#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:21:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181031 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/11/2211129.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211129_Fobs loop_ _publ_author_name 'Yu, Bin' 'Wang, Xiao-Qing' 'Kou, Hui-Zhong' 'Shen, Guang-Qiu' 'Shen, De-Zhong' _publ_section_title ; Poly[[diaquasamarium(III)]-\m~3~-(biphenyl-4,4'-dicarboxylato)-\m~3~-(4'-carboxylbiphenyl-4-carboxylato)] ; _journal_coeditor_code NG2106 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3078 _journal_page_last m3079 _journal_volume 62 _journal_year 2006 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 27.6650 _cell_length_b 8.6510 _cell_length_c 9.9345 _exptl_crystal_F_000 1324.00 _reflns_d_resolution_high 0.7487 _cod_data_source_file ng2106Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title Pbcn _shelx_refln_list_code 4 _shelx_f_calc_maximum 353.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 69947.52 45755.70 762.67 o 4 0 0 44326.29 38800.88 418.37 o 6 0 0 54298.08 47161.63 903.17 o 8 0 0 887.93 997.07 58.60 o 10 0 0 534.41 438.63 35.11 o 12 0 0 1642.70 2407.76 68.29 o 14 0 0 47404.79 44707.71 658.18 o 16 0 0 30848.24 29021.08 364.67 o 18 0 0 24472.84 23829.85 325.05 o 20 0 0 32006.03 30342.73 400.83 o 22 0 0 26166.87 25360.05 362.95 o 24 0 0 19665.12 19531.63 313.41 o 26 0 0 21313.72 20339.01 471.49 o 28 0 0 15492.95 15655.80 438.07 o 30 0 0 12360.65 12498.53 398.20 o 32 0 0 8123.14 8755.52 334.84 o 34 0 0 7131.86 7229.34 313.40 o 1 1 0 65309.98 61289.14 500.00 o 3 1 0 44967.43 43959.66 375.37 o 5 1 0 35815.58 35813.43 306.83 o 7 1 0 22775.26 22291.36 208.38 o 9 1 0 22937.03 22542.70 458.61 o 11 1 0 30229.05 29225.50 324.02 o 13 1 0 64469.29 61497.50 510.63 o 15 1 0 32651.50 31400.79 308.37 o 17 1 0 27474.53 26197.27 275.86 o 19 1 0 18651.69 18350.72 196.00 o 21 1 0 15260.39 14380.08 398.15 o 23 1 0 14098.86 13583.42 248.72 o 25 1 0 15998.08 15126.46 227.04 o 27 1 0 5501.61 5998.15 138.85 o 29 1 0 9076.04 9355.02 199.93 o 31 1 0 10219.70 10377.65 257.21 o 33 1 0 6133.95 5819.68 195.67 o 35 1 0 6695.35 6558.81 306.78 o 0 2 0 28827.01 30285.78 271.58 o 2 2 0 33882.01 34372.48 190.53 o 4 2 0 18977.70 19132.67 164.81 o 6 2 0 16862.00 16710.08 174.03 o 8 2 0 14466.51 13763.89 149.17 o 10 2 0 18073.12 17841.65 188.75 o 12 2 0 15893.65 15294.46 174.08 o 14 2 0 31187.50 31602.41 445.59 o 16 2 0 24855.79 25148.23 