#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/11/2211109.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211109_Fobs loop_ _publ_author_name 'Yathirajan, H. S.' 'Vijaya Raj, K. K.' 'Narayana, B.' 'Sarojini, B. K.' 'Bolte, Michael' _publ_section_title ; 3-(2-Bromo-5-methoxyphenyl)-5-methyl-1-(4-phenyl-1,3-thiazol-2-yl)-1H-1,2,4-triazole ; _journal_coeditor_code LH2202 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5013 _journal_page_last o5014 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.863 _cell_angle_gamma 90.000 _cell_length_a 11.9585 _cell_length_b 5.0552 _cell_length_c 29.0105 _exptl_crystal_F_000 864.00 _reflns_d_resolution_high 0.8182 _[local]_cod_data_source_file lh2202Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat46 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 347.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2174.19 2147.81 37.25 o 4 0 0 192.86 188.81 18.02 o 6 0 0 712.78 678.26 53.37 o 8 0 0 2075.98 2165.77 94.16 o 10 0 0 744.32 727.63 38.04 o 12 0 0 99.35 97.03 14.40 o 14 0 0 1.14 9.68 15.93 o 1 1 0 232.63 193.16 15.38 o 2 1 0 3605.85 3218.72 53.67 o 3 1 0 1850.48 1852.97 44.90 o 4 1 0 2127.95 1905.82 65.67 o 5 1 0 136.75 155.87 10.84 o 6 1 0 2053.76 1794.89 40.69 o 7 1 0 93.91 74.69 9.19 o 8 1 0 67.44 84.91 9.81 o 9 1 0 2200.27 2321.94 76.98 o 10 1 0 2615.96 2750.42 126.53 o 11 1 0 118.80 136.90 10.40 o 12 1 0 482.52 525.83 35.88 o 13 1 0 425.67 427.39 15.82 o 14 1 0 740.84 709.35 43.21 o 0 2 0 3428.34 3360.54 37.70 o 1 2 0 459.50 421.52 15.13 o 2 2 0 2803.13 2813.32 82.71 o 3 2 0 3158.58 3128.46 63.16 o 4 2 0 36.44 42.21 9.00 o 5 2 0 3122.08 2981.27 58.54 o 6 2 0 980.51 949.76 39.06 o 7 2 0 1248.87 1177.18 38.48 o 8 2 0 11.19 27.45 10.46 o 9 2 0 0.76 -10.12 10.12 o 10 2 0 291.65 299.61 17.82 o 11 2 0 356.78 376.57 20.29 o 12 2 0 13.74 29.42 10.72 o 13 2 0 388.26 408.29 23.77 o 1 3 0 3506.45 3423.97 75.83 o 2 3 0 1460.41 1482.55 38.96 o 3 3 0 944.32 925.49 22.85 o 4 3 0 184.44 190.39 11.09 o 5 3 0 21.69 20.27 9.41 o 6 3 0 507.13 476.11 23.84 o 7 3 0 397.46 399.65 13.53 o 8 3 0 2.56 16.42 10.01 o 9 3 0 1137.62 1160.00 61.09 o 10 3 0 251.01 247.33 13.33 o 11 3 0 529.57 520.38 29.45 o 12 3 0 74.90 62.25 11.88 o 0 4 0 814.37 776.11 23.19 o 1 4 0 492.31 540.22 20.57 o 2 4 0 433.92 441.75 13.09 o 3 4 0 481.40 489.77 17.78 o 4 4 0 3.76 -3.81 10.22 o 5 4 0 2289.03 2190.03 48.82 o 6 4 0 1191.24 1143.10 27.14 o 7 4 0 169.09 143.04 11.91 o 8 4 0 387.47 388.66 