#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211377.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211377_Fobs loop_ _publ_author_name 'Deng, Zhao-Peng' 'Gao, Shan' 'Huo, Li-Hua' 'Zhao, Hui' _publ_section_title ; Diaquabis(4-formylbenzoato-\kO)zinc(II) monohydrate ; _journal_coeditor_code EZ2050 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3524 _journal_page_last m3526 _journal_volume 62 _journal_year 2006 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.687 _cell_angle_gamma 90.000 _cell_length_a 7.9390 _cell_length_b 5.7474 _cell_length_c 18.7363 _exptl_crystal_F_000 428.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file ez2050Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' d in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 786.03 870.77 12.03 o 3 0 0 15.19 12.30 1.48 o 4 0 0 1624.53 1588.97 37.78 o 5 0 0 1977.21 2011.41 40.85 o 6 0 0 2368.48 2462.11 55.66 o 7 0 0 293.38 309.38 8.43 o 8 0 0 4.31 5.99 2.80 o 9 0 0 18.13 19.39 3.93 o 10 0 0 79.49 77.87 5.40 o 0 1 0 424.26 403.30 6.11 o 1 1 0 1663.70 1766.59 16.36 o 2 1 0 22056.05 22170.14 578.04 o 3 1 0 1888.37 1952.79 21.99 o 4 1 0 1155.88 1145.28 14.45 o 5 1 0 664.15 664.14 9.31 o 6 1 0 198.39 196.13 4.59 o 7 1 0 213.70 221.20 3.80 o 8 1 0 284.69 292.73 4.91 o 9 1 0 68.30 74.83 3.86 o 10 1 0 4.97 6.04 2.14 o 0 2 0 217.84 234.76 4.00 o 1 2 0 586.60 580.59 9.72 o 2 2 0 6814.19 7148.30 110.73 o 3 2 0 3738.27 4072.59 58.53 o 4 2 0 3031.63 3056.08 41.97 o 5 2 0 86.93 82.62 1.84 o 6 2 0 4.31 4.51 1.11 o 7 2 0 179.78 173.81 3.54 o 8 2 0 174.08 176.76 3.92 o 9 2 0 30.61 33.56 2.27 o 0 3 0 5618.93 6235.52 215.46 o 1 3 0 1612.29 1680.21 49.81 o 2 3 0 28.02 47.90 1.13 o 3 3 0 226.20 212.18 2.86 o 4 3 0 344.03 332.83 4.02 o 5 3 0 505.40 482.53 6.04 o 6 3 0 660.97 634.76 8.55 o 7 3 0 15.68 17.03 1.44 o 8 3 0 4.42 6.85 1.61 o 9 3 0 32.30 30.85 2.31 o 0 4 0 58.26 49.40 2.13 o 1 4 0 827.62 834.33 22.04 o 2 4 0 202.08 205.38 2.74 o 3 4 0 64.81 57.95 1.52 o 4 4 0 7.00 4.83 0.79 o 5 4 0 85.89 89.10 2.00 o 6 4 0 260.62 251.38 4.15 o 7 4 0 72.19 67.33 2.56 o 8 4 0 65.28 54.23 2.68 o 0 5 0 11.68 11.24 1.49 o 1 5 0 120.10 121.97 2.19 o 2 5 0 1.45 1.19 0.77 o 3 5 0 96.63 97.66 2.18 o 4 5 0 205.99 192.33 3.35 