234.85 o 18 2 0 15805.51 15446.71 196.89 o 20 2 0 35201.68 33447.20 407.82 o 22 2 0 10535.11 9985.92 172.69 o 24 2 0 5179.06 5315.92 126.16 o 26 2 0 10895.56 10057.64 185.14 o 28 2 0 2457.89 2799.62 105.37 o 30 2 0 1839.73 2268.86 95.30 o 32 2 0 1592.39 1504.64 98.30 o 34 2 0 5479.42 5628.48 283.53 o 36 2 0 6318.23 6343.45 311.23 o 1 3 0 171.15 273.54 17.03 o 3 3 0 22972.99 23594.76 145.31 o 5 3 0 3452.39 3222.35 49.43 o 7 3 0 16856.50 17082.08 182.61 o 9 3 0 19990.95 20542.37 313.64 o 11 3 0 19456.96 19807.36 213.88 o 13 3 0 3636.74 3659.62 74.62 o 15 3 0 6345.20 6471.25 107.96 o 17 3 0 9283.61 8937.93 137.82 o 19 3 0 5890.35 5506.36 280.16 o 21 3 0 2107.93 1954.26 75.20 o 23 3 0 4532.16 4184.18 114.50 o 25 3 0 680.99 869.90 127.53 o 27 3 0 2295.27 2278.79 99.69 o 29 3 0 1621.46 1738.41 104.73 o 31 3 0 1329.94 1425.87 98.96 o 33 3 0 6027.75 5942.48 272.27 o 35 3 0 2937.37 2551.91 203.68 o 0 4 0 107.70 73.39 19.26 o 2 4 0 4732.81 5338.83 61.86 o 4 4 0 3704.79 3816.09 51.26 o 6 4 0 19203.91 20922.51 140.23 o 8 4 0 275.73 197.99 25.81 o 10 4 0 6.63 11.25 26.90 o 12 4 0 73.76 65.03 21.76 o 14 4 0 2940.33 2767.72 79.98 o 16 4 0 74.87 69.72 48.84 o 18 4 0 418.49 313.63 64.86 o 20 4 0 4922.97 4476.67 149.26 o 22 4 0 6366.49 5736.22 174.83 o 24 4 0 857.20 875.67 66.23 o 26 4 0 1027.68 1001.40 73.08 o 28 4 0 805.46 1093.78 112.51 o 30 4 0 49.55 64.15 61.81 o 32 4 0 188.59 204.05 110.39 o 34 4 0 4.29 -45.45 54.06 o 1 5 0 4924.60 5135.77 66.43 o 3 5 0 38.31 74.33 16.72 o 5 5 0 1007.72 1127.74 31.27 o 7 5 0 2246.33 2432.21 49.31 o 9 5 0 100.50 140.40 22.24 o 11 5 0 97.14 73.65 41.08 o 13 5 0 247.80 222.55 55.45 o 15 5 0 2219.57 2119.44 101.68 o 17 5 0 875.52 841.47 79.16 o 19 5 0 3276.94 2850.43 185.67 o 21 5 0 6480.42 6238.68 187.44 o 23 5 0 114.86 183.22 66.49 o 25 5 0 1054.95 965.40 95.47 o 27 5 0 1143.00 995.31 177.84 o 29 5 0 192.74 193.65 72.33 o 31 5 0 374.74 313.16 101.12 o 0 6 0 1878.33 1827.05 60.69 o 2 6 0 2796.91 2824.46 52.99 o 4 6 0 1208.47 1072.50 34.08 o 6 6 0 3034.41 3007.91 55.72 o 8 6 0 5692.42 5528.66 93.29 o 10 6 0 8443.28 8432.29 282.86 o 12 6 0 5521.11 5500.08 161.09 o 14 6 0 3711.85 3592.52 134.54 o 16 6 0 4805.30 4529.65 154.48 o 18 6 0 1456.37 1346.47 90.92 o 20 6 0 1465.45 1307.33 93.59 o 22 6 0 945.72 1049.95 111.43 o 24 6 0 1070.00 1208.76 265.34 o 26 6 0 1901.47 1602.97 111.38 o 28 6 0 1483.68 1479.11 111.53 o 30 6 0 531.29 907.38 191.93 o 1 7 0 7357.91 7245.93 95.02 o 3 7 0 