13.11 o 9 4 0 1.44 26.55 13.73 o 10 4 0 83.41 114.25 16.90 o 11 4 0 73.60 77.19 14.15 o 1 5 0 64.34 78.67 11.49 o 2 5 0 8.45 35.87 13.00 o 3 5 0 14.34 18.04 11.56 o 4 5 0 1932.03 1958.99 32.63 o 5 5 0 43.50 54.30 11.78 o 6 5 0 196.74 194.44 13.92 o 7 5 0 129.69 126.90 13.15 o 8 5 0 65.07 42.11 11.71 o 0 6 0 5.71 16.29 20.51 o 1 6 0 145.96 134.67 11.90 o 2 6 0 285.65 271.95 13.03 o 3 6 0 35.72 41.55 12.25 o -13 0 1 55.64 60.15 15.32 o -11 0 1 423.03 421.24 18.74 o -9 0 1 186.99 212.46 16.23 o -7 0 1 8823.41 8557.19 268.64 o -5 0 1 4639.14 4590.07 86.76 o -3 0 1 11300.00 11044.81 514.91 o -1 0 1 4612.43 4303.15 86.87 o 1 0 1 14557.67 10640.95 132.24 o 3 0 1 24215.39 23572.17 261.96 o 5 0 1 2507.89 2551.80 31.49 o 7 0 1 561.13 573.33 17.35 o 9 0 1 2002.88 2030.37 83.61 o 11 0 1 229.53 223.19 19.14 o 13 0 1 909.97 907.45 45.93 o -14 1 1 488.57 451.42 29.67 o -13 1 1 2.77 17.47 11.57 o -12 1 1 8.39 15.12 11.61 o -11 1 1 499.45 551.39 29.99 o -10 1 1 4.76 13.63 9.14 o -9 1 1 3676.76 3864.37 121.91 o -8 1 1 507.23 477.68 17.27 o -7 1 1 390.18 396.01 13.95 o -6 1 1 5153.96 5208.81 104.47 o -5 1 1 2378.79 2425.51 85.73 o -4 1 1 4031.94 4312.78 161.53 o -3 1 1 669.23 716.29 23.29 o -2 1 1 12533.50 11778.14 347.34 o -1 1 1 6552.23 5998.08 177.68 o 0 1 1 155.34 138.70 17.64 o 1 1 1 10860.43 9980.59 123.42 o 2 1 1 4202.88 3680.93 91.30 o 3 1 1 1595.56 1413.16 50.28 o 4 1 1 888.34 808.23 17.51 o 5 1 1 6471.75 6543.33 245.73 o 6 1 1 9.20 4.70 9.20 o 7 1 1 6777.42 7042.07 278.39 o 8 1 1 84.99 84.13 10.28 o 9 1 1 869.99 908.52 32.49 o 10 1 1 4820.41 5089.00 157.02 o 11 1 1 0.84 -3.25 10.47 o 12 1 1 21.03 28.61 11.85 o 13 1 1 4.85 -3.26 11.04 o 14 1 1 20.15 17.07 13.31 o -13 2 1 295.88 290.31 22.39 o -12 2 1 256.78 303.63 24.04 o -11 2 1 1.41 7.96 9.93 o -10 2 1 875.05 887.10 31.02 o -9 2 1 74.81 70.22 10.26 o -8 2 1 1282.66 1348.09 47.05 o -7 2 1 73.86 73.37 9.73 o -6 2 1 1142.56 1165.78 31.09 o -5 2 1 927.64 866.52 34.16 o -4 2 1 3284.18 3111.78 106.10 o -3 2 1 11673.37 12187.29 358.72 o -2 2 1 2618.47 2422.50 39.75 o -1 2 1 2767.47 2806.40 57.83 o 0 2 1 7932.63 7794.53 130.46 o 1 2 1 226.18 238.85 15.25 o 2 2 1 5.87 0.16 12.17 o 3 2 1 1400.46 1436.12 36.15 o 4 2 1 4658.15 4882.67 203.50 o 5 2 1 504.14 475.22 18.07 o 6 2 1 648.33 611.04 27.12 o 7 2 1 422.58 462.33 23.48 o 8 2 1 4603.99 4804.39 245.32 o 9 2 1 394.86 406.40 23.73 o 10 2 1 1293.95 1341.19 54.77 o 11 2 1 584.65 580.58 31.74 o 12 2 1 43.83 37.24 10.47 o 13 2 1 173.21 