o 5 5 0 11.97 9.41 1.55 o 6 5 0 2.70 2.50 1.05 o 7 5 0 33.03 33.65 2.62 o 0 6 0 126.87 120.23 2.78 o 1 6 0 1.35 1.51 0.68 o 2 6 0 37.13 37.44 1.50 o 3 6 0 49.69 47.10 1.86 o 4 6 0 3.41 4.09 1.04 o 5 6 0 24.12 26.05 2.19 o 6 6 0 0.80 0.67 1.04 o 0 7 0 36.38 26.04 2.31 o 1 7 0 0.27 0.04 0.69 o 2 7 0 13.74 13.94 1.61 o 3 7 0 10.52 9.48 2.02 o -10 1 1 22.32 20.15 2.88 o -9 1 1 3.12 3.07 1.69 o -8 1 1 1.67 2.45 1.68 o -7 1 1 3.22 2.24 1.31 o -6 1 1 15.61 29.62 3.79 o -5 1 1 29.93 35.83 1.44 o -4 1 1 2442.32 2656.05 39.43 o -3 1 1 17.63 21.65 1.09 o -2 1 1 7203.36 7436.41 126.16 o -1 1 1 25.53 33.28 0.67 o 0 1 1 790.85 939.96 15.29 o 1 1 1 23.00 23.98 0.51 o 2 1 1 8056.32 8637.99 141.75 o 3 1 1 1.96 2.01 0.53 o 4 1 1 274.02 319.82 3.44 o 5 1 1 13.96 20.14 1.33 o 6 1 1 249.25 243.97 3.47 o 7 1 1 5.91 5.66 1.46 o 8 1 1 19.82 26.64 4.11 o 9 1 1 0.09 0.53 1.75 o 10 1 1 4.48 7.64 2.32 o -9 2 1 0.16 0.80 1.77 o -8 2 1 1.35 3.03 1.69 o -7 2 1 1.03 1.30 1.29 o -6 2 1 666.68 640.91 8.40 o -5 2 1 35.98 34.58 1.22 o -4 2 1 994.65 1118.13 13.31 o -3 2 1 2.63 1.94 0.57 o -2 2 1 314.35 326.49 3.83 o -1 2 1 73.43 74.45 1.87 o 0 2 1 176.38 197.86 2.47 o 1 2 1 64.62 59.60 1.08 o 2 2 1 663.56 832.28 7.23 o 3 2 1 104.58 128.58 2.79 o 4 2 1 3311.38 3486.10 50.35 o 5 2 1 55.84 56.65 1.39 o 6 2 1 20.34 23.84 1.46 o 7 2 1 1.52 2.13 1.23 o 8 2 1 79.12 83.69 3.00 o 9 2 1 24.52 23.98 2.84 o -9 3 1 20.27 18.03 2.18 o -8 3 1 449.65 405.09 6.78 o -7 3 1 11.29 10.95 1.83 o -6 3 1 27.66 22.84 1.79 o -5 3 1 6.10 5.78 1.03 o -4 3 1 55.75 57.77 1.37 o -3 3 1 88.81 75.80 1.46 o -2 3 1 107.58 83.42 1.60 o -1 3 1 281.94 287.21 6.95 o 0 3 1 113.65 90.42 1.98 o 1 3 1 21.46 33.19 1.16 o 2 3 1 246.29 263.77 2.94 o 3 3 1 139.46 131.48 2.13 o 4 3 1 223.76 207.97 3.35 o 5 3 1 1.59 0.51 0.84 o 6 3 1 766.44 732.29 9.32 o 7 3 1 99.87 96.46 2.71 o 8 3 1 6.27 8.10 1.58 o 9 3 1 8.48 7.92 1.91 o -8 4 1 0.92 2.75 1.51 o -7 4 1 49.65 50.26 1.97 o -6 4 1 152.73 145.47 3.87 o -5 4 1 0.91 0.06 0.84 o -4 4 1 175.16 193.62 4.42 o -3 4 1 200.56 195.13 2.65 o -2 4 1 118.51 105.68 1.78 o -1 4 1 11.27 9.74 0.77 o 0 4 1 6.17 3.27 0.70 o 1 4 1 175.98 170.47 5.05 o 2 4 1 1157.32 1207.10 15.36 o 3 4 1 64.05 70.49 1.55 o 4 4 1 156.86 144.74 3.02 o 5 4 1 