#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/14/2211473.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211473_Fobs loop_ _publ_author_name 'Wang, Xiao-Yan' 'Deng, Xiao-Tao' 'Wang, Cheng-Gang' _publ_section_title ; Bis(acetato-\k^2^O,O')diaquacopper(II) ; _journal_coeditor_code IS2100 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3578 _journal_page_last m3579 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.230 _cell_angle_gamma 90.000 _cell_length_a 5.4731 _cell_length_b 10.1990 _cell_length_c 7.5187 _exptl_crystal_F_000 222.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file is2100Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 060401em in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3396.24 3339.60 98.90 o 2 0 0 3409.67 3607.66 52.31 o 3 0 0 2563.12 2582.15 55.81 o 4 0 0 459.06 464.83 29.75 o 5 0 0 2.94 1.75 0.63 o 6 0 0 200.99 208.94 12.07 o 1 1 0 1312.76 1458.27 16.36 o 2 1 0 30.85 31.92 0.93 o 3 1 0 8.51 14.69 0.54 o 4 1 0 424.99 412.47 6.06 o 5 1 0 0.75 0.38 0.36 o 6 1 0 0.12 -0.57 0.51 o 0 2 0 950.03 902.25 15.88 o 1 2 0 4247.61 4097.59 50.61 o 2 2 0 1319.48 1271.65 14.31 o 3 2 0 1326.60 1353.63 15.62 o 4 2 0 320.72 339.22 5.16 o 5 2 0 579.02 586.66 8.56 o 6 2 0 239.95 229.54 5.13 o 1 3 0 7.43 1.63 0.48 o 2 3 0 1085.06 1177.68 14.64 o 3 3 0 61.68 64.26 1.22 o 4 3 0 55.24 49.97 1.36 o 5 3 0 67.37 71.35 2.27 o 6 3 0 0.30 0.12 0.61 o 0 4 0 6581.46 6498.19 113.57 o 1 4 0 5684.78 5713.00 80.29 o 2 4 0 2556.63 2574.20 42.65 o 3 4 0 650.68 683.27 10.23 o 4 4 0 463.37 472.38 8.31 o 5 4 0 91.95 96.80 2.78 o 6 4 0 24.15 21.47 1.54 o 1 5 0 74.45 89.54 1.51 o 2 5 0 0.85 3.13 0.30 o 3 5 0 9.35 14.82 1.17 o 4 5 0 44.56 35.48 1.84 o 5 5 0 2.37 3.83 0.91 o 6 5 0 0.22 0.21 1.37 o 0 6 0 471.07 335.65 6.54 o 1 6 0 1260.92 1229.69 15.46 o 2 6 0 1397.99 1409.61 20.66 o 3 6 0 147.64 137.24 3.53 o 4 6 0 540.46 556.37 9.44 o 5 6 0 294.10 271.59 8.75 o 6 6 0 99.66 99.40 6.02 o 1 7 0 275.47 280.40 4.82 o 2 7 0 10.95 10.65 0.75 o 3 7 0 116.56 116.09 3.27 o 4 7 0 84.96 79.20 2.75 o 5 7 0 2.24 3.19 1.01 o 0 8 0 1116.78 1125.04 29.71 o 1 8 0 1767.01 1683.72 24.69 o 2 8 0 644.22 624.68 12.15 o 3 8 0 504.60 498.57 10.18 o 4 8 0 116.97 113.32 3.91 o 5 8 0 121.87 