#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211236.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211236_Fobs loop_ _publ_author_name 'Sarala, G.' 'Thimme Gowda, N. R.' 'Rangappa, K. S.' 'Sridhar, M. A.' 'Shashidhara Prasad, J.' _publ_section_title ; 10-(2-Bromo-4,5-dimethoxybenzyl)-7-chloro-5-cyclopropyl-9-methyl-5,10-dihydro-4,5,6,10-tetraazadibenzo[a,d]cyclohepten-11-one ; _journal_coeditor_code WW2048 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5110 _journal_page_last o5111 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.260 _cell_angle_gamma 90.000 _cell_length_a 9.0680 _cell_length_b 16.7840 _cell_length_c 16.1960 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file ww2048Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iv5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4644.69 -0.64 0.43 o 2 0 0 425.25 685.29 26.07 o 3 0 0 13256.51 11852.80 427.18 o 4 0 0 227.69 515.00 32.56 o 6 0 0 2445.59 2446.03 130.33 o 7 0 0 695.53 795.17 39.64 o 8 0 0 87.63 94.23 35.24 o 9 0 0 146.80 169.79 32.43 o 10 0 0 245.39 320.10 46.11 o 2 1 0 1351.98 1290.41 33.47 o 3 1 0 1323.08 1285.72 34.50 o 4 1 0 350.46 337.63 13.73 o 5 1 0 62.18 71.54 10.57 o 6 1 0 129.57 173.06 13.89 o 7 1 0 30.88 57.15 17.21 o 8 1 0 13.70 -14.05 19.69 o 9 1 0 21.32 22.60 24.01 o 10 1 0 18.93 10.28 28.23 o 0 2 0 44747.43 97.08 42.42 o 1 2 0 446.82 292.00 7.95 o 2 2 0 5158.58 4730.35 122.36 o 3 2 0 1137.44 985.38 26.65 o 4 2 0 354.49 372.50 26.91 o 5 2 0 2583.69 2527.25 77.06 o 6 2 0 37.12 44.27 12.60 o 7 2 0 215.96 250.91 20.36 o 8 2 0 23.98 11.80 21.66 o 9 2 0 2.65 -9.76 23.16 o 10 2 0 24.80 38.59 25.75 o 1 3 0 1088.79 947.32 24.33 o 2 3 0 2680.21 2548.55 74.66 o 3 3 0 975.13 954.85 26.23 o 4 3 0 1552.13 1362.00 42.16 o 5 3 0 16.59 -0.31 19.87 o 6 3 0 29.08 37.68 12.41 o 7 3 0 128.70 144.16 20.78 o 8 3 0 20.27 -16.23 28.01 o 9 3 0 0.06 -20.42 24.83 o 10 3 0 36.38 33.07 44.98 o 0 4 0 6138.41 6103.43 308.83 o 1 4 0 14302.03 13971.90 361.42 o 2 4 0 4779.02 4278.23 131.01 o 3 4 0 2534.15 2429.61 79.41 o 4 4 0 1310.39 1098.26 32.03 o 5 4 0 506.89 469.22 17.04 o 6 4 0 1055.03 1039.94 36.33 o 7 4 0 356.14 371.25 20.69 o 8 4 0 264.91 308.18 21.79 o 9 4 0 128.06 130.10 56.93 o 10 4 0 83.54 80.04 37.19 o 1 5 0 1205.61 1385.66 37.25 o 2 5 0 714.69 