#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211193_Fobs loop_ _publ_author_name 'Kennepohl, Dietmar' 'Thomas, Angela' 'McDonald, Robert' _publ_section_title ; Bis{\m:\k^2^,\k^2^-6,6'-bis[2-(2-pyridyl)ethyliminomethyl]-2,2'-bipyridine}dicopper(I) bis(hexafluorophosphate) ; _journal_coeditor_code SG2072 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2967 _journal_page_last m2969 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.330 _cell_angle_gamma 90.000 _cell_length_a 13.6235 _cell_length_b 16.6329 _cell_length_c 23.8071 _exptl_crystal_F_000 2560.00 _reflns_d_resolution_high 0.7993 _[local]_cod_data_source_file sg2072Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ath0202 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 632.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4469.37 5374.12 193.31 o 4 0 0 133748.06 140561.30 2779.68 o 6 0 0 7870.95 10269.59 219.85 o 8 0 0 52093.44 48594.75 1209.03 o 10 0 0 105.11 66.05 39.33 o 12 0 0 3537.75 3387.89 133.28 o 14 0 0 5097.54 5238.80 270.64 o 16 0 0 6027.03 5954.06 309.30 o 3 1 0 45399.69 46419.75 796.96 o 5 1 0 2481.85 2316.44 71.85 o 7 1 0 25354.42 26492.11 421.47 o 9 1 0 1370.96 1593.60 85.80 o 11 1 0 2504.69 2415.38 161.51 o 13 1 0 9.20 19.20 40.46 o 15 1 0 836.96 954.18 87.09 o 2 2 0 145841.53 164778.36 3253.22 o 4 2 0 2.58 125.51 38.76 o 6 2 0 617.32 206.86 22.52 o 8 2 0 3514.58 2664.33 66.80 o 10 2 0 5245.05 5027.52 113.75 o 12 2 0 1084.11 918.69 58.46 o 14 2 0 2.09 -29.18 54.63 o 16 2 0 83.95 176.19 55.67 o 1 3 0 20964.23 23020.71 737.01 o 3 3 0 24485.77 29660.54 1194.60 o 5 3 0 13165.97 12836.79 472.91 o 7 3 0 1719.79 1840.88 71.87 o 9 3 0 1491.62 1015.38 43.73 o 11 3 0 61.30 49.49 30.79 o 13 3 0 4283.41 4252.74 130.07 o 15 3 0 1824.42 2014.83 92.82 o 0 4 0 6371.07 7155.62 236.81 o 2 4 0 54225.84 59835.68 1014.92 o 4 4 0 19303.18 19591.12 433.15 o 6 4 0 4756.52 4979.56 234.25 o 8 4 0 27484.76 26133.95 464.81 o 10 4 0 4203.85 4065.57 97.81 o 12 4 0 3906.01 3734.27 146.16 o 14 4 0 2580.74 2882.84 107.59 o 16 4 0 3773.08 3823.99 174.00 o 1 5 0 29008.69 34679.18 880.84 o 3 5 0 47715.05 50400.45 1070.76 o 5 5 0 20096.94 21707.65 514.53 o 7 5 0 3124.87 4030.77 89.08 o 9 5 0 97.06 304.06 72.81 o 11 5 0 3376.74 3463.66 90.77 o 13 5 0 2283.34 2085.07 85.19 o 15 5 0 33.43 100.70 64.74 o 0 6 0 454.07 497.78 48.33 o 2 6 0 338.82 429.34 24.88 o 4 6 0 3700.34 