#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/11/2211160.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211160_Fobs loop_ _publ_author_name 'Zhang, Xian-Fa' 'Gao, Shan' 'Huo, Li-Hua' 'Ng, Seik Weng' _publ_section_title ; cyclo-Tetrakis(\m-1H-imidazole-4,5-dicarboxylato-\k^4^N,O:N',O')tetrakis[(2,2'-bipyridine-\k^2^N,N')cobalt(III)] hexadecahydrate ; _journal_coeditor_code OB3024 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2860 _journal_page_last m2862 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 65.066 _cell_angle_beta 72.973 _cell_angle_gamma 73.131 _cell_length_a 11.7238 _cell_length_b 13.5350 _cell_length_c 13.6101 _exptl_crystal_F_000 904.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file ob3024Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7497.75 2.29 3.37 o 2 0 0 6168.35 6589.26 39.03 o 3 0 0 5472.61 5386.24 66.91 o 4 0 0 651.49 510.08 15.78 o 5 0 0 1.57 6.14 9.24 o 6 0 0 986.17 926.66 42.02 o 7 0 0 71.06 146.12 12.28 o 8 0 0 23.77 13.31 16.25 o 9 0 0 36.25 70.55 17.27 o 10 0 0 12.26 16.64 22.66 o 11 0 0 427.25 431.41 23.25 o 12 0 0 115.50 114.18 23.15 o 13 0 0 27.06 58.81 25.41 o 14 0 0 30.44 54.96 28.07 o -14 1 0 1.09 -11.34 33.41 o -13 1 0 18.15 0.54 24.43 o -12 1 0 14.96 -5.95 27.22 o -11 1 0 17.06 7.76 21.52 o -10 1 0 65.37 89.90 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