108.53 104.10 2.30 o 6 4 1 42.20 44.24 1.99 o 7 4 1 42.10 43.84 2.66 o 8 4 1 181.45 167.64 3.95 o -7 5 1 11.37 14.27 1.85 o -6 5 1 132.06 132.65 3.17 o -5 5 1 245.61 229.41 5.18 o -4 5 1 226.37 217.44 3.34 o -3 5 1 2.12 1.56 0.82 o -2 5 1 31.46 38.24 1.31 o -1 5 1 141.14 137.43 2.01 o 0 5 1 432.64 407.15 7.76 o 1 5 1 109.91 111.94 2.19 o 2 5 1 130.63 126.53 2.45 o 3 5 1 166.95 162.45 3.57 o 4 5 1 226.33 230.03 3.93 o 5 5 1 124.60 123.34 2.99 o 6 5 1 48.25 49.49 1.72 o 7 5 1 18.16 19.17 1.63 o -6 6 1 4.05 4.76 1.87 o -5 6 1 59.33 59.98 2.25 o -4 6 1 80.64 83.56 1.91 o -3 6 1 102.19 99.68 2.34 o -2 6 1 215.90 206.22 2.96 o -1 6 1 19.57 18.61 2.43 o 0 6 1 183.96 181.08 2.50 o 1 6 1 193.30 186.20 3.61 o 2 6 1 56.35 54.24 1.25 o 3 6 1 91.71 91.72 2.62 o 4 6 1 54.05 55.99 1.88 o 5 6 1 66.73 59.06 2.73 o 6 6 1 80.23 76.01 5.35 o -3 7 1 82.60 79.36 2.63 o -2 7 1 190.20 187.23 3.21 o -1 7 1 115.96 104.96 2.12 o 0 7 1 55.31 51.08 3.16 o 1 7 1 26.48 26.33 1.46 o 2 7 1 38.79 35.51 5.35 o 3 7 1 71.86 66.84 5.07 o -10 0 2 30.58 39.33 8.25 o -9 0 2 64.35 69.97 4.57 o -8 0 2 380.43 403.77 11.49 o -7 0 2 170.05 168.91 4.99 o -6 0 2 945.27 897.92 21.07 o -5 0 2 1646.96 1634.21 32.14 o -4 0 2 3468.96 3395.33 72.10 o -3 0 2 104.05 124.59 2.23 o -2 0 2 23489.70 23450.28 982.88 o -1 0 2 8874.39 8589.00 237.04 o 1 0 2 2635.24 2653.89 38.95 o 2 0 2 375.65 358.17 14.52 o 3 0 2 111.88 93.34 2.08 o 4 0 2 1315.12 1282.60 21.16 o 5 0 2 1710.59 1766.39 34.88 o 6 0 2 473.14 435.10 9.68 o 7 0 2 28.75 34.12 2.59 o 8 0 2 78.90 82.29 4.00 o 9 0 2 16.66 17.37 3.63 o 10 0 2 49.57 55.67 4.01 o -10 1 2 76.11 79.50 5.10 o -9 1 2 73.67 77.00 2.96 o -8 1 2 105.87 110.97 3.41 o -7 1 2 272.64 271.16 5.01 o -6 1 2 1046.15 1055.68 14.71 o -5 1 2 317.22 317.16 4.45 o -4 1 2 5026.80 5305.22 93.84 o -3 1 2 2312.51 2379.46 31.68 o -2 1 2 3180.50 3168.86 45.18 o -1 1 2 686.61 728.25 6.60 o 0 1 2 11849.62 11820.89 301.23 o 1 1 2 2954.48 3057.98 37.13 o 2 1 2 513.84 453.34 3.67 o 3 1 2 1536.62 1528.00 16.14 o 4 1 2 736.72 666.26 6.88 o 5 1 2 263.11 246.66 3.09 o 6 1 2 381.41 378.90 5.35 o 7 1 2 164.90 168.97 3.53 o 8 1 2 105.88 104.01 3.32 o 9 1 2 11.19 10.09 1.90 o 10 1 2 52.88 60.24 3.91 o -9 2 2 60.36 65.97 2.76 o -8 2 2 130.46 139.56 