4438.30 127.65 o 6 6 0 1632.10 1700.64 47.99 o 8 6 0 1573.61 1457.20 49.15 o 10 6 0 86.90 18.59 33.21 o 12 6 0 1514.95 1619.18 72.24 o 14 6 0 103.87 78.20 45.19 o 16 6 0 1137.82 1294.74 80.28 o 1 7 0 140.05 290.20 24.80 o 3 7 0 3885.73 3281.48 135.55 o 5 7 0 13349.59 15909.67 465.97 o 7 7 0 89.98 219.09 25.65 o 9 7 0 6.18 57.14 38.93 o 11 7 0 1667.49 1764.46 72.24 o 13 7 0 12.87 38.76 42.38 o 15 7 0 135.97 188.27 50.81 o 0 8 0 667.65 579.94 57.99 o 2 8 0 33138.25 33507.97 1111.55 o 4 8 0 942.58 1095.88 28.85 o 6 8 0 25347.71 24659.19 454.98 o 8 8 0 833.28 866.38 44.12 o 10 8 0 8068.19 8254.76 171.11 o 12 8 0 3387.26 3295.35 108.61 o 14 8 0 2139.23 2079.43 112.62 o 1 9 0 45.21 5.34 36.25 o 3 9 0 1137.45 1224.32 47.38 o 5 9 0 3004.19 2995.31 106.32 o 7 9 0 5.15 -26.70 26.70 o 9 9 0 1453.91 1328.15 54.36 o 11 9 0 24.60 25.37 65.24 o 13 9 0 810.34 814.74 57.99 o 15 9 0 145.78 100.55 61.23 o 0 10 0 27809.63 29432.02 1039.06 o 2 10 0 12339.63 14068.54 294.14 o 4 10 0 24171.06 23131.07 474.71 o 6 10 0 488.86 339.55 32.33 o 8 10 0 15860.93 15707.82 297.31 o 10 10 0 619.46 524.92 42.61 o 12 10 0 1549.68 1528.49 79.74 o 14 10 0 22.75 53.70 45.29 o 1 11 0 276.94 188.04 42.61 o 3 11 0 58.09 20.21 62.83 o 5 11 0 20.96 50.32 33.83 o 7 11 0 2219.05 2402.11 120.82 o 9 11 0 22.22 0.00 32.33 o 11 11 0 1661.90 1430.44 70.60 o 13 11 0 11.24 87.53 43.81 o 0 12 0 21.48 164.32 57.99 o 2 12 0 6404.75 6564.84 350.38 o 4 12 0 636.47 769.78 59.73 o 6 12 0 7185.85 6168.70 157.31 o 8 12 0 604.87 750.07 55.58 o 10 12 0 4750.87 4488.91 171.57 o 12 12 0 12.13 -21.75 42.87 o 1 13 0 1154.79 1031.23 66.57 o 3 13 0 199.81 140.15 44.03 o 5 13 0 127.22 94.84 41.08 o 7 13 0 1755.05 1689.99 72.38 o 9 13 0 19.04 -42.29 79.74 o 11 13 0 199.70 196.33 54.36 o 13 13 0 929.01 997.69 83.67 o 0 14 0 348.12 318.97 72.49 o 2 14 0 1594.53 1356.36 78.38 o 4 14 0 5558.83 4975.87 167.34 o 6 14 0 1787.79 1940.18 79.57 o 8 14 0 1430.70 1307.69 67.94 o 10 14 0 657.82 772.45 77.33 o 12 14 0 1578.44 1444.74 111.16 o 1 15 0 1178.37 1171.94 75.18 o 3 15 0 8508.63 8805.66 263.07 o 5 15 0 823.63 727.73 54.09 o 7 15 0 466.93 429.13 49.03 o 9 15 0 275.07 125.51 74.91 o 11 15 0 1053.16 1305.25 92.27 o 0 16 0 253.71 502.62 82.16 o 2 16 0 190.26 254.92 52.89 o 4 16 0 5.74 74.10 50.92 o 6 16 0 1378.42 1399.53 72.38 o 8 16 0 40.91 49.76 43.81 o 10 16 0 65.79 54.04 56.31 o 1 17 0 477.41 439.50 