#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211459.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211459_Fobs loop_ _publ_author_name 'Li, Rong' _publ_section_title ; 4,4'-Bis[(phenylsulfanyl)methyl]biphenyl ; _journal_coeditor_code HK2159 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5600 _journal_page_last o5601 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.216 _cell_angle_gamma 90.000 _cell_length_a 23.2051 _cell_length_b 5.5097 _cell_length_c 8.0412 _exptl_crystal_F_000 420.00 _reflns_d_resolution_high 0.8401 _[local]_cod_data_source_file hk2159Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 808.44 794.55 9.83 o 4 0 0 1249.90 1154.59 14.13 o 5 0 0 76.48 63.05 1.40 o 6 0 0 3992.01 3772.64 38.69 o 7 0 0 0.89 1.13 0.33 o 8 0 0 426.31 429.30 4.28 o 9 0 0 400.74 425.48 4.69 o 10 0 0 4994.24 5225.32 53.62 o 11 0 0 1188.36 1499.87 14.47 o 12 0 0 120.72 110.80 1.86 o 13 0 0 898.61 947.21 10.85 o 14 0 0 94.14 85.34 1.53 o 15 0 0 378.36 387.66 4.47 o 16 0 0 611.42 606.96 8.58 o 17 0 0 101.22 91.68 4.00 o 18 0 0 38.18 41.49 2.50 o 19 0 0 152.01 152.24 3.28 o 20 0 0 80.74 81.10 2.91 o 21 0 0 265.01 246.53 7.74 o 22 0 0 405.55 395.66 11.03 o 23 0 0 1.33 5.21 2.87 o 24 0 0 34.61 41.50 3.91 o 25 0 0 11.25 8.88 3.49 o 26 0 0 98.65 117.88 5.65 o 27 0 0 81.61 95.51 5.73 o 1 1 0 46.45 47.51 1.28 o 2 1 0 371.48 350.20 5.59 o 3 1 0 308.09 303.88 2.60 o 4 1 0 39.85 35.18 0.45 o 5 1 0 1018.46 1002.48 7.58 o 6 1 0 59.18 58.11 0.77 o 7 1 0 401.01 398.40 3.16 o 8 1 0 24.81 21.84 0.56 o 9 1 0 552.25 577.25 4.89 o 10 1 0 145.80 146.01 1.50 o 11 1 0 278.89 267.55 2.92 o 12 1 0 523.42 569.73 4.76 o 13 1 0 39.52 36.77 0.71 o 14 1 0 33.79 32.79 0.98 o 15 1 0 332.19 323.00 3.27 o 16 1 0 106.39 107.64 1.60 o 17 1 0 389.11 392.90 4.25 o 18 1 0 281.75 268.09 3.47 o 19 1 0 28.36 32.82 1.51 o 20 1 0 54.12 58.13 1.82 o 21 1 0 2.36 0.55 1.30 o 22 1 0 39.36 34.20 3.43 o 23 1 0 17.81 20.12 1.94 o 24 1 0 8.68 6.26 1.93 o 25 1 0 27.13 24.50 2.29 o 26 1 0 6.30 5.52 2.64 o 27 1 0 7.40 5.71 2.93 o 0 2 0 3.04 3.76 0.73 o 1 2 0 0.68 0.04 0.46 o 2 2 0 832.83 779.27 9.12 o 3 2 0 128.75 125.35 1.64 o 4 2 0 3125.00 3095.34 32.64 o 5 2 0 34.89 32.99 0.90 o 6 2 0 251.26 300.35 2.57 o 