#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:22:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181033 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/13/2211323.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211323_Fobs loop_ _publ_author_name 'Fan, Le-Qing' 'Chen, Ling' 'Wu, Li-Ming' _publ_section_title ; catena-Poly[tris(2,2'-bipyridine)nickel(II) [hexa-\m-iodo-diplumbate(II)]] ; _journal_coeditor_code CF2073 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3373 _journal_page_last m3374 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.409 _cell_angle_gamma 90.000 _cell_length_a 17.2337 _cell_length_b 14.7012 _cell_length_c 16.4273 _exptl_crystal_F_000 3024.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file cf2073Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1030.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 11436.45 11190.27 310.17 o 4 0 0 4122.22 5402.96 308.62 o 5 0 0 2309.74 2037.98 162.33 o 6 0 0 45179.83 47052.06 845.12 o 7 0 0 36360.57 36092.36 726.40 o 8 0 0 29498.06 33729.59 685.43 o 9 0 0 14854.79 15855.98 571.92 o 10 0 0 16926.70 20104.00 680.35 o 11 0 0 37029.88 42185.89 1182.60 o 12 0 0 137949.66 152484.00 4388.67 o 13 0 0 145690.22 154607.67 6139.18 o 14 0 0 97843.17 118697.22 4115.93 o 15 0 0 37956.06 37291.47 1656.29 o 16 0 0 4413.87 5268.61 540.90 o 17 0 0 1407.78 2618.32 686.81 o 18 0 0 2529.64 2194.33 815.75 o 19 0 0 12039.04 15687.63 1837.29 o 20 0 0 955.13 1063.69 748.80 o 21 0 0 11951.09 12903.18 1872.00 o 3 1 0 106754.69 100681.43 1309.85 o 4 1 0 266.33 991.66 202.86 o 5 1 0 24441.24 22606.84 328.77 o 6 1 0 31451.63 31152.08 481.59 o 7 1 0 128628.69 133512.98 2746.35 o 8 1 0 25753.73 28945.64 532.37 o 9 1 0 11477.37 13348.68 347.49 o 10 1 0 7450.37 8425.82 300.99 o 11 1 0 21789.87 23996.80 620.03 o 12 1 0 80899.14 86138.11 1463.02 o 13 1 0 56324.82 59525.09 1323.44 o 14 1 0 96681.62 103392.19 3608.88 o 15 1 0 9702.63 9634.56 674.25 o 16 1 0 3108.29 3133.62 449.50 o 17 1 0 292.91 721.78 675.66 o 18 1 0 1814.53 987.51 1102.13 o 19 1 0 228.48 -62.19 474.94 o 20 1 0 15993.53 20094.81 2009.61 o 21 1 0 203.24 712.62 690.53 o 1 2 0 312.59 491.22 62.64 o 2 2 0 243498.44 239635.97 1261.61 o 3 2 0 1649.58 2782.65 110.90 o 4 2 0 96101.08 99556.70 1356.52 o 5 2 0 37791.92 38742.15 653.90 o 6 2 0 661691.13 668937.75 3583.72 o 7 2 0 134706.02 139313.45 1016.38 o 8 2 0 310004.56 317200.78 3867.32 