#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/11/2211114.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211114_Fobs loop_ _publ_author_name 'Cobo, Debora' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; (Z)-3-(4-Methylphenyl)-2-(3-thienyl)acrylonitrile ; _journal_coeditor_code LH2209 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5179 _journal_page_last o5180 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.439 _cell_angle_gamma 90.000 _cell_length_a 13.7415 _cell_length_b 10.8492 _cell_length_c 8.0238 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file lh2209Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 896 P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 627.32 266.98 61.50 o 3 0 0 4420.17 3888.94 41.22 o 4 0 0 2974.89 2719.90 21.74 o 5 0 0 859.62 812.73 6.75 o 7 0 0 1380.05 1378.65 10.88 o 8 0 0 1.67 2.59 0.60 o 9 0 0 1533.55 1458.36 13.08 o 10 0 0 936.78 940.92 11.15 o 11 0 0 33.40 35.01 1.27 o 12 0 0 10.49 15.23 1.09 o 13 0 0 28.83 29.94 1.95 o 14 0 0 49.99 47.15 2.24 o 15 0 0 674.35 673.63 53.25 o 16 0 0 63.08 50.71 5.94 o 17 0 0 5.11 8.25 4.11 o 1 1 0 376.78 271.84 10.48 o 2 1 0 2394.55 2163.52 24.34 o 3 1 0 333.36 323.34 3.59 o 4 1 0 18.60 8.94 0.29 o 5 1 0 242.06 205.73 1.37 o 6 1 0 764.34 847.08 4.87 o 7 1 0 2.36 8.03 0.55 o 8 1 0 1144.58 1112.81 7.68 o 9 1 0 341.25 335.65 2.70 o 10 1 0 483.11 462.58 4.14 o 11 1 0 246.25 239.06 2.75 o 12 1 0 527.74 484.98 5.64 o 13 1 0 92.77 91.37 1.90 o 14 1 0 148.26 152.58 3.43 o 15 1 0 2.76 5.72 1.64 o 16 1 0 157.75 166.70 9.17 o 17 1 0 329.35 349.82 19.44 o 0 2 0 3814.99 3146.62 44.08 o 1 2 0 5629.35 4611.07 183.98 o 2 2 0 53.86 42.35 0.56 o 3 2 0 689.73 638.77 4.28 o 4 2 0 830.68 823.46 5.54 o 5 2 0 12.61 10.24 0.51 o 6 2 0 518.26 507.45 3.21 o 7 2 0 2096.36 2228.89 13.08 o 8 2 0 93.96 76.17 1.13 o 9 2 0 97.60 92.57 1.16 o 10 2 0 721.82 729.18 6.55 o 11 2 0 215.16 223.27 2.63 o 12 2 0 407.73 418.73 5.14 o 13 2 0 75.62 89.05 2.29 o 14 2 0 7.27 6.98 1.16 o 15 2 0 128.83 130.04 4.50 o 16 2 0 169.42 146.15 7.83 o 1 3 0 1840.30 1735.44 14.97 o 2 3 0 2337.74 2110.68 16.14 o 3 3 0 2021.25 2036.15 17.40 o 4 3 0 2922.63 2918.21 20.76 o 5 3 0 1377.13 1371.23 9.02 o 6 3 0 4.40 3.86 0.49 o 7 3 0 1895.44 1877.89 11.12 o 8 3 0 592.83 591.74 4.15 o 9 3 0 443.51 446.12 3.93 o 10 3 0 2116.14 2128.17 16.86 o 11 3 0 1125.26 1116.88 11.00 o 12 3 0 80.18 81.47 1.64 o 13 3 0 66.70 80.26 1.93 o 14 3 0 325.24 330.57 