122.51 4.36 o 1 9 0 49.67 50.87 1.61 o 2 9 0 20.90 16.85 1.79 o 3 9 0 8.14 7.67 1.08 o 4 9 0 28.96 32.27 2.47 o 0 10 0 950.52 899.08 24.79 o 1 10 0 117.89 109.13 4.25 o 2 10 0 245.42 247.45 4.84 o 3 10 0 311.32 310.11 7.28 o 4 10 0 179.37 182.00 5.19 o 1 11 0 0.42 1.11 0.63 o 2 11 0 35.49 42.58 2.83 o 3 11 0 59.09 66.88 2.84 o 0 12 0 275.78 265.45 9.67 o 1 12 0 315.55 325.84 7.92 o 2 12 0 192.76 188.53 7.89 o 1 13 0 0.06 -1.05 1.11 o -6 1 1 319.94 306.42 6.21 o -5 1 1 216.19 203.71 4.29 o -4 1 1 473.87 457.19 12.76 o -3 1 1 1407.16 1484.44 17.02 o -2 1 1 6.13 5.77 0.28 o -1 1 1 2249.59 2260.33 28.93 o 0 1 1 5065.06 4562.86 65.24 o 1 1 1 2304.81 2166.08 26.90 o 2 1 1 3126.31 2952.93 33.20 o 3 1 1 2940.20 2845.82 42.48 o 4 1 1 521.91 529.65 7.60 o 5 1 1 382.79 408.27 6.34 o 6 1 1 234.18 220.30 4.96 o -6 2 1 15.09 13.01 1.25 o -5 2 1 1.38 1.33 0.51 o -4 2 1 113.24 111.81 2.18 o -3 2 1 286.55 315.30 4.04 o -2 2 1 35.08 29.52 0.80 o -1 2 1 172.56 258.76 4.92 o 0 2 1 234.81 210.71 3.25 o 1 2 1 626.46 612.10 10.93 o 2 2 1 755.90 915.63 14.35 o 3 2 1 72.37 84.18 1.89 o 4 2 1 0.06 0.16 0.28 o 5 2 1 24.19 22.63 1.10 o 6 2 1 0.60 1.71 1.85 o -6 3 1 283.48 279.67 5.90 o -5 3 1 287.08 286.37 5.72 o -4 3 1 440.63 451.91 7.86 o -3 3 1 170.30 182.90 2.59 o -2 3 1 2341.21 2615.61 36.06 o -1 3 1 589.29 637.48 11.51 o 0 3 1 2921.62 3011.82 42.35 o 1 3 1 4108.59 3926.90 55.22 o 2 3 1 3366.40 3305.53 40.43 o 3 3 1 1032.29 917.73 10.90 o 4 3 1 837.37 840.19 11.57 o 5 3 1 363.57 371.75 7.09 o 6 3 1 86.75 79.65 3.26 o -6 4 1 1.36 2.51 0.76 o -5 4 1 2.49 3.09 0.68 o -4 4 1 24.00 19.39 1.13 o -3 4 1 15.42 15.92 0.80 o -2 4 1 54.64 47.50 1.17 o -1 4 1 52.80 80.92 1.66 o 0 4 1 619.07 603.13 7.73 o 1 4 1 26.41 38.10 1.00 o 2 4 1 44.18 40.96 0.94 o 3 4 1 3.11 3.68 0.87 o 4 4 1 1.44 2.35 0.69 o 5 4 1 49.24 48.91 1.94 o 6 4 1 20.83 22.91 1.95 o -6 5 1 63.56 71.83 7.45 o -5 5 1 507.00 485.22 10.68 o -4 5 1 286.84 315.85 5.73 o -3 5 1 432.20 485.55 9.48 o -2 5 1 440.38 530.48 10.04 o -1 5 1 1180.99 1336.53 16.64 o 0 5 1 667.43 629.54 8.12 o 1 5 1 2919.72 2963.45 36.36 o 2 5 1 1085.46 987.37 12.59 o 3 5 1 1012.10 995.04 18.32 o 4 5 1 918.86 924.50 18.31 o 5 5 1 179.85 173.47 5.10 o 6 5 1 112.86 121.02 6.73 o -6 6 