4714.15 4826.19 85.32 o 5 7 0 13116.78 13202.94 152.90 o 7 7 0 6380.56 6364.44 135.80 o 9 7 0 5831.37 5477.43 190.73 o 11 7 0 6873.60 6966.35 190.32 o 13 7 0 4968.59 4821.78 161.55 o 15 7 0 6064.20 5808.85 182.30 o 17 7 0 1049.87 1174.07 99.38 o 19 7 0 14601.23 13980.09 311.25 o 21 7 0 6935.48 6495.45 210.62 o 23 7 0 2987.57 2915.73 145.92 o 25 7 0 5675.08 5773.70 208.82 o 27 7 0 4189.95 4028.02 179.03 o 0 8 0 3041.20 3179.24 118.50 o 2 8 0 10537.36 10555.61 158.70 o 4 8 0 11684.28 11556.95 197.78 o 6 8 0 12869.54 12798.42 215.54 o 8 8 0 7412.46 7308.76 156.44 o 10 8 0 7804.99 7807.02 211.00 o 12 8 0 8487.22 8511.12 226.57 o 14 8 0 3820.48 3856.31 185.25 o 16 8 0 2765.10 2613.11 131.73 o 18 8 0 8006.81 7679.50 230.94 o 20 8 0 7757.31 7591.11 235.31 o 22 8 0 3352.07 3267.83 158.23 o 24 8 0 8237.26 7969.35 254.86 o 1 9 0 20005.42 20298.31 291.88 o 3 9 0 6274.38 6499.98 152.26 o 5 9 0 11372.36 11564.16 210.95 o 7 9 0 6489.49 6512.01 155.99 o 9 9 0 3534.87 3684.09 149.51 o 11 9 0 2130.55 2224.11 121.15 o 13 9 0 1907.78 2003.60 126.71 o 15 9 0 5882.79 5340.94 194.37 o 17 9 0 6683.87 6773.76 224.67 o 19 9 0 8899.22 8697.08 262.27 o 0 10 0 894.28 973.93 112.38 o 2 10 0 4743.74 4778.55 166.58 o 4 10 0 7127.81 7119.57 206.70 o 6 10 0 3741.98 3988.57 131.58 o 8 10 0 5623.95 5724.44 224.51 o 10 10 0 4522.35 4608.82 179.42 o 12 10 0 6371.01 6183.95 212.16 o 14 10 0 4054.90 3851.47 172.68 o 16 10 0 5524.52 5931.65 316.65 o 1 11 0 2835.99 2713.37 134.88 o 3 11 0 3474.30 3541.71 152.83 o 5 11 0 1002.97 1198.26 187.96 o 7 11 0 2517.91 2566.12 193.32 o 9 11 0 2360.36 2021.46 188.62 o 11 11 0 1336.51 1448.13 175.01 o 1 1 1 15594.55 16696.58 88.82 o 2 1 1 104.53 141.12 6.79 o 3 1 1 3815.34 4105.92 39.97 o 4 1 1 933.69 955.51 19.13 o 5 1 1 2672.59 2655.75 33.92 o 6 1 1 312.36 323.50 27.41 o 7 1 1 2609.29 2544.86 38.91 o 8 1 1 4639.91 4758.87 45.29 o 9 1 1 3933.00 3708.58 40.63 o 10 1 1 3162.37 3213.69 39.10 o 11 1 1 5882.19 5648.77 56.44 o 12 1 1 9930.82 10709.79 99.15 o 13 1 1 4919.25 4921.99 52.48 o 14 1 1 2425.00 2545.33 37.74 o 15 1 1 5061.98 5048.01 56.51 o 16 1 1 750.73 785.09 31.02 o 17 1 1 5160.32 5134.26 62.93 o 18 1 1 240.02 325.76 25.72 o 19 1 1 2531.92 2555.27 44.21 o 20 1 1 2160.43 2076.19 41.36 o 21 1 1 23.32 110.25 19.44 o 22 1 1 167.52 173.11 24.75 o 23 1 1 1306.41 1267.04 39.21 o 24 1 1 76.95 54.68 20.31 o 25 1 1 447.80 584.55 42.87 o 26 1 1 752.07 669.23 38.07 o 27 1 1 1917.76 1860.58 55.37 o 28 1 1 