857.34 26.16 o 3 5 0 1416.71 1482.99 54.98 o 4 5 0 1649.34 1564.40 48.58 o 5 5 0 487.96 491.36 27.59 o 6 5 0 14.91 29.62 12.60 o 7 5 0 140.97 131.77 17.51 o 8 5 0 142.57 152.23 21.66 o 9 5 0 2.12 -48.47 32.31 o 0 6 0 6137.12 5853.21 214.56 o 1 6 0 14839.88 14832.91 374.76 o 2 6 0 108.35 193.89 9.50 o 3 6 0 8434.67 8183.34 244.64 o 4 6 0 3886.02 3599.25 122.98 o 5 6 0 1007.94 939.59 27.60 o 6 6 0 5552.70 5841.91 173.88 o 7 6 0 10.14 -7.33 19.36 o 8 6 0 275.74 320.32 28.82 o 9 6 0 77.11 78.57 31.64 o 1 7 0 788.94 1007.48 30.36 o 2 7 0 647.57 660.10 17.79 o 3 7 0 497.33 561.68 16.78 o 4 7 0 192.53 202.61 10.45 o 5 7 0 28.50 23.37 18.42 o 6 7 0 425.41 430.56 24.61 o 7 7 0 68.98 61.64 17.01 o 8 7 0 2.90 6.14 19.31 o 9 7 0 34.16 8.29 23.07 o 0 8 0 389.29 479.45 33.24 o 1 8 0 1029.40 1098.71 37.70 o 2 8 0 2076.62 2302.53 129.13 o 3 8 0 19.73 7.88 4.96 o 4 8 0 1.41 8.22 6.95 o 5 8 0 131.38 119.52 11.41 o 6 8 0 434.86 426.97 18.04 o 7 8 0 288.85 293.15 18.37 o 8 8 0 43.66 44.18 22.96 o 9 8 0 4.36 27.01 27.40 o 1 9 0 1184.16 1205.68 50.88 o 2 9 0 460.89 496.24 14.26 o 3 9 0 215.23 235.56 9.15 o 4 9 0 398.91 371.96 20.91 o 5 9 0 0.64 0.43 9.71 o 6 9 0 122.76 113.91 14.06 o 7 9 0 172.18 145.19 17.64 o 8 9 0 11.69 32.11 26.54 o 9 9 0 17.47 38.71 28.98 o 0 10 0 2467.57 2169.06 118.65 o 1 10 0 3151.08 3160.95 184.40 o 2 10 0 3782.06 3824.44 163.32 o 3 10 0 2720.21 2855.76 74.47 o 4 10 0 1630.43 1573.46 87.89 o 5 10 0 1603.18 1693.39 53.04 o 6 10 0 826.43 829.26 48.78 o 7 10 0 107.26 105.27 14.27 o 8 10 0 92.63 95.65 17.03 o 1 11 0 295.93 347.08 36.97 o 2 11 0 374.58 384.85 12.75 o 3 11 0 69.42 67.57 13.27 o 4 11 0 141.84 142.43 27.56 o 5 11 0 207.31 186.37 12.59 o 6 11 0 78.54 67.69 13.48 o 7 11 0 66.92 65.79 19.49 o 8 11 0 0.64 -5.14 18.01 o 1 12 0 1218.12 1136.11 92.30 o 2 12 0 1651.07 1604.94 163.26 o 3 12 0 314.17 300.47 17.22 o 4 12 0 157.65 144.21 13.77 o 5 12 0 800.18 780.36 63.96 o 6 12 0 83.38 85.89 11.99 o 7 12 0 93.40 94.09 16.77 o 8 12 0 74.36 45.74 22.79 o 1 13 0 36.00 41.89 8.39 o 2 13 0 237.84 243.08 15.73 o 3 13 0 49.97 44.96 5.74 o 4 13 0 138.63 132.09 9.09 o 5 13 0 136.76 137.27 16.96 o 6 13 0 0.05 5.77 9.62 o 7 13 0 68.95 57.30 18.18 o 2 14 0 180.15 172.23 13.68 o 3 14 0 270.85 225.66 26.84 o 4 14 0 1123.66 901.72 31.66 o 5 14 0 