#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211116.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211116_Fobs loop_ _publ_author_name 'Chase, Preston A.' 'Parvez, Masood' 'Piers, Warren E.' _publ_section_title ; Trimethylphosphine--tris(pentafluorophenyl)borane ; _journal_coeditor_code LH2211 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5181 _journal_page_last o5183 _journal_volume 62 _journal_year 2006 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 12.1410 _cell_length_b 12.1410 _cell_length_c 24.5030 _exptl_crystal_F_000 1740.00 _reflns_d_resolution_high 0.7682 _[local]_cod_data_source_file lh2211Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_f_calc_maximum 287.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 3 0 124.96 121.91 10.05 o -2 4 0 22894.76 22225.18 418.27 o -4 5 0 12955.92 12596.91 262.74 o -1 5 0 12472.32 11979.52 233.68 o -3 6 0 5773.63 5955.42 104.47 o 0 6 0 27130.58 27804.67 523.29 o -5 7 0 742.88 786.08 46.25 o -2 7 0 123.00 116.57 25.82 o -7 8 0 3188.89 2721.29 542.92 o -4 8 0 769.28 855.29 32.71 o -1 8 0 12854.95 13193.93 307.09 o -6 9 0 735.82 848.47 38.22 o -3 9 0 3198.82 3089.72 128.94 o 0 9 0 11636.92 12558.17 497.11 o -8 10 0 775.38 696.38 57.73 o -5 10 0 4641.94 4517.02 169.31 o -2 10 0 17.74 -6.53 38.48 o -10 11 0 50.92 127.26 52.13 o -7 11 0 511.00 446.22 41.80 o -4 11 0 411.30 441.92 47.88 o -1 11 0 2303.45 2198.79 122.06 o -9 12 0 195.83 107.87 43.37 o -6 12 0 277.06 234.16 69.01 o -3 12 0 1831.79 1933.30 109.41 o 0 12 0 219.90 310.69 134.99 o -11 13 0 84.65 114.28 131.78 o -8 13 0 62.07 85.71 99.64 o -5 13 0 5591.98 5756.60 340.18 o -2 13 0 202.63 96.07 103.21 o -13 14 0 710.00 738.01 104.51 o -10 14 0 2784.18 3155.51 342.48 o -7 14 0 595.65 660.38 119.91 o -1 14 0 1535.14 1480.09 149.20 o -6 15 0 414.32 618.17 172.49 o -3 2 1 11.48 3.02 7.63 o 0 2 1 12.68 14.79 3.92 o -5 3 1 70581.16 68617.91 1634.23 o -2 3 1 1425.39 1386.55 34.74 o 1 3 1 6965.10 6942.45 126.68 o -7 4 1 9620.98 9936.56 224.68 o -4 4 1 118.63 146.68 13.90 o -1 4 1 2371.39 2301.49 47.98 o 2 4 1 29776.09 30502.30 545.82 o -9 5 1 4679.66 4582.06 109.47 o -6 5 1 1939.73 1623.78 58.85 o -3 5 1 19218.89 19674.62 401.87 o 0 5 1 69.14 150.26 18.76 o 3 5 1 468.82 443.37 24.37 o -11 6 1 3525.68 3777.00 163.77 o -8 6 1 0.67 -7.88 22.76 o -5 6 1 1634.96 1743.77 72.58 o -2 6 1 670.01 660.15 24.62 o 1 6 1 19341.13 19406.70 344.42 o 