178.17 224.55 32.31 o 29 1 1 2693.25 2298.89 70.76 o 30 1 1 100.67 118.87 38.25 o 31 1 1 2041.84 1977.20 77.16 o 32 1 1 19.60 41.53 45.51 o 33 1 1 2485.55 2356.45 104.81 o 34 1 1 285.88 220.67 74.97 o 35 1 1 703.85 654.35 129.54 o 36 1 1 50.35 30.80 63.40 o 0 2 1 1549.70 1797.32 45.66 o 1 2 1 53971.03 55644.96 231.53 o 2 2 1 22016.24 23199.93 106.48 o 3 2 1 4600.42 4808.32 38.49 o 4 2 1 14586.13 15007.70 93.48 o 5 2 1 1288.35 1328.44 20.98 o 6 2 1 15472.73 15534.53 118.65 o 7 2 1 30.09 46.15 8.53 o 8 2 1 15568.12 15142.55 113.96 o 9 2 1 220.28 162.87 13.63 o 10 2 1 17283.48 16842.49 127.74 o 11 2 1 1222.09 1094.08 26.08 o 12 2 1 36869.79 36565.15 242.74 o 13 2 1 6695.46 6988.14 80.27 o 14 2 1 14746.14 14395.67 113.41 o 15 2 1 616.03 695.38 45.44 o 16 2 1 12406.52 12070.16 104.99 o 17 2 1 187.93 301.22 20.83 o 18 2 1 9135.71 9048.95 86.18 o 19 2 1 1698.26 1676.50 40.78 o 20 2 1 3874.89 4097.07 64.61 o 21 2 1 2.56 48.33 19.26 o 22 2 1 5997.27 6052.99 82.88 o 23 2 1 62.93 145.61 26.88 o 24 2 1 6275.13 6053.25 95.50 o 25 2 1 5.31 57.24 24.89 o 26 2 1 3024.55 3240.05 72.03 o 27 2 1 66.82 150.26 30.07 o 28 2 1 5523.98 5154.16 113.08 o 29 2 1 109.25 240.25 41.25 o 30 2 1 5027.44 4841.42 105.14 o 31 2 1 0.38 111.84 47.04 o 32 2 1 4284.68 3975.76 111.57 o 33 2 1 13.18 74.10 39.56 o 34 2 1 1409.28 1437.41 73.31 o 35 2 1 26.39 23.15 61.04 o 1 3 1 19994.32 20017.01 90.42 o 2 3 1 11444.12 12206.20 75.72 o 3 3 1 45171.16 44679.22 223.89 o 4 3 1 2318.47 2397.67 25.97 o 5 3 1 11989.04 11792.13 84.28 o 6 3 1 1350.78 1416.33 26.25 o 7 3 1 16123.82 16405.52 123.46 o 8 3 1 3328.14 3794.37 50.53 o 9 3 1 27400.52 27845.77 193.09 o 10 3 1 16.52 19.61 10.70 o 11 3 1 32087.95 32106.68 220.56 o 12 3 1 502.14 502.30 51.28 o 13 3 1 21698.21 20891.93 195.83 o 14 3 1 624.79 553.62 43.87 o 15 3 1 20649.67 20256.75 188.39 o 16 3 1 122.12 249.96 28.06 o 17 3 1 26889.45 26243.96 297.69 o 18 3 1 354.61 544.78 59.41 o 19 3 1 16604.58 16231.85 155.54 o 20 3 1 4780.13 4482.60 86.25 o 21 3 1 5584.28 5935.83 92.70 o 22 3 1 0.00 47.29 22.31 o 23 3 1 8646.65 8602.35 117.67 o 24 3 1 10.14 47.82 25.60 o 25 3 1 6123.95 5862.27 110.45 o 26 3 1 7.08 91.38 35.27 o 27 3 1 8668.38 8576.67 140.36 o 28 3 1 26.09 144.78 34.10 o 29 3 1 7499.99 7135.27 131.32 o 30 3 1 3.54 166.55 37.42 o 31 3 1 5991.83 5897.02 122.01 o 32 3 1 235.72 452.74 75.22 o 33 3 1 7077.02 6969.54 154.01 o 34 3 1 59.53 209.05 57.89 o 35 3 1 4932.90 4938.53 186.64 o 0 4 1 20862.49 