o 9 2 0 31065.80 29723.07 542.90 o 10 2 0 28299.71 27309.57 529.70 o 11 2 0 18637.18 19146.14 469.65 o 12 2 0 50204.93 55197.00 1375.01 o 13 2 0 72606.62 75343.40 1491.53 o 14 2 0 34959.73 34541.72 1230.53 o 15 2 0 21917.22 21606.19 761.21 o 16 2 0 2367.97 2665.73 479.97 o 17 2 0 1704.46 1974.86 444.96 o 18 2 0 1712.97 1749.75 1217.42 o 19 2 0 13623.16 15591.92 1434.07 o 20 2 0 2317.48 3808.63 1157.91 o 21 2 0 11813.03 11747.47 1234.23 o 1 3 0 28743.86 28042.16 472.27 o 2 3 0 6476.54 6485.28 189.30 o 3 3 0 3135.43 3133.30 151.25 o 4 3 0 16213.93 15063.08 288.46 o 5 3 0 404744.66 416864.50 4185.35 o 6 3 0 147675.67 140725.50 1412.56 o 7 3 0 662578.63 672433.44 6929.30 o 8 3 0 142344.53 140167.91 2316.21 o 9 3 0 95035.64 100805.06 1172.09 o 10 3 0 6473.81 6056.76 375.33 o 11 3 0 606.77 664.21 264.04 o 12 3 0 17756.05 17113.37 492.51 o 13 3 0 4561.04 4596.94 361.26 o 14 3 0 35948.88 40495.66 992.17 o 15 3 0 164.35 558.94 237.64 o 16 3 0 1717.85 1649.68 491.11 o 17 3 0 191.12 326.49 356.10 o 18 3 0 4402.36 5757.57 944.75 o 19 3 0 809.98 -142.68 603.68 o 20 3 0 17026.30 19804.07 1433.28 o 21 3 0 97.22 139.10 585.58 o 0 4 0 121827.48 103451.77 1673.32 o 1 4 0 62.47 255.36 80.80 o 2 4 0 27461.87 26810.27 788.44 o 3 4 0 606.19 331.00 114.68 o 4 4 0 190418.41 187394.05 2600.74 o 5 4 0 55768.77 60431.05 856.74 o 6 4 0 1062935.25 1069912.00 7193.10 o 7 4 0 148316.14 152255.95 1369.26 o 8 4 0 357343.59 358250.53 4751.23 o 9 4 0 15420.52 12008.79 427.54 o 10 4 0 4473.51 4492.06 337.97 o 11 4 0 1002.23 773.63 236.79 o 12 4 0 12511.03 12439.91 385.84 o 13 4 0 31549.79 33676.88 1526.79 o 14 4 0 18704.64 17448.12 573.96 o 15 4 0 22607.66 24532.23 938.72 o 16 4 0 4975.04 4891.01 675.32 o 17 4 0 6473.83 6041.33 601.54 o 18 4 0 2949.98 3584.93 757.39 o 19 4 0 18040.48 17925.81 2791.89 o 20 4 0 2146.01 2060.58 685.86 o 21 4 0 7550.38 7593.67 1314.47 o 1 5 0 273196.31 224185.69 1413.70 o 2 5 0 731.72 785.87 127.14 o 3 5 0 38760.34 34662.87 594.87 o 4 5 0 12877.26 12175.54 328.66 o 5 5 0 119143.83 119064.03 974.26 o 6 5 0 89908.30 89467.25 1012.98 o 7 5 0 173514.31 176769.30 4209.76 o 8 5 0 50423.04 51668.63 847.24 o 9 5 0 3070.71 3210.22 292.09 o 10 5 0 903.18 1363.77 264.12 o 11 5 0 921.09 1283.90 463.32 o 12 5 0 11928.02 11297.42 560.15 o 13 5 0 17239.30 19280.28 647.15 o 14 5 0 43184.40 47811.41 1114.39 o 15 5 0 5366.80 5672.09 460.81 o 16 5 0 8857.94 10011.40 626.30 o 17 5 0 43.16 