4 6 1 3635.40 3407.60 104.44 o -13 7 1 87.66 14.28 99.28 o -10 7 1 4731.85 4963.76 199.04 o -7 7 1 1185.25 1211.52 43.61 o -4 7 1 5774.27 6192.90 106.28 o -1 7 1 21.85 15.48 10.89 o 2 7 1 159.71 147.03 28.80 o 5 7 1 834.59 751.48 46.93 o -15 8 1 181.84 277.84 185.35 o -12 8 1 908.05 791.37 108.21 o -9 8 1 309.78 324.07 33.75 o -6 8 1 1091.15 1303.50 45.14 o -3 8 1 2884.78 2899.33 71.74 o 0 8 1 1243.62 1283.99 68.71 o 3 8 1 1948.49 2190.14 80.06 o 6 8 1 564.32 354.26 143.92 o -14 9 1 577.01 432.47 149.28 o -11 9 1 42.19 51.33 36.04 o -8 9 1 5382.16 5413.45 148.61 o -5 9 1 5992.88 5977.99 143.87 o -2 9 1 444.26 419.26 41.04 o 1 9 1 405.47 341.48 51.24 o 4 9 1 338.00 247.13 129.63 o -13 10 1 155.19 -118.21 89.64 o -10 10 1 3.20 13.82 48.38 o -7 10 1 1118.20 1183.53 43.66 o -4 10 1 3448.69 3262.03 99.52 o -1 10 1 12.27 -32.29 37.84 o 2 10 1 1675.45 1640.97 134.84 o 5 10 1 7.11 64.28 171.42 o -15 11 1 4.71 -24.43 82.40 o -12 11 1 1073.69 955.13 116.70 o -9 11 1 6.76 -21.07 53.21 o -6 11 1 2027.93 1854.56 78.35 o -3 11 1 3.87 -0.99 46.59 o 0 11 1 264.93 347.12 73.06 o 3 11 1 971.87 1088.14 208.92 o -14 12 1 2186.43 2310.71 302.84 o -11 12 1 1904.82 1933.55 121.43 o -8 12 1 195.65 157.49 64.64 o -5 12 1 667.22 915.92 179.63 o -2 12 1 26.79 61.45 47.97 o 1 12 1 172.73 -99.64 139.63 o -13 13 1 76.65 63.13 76.49 o -10 13 1 6.99 -14.28 99.28 o -7 13 1 0.52 -24.01 89.10 o -4 13 1 55.89 20.53 78.81 o -12 14 1 243.40 146.80 77.55 o -9 14 1 0.54 -11.45 169.81 o -6 14 1 1565.03 1328.33 136.68 o -3 14 1 44.35 46.43 84.76 o -11 15 1 702.15 410.33 208.20 o -8 15 1 32.80 43.21 136.06 o -5 15 1 0.14 29.10 81.69 o 1 2 2 28056.87 25869.46 481.35 o -4 3 2 9703.49 9378.04 221.06 o -1 3 2 640.77 691.84 21.55 o 2 3 2 238.81 192.67 12.55 o -6 4 2 322.08 361.44 22.38 o -3 4 2 2695.12 2817.08 56.85 o 0 4 2 5473.53 5232.04 108.95 o 3 4 2 11512.46 12041.04 372.73 o -8 5 2 7012.12 7119.20 278.95 o -5 5 2 1115.47 1178.38 54.62 o -2 5 2 5163.40 4839.35 108.55 o 1 5 2 6355.61 6939.50 136.42 o 4 5 2 96.18 103.04 17.89 o -10 6 2 8668.96 9221.93 296.25 o -7 6 2 5673.35 5320.89 187.11 o -4 6 2 3173.87 3653.37 68.43 o -1 6 2 18.90 34.06 10.72 o 2 6 2 5833.34 5696.90 133.04 o 5 6 2 63.18 72.17 51.49 o -12 7 2 870.35 828.05 62.62 o -9 7 2 7.89 -3.59 31.16 o -6 7 2 8892.03 9395.70 513.54 o -3 7 2 16.90 17.21 14.67 o 0 7 2 4402.03 4173.02 94.21 o 3 7 2 1176.40 1177.62 62.78 o 6 7 2 1978.14 2091.25 146.96 