59.73 o 3 17 0 522.84 534.53 64.66 o 5 17 0 74.73 77.84 44.63 o 7 17 0 662.12 654.77 89.41 o 9 17 0 51.65 125.65 89.41 o 0 18 0 4461.12 4272.23 227.14 o 2 18 0 7417.06 6845.62 227.23 o 4 18 0 1700.80 1460.95 92.27 o 6 18 0 1299.62 1274.53 72.38 o 8 18 0 237.06 295.01 66.57 o 1 19 0 3037.10 3178.18 139.99 o 3 19 0 1585.96 1759.76 130.49 o 5 19 0 431.99 387.19 57.99 o 0 20 0 202.54 154.65 86.99 o 2 20 0 550.09 596.99 74.95 o 4 20 0 274.59 242.73 65.24 o -15 1 1 31.68 18.56 48.14 o -13 1 1 24.45 67.20 41.25 o -11 1 1 495.04 335.96 36.93 o -9 1 1 14223.01 13151.85 335.53 o -7 1 1 4404.69 4850.93 91.54 o -5 1 1 6298.08 5152.76 90.31 o -3 1 1 27831.85 30250.73 558.75 o 3 1 1 1780.91 1550.92 44.52 o 5 1 1 4506.16 4281.18 86.77 o 7 1 1 18572.30 18039.74 394.46 o 9 1 1 5657.00 4940.47 99.15 o 11 1 1 508.75 478.43 45.51 o 13 1 1 280.01 303.16 55.51 o 15 1 1 561.78 467.24 73.41 o -16 2 1 74.52 85.79 51.72 o -14 2 1 373.25 386.80 52.43 o -12 2 1 1930.31 2036.74 82.55 o -10 2 1 205.50 111.16 30.76 o -8 2 1 217.13 103.30 31.27 o -6 2 1 2196.65 2394.19 78.14 o -4 2 1 29.14 18.92 16.07 o -2 2 1 5707.81 5540.60 145.21 o 2 2 1 2181.39 2473.00 48.65 o 4 2 1 2065.09 2419.42 51.58 o 6 2 1 2636.77 2092.57 52.11 o 8 2 1 368.99 267.60 26.83 o 10 2 1 1434.86 1376.65 53.71 o 12 2 1 311.03 335.26 44.53 o 14 2 1 151.68 203.10 48.00 o 16 2 1 1.84 35.10 67.66 o -15 3 1 23.50 60.79 48.00 o -13 3 1 366.13 366.30 87.48 o -11 3 1 799.18 926.61 56.42 o -9 3 1 202.74 337.09 30.46 o -7 3 1 12133.06 9771.15 184.69 o -5 3 1 7766.64 10695.62 256.43 o -3 3 1 195327.70 218112.39 3712.37 o -1 3 1 18738.80 23794.09 730.84 o 1 3 1 13290.30 13174.51 324.65 o 3 3 1 10192.25 11993.12 431.25 o 5 3 1 1259.40 755.61 28.87 o 7 3 1 8.07 -19.12 20.25 o 9 3 1 15656.18 15332.91 285.48 o 11 3 1 132.18 90.16 30.79 o 13 3 1 208.47 120.08 44.47 o 15 3 1 37.92 22.14 48.00 o -16 4 1 844.40 995.86 74.92 o -14 4 1 1147.71 1073.01 68.56 o -12 4 1 313.54 430.07 46.90 o -10 4 1 2313.22 2370.23 68.35 o -8 4 1 6756.60 6657.28 134.86 o -6 4 1 21.99 -11.89 22.26 o -4 4 1 111.93 63.24 29.71 o -2 4 1 36132.50 40107.16 1058.09 o 0 4 1 389.58 250.70 44.28 o 2 4 1 25131.01 29999.39 786.67 o 4 4 1 38.47 45.35 14.85 o 6 4 1 14364.52 14455.64 335.04 o 8 4 1 4558.20 4879.81 106.09 o 10 4 1 10896.39 10213.84 201.65 o 12 4 1 510.80 440.28 48.65 o 14 4 1 1316.70 1240.45 74.42 o 16 4 1 102.00 133.17 55.25 o -15 5 1 