8.41 o 15 3 0 20.48 24.37 2.05 o 16 3 0 403.63 460.35 18.90 o 0 4 0 0.39 0.99 0.74 o 1 4 0 35.95 37.10 1.06 o 2 4 0 0.18 2.12 0.53 o 3 4 0 283.23 254.33 2.43 o 4 4 0 359.67 384.97 3.59 o 5 4 0 66.27 85.17 1.31 o 6 4 0 304.26 288.51 2.44 o 7 4 0 194.30 210.06 2.10 o 8 4 0 39.29 27.88 0.96 o 9 4 0 4.75 4.11 0.66 o 10 4 0 1265.16 1273.90 13.50 o 11 4 0 187.29 201.44 3.13 o 12 4 0 365.48 379.31 5.89 o 13 4 0 277.69 287.10 5.71 o 14 4 0 2.24 3.30 1.60 o 15 4 0 18.32 16.44 1.92 o 16 4 0 338.87 372.02 15.59 o 1 5 0 232.62 233.29 2.95 o 2 5 0 586.51 579.47 4.75 o 3 5 0 328.28 376.41 3.84 o 4 5 0 302.18 312.35 2.91 o 5 5 0 473.99 486.37 4.70 o 6 5 0 47.36 46.33 0.97 o 7 5 0 317.41 322.69 3.05 o 8 5 0 754.36 784.63 7.75 o 9 5 0 127.63 122.14 1.89 o 10 5 0 56.28 59.74 1.50 o 11 5 0 693.16 730.62 10.87 o 12 5 0 89.44 91.29 2.33 o 13 5 0 65.23 60.94 2.35 o 14 5 0 329.23 337.97 9.70 o 15 5 0 119.44 115.41 4.98 o 16 5 0 2.98 4.92 4.03 o 0 6 0 758.99 747.62 11.32 o 1 6 0 468.84 484.38 4.61 o 2 6 0 180.66 174.87 2.12 o 3 6 0 725.46 742.08 6.36 o 4 6 0 21.60 14.31 0.81 o 5 6 0 111.71 95.21 1.79 o 6 6 0 505.64 505.04 5.03 o 7 6 0 91.34 83.10 1.62 o 8 6 0 5.51 2.95 0.77 o 9 6 0 730.14 762.54 9.41 o 10 6 0 104.71 107.53 2.30 o 11 6 0 4.15 0.98 1.03 o 12 6 0 99.79 93.15 2.66 o 13 6 0 11.50 10.18 1.69 o 14 6 0 42.13 32.41 3.19 o 15 6 0 171.01 154.06 6.90 o 1 7 0 935.67 981.85 9.86 o 2 7 0 20.81 15.23 1.03 o 3 7 0 1113.51 1237.76 12.86 o 4 7 0 689.89 693.94 7.75 o 5 7 0 579.26 569.57 6.13 o 6 7 0 20.81 19.93 0.93 o 7 7 0 159.48 181.81 2.81 o 8 7 0 60.43 63.10 1.72 o 9 7 0 988.38 1011.83 13.24 o 10 7 0 33.47 34.45 1.45 o 11 7 0 157.65 170.59 4.48 o 12 7 0 1.27 1.70 2.06 o 13 7 0 112.63 114.93 5.20 o 14 7 0 241.11 250.66 11.45 o 0 8 0 72.86 79.04 2.65 o 1 8 0 4.72 3.33 1.00 o 2 8 0 142.59 140.28 2.76 o 3 8 0 263.18 253.25 3.92 o 4 8 0 10.41 4.74 1.15 o 5 8 0 53.49 52.68 1.50 o 6 8 0 52.48 47.49 1.79 o 7 8 0 14.81 13.63 1.15 o 8 8 0 80.79 78.30 1.97 o 9 8 0 198.05 188.05 3.98 o 10 8 0 204.43 198.73 4.47 o 11 8 0 1.45 1.82 1.94 o 12 8 0 13.41 14.44 2.64 o 13 8 0 51.62 46.29 3.33 o 14 8 0 6.95 10.24 2.65 o 1 9 0 64.44 56.76 2.16 o 2 9 0 102.42 90.76 2.33 o 3 9 0 0.40 0.82 1.08 o 4 9 0 138.46 126.28 3.00 o 5 9 0 281.00 273.49 4.27 o 6 9 0 147.28 136.35 4.50 o 7 9 0 0.21 1.20 1.38 o 8 9 0 22.22 22.75 1.49 o 9 9 0 19.25 15.81 1.61 o 10 9 0 69.43 61.86 2.63 o 11 9 0 197.96 199.56 6.45 o 12 9 0 14.53 14.53 3.90 o 13 9 0 53.99 