3.60 o -7 2 2 206.73 206.03 4.10 o -6 2 2 642.45 623.99 8.69 o -5 2 2 264.60 268.90 3.67 o -4 2 2 1436.78 1459.11 16.26 o -3 2 2 2520.98 2712.51 34.75 o -2 2 2 2513.53 2633.20 29.33 o -1 2 2 510.95 494.57 6.48 o 0 2 2 956.91 929.82 10.89 o 1 2 2 825.31 813.29 20.77 o 2 2 2 6160.95 6366.86 94.61 o 3 2 2 2404.02 2470.55 27.37 o 4 2 2 73.64 65.94 1.83 o 5 2 2 21.47 18.57 1.06 o 6 2 2 194.90 191.68 3.59 o 7 2 2 106.74 112.06 3.46 o 8 2 2 229.04 230.48 5.89 o 9 2 2 78.44 81.36 3.11 o -9 3 2 5.05 5.29 1.91 o -8 3 2 73.41 69.75 2.96 o -7 3 2 127.29 123.18 2.72 o -6 3 2 119.30 117.91 2.32 o -5 3 2 580.36 561.91 7.09 o -4 3 2 158.21 153.73 2.20 o -3 3 2 264.18 274.43 4.71 o -2 3 2 1337.91 1520.40 16.58 o -1 3 2 1720.52 1835.52 23.09 o 0 3 2 687.56 609.21 12.90 o 1 3 2 627.01 594.44 9.64 o 2 3 2 659.03 653.38 8.03 o 3 3 2 157.47 151.53 1.85 o 4 3 2 1079.52 1139.75 12.13 o 5 3 2 322.16 325.01 5.57 o 6 3 2 69.85 66.16 2.12 o 7 3 2 57.51 58.67 2.84 o 8 3 2 61.88 61.76 3.28 o 9 3 2 32.01 30.40 2.61 o -8 4 2 8.35 8.03 1.49 o -7 4 2 14.47 16.14 1.63 o -6 4 2 2.69 4.06 1.20 o -5 4 2 232.03 225.85 4.80 o -4 4 2 107.02 100.67 2.32 o -3 4 2 269.51 264.23 3.43 o -2 4 2 5.38 6.05 0.86 o -1 4 2 539.60 556.26 6.31 o 0 4 2 1126.70 1184.85 25.89 o 1 4 2 453.83 442.04 6.20 o 2 4 2 19.44 16.57 1.30 o 3 4 2 6.01 7.61 1.24 o 4 4 2 428.07 414.52 8.01 o 5 4 2 277.37 275.96 3.97 o 6 4 2 256.26 254.13 4.00 o 7 4 2 72.32 67.28 2.83 o 8 4 2 0.92 -0.14 1.11 o -7 5 2 12.57 12.47 1.85 o -6 5 2 15.95 11.45 1.32 o -5 5 2 8.60 8.03 1.31 o -4 5 2 16.32 9.44 1.30 o -3 5 2 249.22 244.42 3.54 o -2 5 2 58.64 48.70 1.31 o -1 5 2 95.58 98.89 1.96 o 0 5 2 0.83 1.22 0.55 o 1 5 2 44.57 44.91 1.04 o 2 5 2 490.22 476.42 6.37 o 3 5 2 197.03 189.55 2.46 o 4 5 2 3.72 4.22 1.07 o 5 5 2 19.03 17.47 1.32 o 6 5 2 60.66 54.53 2.03 o 7 5 2 46.66 39.63 1.81 o -6 6 2 3.50 4.44 1.47 o -5 6 2 4.80 3.70 1.56 o -4 6 2 3.79 3.15 1.21 o -3 6 2 11.67 11.46 1.51 o -2 6 2 22.64 21.05 1.46 o -1 6 2 13.68 12.07 0.96 o 0 6 2 27.61 23.79 1.12 o 1 6 2 42.31 37.17 1.22 o 2 6 2 12.25 11.34 1.04 o 3 6 2 59.11 55.68 2.05 o 4 6 2 75.83 64.35 2.00 o 5 6 2 12.20 6.72 3.40 o -3 7 2 7.07 8.08 1.04 o -2 7 2 0.50 0.23 0.71 o -1 7 2 4.49 3.92 1.01 o 0 7 2 4.25 4.20 1.14 o 1 