388.87 518.64 58.06 o -13 5 1 2182.01 1975.22 84.17 o -11 5 1 1651.99 1684.05 71.17 o -9 5 1 27214.91 25485.92 458.37 o -7 5 1 5187.97 7484.39 154.52 o -5 5 1 8850.03 6621.89 194.62 o -3 5 1 26151.83 29077.74 559.02 o -1 5 1 146814.48 164376.81 3213.42 o 1 5 1 10983.65 12213.53 251.12 o 3 5 1 6070.54 5620.40 158.38 o 5 5 1 16659.51 19819.32 416.87 o 7 5 1 41804.11 39567.09 1190.23 o 9 5 1 463.13 528.63 34.28 o 11 5 1 8149.71 7730.02 163.51 o 13 5 1 3419.39 3801.18 142.99 o 15 5 1 3746.11 3948.01 146.85 o -16 6 1 13.13 5.86 50.81 o -14 6 1 571.60 498.05 55.41 o -12 6 1 2423.91 2723.43 96.10 o -10 6 1 167.85 228.01 31.07 o -8 6 1 1179.27 1143.60 43.58 o -6 6 1 10179.79 9827.55 185.74 o -4 6 1 14795.44 15648.48 449.85 o -2 6 1 13851.10 14627.89 258.52 o 0 6 1 303.67 369.64 25.11 o 2 6 1 14974.63 14253.23 478.45 o 4 6 1 7184.23 7636.22 289.41 o 6 6 1 3944.40 4069.32 152.66 o 8 6 1 339.42 487.46 33.07 o 10 6 1 1099.69 1054.79 47.20 o 12 6 1 28.62 74.67 40.50 o 14 6 1 1558.56 1570.67 78.83 o 16 6 1 36.54 30.66 53.62 o -15 7 1 708.26 747.83 64.05 o -13 7 1 18.00 65.00 42.38 o -11 7 1 1751.36 1745.57 73.23 o -9 7 1 6324.44 6039.65 158.01 o -7 7 1 4627.21 3771.09 76.95 o -5 7 1 8890.68 7782.28 120.16 o -3 7 1 2471.93 3151.76 160.79 o -1 7 1 1613.10 1915.86 54.83 o 1 7 1 14989.03 17364.16 306.69 o 3 7 1 53.28 99.56 18.11 o 5 7 1 3961.14 5390.27 157.59 o 7 7 1 3.33 35.74 38.28 o 9 7 1 152.73 152.93 31.62 o 11 7 1 130.18 155.01 33.07 o 13 7 1 574.40 502.32 84.37 o 15 7 1 1.41 33.30 49.09 o -14 8 1 2.76 7.85 125.65 o -12 8 1 3970.89 3902.76 102.60 o -10 8 1 1520.91 1493.27 56.71 o -8 8 1 3754.85 4227.33 88.34 o -6 8 1 73.63 49.17 28.60 o -4 8 1 1185.87 1541.93 39.76 o -2 8 1 4464.52 4772.68 96.12 o 0 8 1 680.14 802.22 38.06 o 2 8 1 23410.73 22621.20 505.03 o 4 8 1 32.73 38.92 18.45 o 6 8 1 9531.57 10627.49 179.95 o 8 8 1 878.95 742.69 60.00 o 10 8 1 1344.76 1478.47 55.99 o 12 8 1 589.39 539.75 56.60 o 14 8 1 18.81 115.44 59.15 o -15 9 1 1588.50 1782.68 110.71 o -13 9 1 2599.74 2527.90 123.24 o -11 9 1 5097.42 5344.89 186.06 o -9 9 1 13949.70 13914.98 266.55 o -7 9 1 5204.88 5681.02 123.02 o -5 9 1 10950.70 9594.76 207.69 o -3 9 1 1889.52 1626.11 46.75 o -1 9 1 9189.79 9034.98 168.88 o 1 9 1 4058.16 3422.79 115.99 o 3 9 1 16296.66 15229.16 338.30 o 5 9 1 9606.82 10085.30 193.06 o 7 9 1 12319.14 11575.00 287.55 o 9 9 1 7729.67 7389.43 157.20 o 