o -14 8 2 1.55 18.56 60.90 o -11 8 2 11449.21 11492.68 392.30 o -8 8 2 741.82 667.20 43.47 o -5 8 2 875.66 855.97 27.90 o -2 8 2 1443.34 1519.25 54.50 o 1 8 2 109.16 116.82 22.47 o 4 8 2 2491.69 2574.13 154.41 o 7 8 2 48.27 -118.33 94.55 o -13 9 2 682.56 928.87 142.13 o -10 9 2 506.24 448.29 45.09 o -7 9 2 3413.66 3340.42 100.95 o -4 9 2 1511.00 1592.92 64.07 o -1 9 2 15931.99 16215.25 434.69 o 2 9 2 3366.30 2528.36 859.95 o 5 9 2 409.81 415.33 175.35 o -9 10 2 804.05 543.18 111.42 o -6 10 2 1083.31 1123.37 50.71 o -3 10 2 12705.28 12799.05 320.92 o 0 10 2 136.05 56.78 49.64 o 3 10 2 411.58 386.19 93.53 o -14 11 2 67.10 135.71 96.07 o -11 11 2 67.18 57.56 55.75 o -8 11 2 23.18 8.55 24.14 o -5 11 2 16.55 -18.30 46.69 o -2 11 2 10267.67 10681.73 353.71 o 1 11 2 735.63 899.68 110.05 o -13 12 2 1237.14 1052.79 166.78 o -7 12 2 62.43 -51.80 38.17 o -4 12 2 108.90 71.07 71.42 o -1 12 2 256.34 169.56 82.49 o 2 12 2 0.07 106.41 120.58 o -12 13 2 789.03 432.47 186.42 o -9 13 2 1723.87 1657.93 332.30 o -6 13 2 3156.88 3241.63 196.34 o -3 13 2 857.32 700.67 173.92 o 0 13 2 960.91 772.09 152.85 o -11 14 2 190.24 356.76 167.13 o -8 14 2 360.04 310.69 134.99 o -2 14 2 22.69 131.78 135.71 o -7 15 2 2117.31 2616.62 262.84 o -4 15 2 375.60 250.70 168.56 o 1 1 3 89.29 72.71 23.51 o -1 2 3 29507.10 28030.44 1109.58 o 2 2 3 14776.76 13839.93 299.90 o -3 3 3 31805.98 29845.71 786.19 o 0 3 3 2722.50 2594.83 57.82 o 3 3 3 20138.94 19347.97 349.94 o -5 4 3 19777.53 19832.36 510.55 o -2 4 3 1602.44 1811.89 43.36 o 1 4 3 1719.92 1446.62 31.79 o 4 4 3 14356.06 15005.33 278.09 o -7 5 3 33.92 24.82 19.58 o -4 5 3 75935.15 56984.27 17117.28 o -1 5 3 38593.47 36911.19 705.61 o 2 5 3 17.49 12.98 13.92 o 5 5 3 13413.41 14461.92 465.99 o -9 6 3 2683.10 2665.14 108.65 o -6 6 3 1411.23 1425.32 44.60 o -3 6 3 4677.79 4825.52 87.15 o 0 6 3 827.75 754.88 24.60 o 3 6 3 2085.91 1981.65 55.86 o 6 6 3 75.07 35.27 43.75 o -11 7 3 2071.34 1918.93 79.03 o -8 7 3 519.10 523.21 34.73 o -5 7 3 136.90 97.56 28.97 o -2 7 3 354.03 426.21 21.28 o 1 7 3 0.07 -11.17 19.60 o 4 7 3 557.08 572.95 61.51 o 7 7 3 234.86 162.89 102.11 o -13 8 3 70.67 123.35 74.35 o -10 8 3 875.08 807.73 49.53 o -7 8 3 1930.50 1966.41 55.92 o -4 8 3 2940.90 2868.82 71.60 o -1 8 3 1083.46 1070.53 43.35 o 2 8 3 250.42 266.72 30.21 o 5 8 3 14.64 -110.71 89.28 o -15 9 3 60.78 55.26 101.78 o -12 9 3 3381.88 3044.70 267.84 o -9 9 3 1718.21 