160.72 12.31 o -12 3 1 373.27 351.04 32.70 o -11 3 1 122.69 121.25 12.85 o -10 3 1 68.53 84.75 10.71 o -9 3 1 96.91 85.13 10.55 o -8 3 1 489.36 572.13 30.78 o -7 3 1 508.48 491.26 22.52 o -6 3 1 2363.20 2302.48 86.58 o -5 3 1 143.21 136.44 11.04 o -4 3 1 3469.34 3424.76 118.19 o -3 3 1 150.87 148.73 11.43 o -2 3 1 1.91 2.46 10.42 o -1 3 1 367.34 358.39 12.86 o 0 3 1 535.72 525.81 17.15 o 1 3 1 0.63 8.77 11.59 o 2 3 1 1779.78 1726.00 55.11 o 3 3 1 33.86 27.72 10.46 o 4 3 1 4541.33 4564.24 142.70 o 5 3 1 5.80 11.27 9.51 o 6 3 1 222.62 214.64 10.46 o 7 3 1 75.56 104.68 11.36 o 8 3 1 468.99 456.40 38.49 o 9 3 1 258.92 284.09 15.44 o 10 3 1 254.01 266.33 22.62 o 11 3 1 150.31 136.56 13.28 o 12 3 1 613.68 576.89 32.73 o -11 4 1 0.59 -0.03 11.90 o -10 4 1 633.58 530.29 27.81 o -9 4 1 72.43 78.25 13.33 o -8 4 1 25.57 25.66 10.81 o -7 4 1 22.04 38.38 11.37 o -6 4 1 46.48 39.52 11.38 o -5 4 1 623.88 607.94 13.87 o -4 4 1 1458.40 1492.00 41.23 o -3 4 1 198.97 186.56 12.72 o -2 4 1 2026.87 2081.26 48.03 o -1 4 1 148.02 141.46 13.21 o 0 4 1 14.20 20.96 11.75 o 1 4 1 495.22 504.91 13.33 o 2 4 1 15.00 -3.93 13.11 o 3 4 1 657.80 672.86 16.74 o 4 4 1 178.36 189.92 12.14 o 5 4 1 171.79 166.37 10.71 o 6 4 1 1004.95 1034.63 45.39 o 7 4 1 188.42 186.12 13.39 o 8 4 1 28.73 42.04 10.65 o 9 4 1 123.22 96.56 12.56 o 10 4 1 324.65 292.74 20.90 o 11 4 1 158.14 143.69 15.60 o -8 5 1 64.69 59.48 11.58 o -7 5 1 100.56 85.10 11.93 o -6 5 1 10.69 23.83 11.61 o -5 5 1 0.80 10.93 13.49 o -4 5 1 679.48 689.37 16.02 o -3 5 1 1302.01 1291.73 17.50 o -2 5 1 203.17 200.36 13.44 o -1 5 1 1351.71 1412.69 25.06 o 0 5 1 4.24 1.37 12.51 o 1 5 1 428.85 425.34 14.59 o 2 5 1 31.13 41.71 13.02 o 3 5 1 321.63 319.55 12.01 o 4 5 1 69.67 83.63 12.20 o 5 5 1 595.75 556.69 16.74 o 6 5 1 24.22 25.36 12.17 o 7 5 1 198.08 183.30 12.84 o 8 5 1 63.02 62.96 11.98 o -3 6 1 236.95 210.93 13.05 o -2 6 1 131.23 140.74 13.27 o -1 6 1 315.46 284.36 15.29 o 0 6 1 75.96 61.36 13.27 o 1 6 1 115.95 125.17 13.74 o 2 6 1 4.73 11.50 12.13 o 3 6 1 569.59 500.92 20.56 o -14 0 2 998.56 934.39 105.75 o -12 0 2 22.29 17.98 14.48 o -10 0 2 2235.16 2351.23 100.47 o -8 0 2 1857.19 1922.95 91.07 o -6 0 2 1115.15 1080.90 29.86 o -4 0 2 14060.33 14309.42 829.68 o -2 0 2 6742.49 6268.68 312.26 o 2 0 2 11.87 21.75 14.49 o 4 0 2 15674.69 14694.72 504.58 o 6 0 2 8341.96 9183.62 483.88 o 8 0 2 8516.68 8923.10 474.02 o 10 0 2 674.27 737.70 59.95 o 12 0 2 2117.94 2342.51 149.20 o 14 0 2 128.34 117.38 