1 2.84 2.38 0.86 o -5 6 1 8.87 9.91 1.32 o -4 6 1 0.01 -0.12 0.41 o -3 6 1 48.73 48.82 1.85 o -2 6 1 3.93 5.61 1.64 o -1 6 1 67.89 61.22 1.16 o 0 6 1 1.07 0.55 0.21 o 1 6 1 116.38 101.01 1.79 o 2 6 1 100.53 97.75 2.16 o 3 6 1 11.50 13.96 1.27 o 4 6 1 18.29 16.64 1.47 o 5 6 1 0.03 0.65 0.80 o -5 7 1 230.52 226.16 11.67 o -4 7 1 183.11 189.06 4.88 o -3 7 1 102.93 118.93 3.34 o -2 7 1 1458.05 1443.56 92.07 o -1 7 1 548.60 605.94 9.45 o 0 7 1 764.80 747.80 22.46 o 1 7 1 1986.96 1998.99 24.91 o 2 7 1 1231.16 1216.27 18.14 o 3 7 1 312.57 302.47 8.91 o 4 7 1 441.42 407.67 12.37 o 5 7 1 221.28 230.08 7.41 o -5 8 1 1.04 2.95 1.03 o -4 8 1 18.80 16.20 1.38 o -3 8 1 119.00 113.30 3.90 o -2 8 1 9.71 10.49 1.02 o -1 8 1 234.52 241.90 4.43 o 0 8 1 2.12 1.76 0.40 o 1 8 1 21.95 22.57 1.01 o 2 8 1 244.73 240.93 4.51 o 3 8 1 14.98 15.75 1.80 o 4 8 1 22.05 24.94 2.42 o 5 8 1 2.76 1.71 1.26 o -5 9 1 74.36 68.54 3.98 o -4 9 1 261.34 256.86 6.62 o -3 9 1 334.65 340.89 7.97 o -2 9 1 65.95 74.50 2.09 o -1 9 1 391.12 424.83 7.20 o 0 9 1 678.30 729.72 14.42 o 1 9 1 232.30 225.13 5.49 o 2 9 1 388.65 403.56 8.61 o 3 9 1 574.73 571.61 11.72 o 4 9 1 206.72 210.55 5.57 o -4 10 1 3.17 1.33 0.90 o -3 10 1 8.95 8.08 1.19 o -2 10 1 13.42 12.30 1.00 o -1 10 1 7.69 8.18 1.38 o 0 10 1 12.54 14.19 1.34 o 1 10 1 2.34 5.31 1.18 o 2 10 1 3.93 3.09 0.82 o 3 10 1 38.61 42.50 2.21 o 4 10 1 1.68 3.05 1.00 o -3 11 1 245.47 254.70 7.21 o -2 11 1 125.08 135.40 4.16 o -1 11 1 362.77 356.70 8.24 o 0 11 1 371.04 358.40 8.30 o 1 11 1 280.72 279.83 6.87 o 2 11 1 309.84 309.14 10.84 o 3 11 1 244.30 238.90 9.12 o -3 12 1 0.01 -0.27 1.18 o -2 12 1 0.36 0.14 1.16 o -1 12 1 2.46 4.38 1.01 o 0 12 1 3.69 6.63 1.11 o 1 12 1 15.99 19.33 1.69 o 2 12 1 2.44 0.90 1.30 o -1 13 1 67.83 73.01 4.39 o 0 13 1 167.78 179.66 5.39 o -7 0 2 165.04 174.50 8.29 o -6 0 2 230.06 251.77 9.89 o -5 0 2 108.42 113.55 3.33 o -4 0 2 2063.62 1807.62 73.24 o -3 0 2 1207.09 1245.22 23.08 o -2 0 2 277.31 302.36 6.00 o -1 0 2 5059.41 5381.83 79.29 o 0 0 2 3542.26 3634.67 63.47 o 1 0 2 380.90 365.37 7.01 o 2 0 2 2591.60 2676.90 48.66 o 3 0 2 1968.35 1692.09 106.69 o 4 0 2 170.84 145.33 4.80 o 5 0 2 385.97 410.32 12.45 o 6 0 2 141.87 146.07 6.22 o -7 1 2 0.09 -0.11 0.87 o -6 1 2 36.87 37.78 1.69 o -5 1 2 162.65 161.05 2.99 o -4 1 2 68.32 69.78 1.55 o -3 1 2 35.69 28.85 0.82 o -2 1 2 197.78 205.50 2.42 o -1 1 2 2600.85 2731.40 30.44 o 0 1 2 1983.43 2156.66 26.47 o 1 1 2 5.31 4.20 0.46 o 2 1 2 33.21 34.79 0.77 o 3 1 2 180.03 171.25 2.93 o 4 1 2 146.08 153.54 2.87 o 5 1 2 11.40 13.97 1.08 o 6 1 2 4.62 5.71 1.07 o -7 2 2 231.40 247.79 8.80 o -6 2 2 525.69 549.89 9.89 o -5 2 2 953.96 924.91 15.04 o -4 2 2 852.52 842.98 11.40 o -3 2 2 1349.30 1393.02 16.04 o -2 2 2 544.86 536.69 6.38 o -1 2 2 42.10 57.88 2.06 o 0 2 2 22.81 20.15 0.69 o 1 2 2 180.25 152.55 8.17 o 2 2 2 1179.27 1114.47 14.26 o 3 2 2 508.87 499.33 7.08 o 4 2 2 888.36 899.57 12.36 o 5 2 2 639.11 653.67 10.91 o 6 2 2 258.46 275.29 9.75 o -6 3 2 8.94 9.69 1.07 o -5 3 2 34.67 33.01 1.48 o -4 3 2 0.93 1.14 0.99 o -3 3 2 290.51 318.71 4.12 o -2 3 2 8.85 11.98 0.48 o -1 3 2 31.44 57.75 1.59 o 0 3 2 27.15 43.48 1.04 o 2 3 2 188.80 190.76 3.33 o 3 3 2 4.25 3.04 0.48 o 4 3 2 154.42 149.89 2.89 o 5 3 2 14.36 15.31 2.28 o 6 3 2 5.85 5.24 1.43 o -6 4 2 138.42 141.47 3.78 o -5 4 2 426.43 423.17 7.84 o -4 4 2 604.22 555.76 8.04 o -3 4 2 848.94 792.88 33.74 o -2 4 2 1812.97 1946.31 34.17 o -1 4 2 1170.01 1272.33 18.21 o 0 4 2 1778.30 2025.45 28.70 o 1 4 2 2235.36 2409.46 41.35 o 2 4 2 762.31 824.65 12.24 o 3 4 2 1038.99 993.83 14.85 o 4 4 2 536.64 561.49 9.40 o 5 4 2 129.50 141.54 4.43 o -6 5 2 2.08 1.40 0.75 o -5 5 2 18.31 17.17 1.50 o -4 5 2 89.34 79.70 3.24 o -3 5 2 23.79 20.08 0.85 o -2 5 2 299.29 261.51 5.50 o -1 5 2 163.78 177.48 2.99 o 0 5 2 51.01 60.06 1.37 o 1 5 2 89.42 102.06 2.07 o 2 5 2 28.38 19.81 0.84 o 3 5 2 125.41 121.23 3.56 o 4 5 2 26.14 22.95 1.69 o 5 5 2 0.43 0.27 0.67 o -6 6 2 298.11 320.32 8.18 o -5 6 2 637.75 595.20 12.73 o -4 6 2 391.18 364.52 6.58 o -3 6 2 513.90 474.30 9.46 o -2 6 2 989.43 930.92 75.96 o -1 6 2 38.96 42.74 2.26 o 0 6 2 84.26 124.07 2.38 o 1 6 2 778.99 859.25 11.16 o 2 6 2 191.69 212.67 3.36 o 3 6 2 412.05 449.05 9.24 o 4 6 2 629.52 624.47 13.28 o 5 6 2 244.05 255.05 6.92 o -5 7 2 3.22 1.87 0.79 o -4 7 2 60.64 56.97 1.92 o -3 7 2 38.25 34.94 2.70 o -2 7 2 81.49 68.46 2.45 o -1 7 2 11.01 15.33 0.84 o 0 7 2 8.94 12.00 0.89 o 1 7 2 0.66 4.10 1.40 o 2 7 2 23.55 23.75 1.07 