#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/13/2211339.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211339_Fobs loop_ _publ_author_name 'Fang, Hua' 'Dai, Xuya' _publ_section_title ; Tris(1,10-phenanthroline)nickel(II) di-\m-iodo-bis(diiodomercurate) N,N-dimethylformamide solvate monohydrate ; _journal_coeditor_code CI2216 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3565 _journal_page_last m3566 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.846 _cell_angle_gamma 90.000 _cell_length_a 12.6312 _cell_length_b 18.7561 _cell_length_c 20.1970 _exptl_crystal_F_000 3352.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ci2216Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 050514dm in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1145.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 62086.04 49378.03 1735.86 o 2 0 0 9050.81 10345.02 335.37 o 3 0 0 146297.70 155503.78 4259.67 o 4 0 0 167869.67 172801.69 4447.96 o 5 0 0 115134.73 119733.13 3171.25 o 6 0 0 117498.12 127616.41 3403.80 o 7 0 0 800.72 843.59 159.59 o 8 0 0 75.12 37.34 121.35 o 9 0 0 15887.15 15944.15 680.13 o 10 0 0 78046.09 78164.88 2315.55 o 11 0 0 434.22 442.05 225.56 o 12 0 0 545.96 940.97 211.58 o 13 0 0 504.67 381.55 196.18 o 14 0 0 380.72 192.24 193.36 o 15 0 0 367.24 224.31 323.80 o 16 0 0 40.56 148.66 282.98 o 1 1 0 98805.65 99828.25 2156.37 o 2 1 0 23951.75 26564.64 385.32 o 3 1 0 458.09 725.38 58.32 o 4 1 0 110876.27 111909.08 1841.90 o 5 1 0 798474.88 761673.44 12061.53 o 6 1 0 3979.17 4586.02 154.51 o 7 1 0 4797.37 5166.93 234.71 o 8 1 0 7576.71 6808.30 344.02 o 9 1 0 2036.84 1927.36 229.56 o 10 1 0 12758.10 12455.24 390.03 o 11 1 0 5030.85 4960.27 277.14 o 12 1 0 787.90 838.44 161.92 o 13 1 0 84.01 16.34 118.00 o 14 1 0 676.67 477.74 171.00 o 15 1 0 717.75 464.41 204.70 o 16 1 0 330.32 370.07 285.80 o 0 2 0 506196.88 409955.19 8432.32 o 1 2 0 19502.91 20259.19 443.73 o 2 2 0 6646.88 7840.05 140.68 o 3 2 0 1156.28 1523.44 79.52 o 4 2 0 320.47 407.38 49.72 o 5 2 0 26620.08 26575.20 473.37 o 6 2 0 6472.58 6135.47 179.53 o 7 2 0 6934.14 6801.49 197.84 o 8 2 0 485.77 229.90 97.69 o 9 2 0 818.84 813.61 148.92 o 10 2 0 57.35 147.35 112.66 o 11 2 0 144.24 -33.95 123.43 o 12 2 0 4503.78 3927.14 267.13 o 13 2 0 441.14 456.15 157.19 o 14 2 0 30.23 77.03 150.11 o 15 2 0 111.60 197.26 173.36 o 16 2 0 2445.74 2558.28 353.07 o 1 3 0 4804.53 5598.60 166.18 o 2 3 0 39394.36 43152.02 1049.30 o 3 3 0 844.37 995.72 54.83 o 4 3 0 3297.42 3680.31 181.89 o 5 3 0 6095.45 6243.51 175.09 o 6 3 0 79.73 186.38 139.64 o 7 3 0 9466.43 9179.83 387.56 o 8 3 