15.47 o -14 1 2 511.10 476.18 27.30 o -13 1 2 1798.51 1891.91 97.96 o -12 1 2 185.60 201.18 13.41 o -11 1 2 359.68 388.50 16.99 o -10 1 2 709.65 721.48 31.23 o -9 1 2 70.03 85.64 9.68 o -8 1 2 5666.25 5919.24 169.16 o -7 1 2 366.52 347.95 10.57 o -6 1 2 2058.90 1867.24 58.63 o -5 1 2 5603.00 5571.84 250.29 o -4 1 2 200.45 210.60 10.67 o -3 1 2 2748.13 2844.42 84.79 o -2 1 2 664.89 644.91 18.99 o -1 1 2 2962.12 2769.69 66.70 o 0 1 2 2761.03 2612.47 75.55 o 1 1 2 7511.81 7152.27 146.99 o 2 1 2 11966.65 11542.78 279.40 o 3 1 2 1907.51 1814.67 62.07 o 4 1 2 1245.43 1178.39 53.45 o 5 1 2 231.03 219.81 11.51 o 6 1 2 23.46 16.00 9.68 o 7 1 2 14.45 13.51 8.90 o 8 1 2 1309.30 1418.87 42.92 o 9 1 2 734.49 763.49 36.90 o 10 1 2 146.63 142.99 11.21 o 11 1 2 572.80 575.81 35.05 o 12 1 2 655.07 683.09 29.81 o 13 1 2 412.47 416.05 33.79 o 14 1 2 17.84 12.42 13.47 o -13 2 2 37.07 39.77 11.41 o -12 2 2 14.22 16.10 9.98 o -11 2 2 381.36 355.64 18.23 o -10 2 2 412.83 435.73 19.65 o -9 2 2 16.31 28.54 11.76 o -8 2 2 13.32 21.19 9.10 o -7 2 2 3126.28 3055.60 101.00 o -6 2 2 435.70 454.80 23.52 o -5 2 2 1312.05 1260.41 53.87 o -4 2 2 299.89 294.17 17.79 o -3 2 2 2434.95 2664.17 80.78 o -2 2 2 2487.73 2429.63 68.19 o -1 2 2 1803.02 1835.90 36.10 o 0 2 2 279.35 239.49 12.89 o 1 2 2 9804.84 9678.57 132.77 o 2 2 2 335.89 356.57 12.94 o 3 2 2 11251.61 11619.01 426.04 o 4 2 2 11.85 30.67 9.87 o 5 2 2 53.71 47.54 10.00 o 6 2 2 3385.99 3448.10 159.82 o 7 2 2 68.81 84.44 10.92 o 8 2 2 2.17 -6.25 10.74 o 9 2 2 2297.30 2412.10 122.56 o 10 2 2 12.61 15.17 10.05 o 11 2 2 1911.50 1987.14 84.92 o 12 2 2 15.19 19.41 11.41 o 13 2 2 12.60 20.32 10.67 o -12 3 2 189.41 218.78 18.87 o -11 3 2 591.04 594.93 31.82 o -10 3 2 12.41 14.67 10.98 o -9 3 2 400.18 402.79 16.83 o -8 3 2 29.97 38.29 9.55 o -7 3 2 5.03 14.64 10.17 o -6 3 2 4.50 16.99 8.73 o -5 3 2 633.01 589.63 21.10 o -4 3 2 207.51 181.07 10.96 o -3 3 2 4160.25 4084.52 126.86 o -2 3 2 10.14 18.38 12.45 o -1 3 2 2728.59 2806.36 60.36 o 0 3 2 0.82 12.31 12.76 o 1 3 2 293.36 330.05 16.40 o 2 3 2 2063.38 2220.51 56.09 o 3 3 2 674.27 686.59 14.46 o 4 3 2 435.53 417.54 17.10 o 5 3 2 3798.62 3793.82 83.69 o 6 3 2 19.48 21.78 10.22 o 7 3 2 2883.35 2863.18 144.69 o 8 3 2 178.84 199.53 12.56 o 9 3 2 122.27 107.46 11.07 o 10 3 2 908.35 852.71 36.51 o 11 3 2 138.42 157.37 18.15 o 12 3 2 3.56 8.73 11.58 o -11 4 2 4.09 12.44 13.35 o -10 4 2 98.97 113.67 15.12 o -9 4 2 906.06 919.95 52.69 o -8 4 2 8.52 11.15 10.86 