64.60 5.93 o 0 10 0 608.20 700.23 19.39 o 1 10 0 1.15 2.80 1.42 o 2 10 0 393.04 395.32 6.98 o 3 10 0 418.10 395.01 6.97 o 4 10 0 108.35 91.62 2.92 o 5 10 0 9.79 16.64 1.98 o 6 10 0 1.11 0.42 1.66 o 7 10 0 1.04 1.14 1.22 o 8 10 0 26.23 22.36 1.84 o 9 10 0 95.97 89.93 3.58 o 10 10 0 16.38 10.78 3.30 o 11 10 0 104.72 86.55 5.66 o 12 10 0 136.33 117.22 8.43 o 1 11 0 45.10 39.94 2.96 o 2 11 0 183.71 193.08 11.51 o 3 11 0 8.42 3.93 3.62 o 4 11 0 4.34 5.04 1.79 o 5 11 0 4.27 8.92 1.72 o 6 11 0 27.24 19.56 2.12 o 7 11 0 39.67 37.27 2.68 o 8 11 0 109.07 108.66 4.99 o 9 11 0 11.78 12.39 2.93 o 10 11 0 5.44 7.74 3.19 o 0 12 0 496.40 551.51 22.90 o 1 12 0 0.06 0.62 4.36 o 2 12 0 5.95 3.99 4.78 o 3 12 0 13.32 7.83 4.09 o 4 12 0 4.41 4.79 2.96 o 5 12 0 18.82 23.46 8.47 o 6 12 0 20.95 13.18 2.53 o 7 12 0 0.07 -0.61 3.28 o 8 12 0 31.50 30.45 3.36 o 1 13 0 5.06 5.15 5.19 o 2 13 0 24.33 35.54 5.13 o 3 13 0 0.61 0.56 4.24 o 4 13 0 19.47 27.63 4.08 o 5 13 0 8.09 16.76 3.27 o 6 13 0 66.51 72.13 8.13 o 0 14 0 75.56 28.84 10.61 o 1 14 0 140.44 148.56 7.69 o -17 1 1 109.31 119.67 7.27 o -16 1 1 1.05 -0.24 1.83 o -15 1 1 3.70 4.92 2.11 o -14 1 1 2.83 2.93 1.25 o -13 1 1 248.92 234.78 3.54 o -12 1 1 2.68 1.90 0.82 o -11 1 1 417.95 431.51 4.16 o -10 1 1 257.87 284.12 3.04 o -9 1 1 567.17 608.20 4.45 o -8 1 1 388.90 405.48 2.98 o -7 1 1 7.03 12.45 0.52 o -6 1 1 283.13 285.44 2.11 o -5 1 1 114.60 114.08 1.13 o -4 1 1 1375.12 1377.73 10.34 o -3 1 1 1613.49 1559.17 12.12 o -2 1 1 1714.84 1543.35 47.24 o 0 1 1 0.13 -0.28 0.28 o 1 1 1 76.13 68.87 1.36 o 2 1 1 476.63 488.80 3.59 o 3 1 1 22.58 23.75 0.37 o 4 1 1 29.36 28.68 0.38 o 5 1 1 333.80 340.39 3.25 o 6 1 1 401.91 447.96 2.64 o 7 1 1 6.50 6.31 0.49 o 8 1 1 148.72 159.58 1.54 o 9 1 1 15.97 17.96 0.64 o 10 1 1 72.05 65.40 1.01 o 11 1 1 39.86 47.95 0.96 o 12 1 1 224.60 185.53 2.60 o 13 1 1 30.91 24.26 0.94 o 14 1 1 27.00 23.99 1.96 o 15 1 1 11.56 8.04 2.07 o 16 1 1 19.63 19.56 3.79 o -17 2 1 112.39 112.77 5.82 o -16 2 1 2.85 3.78 3.53 o -15 2 1 4.45 2.06 2.09 o -14 2 1 188.11 167.57 3.78 o -13 2 1 91.50 92.16 2.02 o -12 2 1 7.09 6.28 0.70 o -11 2 1 666.58 667.60 6.20 o -10 2 1 49.75 42.47 0.89 o -9 2 1 144.05 126.55 1.39 o -8 2 1 74.91 79.86 1.13 o -7 2 1 86.26 115.32 1.16 o -6 2 1 166.02 182.90 1.82 o -5 2 1 371.81 419.54 3.51 o -4 2 1 41.56 47.15 0.66 o -3 2 1 12.69 18.55 0.57 o -2 2 1 184.63 174.68 1.59 o -1 2 1 11123.67 8840.60 176.92 o 0 2 1 1344.81 1298.20 10.63 o 1 2 