7 2 0 348.86 379.62 3.48 o 8 2 0 7.34 12.05 0.49 o 9 2 0 166.05 170.77 1.93 o 10 2 0 278.10 276.95 2.44 o 11 2 0 0.77 -0.02 0.38 o 12 2 0 135.46 137.53 2.28 o 13 2 0 9.08 7.58 0.65 o 14 2 0 187.67 172.24 2.90 o 15 2 0 36.85 38.02 1.13 o 16 2 0 33.72 31.41 1.10 o 17 2 0 921.06 903.59 9.72 o 18 2 0 45.28 44.02 1.35 o 19 2 0 0.01 -0.34 0.99 o 20 2 0 37.42 30.37 3.45 o 21 2 0 3.34 3.09 1.34 o 22 2 0 10.25 11.71 1.81 o 23 2 0 6.92 7.89 1.69 o 24 2 0 4.36 1.82 1.77 o 25 2 0 0.19 -0.40 1.90 o 26 2 0 18.03 9.80 2.14 o 1 3 0 379.07 373.94 4.31 o 2 3 0 5.52 5.30 0.60 o 3 3 0 222.91 210.30 2.67 o 4 3 0 410.35 432.02 5.00 o 5 3 0 393.07 395.33 5.13 o 6 3 0 148.99 152.39 3.55 o 7 3 0 608.60 596.70 5.81 o 8 3 0 6.34 3.96 0.52 o 9 3 0 100.03 88.57 1.63 o 10 3 0 0.17 0.23 0.44 o 11 3 0 178.69 178.00 2.90 o 12 3 0 0.49 0.61 0.70 o 13 3 0 421.77 409.64 4.87 o 14 3 0 204.06 200.16 2.85 o 15 3 0 532.87 515.33 6.04 o 16 3 0 18.15 19.17 1.37 o 17 3 0 114.46 110.35 2.37 o 18 3 0 15.75 18.35 1.98 o 19 3 0 0.26 0.75 1.36 o 20 3 0 21.69 20.49 1.75 o 21 3 0 26.30 21.91 3.76 o 22 3 0 15.64 13.20 1.84 o 23 3 0 34.79 36.79 3.73 o 24 3 0 4.70 4.52 2.35 o 0 4 0 0.06 0.47 1.14 o 1 4 0 4.23 3.80 0.85 o 2 4 0 122.12 135.06 2.16 o 3 4 0 3.46 4.25 0.95 o 4 4 0 12.59 15.15 0.86 o 5 4 0 7.57 6.75 0.82 o 6 4 0 115.11 126.35 2.97 o 7 4 0 9.22 12.11 1.25 o 8 4 0 42.92 46.84 1.42 o 9 4 0 2.89 2.10 0.81 o 10 4 0 6.37 8.29 1.05 o 11 4 0 8.51 6.28 1.07 o 12 4 0 72.34 77.89 2.26 o 13 4 0 17.40 18.88 2.08 o 14 4 0 0.38 0.57 1.31 o 15 4 0 26.79 25.88 1.80 o 16 4 0 11.37 7.35 1.71 o 17 4 0 33.94 27.44 1.37 o 18 4 0 0.26 0.43 1.30 o 19 4 0 18.24 17.95 2.40 o 20 4 0 25.03 22.33 2.27 o 21 4 0 0.12 0.12 1.70 o 1 5 0 0.35 0.66 1.23 o 2 5 0 144.62 152.77 2.94 o 3 5 0 86.17 93.10 1.92 o 4 5 0 20.63 18.92 1.16 o 5 5 0 13.02 13.45 1.36 o 6 5 0 4.97 4.38 1.67 o 7 5 0 0.01 -0.59 1.62 o 8 5 0 10.23 13.11 1.39 o 9 5 0 0.82 0.30 1.37 o 10 5 0 4.82 3.02 1.48 o 11 5 0 16.40 13.24 1.69 o 12 5 0 0.19 0.79 1.57 o 13 5 0 78.61 77.06 2.55 o 14 5 0 1.71 0.93 1.68 o 15 5 0 0.04 1.26 1.74 o 16 5 0 11.83 5.95 2.69 o 17 5 0 0.29 1.78 2.55 o 0 6 0 32.88 30.30 3.25 o 1 6 0 0.43 1.17 1.95 o 2 6 0 66.78 66.44 3.78 o 3 6 0 20.81 22.31 3.19 o 4 6 0 