1821.21 77.73 o -6 9 3 1005.83 1027.41 56.29 o -3 9 3 1277.72 1284.77 47.66 o 0 9 3 2228.50 2247.14 78.17 o 3 9 3 324.63 363.55 125.35 o 6 9 3 706.05 532.11 201.42 o -14 10 3 473.33 385.61 87.65 o -11 10 3 1886.61 1840.95 241.06 o -8 10 3 518.09 416.62 52.99 o -5 10 3 1721.88 1712.12 56.72 o -2 10 3 5176.17 5253.76 153.42 o 1 10 3 1270.02 1436.81 113.03 o 4 10 3 708.50 720.81 175.70 o -13 11 3 348.61 488.90 129.63 o -10 11 3 829.01 701.71 114.38 o -7 11 3 1311.13 1401.38 84.75 o -4 11 3 1.67 -15.17 18.43 o -1 11 3 2.60 -110.71 85.35 o 2 11 3 29.92 86.19 66.99 o -12 12 3 442.94 680.60 93.35 o -6 12 3 286.96 389.46 67.82 o -3 12 3 133.69 77.10 105.71 o 0 12 3 1438.32 1569.90 161.06 o -14 13 3 126.42 230.13 138.92 o -11 13 3 116.09 71.07 120.71 o -5 13 3 4312.20 4014.49 243.81 o -2 13 3 167.79 75.00 167.85 o 1 13 3 436.19 479.27 108.24 o -13 14 3 63.75 136.82 88.73 o -10 14 3 101.66 82.49 118.21 o -4 14 3 21.94 -71.07 124.99 o -1 14 3 451.13 424.97 177.49 o -9 15 3 135.76 -39.28 117.85 o -6 15 3 1662.42 1880.65 176.77 o -3 2 4 40138.98 37614.03 835.59 o 0 2 4 8799.63 7993.60 146.55 o -5 3 4 6939.95 6709.42 117.60 o -2 3 4 10699.37 10407.43 204.96 o 1 3 4 1057.65 1145.69 25.78 o -7 4 4 1114.13 1283.49 44.19 o -4 4 4 2384.58 2177.76 100.17 o -1 4 4 2024.92 1930.86 57.17 o 2 4 4 5420.19 5477.96 101.65 o -9 5 4 181.70 147.12 32.24 o -6 5 4 97.16 154.88 76.78 o -3 5 4 4311.07 3911.46 86.01 o 0 5 4 5996.20 5940.61 107.49 o 3 5 4 1.78 34.65 14.53 o -11 6 4 8810.85 9544.38 372.09 o -8 6 4 10091.03 10021.03 221.93 o -5 6 4 1686.15 1925.72 52.28 o -2 6 4 23627.41 23707.80 442.23 o 1 6 4 22106.95 22610.63 374.40 o 4 6 4 631.46 653.75 32.85 o -13 7 4 481.74 417.90 83.42 o -10 7 4 16.41 32.41 32.47 o -7 7 4 1751.63 1749.82 66.44 o -4 7 4 9618.17 10535.36 229.64 o -1 7 4 4936.68 5428.56 106.89 o 2 7 4 12.35 43.86 21.39 o 5 7 4 181.63 160.62 49.54 o -15 8 4 2.05 -83.97 87.83 o -12 8 4 4334.13 4363.94 267.44 o -9 8 4 0.38 3.46 30.46 o -6 8 4 5786.85 5956.95 139.66 o -3 8 4 884.54 824.29 46.87 o 0 8 4 41.34 59.60 19.15 o 3 8 4 10.00 43.15 28.04 o 6 8 4 89.20 21.91 51.60 o -14 9 4 242.42 412.12 98.96 o -11 9 4 43.53 52.10 53.20 o -8 9 4 1085.06 1101.48 106.93 o -5 9 4 1275.61 1374.47 54.20 o -2 9 4 19413.93 20538.69 449.43 o 1 9 4 1476.56 1321.14 79.43 o 4 9 4 10.21 99.64 114.64 o -13 10 4 663.35 869.41 107.87 o -10 10 4 1756.25 1741.60 150.77 o -7 10 4 937.91 1032.74 64.94 o -4 10 