20840.45 155.66 o 1 4 1 846.17 893.90 17.28 o 2 4 1 50461.73 51102.72 216.74 o 3 4 1 2165.13 2228.20 27.40 o 4 4 1 44566.79 45230.84 203.39 o 5 4 1 1506.03 1525.82 30.40 o 6 4 1 28622.97 29109.95 158.54 o 7 4 1 1.87 -11.25 12.72 o 8 4 1 34010.46 34436.59 220.88 o 9 4 1 50.49 74.84 15.37 o 10 4 1 18948.98 19095.31 130.76 o 11 4 1 33.95 11.46 13.67 o 12 4 1 15792.30 15687.11 187.25 o 13 4 1 156.01 127.05 24.42 o 14 4 1 8542.22 8462.54 110.20 o 15 4 1 632.52 677.26 37.18 o 16 4 1 11488.82 11658.87 138.39 o 17 4 1 16.01 84.94 32.34 o 18 4 1 10984.36 10722.38 163.25 o 19 4 1 493.32 713.64 59.58 o 20 4 1 9017.35 8867.33 150.92 o 21 4 1 455.89 721.01 60.31 o 22 4 1 22580.94 21155.76 295.03 o 23 4 1 169.88 236.87 63.17 o 24 4 1 16900.61 16217.59 200.78 o 25 4 1 42.01 194.19 35.96 o 26 4 1 12390.40 12397.18 195.04 o 27 4 1 786.06 1009.95 56.95 o 28 4 1 13426.97 13075.32 186.60 o 29 4 1 150.91 319.71 44.90 o 30 4 1 9621.25 9464.59 216.85 o 31 4 1 49.91 168.18 44.06 o 32 4 1 7046.01 6922.98 169.47 o 33 4 1 718.81 1021.80 95.63 o 34 4 1 4128.27 4207.68 278.93 o 1 5 1 16493.79 16793.87 99.69 o 2 5 1 1219.79 1323.05 24.28 o 3 5 1 24796.16 24929.82 131.14 o 4 5 1 505.75 569.10 21.77 o 5 5 1 25731.76 26050.54 135.96 o 6 5 1 199.88 250.43 16.69 o 7 5 1 31249.98 31841.78 221.53 o 8 5 1 20.59 48.69 21.32 o 9 5 1 26951.79 26766.69 180.59 o 10 5 1 2.30 93.57 24.11 o 11 5 1 21665.88 21331.97 265.86 o 12 5 1 42.97 118.86 25.62 o 13 5 1 14521.11 14507.93 159.09 o 14 5 1 140.30 197.87 39.15 o 15 5 1 10425.78 10608.38 162.02 o 16 5 1 221.23 250.43 42.34 o 17 5 1 12489.53 12598.56 184.84 o 18 5 1 1924.61 1810.88 70.17 o 19 5 1 6619.47 6673.58 153.06 o 20 5 1 369.92 519.96 75.96 o 21 5 1 15395.48 15299.67 219.36 o 22 5 1 157.43 330.63 49.99 o 23 5 1 12306.00 12251.09 198.16 o 24 5 1 44.69 177.34 43.42 o 25 5 1 11586.78 11611.82 197.54 o 26 5 1 149.99 304.04 51.55 o 27 5 1 9453.68 9577.24 176.88 o 28 5 1 385.33 482.50 60.62 o 29 5 1 8265.55 8357.01 175.33 o 30 5 1 5.47 216.25 50.39 o 31 5 1 7701.06 7522.78 168.88 o 32 5 1 734.23 839.03 89.52 o 0 6 1 13137.75 13261.10 128.01 o 1 6 1 131.37 158.09 15.75 o 2 6 1 7223.29 7244.21 62.45 o 3 6 1 104.97 136.16 16.22 o 4 6 1 12568.95 12542.86 97.86 o 5 6 1 394.68 557.95 23.76 o 6 6 1 11452.19 11163.11 84.88 o 7 6 1 1967.76 2183.76 37.78 o 8 6 1 18739.30 18915.07 151.07 o 9 6 1 121.44 158.79 21.80 o 10 6 1 16533.02 16504.87 139.87 o 11 6 1 45.05 91.28 20.93 o 12 6 1 13157.88 13397.62 