21.32 15.40 3.11 o 5 6 0 1.76 1.78 2.25 o 6 6 0 1.21 0.94 2.21 o 7 6 0 0.50 0.63 1.66 o 8 6 0 23.15 22.44 2.23 o 9 6 0 0.01 0.53 1.99 o 10 6 0 0.24 -0.47 2.02 o 11 6 0 6.35 5.92 2.14 o -27 1 1 16.17 22.52 4.68 o -26 1 1 53.93 63.71 7.40 o -25 1 1 7.08 3.60 1.92 o -24 1 1 16.19 20.63 2.11 o -23 1 1 0.84 1.20 1.53 o -22 1 1 208.27 217.10 4.82 o -21 1 1 0.01 0.06 1.16 o -20 1 1 39.92 38.96 1.38 o -19 1 1 113.42 118.17 2.09 o -18 1 1 274.38 278.24 3.22 o -17 1 1 505.50 488.73 5.13 o -16 1 1 398.48 376.78 4.08 o -15 1 1 65.58 72.29 1.45 o -14 1 1 441.13 442.78 3.90 o -13 1 1 462.83 476.48 4.11 o -12 1 1 324.97 312.87 3.29 o -11 1 1 326.73 368.14 3.13 o -10 1 1 403.64 360.97 3.19 o -9 1 1 54.26 60.30 0.86 o -8 1 1 26.45 20.86 0.53 o -7 1 1 465.89 479.44 4.35 o -6 1 1 764.24 739.21 6.07 o -5 1 1 8.79 9.61 1.04 o -4 1 1 73.74 73.48 0.76 o -3 1 1 1908.34 1863.86 14.97 o -2 1 1 999.73 1005.43 9.44 o -1 1 1 6295.61 6205.14 58.93 o 0 1 1 20809.09 19509.99 390.38 o 1 1 1 2711.26 2641.51 25.75 o 2 1 1 574.74 563.59 4.90 o 3 1 1 95.41 87.41 0.76 o 4 1 1 1965.19 1884.19 13.78 o 5 1 1 13.48 13.48 0.30 o 6 1 1 536.06 505.61 4.15 o 7 1 1 0.15 -0.44 0.29 o 8 1 1 677.06 663.31 6.20 o 9 1 1 3.47 3.12 0.44 o 10 1 1 3990.21 4095.56 34.55 o 11 1 1 7.62 12.72 0.54 o 12 1 1 353.66 350.44 3.28 o 13 1 1 30.65 34.54 1.23 o 14 1 1 161.87 145.03 2.18 o 15 1 1 27.51 22.81 0.89 o 16 1 1 69.10 76.03 1.44 o 17 1 1 138.13 130.16 2.46 o 18 1 1 36.88 34.98 1.33 o 19 1 1 25.67 22.48 1.38 o 20 1 1 28.59 31.70 1.59 o 21 1 1 190.02 178.92 3.34 o 22 1 1 91.66 87.08 2.38 o 23 1 1 2.05 3.25 1.59 o 24 1 1 55.43 56.19 2.25 o 25 1 1 18.53 23.78 2.25 o 26 1 1 31.60 28.30 3.04 o 27 1 1 78.41 84.27 4.97 o -26 2 1 6.78 7.30 2.38 o -25 2 1 42.27 39.79 9.88 o -24 2 1 9.51 9.22 1.88 o -23 2 1 3.44 4.71 1.71 o -22 2 1 1.13 1.17 1.43 o -21 2 1 10.03 11.77 1.49 o -20 2 1 167.49 168.12 2.91 o -19 2 1 144.57 142.24 2.42 o -18 2 1 96.65 95.29 1.93 o -17 2 1 119.49 121.29 2.11 o -16 2 1 282.69 291.51 3.65 o -15 2 1 298.30 299.54 3.69 o -14 2 1 0.61 0.32 0.67 o -13 2 1 444.42 443.93 4.69 o -12 2 1 116.45 107.62 2.06 o -11 2 1 472.99 454.29 4.12 o -10 2 1 6.20 6.58 0.41 o -9 2 1 394.35 381.70 4.18 o -8 2 1 64.66 74.72 1.40 o -7 2 1 