7 2 14.73 10.88 2.14 o 2 7 2 6.37 3.58 2.27 o 3 7 2 2.13 0.71 1.66 o -10 1 3 0.21 0.76 1.70 o -9 1 3 0.25 -1.27 1.56 o -8 1 3 4.21 7.30 2.31 o -7 1 3 0.25 0.26 1.27 o -6 1 3 125.67 148.79 3.55 o -5 1 3 151.55 161.02 4.34 o -4 1 3 89.79 124.53 8.06 o -3 1 3 2.68 6.18 1.10 o -2 1 3 0.64 3.36 1.19 o -1 1 3 392.96 434.17 4.21 o 0 1 3 4179.61 4285.03 145.91 o 1 1 3 671.47 676.02 11.96 o 2 1 3 869.72 891.09 10.40 o 3 1 3 195.97 207.79 2.24 o 4 1 3 42.59 45.17 1.19 o 5 1 3 51.04 47.85 1.41 o 6 1 3 205.04 197.88 3.27 o 7 1 3 63.49 68.19 2.46 o 8 1 3 0.04 -0.29 1.14 o 9 1 3 0.84 0.03 1.37 o -9 2 3 0.12 0.40 1.66 o -8 2 3 22.72 27.68 2.32 o -7 2 3 22.20 28.28 1.70 o -6 2 3 21.37 27.72 3.40 o -5 2 3 40.39 40.30 1.33 o -4 2 3 203.66 204.60 2.41 o -3 2 3 5.40 4.53 0.58 o -2 2 3 112.13 107.58 1.91 o -1 2 3 95.11 105.21 3.50 o 0 2 3 2669.02 2863.70 54.48 o 1 2 3 71.07 78.11 1.00 o 2 2 3 1930.30 2130.37 35.04 o 3 2 3 104.86 109.61 2.43 o 4 2 3 781.86 719.77 7.55 o 5 2 3 114.94 111.97 2.17 o 6 2 3 121.63 119.41 2.76 o 7 2 3 36.24 36.17 2.05 o 8 2 3 30.54 37.65 2.10 o 9 2 3 30.95 31.38 2.86 o -9 3 3 7.04 6.11 1.95 o -8 3 3 2.17 3.51 1.53 o -7 3 3 14.00 16.80 1.84 o -6 3 3 12.40 15.82 1.44 o -5 3 3 3.67 6.16 1.40 o -4 3 3 17.20 15.72 1.17 o -3 3 3 210.54 204.57 3.46 o -2 3 3 1641.25 1730.60 19.52 o -1 3 3 161.67 160.07 1.80 o 0 3 3 353.75 334.30 4.22 o 1 3 3 8.94 12.03 0.49 o 2 3 3 1587.26 1531.80 22.55 o 3 3 3 360.93 368.95 3.69 o 4 3 3 1263.69 1305.90 16.39 o 5 3 3 175.62 178.84 2.82 o 6 3 3 41.73 43.66 2.35 o 7 3 3 45.17 45.30 2.53 o 8 3 3 65.84 66.06 2.97 o 9 3 3 29.35 31.61 2.75 o -8 4 3 59.18 56.86 2.60 o -7 4 3 6.68 6.83 1.47 o -6 4 3 12.48 16.48 1.59 o -5 4 3 28.15 31.32 2.22 o -4 4 3 134.81 130.60 3.55 o -3 4 3 214.33 207.73 2.51 o -2 4 3 307.76 307.18 3.52 o -1 4 3 43.51 41.11 1.15 o 0 4 3 707.68 739.20 13.39 o 1 4 3 370.98 367.46 6.45 o 2 4 3 788.65 755.70 7.67 o 3 4 3 259.02 252.32 3.11 o 4 4 3 242.32 249.81 4.09 o 5 4 3 100.82 106.48 2.83 o 6 4 3 235.12 240.35 5.44 o 7 4 3 117.60 116.22 2.66 o 8 4 3 14.22 17.01 1.69 o -7 5 3 16.26 11.42 2.06 o -6 5 3 126.18 123.71 2.64 o -5 5 3 80.64 84.75 2.44 o -4 5 3 71.28 80.90 2.25 o -3 5 3 12.54 12.93 1.05 o -2 5 3 62.32 59.55 2.35 o -1 5 3 232.17 