1 1839.91 1844.74 13.95 o 2 2 1 288.56 279.51 2.40 o 3 2 1 387.31 423.48 3.18 o 4 2 1 643.25 701.02 4.57 o 5 2 1 357.90 412.48 3.78 o 6 2 1 503.29 520.30 3.77 o 7 2 1 563.94 587.19 4.01 o 8 2 1 156.97 168.43 1.59 o 9 2 1 95.24 86.81 1.58 o 10 2 1 12.29 11.76 0.61 o 11 2 1 616.75 554.57 6.93 o 12 2 1 15.30 16.06 0.82 o 13 2 1 2.20 1.95 0.90 o 14 2 1 0.21 2.01 1.07 o 15 2 1 174.02 194.49 10.12 o 16 2 1 0.33 1.26 1.78 o -17 3 1 213.13 199.78 12.96 o -16 3 1 52.91 61.58 4.40 o -15 3 1 4.17 5.76 1.47 o -14 3 1 299.68 277.28 6.40 o -13 3 1 118.48 107.43 2.25 o -12 3 1 104.69 102.23 1.77 o -11 3 1 63.34 64.77 1.35 o -10 3 1 1614.35 1645.47 13.87 o -9 3 1 235.54 229.43 2.25 o -8 3 1 247.28 228.47 2.32 o -7 3 1 9.94 7.99 0.65 o -6 3 1 156.14 168.09 1.85 o -5 3 1 0.15 -0.46 0.46 o -4 3 1 1037.33 1047.67 7.04 o -3 3 1 486.20 471.39 3.71 o -2 3 1 1481.98 1350.34 11.13 o -1 3 1 1441.99 1486.20 11.47 o 0 3 1 993.24 893.36 6.51 o 1 3 1 1355.54 1323.68 9.22 o 2 3 1 4.74 11.01 0.46 o 3 3 1 74.10 75.98 0.90 o 4 3 1 2.31 0.41 0.33 o 5 3 1 0.05 1.31 0.36 o 6 3 1 105.11 123.77 1.24 o 7 3 1 412.14 405.47 3.13 o 8 3 1 134.64 133.84 1.79 o 9 3 1 607.58 593.57 5.51 o 10 3 1 0.95 2.66 0.56 o 11 3 1 13.15 11.10 0.88 o 12 3 1 131.58 106.87 2.22 o 13 3 1 0.32 0.88 0.97 o 14 3 1 51.78 45.48 2.27 o 15 3 1 155.29 161.68 7.61 o 16 3 1 0.08 1.44 2.11 o -16 4 1 15.26 13.43 3.16 o -15 4 1 9.30 7.68 1.65 o -14 4 1 0.18 0.31 1.39 o -13 4 1 136.16 136.01 2.86 o -12 4 1 49.56 46.52 1.43 o -11 4 1 255.95 261.56 3.18 o -10 4 1 1030.11 1012.60 10.02 o -9 4 1 109.62 114.57 1.74 o -8 4 1 1072.55 1128.99 9.55 o -7 4 1 55.14 48.53 1.15 o -6 4 1 67.81 52.38 1.06 o -5 4 1 3.42 4.41 0.53 o -4 4 1 1564.08 1619.35 11.85 o -3 4 1 109.50 119.71 1.47 o -2 4 1 2313.53 2413.12 20.26 o -1 4 1 1561.37 1528.59 11.00 o 0 4 1 1926.44 1812.79 14.58 o 1 4 1 383.69 418.26 3.57 o 2 4 1 467.91 525.43 4.05 o 3 4 1 195.32 178.82 2.01 o 4 4 1 3.75 9.72 0.45 o 5 4 1 574.61 585.50 5.03 o 6 4 1 759.27 699.97 5.02 o 7 4 1 237.18 217.51 2.70 o 8 4 1 136.99 147.30 2.01 o 9 4 1 21.10 18.46 0.76 o 10 4 1 52.49 47.12 1.19 o 11 4 1 82.33 85.66 1.91 o 12 4 1 275.10 266.24 4.46 o 13 4 1 3.08 4.09 1.14 o 14 4 1 198.83 197.69 7.61 o 15 4 1 135.12 125.52 5.71 o -16 5 1 116.13 97.41 6.12 o -15 5 1 24.57 18.50 4.16 o -14 5 1 159.44 153.51 4.12 o -13 5 1 4.69 2.24 1.34 o -12 5 1 32.81 33.13 1.52 o -11 5 1 4.09 5.62 1.34 o -10 5 1 5.20 4.51 0.96 o -9 5 1 79.14 74.20 1.83 o -8 5 