588.25 253.88 o 18 5 0 6354.94 9580.91 967.56 o 19 5 0 109.60 725.76 448.52 o 20 5 0 12223.23 12548.53 1343.88 o 21 5 0 41.11 886.98 528.48 o 0 6 0 962661.00 800954.56 4571.90 o 1 6 0 4501.48 3948.71 191.89 o 2 6 0 349488.31 308520.59 4823.82 o 3 6 0 918.15 835.96 178.30 o 4 6 0 59975.02 56913.32 815.37 o 5 6 0 5047.26 4897.81 242.16 o 6 6 0 101825.38 97988.36 1013.07 o 7 6 0 18478.11 18133.55 520.58 o 8 6 0 27145.37 26015.76 987.04 o 9 6 0 1691.79 2085.01 296.17 o 10 6 0 1985.00 2673.29 324.24 o 11 6 0 6674.68 6473.43 458.79 o 12 6 0 38752.11 42082.23 1751.47 o 13 6 0 57184.32 59784.11 1334.45 o 14 6 0 50095.32 56871.99 1642.67 o 15 6 0 27448.87 27691.16 1171.95 o 16 6 0 9810.42 10330.80 646.90 o 17 6 0 3595.36 3472.21 550.15 o 18 6 0 970.98 1077.30 341.43 o 19 6 0 8999.65 10923.88 1167.83 o 20 6 0 228.92 708.47 299.35 o 1 7 0 582068.06 521138.53 3128.45 o 2 7 0 334.78 537.73 215.49 o 3 7 0 7434.12 5482.75 347.93 o 4 7 0 203.30 330.98 127.42 o 5 7 0 1125.96 1476.57 313.50 o 6 7 0 9704.40 8815.23 326.91 o 7 7 0 14452.15 14092.37 399.66 o 8 7 0 14715.83 13231.38 568.67 o 9 7 0 572.43 865.90 299.11 o 10 7 0 4067.67 4996.88 396.17 o 11 7 0 9480.99 8742.50 494.23 o 12 7 0 38737.87 41046.39 1641.96 o 13 7 0 41094.02 39268.41 1169.70 o 14 7 0 43281.98 44450.83 1747.89 o 15 7 0 3844.63 4031.81 512.83 o 16 7 0 1426.69 872.95 242.50 o 17 7 0 444.48 172.31 275.38 o 18 7 0 484.73 826.26 453.08 o 19 7 0 78.87 107.57 243.48 o 20 7 0 5563.81 5662.91 773.88 o 0 8 0 410571.34 384080.75 3159.28 o 1 8 0 3073.24 3366.11 223.42 o 2 8 0 108371.22 97026.68 1558.51 o 3 8 0 769.99 1500.19 222.40 o 4 8 0 6380.39 4759.41 579.44 o 5 8 0 3266.42 2545.05 233.16 o 6 8 0 70842.70 68771.81 1391.84 o 7 8 0 15520.98 14062.63 688.21 o 8 8 0 75944.05 75937.81 2260.15 o 9 8 0 11082.45 10838.06 625.85 o 10 8 0 32007.07 30885.82 912.64 o 11 8 0 24729.67 24488.65 929.84 o 12 8 0 33954.83 33257.35 1059.95 o 13 8 0 44153.06 45012.03 1374.04 o 14 8 0 16955.46 14979.94 936.16 o 15 8 0 5748.60 4432.41 474.41 o 16 8 0 644.76 392.24 294.42 o 17 8 0 754.00 1154.06 340.53 o 18 8 0 38.88 841.61 351.10 o 19 8 0 2066.18 1563.41 650.72 o 1 9 0 36645.49 34041.46 598.74 o 2 9 0 30.47 180.36 111.45 o 3 9 0 867.62 896.15 136.60 o 4 9 0 390.39 344.04 142.00 o 5 9 0 14212.07 13644.04 666.18 o 6 9 0 15766.37 14762.70 521.01 o 7 9 0 94502.51 92491.78 1577.18 o 8 9 0 17890.35 17159.30 953.24 o 9 9 0 25862.40 23237.87 1325.17 