1125.53 1127.22 11.12 o -6 2 1 64.58 78.89 0.91 o -5 2 1 2572.25 2602.08 21.66 o -4 2 1 41.83 48.89 1.82 o -3 2 1 363.94 367.03 4.42 o -2 2 1 622.68 633.91 6.04 o -1 2 1 158.24 143.92 2.55 o 0 2 1 18.84 17.86 0.72 o 1 2 1 2399.78 2415.98 31.05 o 2 2 1 16.24 23.57 1.03 o 3 2 1 310.76 304.17 3.89 o 4 2 1 71.79 75.77 0.94 o 5 2 1 103.05 86.22 0.85 o 6 2 1 425.38 439.04 3.74 o 7 2 1 563.40 542.85 4.95 o 8 2 1 72.95 71.66 1.34 o 9 2 1 223.26 203.03 2.14 o 10 2 1 31.51 28.09 0.67 o 11 2 1 366.20 343.75 3.04 o 12 2 1 74.41 66.20 1.31 o 13 2 1 179.06 171.58 2.45 o 14 2 1 153.20 146.69 2.00 o 15 2 1 564.68 551.45 5.69 o 16 2 1 201.27 201.25 2.60 o 17 2 1 500.42 486.61 5.19 o 18 2 1 90.33 89.75 1.84 o 19 2 1 0.08 0.16 1.04 o 20 2 1 1.54 1.45 1.20 o 21 2 1 24.00 22.35 1.74 o 22 2 1 0.31 0.07 1.57 o 23 2 1 98.70 100.31 2.95 o 24 2 1 24.56 28.49 2.14 o 25 2 1 30.32 34.36 2.31 o 26 2 1 4.36 2.05 2.11 o -24 3 1 11.02 7.27 2.51 o -23 3 1 1.70 0.65 1.28 o -22 3 1 7.60 8.22 2.43 o -21 3 1 0.80 -0.04 1.60 o -20 3 1 5.92 4.71 1.57 o -19 3 1 22.07 25.24 1.68 o -18 3 1 91.49 87.72 3.17 o -17 3 1 172.13 160.47 2.97 o -16 3 1 25.95 23.77 1.32 o -15 3 1 20.92 22.25 1.61 o -14 3 1 4.76 5.68 1.28 o -13 3 1 0.01 0.45 0.83 o -12 3 1 1.24 1.48 0.81 o -11 3 1 7.91 11.10 1.05 o -10 3 1 0.78 0.23 0.47 o -9 3 1 20.40 23.49 1.24 o -8 3 1 8.80 9.48 0.63 o -7 3 1 536.77 594.01 5.76 o -6 3 1 141.88 154.65 1.88 o -5 3 1 53.50 57.77 1.16 o -4 3 1 52.37 62.09 1.17 o -3 3 1 133.25 130.68 1.78 o -2 3 1 4.61 5.37 0.62 o -1 3 1 47.90 58.83 1.22 o 0 3 1 160.80 176.29 2.35 o 1 3 1 109.45 124.03 2.03 o 2 3 1 53.49 59.67 2.35 o 3 3 1 154.21 154.12 1.95 o 4 3 1 584.92 615.85 6.34 o 5 3 1 0.06 -0.03 0.58 o 6 3 1 686.73 773.15 6.66 o 7 3 1 9.42 9.04 0.47 o 8 3 1 5.68 10.29 0.62 o 9 3 1 19.66 22.59 0.90 o 10 3 1 0.07 -0.12 0.48 o 11 3 1 6.89 6.88 0.74 o 12 3 1 0.02 -0.58 0.70 o 13 3 1 60.77 61.09 2.21 o 14 3 1 480.54 474.93 9.10 o 15 3 1 40.13 39.79 1.48 o 16 3 1 307.11 315.47 4.76 o 17 3 1 286.36 270.29 3.76 o 18 3 1 25.44 25.20 1.47 o 19 3 1 33.82 34.64 1.83 o 20 3 1 24.21 21.34 1.73 o 21 3 1 19.96 16.94 1.81 o 22 3 1 4.95 4.48 1.25 o 23 3 1 2.49 2.09 1.46 o 24 3 1 3.00 2.52 1.56 o -21 4 1 7.90 5.25 1.78 o -20 4 1 0.03 -0.08 