264.41 239.03 12.22 o 6 14 0 11.11 15.79 35.15 o 7 14 0 24.86 14.15 10.46 o 1 15 0 114.67 132.77 11.47 o 2 15 0 4.57 2.14 8.03 o 3 15 0 0.91 -2.06 12.41 o 4 15 0 64.05 93.46 15.07 o 5 15 0 162.43 130.46 28.49 o 6 15 0 0.72 15.18 33.76 o 1 16 0 919.43 824.30 110.20 o 2 16 0 534.03 527.19 45.55 o 3 16 0 429.65 444.60 57.20 o 4 16 0 201.08 220.94 18.99 o 5 16 0 70.89 60.02 18.61 o 6 16 0 63.75 60.66 34.45 o 1 17 0 46.14 32.79 7.22 o 2 17 0 1.51 4.82 7.50 o 3 17 0 0.04 -19.38 12.92 o 4 17 0 0.43 -21.28 14.19 o 5 17 0 18.92 6.42 17.69 o 2 18 0 125.76 123.81 15.97 o 3 18 0 8.19 -8.27 11.86 o 4 18 0 17.38 27.65 11.28 o -10 1 1 3.48 30.37 28.77 o -9 1 1 52.90 48.36 30.76 o -8 1 1 0.26 -10.44 19.60 o -7 1 1 126.52 131.91 17.91 o -6 1 1 60.41 51.87 12.03 o -5 1 1 131.78 149.72 18.69 o -4 1 1 996.53 992.38 27.71 o -3 1 1 133.79 149.12 8.49 o -2 1 1 164.63 214.38 6.97 o 1 1 1 4652.33 2455.42 146.44 o 2 1 1 12629.68 12168.28 449.55 o 3 1 1 0.49 7.09 8.41 o 4 1 1 113.85 109.05 20.98 o 5 1 1 89.12 112.21 11.28 o 6 1 1 356.79 328.27 17.26 o 7 1 1 359.27 363.87 24.25 o 8 1 1 281.03 294.02 23.13 o 9 1 1 13.24 2.66 29.56 o 10 1 1 0.91 29.89 27.93 o -10 2 1 215.60 294.91 34.79 o -9 2 1 244.03 297.32 28.39 o -8 2 1 143.06 150.42 21.53 o -7 2 1 132.17 179.08 23.52 o -6 2 1 2315.54 2280.73 60.81 o -5 2 1 5592.97 4516.32 162.77 o -4 2 1 11990.49 11364.08 286.91 o -3 2 1 16590.75 14651.13 369.64 o -2 2 1 11537.92 10577.25 269.36 o -1 2 1 6756.13 5600.69 187.45 o 0 2 1 81.10 27.63 12.70 o 1 2 1 21590.29 19430.82 493.60 o 2 2 1 11432.83 10038.40 295.23 o 3 2 1 2922.06 2309.31 68.27 o 4 2 1 6640.63 6255.36 158.84 o 5 2 1 592.81 499.84 18.06 o 6 2 1 1925.82 2008.57 54.75 o 7 2 1 2985.10 3262.46 101.41 o 8 2 1 1177.19 1322.96 43.66 o 9 2 1 75.43 175.41 37.98 o 10 2 1 17.66 24.10 27.55 o -10 3 1 7.61 41.53 33.85 o -9 3 1 29.17 52.21 23.39 o -8 3 1 52.28 85.62 24.12 o -7 3 1 85.92 91.65 18.58 o -6 3 1 4.16 16.93 12.74 o -5 3 1 190.40 199.13 11.53 o -4 3 1 19.36 13.08 7.77 o -3 3 1 587.83 545.90 15.72 o -2 3 1 4053.20 4144.25 122.32 o -1 3 1 27.08 26.33 1.90 o 0 3 1 760.05 787.33 28.47 o 1 3 1 3920.46 3868.11 123.22 o 2 3 1 897.82 937.69 24.72 o 3 3 1 229.57 241.62 9.81 o 4 3 1 99.26 76.97 9.07 o 5 3 1 421.96 419.52 17.32 o 6 3 1 56.08 62.54 18.07 o 7 3 1 24.41 -8.74 16.54 