o 10 9 0 6585.72 6916.58 437.87 o 11 9 0 4392.27 3521.68 371.11 o 12 9 0 18105.25 17696.12 1050.76 o 13 9 0 3758.72 3038.26 737.95 o 14 9 0 9412.48 9284.90 591.32 o 15 9 0 198.26 695.35 285.06 o 16 9 0 323.32 579.21 302.48 o 17 9 0 837.59 546.86 250.30 o 18 9 0 125.41 196.87 303.58 o 19 9 0 41.04 -145.80 350.36 o 0 10 0 67795.95 67283.59 1119.59 o 1 10 0 638.30 520.98 185.93 o 2 10 0 10629.99 10297.53 564.96 o 3 10 0 3854.99 3057.42 245.61 o 4 10 0 22398.98 19708.74 624.65 o 5 10 0 9547.54 9066.86 347.73 o 6 10 0 135968.02 126332.76 3334.91 o 7 10 0 23965.73 23211.34 1173.14 o 8 10 0 80474.64 75876.48 2568.70 o 9 10 0 6389.46 6234.30 376.69 o 10 10 0 9298.84 8326.37 460.02 o 11 10 0 1450.89 1364.13 365.62 o 12 10 0 3764.11 3889.28 446.28 o 13 10 0 9161.45 9859.28 608.88 o 14 10 0 2305.69 1637.42 366.93 o 15 10 0 2033.68 2043.34 411.15 o 16 10 0 176.81 -136.09 442.78 o 17 10 0 192.20 357.93 269.43 o 18 10 0 628.63 470.73 324.63 o 1 11 0 10415.01 10242.49 366.99 o 2 11 0 414.59 250.88 96.46 o 3 11 0 1464.31 2106.75 479.95 o 4 11 0 3706.71 3150.47 271.48 o 5 11 0 30479.15 28263.94 829.59 o 6 11 0 14990.54 15076.81 604.70 o 7 11 0 53781.17 49516.31 1732.59 o 8 11 0 1211.80 1043.53 214.84 o 9 11 0 423.74 427.53 195.92 o 10 11 0 762.12 771.56 250.26 o 11 11 0 2636.80 2693.33 486.00 o 12 11 0 657.29 387.66 253.74 o 13 11 0 243.59 453.19 212.37 o 14 11 0 5590.78 4491.38 524.53 o 15 11 0 725.48 728.39 270.42 o 16 11 0 1743.94 1554.23 316.46 o 17 11 0 59.93 358.93 358.33 o 0 12 0 69276.64 73595.68 2366.69 o 1 12 0 19.41 379.64 95.48 o 2 12 0 29822.02 29625.14 827.51 o 3 12 0 143.88 292.17 125.04 o 4 12 0 15400.00 14603.12 469.80 o 5 12 0 4341.48 4357.69 317.80 o 6 12 0 29674.57 27760.30 1298.24 o 7 12 0 11032.28 10892.55 418.56 o 8 12 0 7603.83 6225.68 437.85 o 9 12 0 76.14 363.18 215.60 o 10 12 0 334.39 497.29 221.20 o 11 12 0 316.32 564.13 413.00 o 12 12 0 1618.55 793.39 331.19 o 13 12 0 3392.31 2793.29 319.17 o 14 12 0 5931.12 5330.46 599.63 o 15 12 0 4324.79 4476.08 562.21 o 16 12 0 2079.00 1696.34 503.57 o 17 12 0 2155.45 2732.46 530.34 o 1 13 0 20393.56 19285.08 594.41 o 2 13 0 593.53 466.43 134.96 o 3 13 0 2577.52 2857.19 332.78 o 4 13 0 13.83 119.27 175.61 o 5 13 0 3904.34 4314.30 316.10 o 6 13 0 1925.52 2113.63 229.71 o 7 13 0 2192.48 1799.59 316.51 o 8 13 0 991.59 495.83 235.93 o 9 13 0 1200.16 1001.97 212.22 o 10 13 0 81.03 318.11 142.22 o 11 13 0 544.16 730.25 