1.56 o -19 4 1 19.44 17.44 1.61 o -18 4 1 19.78 19.19 1.52 o -17 4 1 4.30 4.71 1.20 o -16 4 1 105.23 109.90 3.59 o -15 4 1 159.65 155.76 8.34 o -14 4 1 0.23 0.58 1.58 o -13 4 1 157.76 157.22 3.92 o -12 4 1 31.15 30.37 3.13 o -11 4 1 55.36 51.28 1.74 o -10 4 1 11.58 11.94 1.16 o -9 4 1 31.31 32.88 1.49 o -8 4 1 46.34 47.44 1.33 o -7 4 1 43.59 42.32 1.34 o -6 4 1 94.59 93.21 1.76 o -5 4 1 44.42 43.35 1.70 o -4 4 1 148.99 158.69 3.28 o -3 4 1 528.04 538.36 5.85 o -2 4 1 3.66 4.38 0.86 o -1 4 1 219.63 224.32 3.06 o 0 4 1 34.08 36.36 1.18 o 1 4 1 0.06 -0.10 0.80 o 2 4 1 8.01 6.33 0.87 o 3 4 1 16.09 14.99 1.12 o 4 4 1 50.74 56.53 1.37 o 5 4 1 53.25 55.37 1.35 o 6 4 1 2.20 1.84 0.91 o 7 4 1 57.70 56.32 1.22 o 8 4 1 0.00 0.36 0.86 o 9 4 1 22.03 22.82 1.19 o 10 4 1 4.55 4.42 1.05 o 11 4 1 72.25 68.19 4.48 o 12 4 1 21.28 18.16 1.45 o 13 4 1 115.85 116.14 2.88 o 14 4 1 193.98 180.17 6.29 o 15 4 1 33.47 30.50 3.81 o 16 4 1 7.89 3.18 1.52 o 17 4 1 20.38 19.91 1.26 o 18 4 1 11.00 10.90 1.40 o 19 4 1 39.88 41.77 1.75 o 20 4 1 1.17 0.36 1.59 o 21 4 1 8.62 8.87 1.82 o -17 5 1 0.53 0.99 2.75 o -16 5 1 0.37 0.12 2.55 o -15 5 1 5.08 5.98 2.27 o -14 5 1 13.71 12.43 2.60 o -13 5 1 0.24 1.12 1.96 o -12 5 1 39.94 44.23 3.32 o -11 5 1 15.67 16.54 2.16 o -10 5 1 1.75 1.06 1.53 o -9 5 1 1.49 1.40 1.43 o -8 5 1 13.18 16.87 1.53 o -7 5 1 2.99 3.35 1.31 o -6 5 1 25.56 28.40 2.23 o -5 5 1 1.20 2.23 1.11 o -4 5 1 100.68 103.45 2.06 o -3 5 1 116.98 135.66 2.13 o -2 5 1 53.01 69.74 1.99 o -1 5 1 22.82 26.73 2.02 o 0 5 1 53.81 50.04 1.91 o 1 5 1 2.14 0.88 1.24 o 2 5 1 260.14 293.88 4.44 o 3 5 1 0.14 1.05 1.10 o 4 5 1 72.00 86.45 3.43 o 5 5 1 1.78 3.28 1.67 o 6 5 1 11.96 14.49 2.36 o 7 5 1 7.52 6.59 1.21 o 8 5 1 58.26 65.84 1.96 o 9 5 1 0.30 -1.87 1.83 o 10 5 1 0.01 -0.58 1.88 o 11 5 1 6.49 5.19 1.97 o 12 5 1 34.14 35.71 2.02 o 13 5 1 2.25 1.07 1.62 o 14 5 1 15.46 21.78 2.33 o 15 5 1 3.93 3.38 1.82 o 16 5 1 1.10 1.63 2.00 o 17 5 1 8.30 6.21 2.22 o -10 6 1 0.69 -0.51 2.65 o -9 6 1 3.11 1.21 2.12 o -8 6 1 0.81 0.24 1.80 o -7 6 1 9.11 11.64 2.07 o -6 6 1 0.06 0.65 1.76 o -5 6 1 3.65 3.29 1.68 o -4 6 1 0.02 -0.74 1.60 o -3 6 1 27.51 25.38 3.49 o -2 6 1 31.03 32.22 2.48 o -1 6 1 0.13 0.56 1.92 o 0 6 1 6.55 4.81 