11 9 1 6692.72 6741.42 239.23 o 13 9 1 805.52 1051.20 111.16 o 15 9 1 1280.35 1346.37 98.40 o -14 10 1 436.42 408.98 96.66 o -12 10 1 3638.64 3761.16 118.91 o -10 10 1 402.31 374.30 45.29 o -8 10 1 2965.79 3519.51 140.15 o -6 10 1 5769.38 5361.93 116.19 o -4 10 1 17376.83 17250.00 312.40 o -2 10 1 25.56 21.46 26.70 o 0 10 1 5492.62 6186.07 181.12 o 2 10 1 19849.75 19558.47 401.43 o 4 10 1 1649.45 1783.73 79.74 o 6 10 1 6074.47 6207.86 133.28 o 8 10 1 207.46 181.31 36.25 o 10 10 1 5548.63 5891.31 134.95 o 12 10 1 2317.73 2239.93 89.27 o 14 10 1 273.09 357.33 53.41 o -13 11 1 78.24 103.56 46.40 o -11 11 1 395.48 376.98 47.38 o -9 11 1 2.94 -29.25 32.33 o -7 11 1 2333.73 2443.00 74.91 o -5 11 1 3.08 -22.35 26.70 o -3 11 1 1521.38 1633.08 74.95 o -1 11 1 426.97 449.50 46.04 o 1 11 1 3567.79 3541.30 173.98 o 3 11 1 107.14 108.84 41.80 o 5 11 1 1863.06 2125.56 68.09 o 7 11 1 794.76 662.10 40.58 o 9 11 1 53.88 51.89 32.33 o 11 11 1 66.41 69.40 41.80 o 13 11 1 4.82 34.20 42.87 o -12 12 1 792.89 738.93 62.60 o -10 12 1 729.39 677.79 54.47 o -8 12 1 2794.38 3160.41 87.09 o -6 12 1 2324.61 1946.54 73.18 o -4 12 1 2597.61 2717.59 107.28 o -2 12 1 2838.41 2855.52 107.61 o 0 12 1 778.63 822.31 58.09 o 2 12 1 8512.14 8029.79 232.38 o 4 12 1 2081.57 2049.02 92.08 o 6 12 1 2939.36 3329.39 100.94 o 8 12 1 3464.25 3354.26 90.51 o 10 12 1 188.41 195.01 41.08 o 12 12 1 7.49 37.45 84.57 o -13 13 1 1967.74 2007.58 90.26 o -11 13 1 2535.88 2518.66 116.19 o -9 13 1 1079.59 1220.75 125.65 o -7 13 1 7692.85 7472.28 188.48 o -5 13 1 3948.81 4090.73 116.20 o -3 13 1 12399.52 12970.18 355.35 o -1 13 1 2450.35 1876.66 101.49 o 1 13 1 18314.08 17814.77 469.87 o 3 13 1 1361.41 1212.75 71.52 o 5 13 1 13102.91 12260.84 280.71 o 7 13 1 2033.53 2178.98 80.42 o 9 13 1 3976.28 4170.91 241.64 o 11 13 1 499.52 668.41 68.09 o 13 13 1 5314.55 5128.06 239.23 o -12 14 1 53.90 118.40 58.09 o -10 14 1 423.07 484.97 101.49 o -8 14 1 3990.90 3916.24 118.91 o -6 14 1 639.65 696.77 52.68 o -4 14 1 815.82 843.07 62.60 o -2 14 1 416.38 345.08 55.58 o 0 14 1 2105.96 1926.20 92.27 o 2 14 1 21.48 10.56 46.04 o 4 14 1 432.52 318.44 54.36 o 6 14 1 478.01 588.57 106.32 o 8 14 1 5728.66 5480.35 205.40 o 10 14 1 662.54 625.55 69.99 o 12 14 1 946.78 904.94 80.25 o -11 15 1 279.53 141.48 171.57 o -9 15 1 166.75 113.06 56.31 o -7 15 1 971.20 759.82 57.08 o -5 15 1 4644.37 3964.73 120.64 o -3 