0 75.89 533.72 278.67 o 9 3 0 2177.03 2371.52 193.76 o 10 3 0 1964.66 1749.69 180.80 o 11 3 0 7592.34 7218.19 345.76 o 12 3 0 1952.52 2165.63 235.41 o 13 3 0 538.40 585.02 209.22 o 14 3 0 3262.85 3791.39 326.34 o 15 3 0 483.03 643.42 194.74 o 16 3 0 86.88 196.38 290.99 o 0 4 0 80247.11 85448.33 1826.85 o 1 4 0 1228.11 1240.98 73.40 o 2 4 0 199.49 462.03 80.65 o 3 4 0 1231.96 1560.62 89.22 o 4 4 0 15119.42 16328.98 289.44 o 5 4 0 10300.14 10012.91 214.29 o 6 4 0 38597.32 39535.73 688.85 o 7 4 0 253.18 383.13 79.71 o 8 4 0 4147.47 4553.74 221.69 o 9 4 0 13055.71 12999.83 388.41 o 10 4 0 277.56 263.49 135.19 o 11 4 0 3905.95 3912.62 318.84 o 12 4 0 3.07 -78.80 134.60 o 13 4 0 177.50 198.34 182.75 o 14 4 0 150.99 251.61 179.67 o 15 4 0 224.90 185.52 202.33 o 16 4 0 112.76 -196.58 284.32 o 1 5 0 47983.60 50207.53 858.93 o 2 5 0 2619.74 2708.82 135.11 o 3 5 0 5707.94 6292.90 176.20 o 4 5 0 15324.39 15791.14 313.41 o 5 5 0 7535.38 8681.57 293.11 o 6 5 0 52482.49 51807.71 797.21 o 7 5 0 61.93 93.79 63.12 o 8 5 0 345.70 367.79 100.92 o 9 5 0 917.47 797.90 148.98 o 10 5 0 8172.65 9101.07 391.50 o 11 5 0 10837.51 10500.05 440.02 o 12 5 0 2676.42 2617.65 260.31 o 13 5 0 732.39 645.36 192.85 o 14 5 0 277.64 161.91 341.44 o 15 5 0 1736.28 1884.60 279.28 o 0 6 0 157238.47 166500.64 5159.48 o 1 6 0 1132.30 1142.96 64.92 o 2 6 0 403.10 260.48 68.55 o 3 6 0 845.81 839.08 79.33 o 4 6 0 7538.77 7301.20 210.03 o 5 6 0 47304.38 47503.16 790.85 o 6 6 0 11017.89 12355.63 348.13 o 7 6 0 9203.70 9068.65 281.66 o 8 6 0 403.16 236.31 112.85 o 9 6 0 320.75 430.31 129.42 o 10 6 0 5524.68 5071.44 314.23 o 11 6 0 7816.70 8193.21 403.28 o 12 6 0 4585.11 4975.59 341.19 o 13 6 0 47.91 185.56 169.53 o 14 6 0 170.30 99.95 187.96 o 15 6 0 370.07 118.76 210.07 o 1 7 0 106751.17 108778.00 1812.29 o 2 7 0 917.69 813.32 174.16 o 3 7 0 886.62 852.35 83.91 o 4 7 0 33370.21 34443.06 737.82 o 5 7 0 225508.70 230499.25 3407.13 o 6 7 0 9791.69 10209.82 267.00 o 7 7 0 141.36 234.40 98.86 o 8 7 0 395.36 677.42 116.18 o 9 7 0 1538.78 1913.16 204.83 o 10 7 0 3759.60 3909.63 287.09 o 11 7 0 8186.99 7961.20 663.02 o 12 7 0 1305.69 1492.69 338.24 o 13 7 0 259.02 246.75 174.59 o 14 7 0 1474.60 1392.22 254.15 o 15 7 0 152.16 23.68 280.09 o 0 8 0 1022934.81 907919.81 23095.72 o 1 8 0 60280.81 59472.28 1042.65 o 2 8 0 384.56 379.08 71.02 o 3 8 0 826.56 734.67 92.34 o 4 8 0 102530.84 106215.93 1800.59 o 5 8 0 18353.22 17508.38 464.17 o 6 8 0 32894.09 33596.94 683.49 o 7 8 0 346.63 333.43 86.11 o 8 8 0 1496.93 1509.61 153.17 o 9 8 0 2723.03 2969.12 286.23 o 10 8 0 27240.23 26841.29 743.00 o 11 8 0 587.32 