o 3 7 2 107.97 102.33 3.19 o 4 7 2 0.27 0.08 0.92 o 5 7 2 5.52 6.12 1.32 o -5 8 2 215.60 216.11 8.77 o -4 8 2 197.00 188.75 4.91 o -3 8 2 448.21 437.55 9.10 o -2 8 2 554.52 542.73 8.81 o -1 8 2 578.53 645.85 10.23 o 0 8 2 670.81 725.15 11.33 o 1 8 2 632.27 711.20 11.15 o 2 8 2 525.32 566.48 9.22 o 3 8 2 280.82 280.46 7.07 o 4 8 2 258.45 277.71 9.59 o -5 9 2 5.80 4.65 1.11 o -4 9 2 12.57 14.04 2.09 o -3 9 2 70.63 74.55 2.69 o -2 9 2 57.20 58.15 2.14 o -1 9 2 31.88 25.39 1.16 o 0 9 2 116.84 112.90 3.43 o 1 9 2 87.44 89.39 2.97 o 2 9 2 43.41 45.75 2.06 o 3 9 2 6.49 9.60 1.56 o 4 9 2 0.61 1.92 1.32 o -4 10 2 396.65 402.90 9.10 o -3 10 2 190.39 182.03 4.96 o -2 10 2 66.24 69.80 3.53 o -1 10 2 309.59 310.56 7.25 o 0 10 2 192.17 199.46 5.25 o 1 10 2 38.74 43.17 2.07 o 2 10 2 221.05 222.47 8.38 o 3 10 2 273.88 285.33 7.03 o -3 11 2 1.82 0.59 0.78 o -2 11 2 2.65 1.79 0.75 o -1 11 2 21.42 25.18 2.25 o 0 11 2 36.13 36.35 2.01 o 1 11 2 1.58 0.52 0.73 o 2 11 2 1.23 2.19 1.39 o 3 11 2 3.18 0.60 1.22 o -2 12 2 137.93 142.36 4.50 o -1 12 2 209.45 210.33 5.83 o 0 12 2 173.47 178.17 5.22 o 1 12 2 158.10 163.78 4.97 o -7 1 3 160.65 159.94 7.80 o -6 1 3 155.53 159.65 3.86 o -5 1 3 415.17 414.89 7.46 o -4 1 3 1900.46 1864.49 24.10 o -3 1 3 1356.87 1294.52 13.60 o -2 1 3 2122.43 2027.59 22.73 o -1 1 3 4277.03 4371.64 54.70 o 0 1 3 945.40 1030.80 13.05 o 1 1 3 243.17 264.81 3.77 o 2 1 3 1174.26 1291.22 14.97 o 3 1 3 238.01 255.40 4.68 o 4 1 3 220.10 215.37 5.26 o 5 1 3 294.87 289.76 9.59 o -6 2 3 7.63 8.11 1.14 o -5 2 3 7.79 9.43 0.88 o -4 2 3 1.60 0.99 0.28 o -3 2 3 312.52 328.90 4.25 o -2 2 3 471.86 472.43 6.35 o -1 2 3 0.08 0.31 0.20 o 0 2 3 84.38 123.95 2.35 o 1 2 3 135.58 138.15 2.62 o 2 2 3 42.70 44.35 1.08 o 3 2 3 71.90 69.58 1.91 o 4 2 3 18.44 17.23 1.35 o 5 2 3 1.15 1.32 0.67 o -6 3 3 248.09 240.66 5.24 o -5 3 3 469.05 460.24 8.29 o -4 3 3 576.86 545.19 7.86 o -3 3 3 2170.86 2059.93 26.73 o -2 3 3 2335.04 2182.97 83.65 o -1 3 3 1832.33 1785.27 25.42 o 0 3 3 957.34 1022.65 14.91 o 1 3 3 1445.90 1617.07 29.49 o 2 3 3 190.54 210.48 3.78 o 3 3 3 364.20 386.89 6.70 o 4 3 3 229.37 238.21 11.77 o 5 3 3 212.17 216.56 8.18 o -6 4 3 31.08 31.71 1.66 o -5 4 3 7.01 5.84 0.82 o -4 4 3 6.64 5.17 0.63 o -3 