205.76 o 12 13 0 2102.28 1405.48 406.08 o 13 13 0 2544.44 1679.51 344.89 o 14 13 0 5707.45 5440.86 601.90 o 15 13 0 1876.11 1130.72 366.04 o 16 13 0 969.48 908.16 451.51 o 0 14 0 25216.91 26238.35 1293.56 o 1 14 0 34.03 362.47 205.95 o 2 14 0 5691.71 6354.98 469.42 o 3 14 0 586.54 269.88 162.32 o 4 14 0 813.77 1252.94 277.21 o 5 14 0 296.98 496.18 151.83 o 6 14 0 9309.41 10069.82 656.75 o 7 14 0 2219.94 1676.71 291.71 o 8 14 0 5339.50 5669.35 431.24 o 9 14 0 1235.10 1191.81 223.31 o 10 14 0 1319.65 1149.58 222.01 o 11 14 0 1729.96 1088.34 298.97 o 12 14 0 3805.31 2859.60 445.34 o 13 14 0 2964.15 1967.25 377.95 o 14 14 0 2859.38 2230.10 446.99 o 1 15 0 4935.08 5303.05 369.27 o 2 15 0 495.57 769.88 197.27 o 3 15 0 107.39 446.50 203.66 o 4 15 0 10.19 275.09 173.37 o 5 15 0 64.39 407.50 142.10 o 6 15 0 1029.34 998.19 278.79 o 7 15 0 2145.25 2131.43 394.39 o 8 15 0 1407.72 1008.49 292.13 o 9 15 0 975.71 1002.55 234.08 o 10 15 0 848.32 984.22 351.61 o 11 15 0 498.00 409.38 254.81 o 12 15 0 2586.72 2078.85 372.02 o 13 15 0 719.15 874.31 266.23 o 0 16 0 5340.39 5362.18 472.76 o 1 16 0 15.13 371.00 138.01 o 2 16 0 805.67 826.26 185.31 o 3 16 0 32.24 474.28 210.25 o 4 16 0 121.66 419.88 190.63 o 5 16 0 225.55 614.88 249.45 o 6 16 0 3559.25 2523.51 366.65 o 7 16 0 574.94 719.96 214.22 o 8 16 0 5302.03 5240.65 465.85 o 9 16 0 180.70 733.73 282.06 o 10 16 0 1831.66 1234.57 304.95 o 11 16 0 447.87 1041.32 332.75 o 1 17 0 2226.72 3323.63 441.90 o 2 17 0 423.27 304.35 157.83 o 3 17 0 34.43 358.51 153.58 o 4 17 0 472.00 515.32 256.25 o 5 17 0 14.14 369.11 204.28 o 6 17 0 209.74 262.29 149.86 o 7 17 0 537.67 642.90 205.28 o 8 17 0 3.58 408.70 240.96 o 9 17 0 42.32 480.04 240.14 o 0 18 0 3073.87 4958.95 1120.72 o 1 18 0 10.54 259.10 291.32 o 2 18 0 932.33 1383.05 304.18 o 3 18 0 209.08 256.20 130.51 o 4 18 0 175.85 37.70 235.23 o 5 18 0 435.55 593.46 236.30 o 6 18 0 1102.65 754.10 249.58 o 7 18 0 23.84 94.25 268.34 o 1 19 0 188.21 494.34 220.60 o 2 19 0 28.64 366.96 267.78 o -22 1 1 12.30 431.09 659.54 o -21 1 1 131.29 314.71 301.96 o -20 1 1 1061.75 1210.09 599.68 o -19 1 1 1085.04 1183.59 497.18 o -18 1 1 5116.00 5086.59 806.97 o -17 1 1 962.64 406.35 280.00 o -16 1 1 1516.62 1445.52 395.46 o -15 1 1 5.53 153.26 232.98 o -14 1 1 6585.48 7304.79 393.13 o -13 1 1 1453.15 1447.88 257.28 o -12 1 1 15566.59 15912.84 495.59 o -11 1 1 254.72 254.11 166.55 o -10 1 1 12021.30 12327.13 