o 8 3 1 0.02 9.15 19.50 o 9 3 1 0.77 -0.74 28.04 o 10 3 1 0.49 10.99 27.16 o -10 4 1 93.11 123.05 42.54 o -9 4 1 158.55 219.66 31.02 o -8 4 1 153.33 196.75 43.47 o -7 4 1 1201.83 1218.31 52.13 o -6 4 1 1583.55 1564.44 43.41 o -5 4 1 1653.21 1549.20 41.97 o -4 4 1 1447.64 1311.49 35.24 o -3 4 1 2464.36 2060.24 53.08 o -2 4 1 397.48 355.35 10.15 o -1 4 1 197.45 239.95 7.62 o 0 4 1 14988.91 16267.02 580.95 o 1 4 1 18735.08 16487.98 590.20 o 2 4 1 11940.14 11217.64 288.04 o 3 4 1 4517.69 3961.96 119.88 o 4 4 1 765.62 715.12 21.59 o 5 4 1 2275.02 2186.81 58.10 o 6 4 1 1612.58 1676.45 54.12 o 7 4 1 824.07 948.56 33.38 o 8 4 1 149.29 206.98 24.15 o 9 4 1 128.11 136.50 23.26 o -10 5 1 1.36 -32.96 49.66 o -9 5 1 27.61 44.25 28.74 o -8 5 1 4.18 13.48 16.94 o -7 5 1 198.83 152.13 15.69 o -6 5 1 147.10 138.08 15.54 o -5 5 1 41.83 44.35 10.28 o -4 5 1 421.05 459.62 18.20 o -3 5 1 1864.85 1763.20 46.08 o -2 5 1 82.44 83.37 4.30 o -1 5 1 57.29 65.57 3.01 o 0 5 1 743.39 794.26 24.36 o 1 5 1 71.40 58.19 3.62 o 2 5 1 4709.06 4731.11 120.47 o 3 5 1 490.01 491.99 15.62 o 4 5 1 266.44 261.98 11.89 o 5 5 1 315.47 312.42 14.63 o 6 5 1 8.75 29.88 17.45 o 7 5 1 47.50 16.61 16.01 o 8 5 1 22.38 6.37 21.60 o 9 5 1 0.41 -13.82 29.19 o -9 6 1 66.43 101.39 28.71 o -8 6 1 171.12 198.20 21.64 o -7 6 1 80.59 70.79 19.61 o -6 6 1 186.63 221.40 25.23 o -5 6 1 1483.94 1435.74 39.23 o -4 6 1 773.22 707.71 20.93 o -3 6 1 1764.23 1673.39 43.20 o -2 6 1 2536.31 2442.69 72.19 o -1 6 1 374.92 375.24 16.44 o 0 6 1 971.91 926.79 36.56 o 1 6 1 7194.44 6882.41 245.33 o 2 6 1 189.69 284.55 11.73 o 3 6 1 146.93 164.99 8.76 o 4 6 1 387.17 359.21 21.98 o 5 6 1 39.04 42.02 12.56 o 6 6 1 727.45 696.46 24.59 o 7 6 1 101.74 113.56 21.39 o 8 6 1 68.38 98.07 22.26 o 9 6 1 18.57 13.41 24.21 o -9 7 1 19.68 56.79 31.75 o -8 7 1 0.21 -5.58 19.21 o -7 7 1 114.45 123.53 17.14 o -6 7 1 2257.05 2337.36 87.59 o -5 7 1 325.63 311.06 13.69 o -4 7 1 678.65 701.20 20.55 o -3 7 1 196.22 148.52 8.25 o -2 7 1 2635.44 2918.94 78.03 o -1 7 1 761.67 890.06 33.04 o 0 7 1 6313.30 6965.30 214.26 o 1 7 1 217.85 193.23 12.89 o 2 7 1 3235.47 3432.88 90.65 o 3 7 1 412.30 368.07 14.99 o 4 7 1 7.40 13.37 9.35 o 5 7 1 10.42 6.41 11.58 o 6 7 1 21.73 27.71 13.02 o 7 7 1 54.29 73.40 16.51 o 8 7 1 84.27 124.75 25.16 o 9 7 1 3.20 -1.09 22.31 o -9 8 1 279.82 311.12 29.52 o -8 8 1 324.67 362.27 20.88 o -7 8 1 1546.20 1715.07 48.42 o -6 8 1 625.77 607.20 37.81 o -5 8 1 1264.29 1240.33 48.48 o -4 8 1 2857.66 2688.70 81.17 o -3 8 1 1192.69 1012.39 32.88 o -2 8 1 9118.70 9566.01 443.06 o -1 8 1 4173.44 4424.14 251.25 o 0 8 1 1321.01 1193.25 37.41 o 1 8 1 10252.08 10845.46 390.33 o 2 8 1 6814.94 6622.19 170.44 o 3 8 1 1890.51 1639.84 49.78 o 4 8 1 3709.22 3589.41 106.43 o 5 8 1 921.98 947.17 42.06 o 6 8 1 70.05 59.68 12.74 o 7 8 1 1344.27 1517.61 45.34 o 8 8 1 348.47 367.86 33.14 o 9 8 1 135.64 173.65 25.43 o -9 9 1 2.71 4.50 24.67 o -8 9 1 97.87 85.62 18.97 o -7 9 1 139.25 116.44 19.59 o -6 9 1 0.61 25.08 16.87 o -5 9 1 90.02 75.63 10.18 o -4 9 1 0.79 -2.77 9.84 o -3 9 1 5.67 2.07 5.13 o -2 9 1 2152.42 2325.21 131.80 o -1 9 1 50.94 62.49 6.50 o 0 9 1 33.52 51.47 4.61 o 1 9 1 56.62 60.01 3.85 o 2 9 1 169.57 180.72 7.01 o 3 9 1 100.49 110.19 7.33 o 4 9 1 7.85 11.53 7.57 o 5 9 1 19.95 2.14 10.93 o 6 9 1 24.36 39.08 17.94 o 7 9 1 0.05 -21.41 14.94 o 8 9 1 28.68 33.92 21.26 o 9 9 1 13.55 26.08 30.03 o -9 10 1 27.46 61.82 25.79 o -8 10 1 0.81 5.14 17.81 o -7 10 1 13.93 30.14 16.23 o -6 10 1 108.82 104.38 19.94 o -5 10 1 349.83 331.12 15.89 o -4 10 1 605.31 593.23 34.43 o -3 10 1 232.24 239.86 12.07 o -2 10 1 186.87 194.00 11.61 o -1 10 1 266.27 251.26 18.11 o 0 10 1 839.56 816.78 60.80 o 1 10 1 427.50 377.86 25.35 o 2 10 1 35.46 30.98 4.77 o 3 10 1 96.79 86.27 8.40 o 4 10 1 2.11 10.82 9.22 o 5 10 1 14.18 10.44 9.53 o 6 10 1 182.20 199.91 17.93 o 7 10 1 90.40 76.54 15.50 o 8 10 1 23.13 37.26 18.87 o -8 11 1 17.66 15.63 15.86 o -7 11 1 1.12 -0.16 12.81 o -6 11 1 299.13 283.94 14.20 o -5 11 1 9.77 7.82 13.80 o -4 11 1 173.24 166.62 9.83 o -3 11 1 241.44 251.73 25.74 o -2 11 1 575.73 658.24 64.78 o -1 11 1 120.80 144.29 16.44 o 0 11 1 159.02 179.55 12.86 o 1 11 1 36.43 45.10 4.57 o 2 11 1 83.13 92.39 6.69 o 3 11 1 159.77 133.34 7.56 o 4 11 1 31.53 25.74 7.43 o 5 11 1 37.48 40.50 15.59 o 6 11 1 89.53 96.80 14.13 o 7 11 1 15.49 17.41 17.60 o 8 11 1 5.83 16.93 20.84 o -8 12 1 75.66 38.18 27.87 o -7 12 1 325.95 321.67 18.37 o -6 12 1 98.15 97.24 29.59 o -5 12 1 742.92 727.04 71.77 o -4 12 1 240.27 261.99 10.00 o -3 12 1 115.84 101.63 12.37 o -2 12 1 1906.90 1922.18 120.39 o -1 12 1 