814.13 246.68 o 12 8 0 1062.80 886.53 216.65 o 13 8 0 37.06 53.78 170.93 o 14 8 0 857.88 687.63 222.07 o 15 8 0 27.44 -292.36 194.91 o 1 9 0 68787.81 69495.84 1213.33 o 2 9 0 15389.50 15062.57 402.44 o 3 9 0 2275.16 2201.71 295.44 o 4 9 0 48464.20 47302.69 887.07 o 5 9 0 264934.00 263313.59 4277.00 o 6 9 0 33363.66 34659.80 710.63 o 7 9 0 5299.78 5046.42 280.97 o 8 9 0 167.42 479.21 155.29 o 9 9 0 5540.93 5231.62 465.42 o 10 9 0 95.99 122.54 155.99 o 11 9 0 929.68 1189.94 215.56 o 12 9 0 1328.41 1547.79 242.36 o 13 9 0 117.05 136.44 256.20 o 14 9 0 102.14 112.62 203.64 o 15 9 0 2355.71 2003.57 444.82 o 0 10 0 184613.31 179386.14 3802.48 o 1 10 0 44607.92 44415.81 823.97 o 2 10 0 17975.92 17201.86 453.25 o 3 10 0 5290.34 5347.22 343.86 o 4 10 0 120.42 203.68 78.20 o 5 10 0 1424.86 1508.22 159.88 o 6 10 0 2478.19 2978.13 728.95 o 7 10 0 5038.38 5436.25 247.38 o 8 10 0 61.96 159.81 117.42 o 9 10 0 64.32 174.72 167.16 o 10 10 0 12605.02 11656.98 530.56 o 11 10 0 9283.62 8352.45 485.88 o 12 10 0 1327.80 1522.46 275.64 o 13 10 0 409.63 489.33 222.64 o 14 10 0 39.78 216.08 239.26 o 1 11 0 101099.12 100642.91 1729.64 o 2 11 0 3153.14 3563.89 199.33 o 3 11 0 863.76 825.50 158.49 o 4 11 0 10903.15 9720.74 599.53 o 5 11 0 3274.07 3460.05 200.82 o 6 11 0 32555.67 32104.06 1143.67 o 7 11 0 5506.89 5547.70 257.23 o 8 11 0 354.81 454.94 145.11 o 9 11 0 266.22 737.52 380.31 o 10 11 0 5404.74 5603.94 402.51 o 11 11 0 3162.61 3318.04 351.38 o 12 11 0 244.38 477.44 227.85 o 13 11 0 84.51 358.37 260.83 o 14 11 0 1833.50 2032.00 350.30 o 0 12 0 21136.35 20286.47 652.94 o 1 12 0 180.92 179.69 84.22 o 2 12 0 395.92 321.40 81.57 o 3 12 0 577.80 468.58 111.96 o 4 12 0 23267.81 22628.84 596.37 o 5 12 0 25039.68 24270.86 753.49 o 6 12 0 48565.26 47012.58 945.24 o 7 12 0 559.49 423.23 119.07 o 8 12 0 6378.38 6304.69 330.31 o 9 12 0 13849.56 14013.45 581.59 o 10 12 0 733.32 612.28 218.35 o 11 12 0 6001.62 5730.57 494.19 o 12 12 0 77.54 208.96 269.91 o 13 12 0 910.52 916.04 279.68 o 14 12 0 42.37 -414.61 276.41 o 1 13 0 54340.34 53425.14 1139.63 o 2 13 0 91.96 58.28 72.51 o 3 13 0 23198.84 21988.50 1212.23 o 4 13 0 19971.78 18457.49 533.44 o 5 13 0 303.80 262.17 95.88 o 6 13 0 16411.08 15858.46 710.42 o 7 13 0 860.33 743.60 145.37 o 8 13 0 468.01 723.26 165.83 o 9 13 0 1200.16 1184.19 412.25 o 10 13 0 4572.65 5256.39 404.35 o 11 13 0 4.16 453.69 234.51 o 12 13 0 116.56 322.60 256.13 o 13 13 0 1339.14 1336.13 304.62 o 0 14 0 494.82 613.21 177.86 o 1 14 0 83.95 380.23 123.50 o 2 14 0 6034.53 5820.18 335.78 o 3 14 0 1518.47 1742.83 186.07 o 4 14 0 1178.10 1358.39 170.12 o 5 14 0 