162.74 o 13 6 1 175.99 271.24 43.50 o 14 6 1 13935.05 14007.53 197.10 o 15 6 1 306.87 448.85 51.98 o 16 6 1 9151.18 8832.13 165.69 o 17 6 1 224.46 317.74 47.19 o 18 6 1 14445.09 13774.20 247.63 o 19 6 1 557.94 715.64 65.16 o 20 6 1 7544.99 7600.19 152.51 o 21 6 1 9.53 79.23 37.75 o 22 6 1 6281.46 6493.28 171.85 o 23 6 1 63.61 129.26 42.39 o 24 6 1 6711.45 6424.83 167.63 o 25 6 1 212.34 303.69 53.47 o 26 6 1 5220.84 5371.13 138.25 o 27 6 1 13.00 64.90 41.54 o 28 6 1 4651.33 4882.80 135.88 o 29 6 1 0.23 52.06 43.53 o 30 6 1 3235.90 3219.83 125.36 o 1 7 1 1899.94 1994.78 39.27 o 2 7 1 173.01 137.38 19.94 o 3 7 1 2239.39 2137.03 40.69 o 4 7 1 214.08 227.25 23.65 o 5 7 1 8768.95 8944.58 108.95 o 6 7 1 275.21 383.39 27.62 o 7 7 1 9250.88 9073.33 92.83 o 8 7 1 5.44 56.13 19.97 o 9 7 1 8487.37 8189.40 143.08 o 10 7 1 3.35 39.65 28.74 o 11 7 1 10595.04 10049.74 164.81 o 12 7 1 9.16 65.45 34.11 o 13 7 1 9330.94 8789.99 156.88 o 14 7 1 231.36 261.78 45.80 o 15 7 1 5993.94 5714.76 128.05 o 16 7 1 645.21 722.77 65.83 o 17 7 1 2074.19 2114.25 81.87 o 18 7 1 132.95 142.55 44.26 o 19 7 1 2537.18 2534.92 91.02 o 20 7 1 1526.04 1395.97 71.52 o 21 7 1 3796.12 3662.14 111.47 o 22 7 1 14.03 -6.71 37.00 o 23 7 1 1891.19 1879.66 84.06 o 24 7 1 326.81 321.15 57.34 o 25 7 1 3577.18 3618.24 117.50 o 26 7 1 36.83 97.73 48.07 o 27 7 1 1763.41 1740.20 87.29 o 0 8 1 6310.06 6147.14 186.94 o 1 8 1 306.54 387.93 31.54 o 2 8 1 3153.32 3022.22 58.01 o 3 8 1 253.25 295.40 30.16 o 4 8 1 1174.95 1117.13 37.71 o 5 8 1 101.40 122.10 24.45 o 6 8 1 1689.47 1668.39 48.69 o 7 8 1 46.98 19.61 22.30 o 8 8 1 879.38 832.61 42.01 o 9 8 1 9.82 -2.78 30.04 o 10 8 1 713.27 766.99 82.46 o 11 8 1 141.86 139.09 42.38 o 12 8 1 521.30 624.46 62.31 o 13 8 1 26.28 -27.68 31.78 o 14 8 1 1113.87 1204.49 70.84 o 15 8 1 5.39 -25.96 33.24 o 16 8 1 1139.65 1158.37 99.81 o 17 8 1 103.69 80.33 40.99 o 18 8 1 1065.37 1142.03 85.94 o 19 8 1 212.43 241.59 55.13 o 20 8 1 1082.75 1104.81 75.60 o 21 8 1 299.27 186.84 51.19 o 22 8 1 353.29 360.58 61.43 o 23 8 1 102.08 -8.42 43.27 o 24 8 1 730.51 975.94 97.53 o 1 9 1 92.92 39.09 28.08 o 2 9 1 18.22 -22.65 25.79 o 3 9 1 38.26 -5.64 25.63 o 4 9 1 1023.97 994.90 46.23 o 5 9 1 230.80 249.04 37.57 o 6 9 1 1.80 -22.93 22.93 o 7 9 1 0.62 -22.88 22.88 o 8 9 1 90.75 31.53 35.74 o 9 9 1 3.65 -33.59 33.59 o 10 9 1 159.65 102.01 42.71 o 11 9 1 139.46 106.53 42.48 o 12 9 1 135.76 71.31 53.13 o 13 9 1 20.65 -19.71 33.84 o 14 9 1 138.43 