 1 802.31 765.92 42.76 o -3 13 1 740.44 754.71 48.79 o -2 13 1 189.65 173.78 11.17 o -1 13 1 1.70 34.37 10.32 o 0 13 1 653.67 729.32 16.76 o 1 13 1 47.59 46.75 13.31 o 2 13 1 1244.74 1292.71 36.10 o 3 13 1 62.66 69.80 8.94 o 4 13 1 169.41 167.60 11.22 o 5 13 1 632.61 595.51 50.58 o -5 14 1 2.55 1.22 11.19 o -4 14 1 17.56 52.48 16.35 o -3 14 1 18.47 36.68 11.88 o -2 14 1 137.34 167.63 15.17 o -1 14 1 28.61 38.73 14.04 o 0 14 1 0.38 19.77 10.64 o 1 14 1 31.82 53.94 9.52 o 2 14 1 1.08 19.41 10.00 o 3 14 1 151.09 167.07 12.98 o 4 14 1 20.80 20.82 8.37 o -3 15 1 315.69 299.51 26.21 o -2 15 1 78.51 71.26 11.04 o -1 15 1 7.14 18.49 12.79 o 0 15 1 469.01 499.98 25.65 o 1 15 1 23.79 50.04 13.03 o 2 15 1 339.54 331.82 21.54 o 3 15 1 5.69 11.25 13.77 o 0 16 1 13.51 33.82 25.46 o -10 0 2 156.61 187.43 36.01 o -9 0 2 1105.34 1034.43 51.95 o -8 0 2 116.46 66.89 27.38 o -7 0 2 5081.32 5015.19 99.88 o -6 0 2 66.44 51.88 26.35 o -5 0 2 3177.40 3281.03 161.19 o -4 0 2 3550.58 3254.05 95.50 o -3 0 2 1985.82 2045.80 46.30 o -2 0 2 10472.70 10451.29 732.53 o 1 0 2 41651.20 53449.48 951.24 o 4 0 2 6079.83 6572.65 111.29 o 5 0 2 86.23 100.10 29.79 o 6 0 2 2218.64 2678.18 65.91 o 7 0 2 1994.58 2687.50 74.74 o 8 0 2 88.47 107.21 24.60 o 9 0 2 268.16 338.24 34.72 o 10 0 2 34.41 60.07 35.68 o -10 1 2 45.12 70.82 31.54 o -9 1 2 0.09 -7.78 23.11 o -8 1 2 8.08 10.46 24.65 o -7 1 2 131.39 134.92 22.50 o -6 1 2 380.88 408.46 18.25 o -5 1 2 261.40 248.21 39.57 o -4 1 2 1213.83 1207.48 81.14 o -3 1 2 2992.89 2727.86 112.80 o -2 1 2 4903.73 4747.73 205.09 o -1 1 2 196.94 230.46 23.98 o 1 1 2 1227.59 1201.32 74.34 o 2 1 2 321.12 303.85 28.24 o 3 1 2 1663.41 1738.47 29.09 o 4 1 2 554.82 652.59 126.60 o 5 1 2 110.08 191.14 60.35 o 6 1 2 103.66 167.96 19.73 o 7 1 2 28.55 43.07 21.19 o 8 1 2 40.07 60.60 20.32 o 9 1 2 37.34 56.66 19.48 o 10 1 2 13.27 13.54 20.44 o -10 2 2 112.83 129.70 32.70 o -9 2 2 361.28 403.66 39.00 o -8 2 2 34.58 20.74 24.72 o -7 2 2 1919.99 1904.07 276.92 o -6 2 2 14.12 28.33 15.79 o -5 2 2 2338.89 2358.36 133.87 o -4 2 2 7484.98 7568.96 70.81 o -3 2 2 4525.02 4350.60 46.75 o -2 2 2 35367.95 38544.18 323.21 o -1 2 2 1279.58 1162.43 89.83 o 0 2 2 6022.76 4986.45 228.42 o 1 2 2 711.60 725.65 47.20 o 2 2 2 10255.32 9973.67 320.43 o 3 2 2 19.23 27.70 16.18 o 4 2 2 7666.77 8275.71 150.79 o 5 2 2 2504.81 2950.55 183.01 o 6 2 2 451.21 500.06 21.03 o 7 2 2 1587.18 2065.92 78.36 o 8 2 2 493.69 590.16 51.72 o 9 2 2 505.85 533.10 97.23 o -10 3 2 77.73 111.25 31.06 o -9 3 2 169.82 252.05 30.80 o -8 3 2 114.69 126.16 29.62 o -7 3 2 83.48 90.60 19.69 o -6 3 2 935.08 991.05 23.66 o -5 3 2 5956.69 6261.55 150.52 o -4 3 2 419.74 380.68 29.86 o -3 3 2 34.59 34.39 13.27 o -2 3 2 103.91 123.43 18.93 o -1 3 2 9706.43 8759.20 513.22 o 0 3 2 4579.98 4280.38 120.87 o 1 3 2 6201.08 5324.82 423.82 o 2 3 2 446.26 461.34 14.09 o 3 3 2 805.25 668.87 70.92 o 4 3 2 4524.25 4613.67 485.53 o 5 3 2 1423.85 1479.63 288.96 o 6 3 2 471.73 559.47 34.71 o 7 3 2 10.29 15.75 20.75 o 8 3 2 575.48 748.78 60.71 o 9 3 2 20.82 29.66 21.12 o -10 4 2 32.72 6.92 31.75 o -9 4 2 17.39 34.55 29.59 o -8 4 2 42.23 56.46 20.65 o -7 4 2 2022.85 1846.70 45.91 o -6 4 2 44.93 76.03 19.38 o -5 4 2 992.95 1110.68 20.45 o -4 4 2 4446.89 4267.98 39.45 o -3 4 2 38.99 62.31 12.86 o -2 4 2 3070.79 2787.21 93.23 o -1 4 2 1012.87 950.23 45.14 o 0 4 2 1009.68 883.33 31.91 o 1 4 2 86.42 99.33 10.79 o 2 4 2 9844.16 9619.59 182.18 o 3 4 2 3.73 9.67 13.56 o 4 4 2 598.24 588.94 48.15 o 5 4 2 322.31 294.44 61.76 o 6 4 2 127.98 139.53 20.42 o 7 4 2 532.09 606.00 108.05 o 8 4 2 16.69 17.01 25.46 o 9 4 2 176.45 197.13 35.44 o -10 5 2 431.29 434.45 35.09 o -9 5 2 14.19 28.18 21.97 o -8 5 2 184.24 154.51 21.48 o -7 5 2 448.04 467.97 28.29 o -6 5 2 282.73 332.86 21.80 o -5 5 2 1706.76 1926.76 26.73 o -4 5 2 5404.59 5340.38 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