1 99.61 108.17 3.25 o -7 5 1 271.86 274.53 2.92 o -6 5 1 27.81 33.61 0.94 o -5 5 1 31.84 11.98 1.05 o -4 5 1 562.68 615.60 4.94 o -3 5 1 2.69 2.55 0.59 o -2 5 1 1949.09 2064.68 16.21 o -1 5 1 452.61 405.59 3.78 o 0 5 1 103.39 122.26 1.62 o 1 5 1 263.24 273.79 2.68 o 2 5 1 4179.10 4420.51 36.37 o 3 5 1 14.54 27.95 1.02 o 4 5 1 35.05 23.04 0.84 o 5 5 1 57.16 41.56 0.92 o 6 5 1 87.69 94.27 1.30 o 7 5 1 119.81 114.18 1.52 o 8 5 1 5164.26 4977.72 41.89 o 9 5 1 41.96 38.60 1.05 o 10 5 1 134.51 133.88 1.96 o 11 5 1 9.79 11.08 0.99 o 12 5 1 17.53 14.22 0.98 o 13 5 1 56.18 54.36 2.28 o 14 5 1 155.67 179.51 10.57 o 15 5 1 71.44 71.99 4.27 o -15 6 1 25.82 22.44 3.82 o -14 6 1 3.20 1.20 2.11 o -13 6 1 33.73 31.62 2.31 o -12 6 1 0.26 -1.54 1.54 o -11 6 1 39.00 39.73 1.94 o -10 6 1 2653.24 2672.28 33.08 o -9 6 1 355.97 354.39 4.68 o -8 6 1 5.33 5.25 1.00 o -7 6 1 241.90 247.72 3.13 o -6 6 1 91.09 69.11 1.29 o -5 6 1 17.59 13.36 1.03 o -4 6 1 2813.45 2871.96 21.80 o -3 6 1 753.19 833.97 6.18 o -2 6 1 61.91 55.58 1.30 o -1 6 1 482.42 520.76 4.45 o 0 6 1 1316.32 1336.10 12.20 o 1 6 1 2.61 0.74 0.78 o 2 6 1 177.38 228.10 2.35 o 3 6 1 0.52 0.67 0.69 o 4 6 1 117.32 114.97 1.69 o 5 6 1 52.24 46.92 1.02 o 6 6 1 209.34 217.17 3.08 o 7 6 1 36.72 33.02 1.03 o 8 6 1 0.01 1.97 1.22 o 9 6 1 555.28 579.23 6.54 o 10 6 1 471.45 466.37 6.94 o 11 6 1 5.57 6.09 1.02 o 12 6 1 11.44 14.55 1.67 o 13 6 1 12.52 10.58 2.19 o 14 6 1 26.28 24.77 3.75 o -15 7 1 0.02 -0.76 3.08 o -14 7 1 100.03 110.01 5.84 o -13 7 1 7.19 5.99 1.68 o -12 7 1 12.00 8.14 2.35 o -11 7 1 1.38 1.10 1.60 o -10 7 1 201.79 213.09 4.96 o -9 7 1 0.15 -0.57 1.15 o -8 7 1 15.89 19.58 1.24 o -7 7 1 38.16 44.49 1.74 o -6 7 1 27.12 24.74 0.85 o -5 7 1 142.52 124.17 1.80 o -4 7 1 217.22 198.17 4.36 o -3 7 1 7.41 8.86 1.29 o -2 7 1 478.28 498.96 5.62 o -1 7 1 122.85 134.41 2.00 o 0 7 1 0.35 -0.12 0.80 o 1 7 1 1645.22 1656.93 14.18 o 2 7 1 1417.79 1462.26 12.52 o 3 7 1 5.64 5.84 0.91 o 4 7 1 522.78 513.98 6.13 o 5 7 1 466.88 471.44 5.08 o 6 7 1 1.00 1.78 0.90 o 7 7 1 807.38 775.74 9.16 o 8 7 1 1627.95 1620.99 18.99 o 9 7 1 85.54 80.61 1.71 o 10 7 1 165.52 157.12 3.46 o 11 7 1 193.91 194.52 4.63 o 12 7 1 28.69 33.82 4.20 o 13 7 1 80.29 63.66 5.94 o 14 7 1 211.04 222.23 8.46 o -14 8 1 69.97 77.23 4.62 o -13 8 1 98.25 86.39 4.06 o -12 8 1 538.82 558.83 17.58 o -11 8 1 204.89 189.68 5.33 o -10 8 1 158.99 151.17 3.72 o -9 8 1 582.46 561.19 10.44 o -8 8 1 192.99 169.33 3.32 o -7 8 1 237.36 235.82 3.45 o -6 8 1 547.82 574.88 7.04 o -5 8 1 3.68 3.68 0.68 o -4 8 1 287.69 291.46 3.86 o -3 8 1 1017.73 986.57 10.61 o -2 8 1 961.12 996.91 10.02 o -1 8 1 2.32 1.06 0.91 o 0 8 1 310.02 328.23 4.26 o 1 8 1 174.15 177.67 3.02 o 2 8 1 46.28 43.73 1.87 o 3 8 1 594.84 572.83 7.10 o 4 8 1 267.35 249.45 4.30 o 5 8 1 23.65 14.92 1.14 o 6 8 1 183.12 189.69 3.16 o 7 8 1 57.95 58.50 1.74 o 8 8 1 8.91 7.69 1.04 o 9 8 1 457.42 466.79 7.45 o 10 8 1 3.16 4.52 1.49 o 11 8 1 4.52 4.23 1.67 o 12 8 1 225.24 236.00 8.70 o 13 8 1 101.85 106.39 6.20 o -13 9 1 133.49 146.37 7.88 o -12 9 1 54.47 54.41 5.05 o -11 9 1 307.70 311.15 9.86 o -10 9 1 84.53 84.72 2.99 o -9 9 1 28.19 31.83 1.98 o -8 9 1 269.03 268.70 5.52 o -7 9 1 95.59 78.20 2.25 o -6 9 1 109.14 111.27 3.52 o -5 9 1 232.88 252.93 3.98 o -4 9 1 150.45 161.26 2.81 o -3 9 1 168.62 162.66 2.98 o -2 9 1 167.50 164.08 3.08 o -1 9 1 329.31 313.27 4.75 o 0 9 1 473.29 470.88 7.13 o 1 9 1 466.65 480.78 7.84 o 2 9 1 13.28 14.01 1.52 o 3 9 1 52.72 38.64 2.29 o 4 9 1 279.64 286.20 4.90 o 5 9 1 31.44 33.01 1.55 o 6 9 1 174.01 155.50 3.43 o 7 9 1 390.31 364.41 7.43 o 8 9 1 4.41 3.83 1.50 o 9 9 1 50.11 48.11 2.16 o 10 9 1 176.75 172.96 5.09 o 11 9 1 144.00 145.03 7.41 o 12 9 1 75.24 74.07 5.41 o -12 10 1 21.54 26.62 4.23 o -11 10 1 14.50 14.50 3.19 o -10 10 1 36.91 32.28 2.95 o -9 10 1 645.14 655.27 16.27 o -8 10 1 64.10 64.33 3.14 o -7 10 1 7.05 11.03 0.96 o -6 10 1 690.99 705.84 13.52 o -5 10 1 208.33 193.26 5.07 o -4 10 1 0.65 2.46 1.48 o -3 10 1 850.64 881.70 15.54 o -2 10 1 249.96 253.65 4.61 o -1 10 1 317.74 321.82 5.71 o 0 10 1 830.42 883.31 15.48 o 1 10 1 387.01 387.02 7.36 o 2 10 1 94.57 104.82 3.43 o 3 10 1 329.04 351.72 8.15 o 4 10 1 258.88 255.63 6.48 o 5 10 1 6.91 2.33 1.61 o 6 10 1 467.77 500.52 10.20 o 7 10 1 158.48 148.49 3.73 o 8 10 1 29.53 31.46 2.09 o 9 10 1 391.47 413.26 19.29 o 10 10 1 98.54 87.99 4.40 o 11 10 1 215.67 228.46 10.91 o -11 11 1 197.28 183.51 21.95 o -10 11 1 2.11 2.10 2.62 o -9 11 1 7.03 6.46 4.02 o -8 11 1 170.00 169.97 6.99 o -7 11 1 157.28 159.65 9.20 o -6 11 1 19.01 18.07 2.24 o -5 11 1 135.65 138.94 4.61 o -4 11 1 33.07 35.28 2.66 o -3 11 1 21.82 19.20 1.86 o -2 11 1 94.91 100.54 4.99 o -1 11 1 164.16 185.88 6.85 o 0 11 1 238.65 243.45 8.94 o 1 11 1 139.36 146.14 5.28 o 2 11 1 137.76 146.39 5.53 o 3 11 1 5.19 5.97 2.95 o 4 11 1 279.41 287.55 9.51 o 5 11 1 106.89 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