232.19 3.26 o 0 5 3 514.42 512.04 8.84 o 1 5 3 422.50 415.53 4.15 o 2 5 3 259.87 275.02 3.89 o 3 5 3 111.49 113.09 2.07 o 4 5 3 84.95 85.88 2.28 o 5 5 3 161.64 153.58 2.76 o 6 5 3 90.56 92.32 2.51 o 7 5 3 15.54 17.28 1.36 o -6 6 3 71.07 72.13 6.81 o -5 6 3 36.65 35.90 2.17 o -4 6 3 87.83 84.23 2.69 o -3 6 3 33.06 36.94 1.35 o -2 6 3 51.60 60.26 1.59 o -1 6 3 185.46 191.72 2.45 o 0 6 3 125.16 127.55 2.31 o 1 6 3 136.67 131.46 2.30 o 2 6 3 54.76 55.91 1.67 o 3 6 3 159.11 147.69 3.10 o 4 6 3 100.14 106.64 4.44 o 5 6 3 48.71 55.07 3.12 o -3 7 3 109.22 103.58 2.60 o -2 7 3 116.12 105.45 2.36 o -1 7 3 36.60 37.81 2.36 o 0 7 3 0.76 0.63 2.31 o 1 7 3 65.22 60.72 2.91 o 2 7 3 51.01 53.35 3.20 o 3 7 3 79.01 77.73 6.11 o -10 0 4 119.31 139.44 8.81 o -9 0 4 38.55 38.86 3.96 o -8 0 4 95.17 93.80 5.53 o -7 0 4 90.21 90.30 3.74 o -6 0 4 1805.12 1742.78 37.34 o -5 0 4 1292.11 1230.35 23.48 o -4 0 4 1572.42 1615.27 28.31 o -3 0 4 14.30 9.79 1.15 o -2 0 4 451.33 371.07 6.58 o -1 0 4 5515.34 5521.67 163.36 o 0 0 4 4086.33 3940.65 66.89 o 1 0 4 1824.42 1839.42 21.59 o 2 0 4 57.44 70.28 1.38 o 3 0 4 49.19 57.80 1.68 o 4 0 4 1684.55 1583.08 27.56 o 5 0 4 418.26 396.17 7.72 o 6 0 4 1075.85 1078.09 26.45 o 7 0 4 80.66 81.33 3.89 o 8 0 4 83.18 82.43 3.55 o 9 0 4 15.28 13.71 2.84 o -10 1 4 45.91 53.54 3.53 o -9 1 4 55.78 59.47 3.41 o -8 1 4 302.59 300.93 6.26 o -7 1 4 167.01 164.21 3.53 o -6 1 4 652.98 639.15 8.57 o -5 1 4 326.94 331.18 5.36 o -4 1 4 1992.61 1953.61 26.18 o -3 1 4 1801.08 1763.78 21.82 o -2 1 4 1310.58 1304.48 14.44 o -1 1 4 893.38 911.10 8.65 o 0 1 4 547.35 519.74 9.56 o 1 1 4 1181.69 1105.88 20.06 o 2 1 4 1359.11 1315.47 13.49 o 3 1 4 430.05 388.81 3.56 o 4 1 4 824.65 803.22 7.95 o 5 1 4 110.00 110.86 2.19 o 6 1 4 548.25 513.79 6.86 o 7 1 4 90.10 89.62 2.43 o 8 1 4 183.45 183.43 3.90 o 9 1 4 31.70 33.63 2.68 o -9 2 4 57.67 62.59 3.06 o -8 2 4 299.60 296.64 8.76 o -7 2 4 232.97 224.97 5.13 o -6 2 4 242.04 248.02 5.48 o -5 2 4 127.85 133.67 2.28 o -4 2 4 868.03 816.78 8.47 o -3 2 4 1974.25 2004.54 23.19 o -2 2 4 2585.58 2746.85 41.27 o -1 2 4 331.48 305.23 3.06 o 0 2 4 117.12 90.05 1.09 o 1 2 4 397.28 374.31 6.49 o 2 2 4 2790.91 2802.43 32.40 o 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