1.92 o 1 6 1 3.39 3.23 2.89 o 2 6 1 45.20 40.60 4.24 o 3 6 1 0.60 0.98 2.72 o 4 6 1 1.56 1.17 2.68 o 5 6 1 12.72 11.91 2.39 o 6 6 1 13.29 8.81 2.22 o 7 6 1 2.30 2.18 2.36 o 8 6 1 15.51 12.10 2.77 o 9 6 1 0.43 -0.82 2.61 o 10 6 1 0.56 0.93 2.07 o -27 0 2 1.80 3.83 3.83 o -26 0 2 39.26 36.15 4.23 o -25 0 2 22.46 19.23 3.79 o -24 0 2 76.16 80.43 4.79 o -23 0 2 27.74 24.46 3.49 o -22 0 2 84.26 90.52 4.71 o -21 0 2 0.09 0.00 1.60 o -20 0 2 0.05 1.43 1.80 o -19 0 2 255.74 262.88 4.60 o -18 0 2 1108.33 1164.76 14.12 o -17 0 2 110.14 113.41 2.96 o -16 0 2 1186.12 1208.26 20.41 o -15 0 2 0.16 0.43 0.94 o -14 0 2 747.45 761.92 8.21 o -13 0 2 414.66 430.63 4.89 o -12 0 2 318.93 288.57 4.25 o -11 0 2 64.69 68.67 1.26 o -10 0 2 280.85 286.53 3.16 o -9 0 2 98.79 97.39 2.72 o -8 0 2 784.69 755.46 8.11 o -7 0 2 277.05 283.94 3.52 o -6 0 2 1274.10 1261.68 13.18 o -5 0 2 489.68 493.77 5.35 o -4 0 2 628.74 603.01 7.34 o -3 0 2 5485.35 5450.05 69.50 o -2 0 2 725.46 709.63 11.44 o -1 0 2 19926.42 19211.81 262.45 o 0 0 2 5982.63 6222.54 76.64 o 1 0 2 3471.11 3530.50 55.30 o 2 0 2 253.81 240.73 3.96 o 3 0 2 206.05 203.75 2.95 o 4 0 2 1990.85 1914.62 23.07 o 5 0 2 425.59 419.89 4.31 o 6 0 2 584.41 541.81 5.49 o 7 0 2 77.74 85.65 1.29 o 8 0 2 1854.66 1778.93 20.61 o 9 0 2 981.69 1042.98 10.80 o 10 0 2 7217.28 7708.37 91.30 o 11 0 2 523.30 538.94 6.23 o 12 0 2 235.86 210.01 2.84 o 13 0 2 6.51 9.81 1.14 o 14 0 2 77.57 64.45 1.70 o 15 0 2 5.49 3.11 1.43 o 16 0 2 684.67 678.63 17.98 o 17 0 2 34.03 36.35 4.70 o 18 0 2 220.44 228.62 5.21 o 19 0 2 67.46 56.41 5.49 o 20 0 2 35.86 21.41 2.30 o 21 0 2 193.90 177.57 9.22 o 22 0 2 88.85 92.54 4.97 o 23 0 2 0.97 5.13 3.37 o 24 0 2 129.20 136.87 6.21 o 25 0 2 56.14 56.94 4.49 o 26 0 2 9.83 6.36 4.07 o -26 1 2 0.81 0.31 2.57 o -25 1 2 43.43 43.35 2.50 o -24 1 2 13.34 10.10 1.85 o -23 1 2 12.77 14.49 1.75 o -22 1 2 1.26 2.23 1.35 o -21 1 2 9.52 8.05 1.19 o -20 1 2 30.25 30.91 1.51 o -19 1 2 483.01 506.11 7.42 o -18 1 2 75.20 79.59 2.64 o -17 1 2 4.43 6.47 0.93 o -16 1 2 158.26 168.67 2.03 o -15 1 2 12.30 12.86 0.76 o -14 1 2 22.55 23.10 0.84 o -13 1 2 585.54 598.44 5.08 o -12 1 2 88.05 84.60 1.13 o -11 1 2 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