o -7 4 2 197.31 198.77 15.18 o -6 4 2 2.87 12.13 9.10 o -5 4 2 1043.98 965.99 14.76 o -4 4 2 472.97 498.87 12.71 o -3 4 2 1342.06 1347.69 40.01 o -2 4 2 845.44 823.13 25.84 o -1 4 2 2153.64 2306.94 92.46 o 0 4 2 545.37 546.73 20.97 o 1 4 2 881.37 922.24 35.65 o 2 4 2 167.83 177.58 11.10 o 3 4 2 179.54 157.18 10.86 o 4 4 2 409.54 406.46 15.00 o 5 4 2 7.21 8.77 10.69 o 6 4 2 268.38 288.03 19.96 o 7 4 2 693.87 633.97 13.41 o 8 4 2 228.04 220.13 12.97 o 9 4 2 203.15 197.35 12.97 o 10 4 2 64.80 67.39 13.81 o 11 4 2 187.33 186.20 16.75 o -8 5 2 532.10 493.07 27.77 o -7 5 2 92.50 79.28 11.62 o -6 5 2 216.35 194.10 12.94 o -5 5 2 24.06 34.27 11.09 o -4 5 2 255.37 234.54 12.51 o -3 5 2 298.53 306.21 12.25 o -2 5 2 415.68 454.45 14.86 o -1 5 2 330.13 369.19 17.17 o 0 5 2 342.87 373.14 14.79 o 1 5 2 6.84 27.30 13.33 o 2 5 2 82.85 96.67 11.64 o 3 5 2 98.95 116.95 12.17 o 4 5 2 182.31 210.04 13.71 o 5 5 2 51.72 62.28 13.13 o 6 5 2 1.34 2.56 14.15 o 7 5 2 75.26 63.51 12.45 o 8 5 2 146.47 143.94 13.93 o -3 6 2 170.12 162.54 13.76 o -2 6 2 211.06 204.52 12.92 o -1 6 2 22.19 28.86 12.11 o 0 6 2 1.28 23.30 12.85 o 1 6 2 23.44 35.61 12.85 o 2 6 2 232.35 206.16 14.06 o 3 6 2 0.46 9.82 12.71 o -13 0 3 9.37 11.76 16.66 o -11 0 3 750.53 814.92 69.24 o -9 0 3 2462.63 2493.74 51.40 o -7 0 3 5628.81 5759.23 116.69 o -5 0 3 1142.37 1081.74 61.19 o -3 0 3 40042.53 36568.58 2097.50 o -1 0 3 4566.76 3575.09 380.24 o 1 0 3 19538.05 17862.31 439.47 o 3 0 3 10630.76 9318.75 501.33 o 5 0 3 3850.18 3583.04 107.43 o 7 0 3 2378.60 2255.85 141.88 o 9 0 3 5097.56 5312.77 580.45 o 11 0 3 1298.80 1397.77 49.95 o 13 0 3 47.08 43.24 16.61 o -14 1 3 110.58 95.79 10.26 o -13 1 3 403.28 392.24 25.99 o -12 1 3 245.96 286.38 19.04 o -11 1 3 897.67 983.83 61.80 o -10 1 3 796.41 814.97 40.18 o -9 1 3 47.64 46.53 9.48 o -8 1 3 159.93 158.46 9.65 o -7 1 3 628.31 633.24 14.62 o -6 1 3 5710.69 5888.45 94.83 o -5 1 3 13690.24 13442.92 402.02 o -4 1 3 1474.01 1416.04 43.11 o -3 1 3 7633.45 7278.60 208.92 o -2 1 3 4879.77 4939.63 150.06 o -1 1 3 2138.56 1936.83 40.77 o 0 1 3 2811.30 2711.47 45.32 o 1 1 3 13153.21 12119.66 134.76 o 2 1 3 12088.66 11736.97 179.04 o 3 1 3 5348.52 5022.29 131.19 o 4 1 3 21.20 25.33 10.31 o 5 1 3 5898.27 5642.68 221.23 o 6 1 3 1438.67 1579.32 41.74 o 7 1 3 10.49 11.93 9.96 o 8 1 3 1150.50 1146.60 29.97 o 9 1 3 959.87 993.81 32.63 o 10 1 3 1075.97 1076.21 31.44 o 11 1 3 334.88 354.47 16.74 o 12 1 3 49.91 50.86 11.51 o 13 1 3 215.68 231.01 14.16 