4 159.32 157.03 70.01 o -1 10 4 1480.41 1477.42 55.55 o 2 10 4 28.67 85.71 81.78 o 5 10 4 5.74 -157.49 147.13 o -15 11 4 192.97 265.89 105.60 o -12 11 4 382.25 228.56 121.06 o -9 11 4 699.99 505.64 54.18 o -6 11 4 138.12 102.90 80.35 o -3 11 4 9835.20 10024.55 401.90 o 0 11 4 152.33 198.24 120.17 o 3 11 4 131.77 161.29 99.72 o -14 12 4 527.71 502.75 95.57 o -11 12 4 198.82 256.41 120.71 o -8 12 4 990.01 726.38 128.92 o -5 12 4 101.33 136.53 48.85 o -2 12 4 1108.03 1026.01 153.20 o 1 12 4 615.72 574.20 111.24 o -13 13 4 110.28 121.06 114.28 o -10 13 4 106.84 -99.64 100.35 o -7 13 4 112.53 -28.21 88.92 o -4 13 4 10.57 28.64 68.18 o -1 13 4 14.52 179.27 118.56 o -6 14 4 660.89 675.67 180.35 o -5 15 4 40.44 142.85 135.71 o 0 1 5 1043.57 913.84 30.98 o -2 2 5 48912.77 45834.18 1009.90 o 1 2 5 1475.43 1306.44 32.86 o -4 3 5 5512.78 5743.36 115.28 o -1 3 5 21633.10 20818.10 494.07 o 2 3 5 411.48 465.99 16.01 o -6 4 5 3770.80 3944.06 81.23 o -3 4 5 15046.75 15182.92 261.02 o 0 4 5 798.55 741.59 22.39 o 3 4 5 1232.46 1492.80 51.91 o -8 5 5 2196.74 2195.38 64.17 o -5 5 5 2971.07 3308.37 93.25 o -2 5 5 10218.69 10313.67 179.11 o 1 5 5 35853.93 35233.06 670.46 o 4 5 5 1580.44 1569.69 49.91 o -10 6 5 5661.68 5539.34 192.83 o -7 6 5 2709.51 2712.77 92.34 o -4 6 5 169.58 186.14 18.11 o -1 6 5 510.80 415.63 25.81 o 2 6 5 3361.52 3520.33 84.87 o 5 6 5 854.18 889.62 72.38 o -12 7 5 2967.98 3236.58 292.48 o -9 7 5 1422.08 1518.83 76.70 o -6 7 5 956.02 1132.37 44.22 o -3 7 5 1686.31 1861.19 59.26 o 0 7 5 1889.05 1950.78 70.88 o 3 7 5 19.50 11.88 22.81 o 6 7 5 881.26 745.57 95.56 o -14 8 5 1819.85 1573.53 171.49 o -11 8 5 0.15 -28.22 32.57 o -8 8 5 4989.83 5652.08 306.04 o -5 8 5 4883.27 4821.96 121.20 o -2 8 5 1618.58 1640.77 39.72 o 1 8 5 5193.74 5569.16 173.12 o 4 8 5 3817.55 3698.26 202.88 o 7 8 5 35.14 -75.00 153.20 o -13 9 5 1040.98 1049.22 181.77 o -10 9 5 77.23 83.86 39.07 o -7 9 5 12875.82 13698.20 415.94 o -4 9 5 3.91 8.01 19.99 o -1 9 5 1418.79 1418.65 47.55 o 2 9 5 436.85 494.62 59.90 o 5 9 5 0.20 16.87 94.42 o -15 10 5 281.78 222.71 120.65 o -12 10 5 460.97 493.31 76.36 o -9 10 5 59.85 49.64 57.14 o -6 10 5 190.09 132.43 36.45 o -3 10 5 2124.64 2182.85 81.82 o 0 10 5 28.65 129.17 60.11 o 3 10 5 2.85 14.88 50.66 o -14 11 5 310.21 202.00 87.91 o -11 11 5 30.65 -71.07 71.42 o -8 11 5 47.41 66.76 173.56 o -5 11 5 1037.01 1070.56 70.04 o -2 11 5 430.34 430.71 54.17 o 1 