392.70 o -9 1 1 111.85 109.59 132.35 o -8 1 1 4964.02 4975.25 200.06 o -7 1 1 1280.76 1284.65 144.53 o -6 1 1 42600.34 39090.99 602.06 o -5 1 1 679.58 713.51 117.22 o -4 1 1 60090.23 56611.30 1233.26 o -3 1 1 9557.74 7748.36 359.67 o 2 1 1 44.01 50.55 27.74 o 3 1 1 3426.32 2658.14 96.86 o 4 1 1 602.71 1493.04 97.58 o 5 1 1 5.81 1256.53 102.45 o 6 1 1 6412.09 6525.25 171.50 o 7 1 1 10451.29 9848.91 249.86 o 8 1 1 6635.68 7243.75 235.82 o 9 1 1 26657.13 25253.93 474.23 o 10 1 1 2.06 371.43 128.84 o 11 1 1 693.79 1094.77 152.61 o 12 1 1 847.29 1203.10 208.33 o 13 1 1 9985.85 10233.62 395.42 o 14 1 1 1257.67 1846.23 315.29 o 15 1 1 10174.12 10529.56 633.04 o 16 1 1 349.69 369.37 467.87 o 17 1 1 2028.86 2462.20 730.27 o 18 1 1 228.34 725.70 475.04 o 19 1 1 240.22 922.82 283.90 o 20 1 1 15.46 19.83 512.19 o 21 1 1 730.68 1063.00 468.03 o -21 2 1 341.54 661.59 545.80 o -20 2 1 1286.57 1628.17 638.91 o -19 2 1 3175.01 3212.53 870.60 o -18 2 1 3555.27 4621.33 1543.47 o -17 2 1 2982.42 3505.57 622.50 o -16 2 1 34.76 136.72 191.47 o -15 2 1 945.87 1433.22 237.76 o -14 2 1 5252.06 5428.25 394.90 o -13 2 1 12415.34 12237.55 451.25 o -12 2 1 1713.25 1352.54 219.74 o -11 2 1 26121.40 24793.86 574.41 o -10 2 1 173.17 475.53 137.27 o -9 2 1 39.98 1182.35 200.22 o -8 2 1 525.99 947.36 135.55 o -7 2 1 30376.73 27458.86 530.06 o -6 2 1 2968.22 2947.44 245.41 o -5 2 1 54943.55 52383.30 810.34 o -4 2 1 2363.83 2515.57 186.46 o -3 2 1 4445.97 4838.89 163.76 o -2 2 1 465.32 916.56 79.47 o -1 2 1 144.87 244.66 46.06 o 0 2 1 3077.16 2532.30 69.65 o 1 2 1 2213.41 1774.92 88.68 o 2 2 1 1312.35 2258.79 118.51 o 3 2 1 46954.54 40468.68 650.99 o 4 2 1 13940.38 14900.52 337.04 o 5 2 1 185.08 1812.67 270.61 o 6 2 1 628.44 3570.21 369.67 o 7 2 1 484.41 430.68 86.16 o 8 2 1 10372.82 8983.46 253.51 o 9 2 1 2793.76 3270.66 214.50 o 10 2 1 7738.85 6480.52 275.52 o 11 2 1 839.01 622.86 146.17 o 12 2 1 1345.39 2064.71 220.60 o 13 2 1 625.80 769.66 166.09 o 14 2 1 20356.07 20492.02 660.38 o 15 2 1 28.32 281.56 254.14 o 16 2 1 10958.10 10837.56 861.38 o 17 2 1 10.15 528.65 418.69 o 18 2 1 393.40 297.19 457.46 o 19 2 1 4.58 -3.60 752.52 o 20 2 1 536.12 789.46 513.25 o 21 2 1 200.35 324.12 406.32 o -21 3 1 42.90 509.87 307.99 o -20 3 1 1001.67 727.89 383.37 o -19 3 1 384.46 959.80 441.78 o -18 3 1 1960.52 1412.84 358.43 o -17 3 1 152.14 392.65 354.95 o -16 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