o 14 1 3 576.01 571.45 55.20 o -13 2 3 3.67 7.44 10.94 o -12 2 3 622.81 621.55 28.76 o -11 2 3 1.80 -0.82 9.69 o -10 2 3 3.18 0.57 11.18 o -9 2 3 1618.00 1615.46 69.42 o -8 2 3 1.94 13.96 10.67 o -7 2 3 883.05 937.85 36.73 o -6 2 3 3444.14 3408.60 65.51 o -5 2 3 366.47 380.96 9.82 o -4 2 3 4382.98 4112.10 134.82 o -3 2 3 106.15 124.66 11.17 o -2 2 3 90.56 68.85 12.31 o -1 2 3 1183.18 1194.86 25.65 o 0 2 3 293.38 293.36 12.89 o 1 2 3 878.13 890.69 23.78 o 2 2 3 7842.39 7801.52 170.31 o 3 2 3 63.93 62.38 10.45 o 4 2 3 5444.76 5279.49 149.32 o 5 2 3 1168.08 1181.02 18.15 o 6 2 3 2428.99 2443.40 82.31 o 7 2 3 3803.38 3839.13 215.67 o 8 2 3 1703.41 1786.82 123.22 o 9 2 3 207.93 233.56 16.53 o 10 2 3 208.61 216.36 11.89 o 11 2 3 279.93 279.74 12.04 o 12 2 3 1713.86 1746.72 115.61 o 13 2 3 24.32 21.11 11.83 o -12 3 3 315.13 301.38 21.29 o -11 3 3 37.88 44.57 12.39 o -10 3 3 557.04 560.13 32.51 o -9 3 3 248.81 253.29 21.58 o -8 3 3 722.98 819.86 45.85 o -7 3 3 90.84 98.50 9.60 o -6 3 3 123.68 135.52 12.48 o -5 3 3 1086.82 1114.01 43.27 o -4 3 3 315.22 345.34 14.98 o -3 3 3 23.04 31.11 10.24 o -2 3 3 1168.47 1147.23 37.92 o -1 3 3 92.60 91.68 12.32 o 0 3 3 4301.39 4300.40 94.65 o 1 3 3 6035.84 6664.80 66.73 o 2 3 3 4218.62 4593.75 94.42 o 3 3 3 635.85 631.70 22.96 o 4 3 3 1467.08 1599.04 51.99 o 5 3 3 15.47 20.78 10.21 o 6 3 3 615.99 644.99 22.23 o 7 3 3 279.16 260.53 14.24 o 8 3 3 2537.05 2416.10 79.55 o 9 3 3 255.70 275.72 15.99 o 10 3 3 660.13 703.94 32.26 o 11 3 3 6.12 8.84 11.57 o 12 3 3 33.75 47.22 12.85 o -11 4 3 37.75 46.83 17.20 o -10 4 3 560.12 475.64 24.53 o -9 4 3 425.73 382.98 25.34 o -8 4 3 188.41 189.16 16.38 o -7 4 3 457.48 426.06 29.47 o -6 4 3 13.41 29.24 9.79 o -5 4 3 171.92 179.29 10.51 o -4 4 3 61.28 66.16 10.89 o -3 4 3 502.64 494.79 14.83 o -2 4 3 827.70 806.91 22.94 o -1 4 3 823.18 814.53 20.43 o 0 4 3 0.97 6.53 12.05 o 1 4 3 488.61 495.66 13.30 o 2 4 3 1254.79 1269.27 22.30 o 3 4 3 32.68 36.04 11.57 o 4 4 3 756.93 760.30 19.71 o 5 4 3 231.29 247.18 12.53 o 6 4 3 340.53 351.25 12.21 o 7 4 3 18.76 25.74 12.34 o 8 4 3 11.96 19.52 11.01 o 9 4 3 114.35 116.50 10.45 o 10 4 3 209.68 215.71 15.84 o -8 5 3 182.73 158.91 12.60 o -7 5 3 131.33 138.97 12.41 o -6 5 3 35.69 27.56 11.78 o -5 5 3 226.39 223.96 12.60 o -4 5 3 82.86 94.35 11.22 o -3 5 3 746.37 744.09 35.53 o -2 5 3 138.48 159.05 13.51 o -1 5 3 772.12 772.91 21.05 o 0 5 3 2.51 8.76 12.26 o 1 5 3 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