97.19 43.61 o 15 9 1 444.96 428.88 61.65 o 16 9 1 246.58 204.83 53.21 o 17 9 1 130.28 86.41 46.03 o 18 9 1 460.58 367.19 63.39 o 19 9 1 54.02 58.10 44.77 o 20 9 1 220.43 151.47 52.38 o 0 10 1 949.17 965.61 88.55 o 1 10 1 473.97 429.83 53.52 o 2 10 1 73.27 119.05 38.16 o 3 10 1 163.84 138.75 37.21 o 4 10 1 412.86 454.67 50.30 o 5 10 1 131.21 93.54 40.94 o 6 10 1 380.77 480.86 103.89 o 7 10 1 0.03 -35.32 35.32 o 8 10 1 639.44 721.80 71.62 o 9 10 1 65.40 10.18 39.23 o 10 10 1 772.55 889.64 90.33 o 11 10 1 54.46 28.02 41.97 o 12 10 1 238.57 308.50 58.10 o 13 10 1 201.97 97.98 50.47 o 14 10 1 485.98 547.65 71.75 o 15 10 1 103.25 73.17 49.96 o 16 10 1 417.63 444.53 98.93 o 1 11 1 811.53 1019.72 83.79 o 2 11 1 21.47 36.10 43.36 o 3 11 1 2153.24 2036.92 96.76 o 4 11 1 3.48 23.88 42.63 o 5 11 1 1174.57 1243.35 78.05 o 6 11 1 20.33 17.15 51.04 o 7 11 1 1547.07 1554.41 91.11 o 8 11 1 10.93 -12.60 62.06 o 9 11 1 941.63 961.73 224.93 o 10 11 1 74.49 43.48 105.15 o 0 0 2 33319.63 33453.02 483.47 o 1 0 2 40646.73 39676.29 1008.19 o 2 0 2 90561.95 77138.65 1225.39 o 3 0 2 438.73 470.60 27.12 o 4 0 2 69177.03 59211.44 784.36 o 5 0 2 354.30 346.47 13.78 o 6 0 2 63865.65 56742.39 677.77 o 7 0 2 258.30 265.04 16.73 o 8 0 2 32165.35 31724.76 327.96 o 9 0 2 3203.33 3289.66 51.63 o 10 0 2 25125.38 25176.38 294.16 o 11 0 2 6446.16 7102.53 88.32 o 12 0 2 16279.25 16329.94 159.01 o 13 0 2 4150.97 4648.36 72.93 o 14 0 2 18151.91 18379.17 180.21 o 15 0 2 805.92 1065.30 78.54 o 16 0 2 20625.87 20437.13 201.93 o 17 0 2 14.88 113.97 35.56 o 18 0 2 19021.13 19264.67 200.69 o 19 0 2 1809.58 2265.17 60.26 o 20 0 2 48104.86 45756.68 593.66 o 22 0 2 14548.46 15097.91 190.74 o 23 0 2 1338.79 1522.14 64.98 o 24 0 2 11163.26 11914.23 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80.32 o 3 8 4 823.46 815.37 47.17 o 4 8 4 8567.68 8541.24 104.11 o 5 8 4 263.51 267.72 31.80 o 6 8 4 4894.84 4994.48 83.91 o 7 8 4 213.54 288.24 35.18 o 8 8 4 7373.32 7513.25 98.90 o 9 8 4 9.34 116.48 25.32 o 10 8 4 11240.39 10954.10 123.28 o 11 8 4 25.75 138.87 29.25 o 12 8 4 6574.14 6795.69 117.55 o 13 8 4 37.97 149.52 34.11 o 14 8 4 8382.54 8111.03 131.94 o 15 8 4 488.16 557.72 54.45 o 16 8 4 6018.58 5897.97 140.92 o 17 8 4 8.99 146.21 44.64 o 18 8 4 8692.08 8288.08 172.44 o 19 8 4 374.39 493.38 64.81 o 20 8 4 3312.37 3358.66 112.37 o 21 8 4 64.76 180.10 49.73 o 22 8 4 1867.22 2150.97 94.68 o 23 8 4 84.40 67.21 84.31 o 1 9 4 2983.21 3059.98 78.31 o 