#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:21:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181031 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/11/2211131.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211131_Fobs loop_ _publ_author_name 'Ballivet-Tkatchenko, Danielle' 'Cattey, H\'el\`ene' 'Plasseraud, Laurent' 'Richard, Philippe' _publ_section_title ; catena-Poly[[di-n-butyltin(IV)]-\m-trifluoromethanesulfonato-[[di-n-butyl(trifluoromethanesulfonato)tin(IV)]-di-\m-hydroxo]] ; _journal_coeditor_code NG2109 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2820 _journal_page_last m2822 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.212 _cell_angle_beta 80.197 _cell_angle_gamma 75.255 _cell_length_a 9.8810 _cell_length_b 11.9158 _cell_length_c 13.4110 _exptl_crystal_F_000 788.00 _reflns_d_resolution_high 0.7639 _cod_data_source_file ng2109Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ; ; _shelx_refln_list_code 4 _shelx_f_calc_maximum 230.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6647.93 6084.34 100.52 o 3 0 0 231.78 220.56 4.27 o 4 0 0 8311.49 7459.77 132.40 o 5 0 0 16553.17 15994.54 313.20 o 6 0 0 9203.27 9241.92 175.51 o 7 0 0 3415.90 3462.56 70.98 o 8 0 0 33.93 27.22 6.24 o 9 0 0 3464.53 3511.78 98.16 o 10 0 0 124.78 109.91 25.71 o 11 0 0 6850.07 7264.38 546.82 o -11 1 0 5373.97 5427.78 390.50 o -10 1 0 333.91 303.85 18.72 o -9 1 0 5908.47 5954.74 334.33 o -8 1 0 101.99 90.66 8.40 o -7 1 0 3445.31 3486.93 65.96 o -6 1 0 3255.05 3203.75 58.51 o -5 1 0 16740.25 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