5058.54 4705.07 279.86 o 6 14 0 808.30 970.66 147.36 o 7 14 0 715.18 663.88 147.12 o 8 14 0 4683.05 4649.59 361.22 o 9 14 0 126.23 203.75 182.29 o 10 14 0 2765.23 2959.81 373.90 o 11 14 0 1889.88 1786.94 302.14 o 12 14 0 1391.10 1507.02 410.48 o 13 14 0 442.95 539.08 320.39 o 1 15 0 13404.76 12618.50 1247.20 o 2 15 0 997.69 799.95 292.20 o 3 15 0 1069.86 502.04 208.30 o 4 15 0 587.78 224.87 166.98 o 5 15 0 103.89 81.24 105.33 o 6 15 0 1996.98 1424.80 289.25 o 7 15 0 401.54 455.78 137.63 o 8 15 0 2598.27 2819.50 262.60 o 9 15 0 281.40 239.18 198.67 o 10 15 0 730.25 619.72 225.48 o 11 15 0 1349.15 1778.36 549.73 o 12 15 0 116.76 344.57 292.23 o 0 16 0 9086.33 9696.42 1187.25 o 1 16 0 1439.30 1408.10 199.36 o 2 16 0 94.71 44.23 119.46 o 3 16 0 1223.19 401.77 273.73 o 4 16 0 7011.02 6991.20 395.47 o 5 16 0 1120.95 1134.50 216.28 o 6 16 0 337.21 211.20 118.12 o 7 16 0 246.25 109.82 134.98 o 8 16 0 304.68 687.25 194.53 o 9 16 0 1238.41 999.89 301.90 o 10 16 0 1629.37 1764.91 350.40 o 11 16 0 650.39 836.43 456.33 o 12 16 0 18.04 324.07 312.32 o 1 17 0 1380.34 1427.90 324.60 o 2 17 0 2976.38 2802.99 294.44 o 3 17 0 202.69 117.15 112.07 o 4 17 0 16.45 91.11 118.53 o 5 17 0 20489.64 20518.70 849.03 o 6 17 0 6389.65 6369.38 540.76 o 7 17 0 143.32 84.03 171.54 o 8 17 0 0.86 -69.99 172.07 o 9 17 0 3899.37 4135.08 583.28 o 10 17 0 2109.58 2032.31 536.86 o 11 17 0 281.59 354.41 304.44 o 0 18 0 15413.81 13578.94 753.29 o 1 18 0 5689.64 5634.36 390.02 o 2 18 0 1020.25 1444.33 253.17 o 3 18 0 1148.49 568.22 327.69 o 4 18 0 383.54 233.64 141.29 o 5 18 0 4213.06 4024.47 357.88 o 6 18 0 337.49 419.90 201.26 o 7 18 0 4171.46 4117.74 385.26 o 8 18 0 27.91 -282.67 217.31 o 9 18 0 27.60 -204.68 287.45 o 10 18 0 5902.99 5939.27 579.92 o 1 19 0 5480.32 5461.16 403.96 o 2 19 0 663.71 275.13 149.65 o 3 19 0 953.94 954.39 240.09 o 4 19 0 12.53 -245.91 163.94 o 5 19 0 2117.51 2883.73 327.12 o 6 19 0 8895.53 8873.63 786.46 o 7 19 0 617.72 655.49 274.54 o 8 19 0 610.05 300.93 251.33 o 9 19 0 25.98 236.00 359.03 o 10 19 0 1215.41 903.72 439.56 o 0 20 0 34.31 -120.79 351.20 o 1 20 0 143.43 377.86 200.87 o 2 20 0 130.73 269.21 188.49 o 3 20 0 25.18 276.94 226.56 o 4 20 0 181.36 307.58 370.77 o 5 20 0 3917.59 4991.30 704.77 o 6 20 0 4059.68 4585.93 584.93 o 7 20 0 164.09 331.31 261.32 o 8 20 0 325.36 241.71 278.80 o 9 20 0 85.96 -29.08 359.03 o 1 21 0 2035.02 2450.10 1084.91 o 2 21 0 67.66 321.55 296.04 o 3 21 0 2460.14 2158.66 500.51 o 4 21 0 1232.30 886.22 258.19 o 5 21 0 370.57 709.95 258.42 o 6 21 0 1205.68 940.11 275.29 o 7 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