15 1 1067.31 995.73 71.52 o -1 15 1 1107.72 1408.81 78.60 o 1 15 1 127.47 79.83 62.83 o 3 15 1 336.60 268.64 72.49 o 5 15 1 187.46 332.94 108.74 o 7 15 1 11.07 70.70 41.66 o 9 15 1 214.17 181.12 47.38 o 11 15 1 339.71 460.40 149.82 o -10 16 1 95.83 29.00 84.57 o -8 16 1 534.95 402.10 52.68 o -6 16 1 3.33 6.77 40.21 o -4 16 1 72.62 53.66 49.46 o -2 16 1 1.78 43.50 47.84 o 0 16 1 6269.46 6036.22 198.21 o 2 16 1 162.73 210.23 51.26 o 4 16 1 758.94 785.97 71.52 o 6 16 1 480.57 457.83 67.66 o 8 16 1 392.66 360.35 49.73 o 10 16 1 6.41 -41.08 58.09 o -9 17 1 718.47 759.40 80.25 o -7 17 1 4525.95 4349.56 260.97 o -5 17 1 472.26 597.78 113.57 o -3 17 1 3639.97 3247.61 140.15 o -1 17 1 2543.77 2584.12 166.73 o 1 17 1 2951.99 3088.56 142.57 o 3 17 1 2957.73 2745.91 169.15 o 5 17 1 3979.49 3701.02 120.64 o 7 17 1 2844.54 3080.93 108.98 o 9 17 1 2583.32 2662.32 129.86 o -8 18 1 138.82 171.69 64.66 o -6 18 1 2459.48 2689.26 118.40 o -4 18 1 10.88 19.33 52.89 o -2 18 1 78.64 70.08 51.26 o 0 18 1 2454.03 2211.91 111.02 o 2 18 1 80.13 99.07 51.26 o 4 18 1 910.43 698.08 75.18 o 6 18 1 2309.31 2319.61 96.51 o 8 18 1 1105.17 1143.82 101.49 o -5 19 1 28.90 94.88 70.08 o -3 19 1 373.81 445.00 84.57 o -1 19 1 360.20 402.64 70.08 o 1 19 1 46.70 49.35 56.31 o 3 19 1 1873.33 1807.30 104.19 o 5 19 1 140.05 114.90 49.03 o -4 20 1 258.79 253.10 63.15 o -2 20 1 64.90 49.75 57.79 o 0 20 1 295.94 235.37 65.24 o 2 20 1 192.90 241.64 86.99 o 4 20 1 29.06 28.17 59.73 o -16 0 2 388.17 386.63 101.49 o -14 0 2 1823.56 1748.04 102.35 o -12 0 2 3950.41 3262.92 133.14 o -10 0 2 50105.39 50967.77 1754.32 o -8 0 2 1178.57 1484.12 128.07 o -6 0 2 158984.23 143892.45 3512.64 o -4 0 2 1325.75 1478.43 65.24 o -2 0 2 55974.46 65902.68 2515.50 o 2 0 2 99864.58 105208.75 3404.74 o 4 0 2 456.82 614.26 27.71 o 6 0 2 79313.98 78549.58 3484.48 o 8 0 2 121.71 152.94 29.22 o 10 0 2 24242.91 23379.52 608.03 o 12 0 2 1450.31 1855.81 140.15 o 14 0 2 7624.02 7258.93 333.47 o 16 0 2 808.92 874.74 125.65 o -15 1 2 5185.14 5066.10 156.20 o -13 1 2 197.06 175.17 43.28 o -11 1 2 1594.55 1740.62 63.20 o -9 1 2 1426.05 1345.78 57.15 o -7 1 2 45053.10 44457.61 696.08 o -5 1 2 2420.90 3058.18 59.90 o -3 1 2 57765.36 63085.71 1215.20 o 3 1 2 10462.84 10584.20 183.33 o 5 1 2 1258.07 837.40 44.74 o 7 1 2 3147.62 2781.65 66.25 o 9 1 2 6312.32 5594.29 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