2 9 4 123.05 160.65 34.55 o 3 9 4 5088.68 5269.37 102.15 o 4 9 4 0.86 70.73 28.46 o 5 9 4 8134.75 8178.18 141.46 o 6 9 4 7.37 100.65 39.37 o 7 9 4 8706.49 8552.79 146.38 o 8 9 4 7.27 125.44 41.33 o 9 9 4 5929.31 6031.79 139.27 o 10 9 4 0.35 98.97 40.01 o 11 9 4 6804.52 7239.46 140.06 o 12 9 4 42.40 148.94 40.45 o 13 9 4 6480.56 6477.28 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7015.03 6680.86 145.00 o 4 3 11 2.72 12.11 30.81 o 5 3 11 4451.11 4344.33 116.14 o 6 3 11 12.97 20.27 32.16 o 7 3 11 3819.89 3777.86 121.58 o 8 3 11 337.74 396.42 42.09 o 9 3 11 4268.53 4500.89 124.17 o 10 3 11 21.26 83.10 30.41 o 11 3 11 4936.60 4982.04 199.52 o 12 3 11 0.17 32.06 35.27 o 13 3 11 2015.69 1977.76 82.92 o 14 3 11 39.36 61.81 36.02 o 15 3 11 3553.47 3590.44 112.66 o 16 3 11 11.35 80.61 51.96 o 18 3 11 2.36 67.93 93.35 o 0 4 11 5204.67 5109.76 309.31 o 1 4 11 474.07 492.13 60.73 o 2 4 11 6325.29 6574.66 149.78 o 3 4 11 8.54 124.96 41.90 o 4 4 11 7308.72 7308.52 158.29 o 5 4 11 96.17 142.57 50.74 o 6 4 11 3573.07 3790.84 165.53 o 7 4 11 329.79 367.34 48.03 o 8 4 11 5351.95 5505.71 213.17 o 9 4 11 72.23 124.57 38.09 o 10 4 11 6134.51 6456.54 224.19 o 11 4 11 37.89 77.06 31.81 o 12 4 11 3253.15 3334.14 122.59 o 13 4 11 148.75 203.65 48.88 o 14 4 11 5160.62 4889.10 187.68 o 15 4 11 26.16 142.24 62.23 o 16 4 11 5232.03 5305.80 285.82 o 1 5 11 5429.93 5381.75 140.57 o 2 5 11 192.68 388.12 58.92 o 3 5 11 6296.01 6659.92 156.86 o 4 5 11 12.82 77.02 34.76 o 5 5 11 4756.36 4807.33 114.45 o 6 5 11 71.63 65.98 36.54 o 7 5 11 2799.05 3079.14 143.83 o 8 5 11 45.61 41.78 35.77 o 9 5 11 5334.79 5564.44 158.58 o 10 5 11 11.66 101.11 50.92 o 11 5 11 3553.02 3621.87 190.31 o 12 5 11 0.88 74.44 89.49 o 13 5 11 4726.91 5037.81 277.15 o 0 0 12 6000.35 6198.19 263.30 o 1 0 12 239.46 242.94 92.14 o 2 0 12 7036.80 7271.13 292.81 o 3 0 12 280.01 169.83 82.99 o 4 0 12 7214.51 6982.90 288.95 o 5 0 12 4.28 23.97 60.95 o 6 0 12 3503.46 3711.09 212.83 o 7 0 12 348.96 213.67 88.17 o 8 0 12 3810.01 4157.10 232.10 o 9 0 12 262.46 254.38 98.04 o 10 0 12 3769.17 3661.70 222.10 o 11 0 12 30.60 52.39 72.27 o 12 0 12 7803.56 7627.17 328.22 o 13 0 12 6.13 173.44 88.89 o 1 1 12 6889.20 6854.64 200.74 o 2 1 12 36.53 -7.12 84.19 o 3 1 12 4515.74 4524.95 131.63 o 4 1 12 46.05 16.83 48.56 o 5 1 12 5406.42 5359.25 180.51 o 6 1 12 3.84 33.55 51.65 o 7 1 12 5286.48 5060.72 204.87 o 8 1 12 20.65 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