11 5 289.62 239.63 131.42 o -13 12 5 1638.76 1381.66 150.20 o -10 12 5 190.83 118.21 67.50 o -4 12 5 336.87 312.10 58.95 o -1 12 5 600.89 747.77 214.27 o 2 12 5 1.03 -92.49 132.13 o -12 13 5 273.98 381.76 154.28 o -9 13 5 14.23 -85.71 99.64 o -6 13 5 1171.96 1328.84 191.77 o -3 13 5 10.08 -85.71 103.92 o 0 13 5 75.65 -64.28 99.64 o -8 14 5 1924.35 2040.94 237.48 o -2 14 5 925.54 1168.50 204.27 o -4 15 5 73.53 114.28 135.35 o 1 1 6 20138.48 19551.28 357.08 o 2 2 6 4033.86 4305.52 83.84 o -3 3 6 82852.05 79830.62 3815.83 o 0 3 6 3.80 6.88 9.87 o 3 3 6 422.14 398.15 22.28 o -5 4 6 17228.79 18081.37 346.01 o -2 4 6 14755.49 14194.83 276.95 o 1 4 6 499.07 428.69 17.97 o 4 4 6 1358.50 1507.26 40.60 o -7 5 6 5768.01 5840.57 128.26 o -4 5 6 298.88 258.67 14.57 o -1 5 6 13.88 41.41 12.82 o 2 5 6 2917.43 2901.72 60.11 o 5 5 6 1203.81 1083.02 67.70 o -9 6 6 37.32 -1.06 26.92 o -6 6 6 6336.78 6531.50 114.25 o -3 6 6 2659.53 2703.13 62.47 o 0 6 6 459.19 471.79 27.00 o 3 6 6 44.95 39.83 28.87 o 6 6 6 45.82 8.63 29.75 o -11 7 6 3064.27 3149.85 157.19 o -8 7 6 417.45 450.63 36.04 o -5 7 6 535.79 419.73 23.94 o -2 7 6 1811.05 1842.73 46.30 o 1 7 6 54.13 36.60 17.15 o 4 7 6 150.11 114.69 66.48 o 7 7 6 232.56 388.73 91.20 o -13 8 6 5.67 -51.60 65.87 o -10 8 6 1975.25 1893.72 84.75 o 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27 4294.20 4352.58 291.77 o 1 1 27 99.04 75.60 66.72 o -1 2 27 156.48 162.62 65.93 o 2 2 27 1.85 14.92 101.62 o -3 3 27 421.58 409.67 93.45 o 0 3 27 1775.47 1698.90 120.52 o 3 3 27 38.73 -48.12 84.52 o -5 4 27 0.58 28.08 85.37 o -2 4 27 2290.11 2722.51 164.75 o 1 4 27 32.93 71.20 90.88 o 4 4 27 12.36 -11.84 101.92 o -7 5 27 13.07 -63.05 106.10 o -4 5 27 11.65 192.84 100.92 o -1 5 27 701.67 770.54 111.90 o 2 5 27 101.35 82.37 83.98 o -6 6 27 1139.45 1000.03 121.13 o -3 6 27 727.76 601.22 93.37 o 0 6 27 180.51 261.64 85.30 o -5 7 27 6.16 46.83 83.27 o -2 7 27 158.22 146.96 103.92 o -4 8 27 70.06 15.93 101.42 o -1 1 28 860.39 834.97 116.78 o -3 2 28 1431.45 1534.87 119.15 o 0 2 28 372.06 359.56 80.08 o -5 3 28 1924.88 1960.97 149.03 o -2 3 28 1319.30 1504.07 131.88 o 1 3 28 466.50 460.15 82.17 o -7 4 28 181.24 320.44 98.65 o -4 4 28 6.38 -13.42 78.55 o -1 4 28 48.92 -20.43 73.83 o 2 4 28 12.59 -15.63 68.59 o -6 5 28 1011.54 982.05 126.27 o -3 5 28 13.67 -99.71 105.89 o 0 5 28 2027.31 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663.46 125.93 o