4 3 24.92 26.53 1.75 o -2 4 3 5.73 3.52 0.54 o -1 4 3 70.29 71.44 1.75 o 0 4 3 3.04 7.60 0.53 o 1 4 3 104.74 98.44 2.10 o 2 4 3 63.09 73.17 1.80 o 3 4 3 9.29 7.03 0.89 o 4 4 3 8.04 7.42 0.87 o 5 4 3 7.89 9.22 1.75 o -6 5 3 150.49 147.87 4.70 o -5 5 3 461.59 446.70 9.91 o -4 5 3 619.14 595.37 9.82 o -3 5 3 962.81 890.02 13.88 o -2 5 3 1533.42 1369.40 24.60 o -1 5 3 487.34 426.34 6.65 o 0 5 3 1366.73 1358.31 19.66 o 1 5 3 215.02 220.70 3.91 o 2 5 3 260.67 284.96 4.95 o 3 5 3 361.98 377.86 11.34 o 4 5 3 307.99 299.59 15.20 o 5 5 3 44.08 41.22 3.23 o -6 6 3 0.19 -0.42 0.73 o -5 6 3 12.87 12.86 1.37 o -4 6 3 1.98 1.54 0.62 o -3 6 3 59.33 60.32 2.14 o -2 6 3 28.60 33.47 1.49 o -1 6 3 9.56 7.95 0.81 o 0 6 3 29.27 29.71 1.34 o 1 6 3 0.34 0.19 0.29 o 2 6 3 64.80 64.02 1.74 o 3 6 3 0.05 0.17 0.55 o 4 6 3 7.29 9.81 1.38 o -5 7 3 236.12 219.49 5.97 o -4 7 3 159.47 148.11 3.83 o -3 7 3 985.95 921.08 14.14 o -2 7 3 1153.34 1075.65 19.89 o -1 7 3 485.26 442.82 8.92 o 0 7 3 658.09 579.38 32.51 o 1 7 3 993.19 947.41 19.75 o 2 7 3 78.44 78.49 2.10 o 3 7 3 209.50 204.87 5.21 o 4 7 3 164.50 170.80 5.25 o -5 8 3 38.60 43.06 2.35 o -4 8 3 0.01 -0.25 0.48 o -3 8 3 135.13 130.65 3.73 o -2 8 3 50.84 47.92 1.61 o -1 8 3 17.55 17.84 1.02 o 0 8 3 165.95 171.15 3.55 o 1 8 3 24.83 24.05 0.98 o 2 8 3 28.33 24.59 1.54 o 3 8 3 13.12 10.65 1.28 o 4 8 3 8.75 13.55 2.18 o -5 9 3 158.03 152.94 4.97 o -4 9 3 428.43 415.11 9.16 o -3 9 3 231.05 204.57 5.47 o -2 9 3 229.27 217.90 4.39 o -1 9 3 599.53 562.02 9.31 o 0 9 3 244.84 239.68 4.68 o 1 9 3 73.74 66.94 2.58 o 2 9 3 290.31 292.26 6.83 o 3 9 3 164.18 154.05 4.54 o -4 10 3 16.68 21.52 2.24 o -3 10 3 3.48 3.95 0.97 o -2 10 3 0.01 -0.52 0.46 o -1 10 3 16.68 20.99 1.26 o 0 10 3 3.60 7.30 1.06 o 1 10 3 5.78 8.19 1.15 o 2 10 3 18.24 18.98 2.45 o 3 10 3 3.89 3.89 1.58 o -3 11 3 157.02 150.88 4.53 o -2 11 3 261.83 245.65 5.06 o -1 11 3 321.59 304.24 7.44 o 0 11 3 206.65 198.89 7.73 o 1 11 3 165.39 159.88 7.39 o 2 11 3 229.43 223.95 8.87 o -2 12 3 22.16 28.23 5.09 o -1 12 3 0.34 1.72 0.82 o 0 12 3 5.58 10.17 1.36 o 1 12 3 1.48 3.14 0.99 o -6 0 4 4.46 4.31 1.46 o -5 0 4 315.47 261.88 36.97 o -3 0 4 483.25 411.96 8.44 o -2 0 4 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