1055.04 1069.75 104.32 o 0 12 1 2247.87 2394.44 205.33 o 1 12 1 755.04 704.60 26.43 o 2 12 1 837.53 932.15 36.30 o 3 12 1 777.55 728.09 29.24 o 4 12 1 642.26 692.49 23.64 o 5 12 1 1370.58 1325.13 43.76 o 6 12 1 228.53 213.21 14.22 o 7 12 1 73.65 56.50 14.61 o 8 12 1 25.24 45.59 24.50 o -7 13 1 5.00 0.00 11.08 o -6 13 1 4.04 1.26 11.30 o -5 13 1 376.16 332.02 31.00 o -4 13 1 36.45 31.68 9.02 o -3 13 1 158.34 174.05 27.55 o -2 13 1 36.67 30.60 10.73 o -1 13 1 6.38 13.44 6.78 o 0 13 1 139.80 167.21 25.10 o 1 13 1 60.64 64.87 6.09 o 2 13 1 7.19 6.90 6.09 o 3 13 1 5.51 13.01 11.14 o 4 13 1 120.30 93.76 16.62 o 5 13 1 53.58 57.41 9.92 o 6 13 1 18.35 -8.57 12.69 o 7 13 1 52.73 43.21 13.48 o -7 14 1 116.80 81.07 14.51 o -6 14 1 36.78 42.83 8.38 o -5 14 1 458.04 473.35 26.13 o -4 14 1 1076.13 1202.00 69.02 o -3 14 1 472.38 507.37 23.53 o 1 14 1 1412.08 1333.86 113.47 o 3 14 1 463.77 387.20 18.43 o 4 14 1 751.34 790.12 56.08 o 5 14 1 238.84 237.68 18.50 o 6 14 1 311.22 262.49 53.09 o 7 14 1 328.25 256.14 21.41 o -6 15 1 40.14 37.45 29.92 o -5 15 1 62.78 61.28 16.72 o -4 15 1 33.67 26.18 14.31 o -3 15 1 27.84 19.04 16.10 o -2 15 1 274.14 257.63 29.52 o -1 15 1 8.23 10.84 6.33 o 0 15 1 58.25 42.06 5.32 o 1 15 1 184.59 177.66 10.29 o 2 15 1 66.86 70.36 10.21 o 3 15 1 1.78 20.98 10.53 o 4 15 1 46.22 43.33 8.02 o 5 15 1 0.79 4.26 7.31 o 6 15 1 18.66 14.42 15.82 o -6 16 1 49.52 44.25 20.49 o -5 16 1 13.38 26.03 16.42 o -4 16 1 89.51 98.37 25.16 o -3 16 1 87.74 76.72 14.24 o -2 16 1 93.51 88.08 9.91 o -1 16 1 2.09 -0.27 11.15 o 1 16 1 289.78 301.52 19.31 o 2 16 1 86.50 70.96 10.98 o 3 16 1 31.48 44.19 11.06 o 4 16 1 1.33 1.16 13.88 o 5 16 1 5.14 26.90 17.69 o -5 17 1 0.60 5.34 18.63 o -4 17 1 0.74 -18.14 13.33 o -3 17 1 0.00 11.15 14.36 o -2 17 1 2.37 1.30 10.11 o -1 17 1 1.84 4.32 7.20 o 1 17 1 173.69 126.11 5.92 o 2 17 1 65.47 51.29 9.21 o 3 17 1 2.03 -9.34 12.34 o 4 17 1 0.36 7.84 15.22 o 5 17 1 38.47 18.75 16.91 o -4 18 1 116.64 151.06 32.66 o -3 18 1 236.44 200.88 23.22 o -2 18 1 394.71 305.60 30.93 o -1 18 1 386.09 324.30 20.04 o 3 18 1 78.60 66.89 15.07 o 4 18 1 220.46 206.48 16.53 o -3 19 1 17.48 149.11 21.09 o -10 0 2 13.36 78.20 54.13 o -8 0 2 1506.89 1650.70 67.82 o -7 0 2 645.84 605.01 46.82 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