#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/15/2211542.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211542_Fobs loop_ _publ_author_name 'Venter, Gertruida J. S.' 'Meijboom, Reinout' 'Roodt, Andreas' _publ_section_title ; Tetrakis(tri-p-tolylphosphine-\kP)silver(I) hexafluorophosphate ; _journal_coeditor_code NG2149 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3453 _journal_page_last m3455 _journal_volume 62 _journal_year 2006 _space_group_IT_number 198 _symmetry_space_group_name_Hall 'P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P 21 3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.6842 _cell_length_b 24.6842 _cell_length_c 24.6842 _exptl_crystal_F_000 6112.00 _reflns_d_resolution_high 0.7483 _[local]_cod_data_source_file ng2149Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6ftv4_0m in P2(1)3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 715.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' 'z, x, y' 'y, z, x' '-z+1/2, -x, y+1/2' '-y, z+1/2, -x+1/2' 'z+1/2, -x+1/2, -y' '-y+1/2, -z, x+1/2' '-z, x+1/2, -y+1/2' 'y+1/2, -z+1/2, -x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 1 1 155.33 35.68 18.06 o 0 1 1 23432.89 -1.96 1.96 o 1 1 1 150.25 23.61 15.80 o 1 0 2 367.65 92.63 22.46 o -1 1 2 6111.75 5425.09 106.81 o 0 1 2 321.29 198.94 15.00 o 1 1 2 6282.56 5459.26 91.93 o -2 2 2 755.81 545.31 55.80 o -1 2 2 8104.45 7913.78 87.25 o 0 2 2 511923.66 522855.09 4568.93 o 1 2 2 8200.76 7973.06 90.12 o 2 2 2 1223.89 946.13 96.59 o 1 0 3 1352.59 1143.84 42.22 o 2 0 3 117.87 111.55 9.77 o -2 1 3 8150.37 6382.98 64.19 o -1 1 3 665.05 583.46 32.52 o 0 1 3 1172.28 961.83 27.71 o 1 1 3 645.70 580.99 29.58 o 2 1 3 7495.48 5805.13 65.50 o -2 2 3 5817.88 6508.25 57.68 o -1 2 3 3715.07 3906.16 40.17 o 0 2 3 5265.00 5994.70 108.08 o 1 2 3 3712.73 3799.01 40.55 o 2 2 3 5925.52 6547.59 63.81 o -3 3 3 20498.20 21782.54 276.35 o -2 3 3 43343.70 42654.95 298.60 o -1 3 3 712.53 764.74 18.15 o 0 3 3 25063.79 24161.80 168.46 o 1 3 3 658.21 719.24 18.68 o 2 3 3 44018.34 43397.12 293.07 o 3 3 3 20380.52 21526.92 317.29 o 0 0 4 22232.82 22730.10 214.98 o 1 0 4 322.59 203.57 11.46 o 2 0 4 6228.98 5396.62 50.48 o 3 0 4 118944.41 117648.74 738.12 o -3 1 4 87189.85 90249.23 550.94 o -2 1 4 7299.92 7828.21 63.99 o -1 1 4 1241.48 1307.86 21.88 o 0 1 4 856.32 997.56 20.19 o 1 1 4 1230.46 1350.63 23.11 o 2 1 4 7025.01 7530.07 62.14 o 3 1 4 86588.37 89770.27 582.58 o -3 2 4 72461.61 76684.38 494.83 o -2 2 4 321489.13 331944.44 2159.13 o -1 2 4 12144.83 12663.27 103.06 o 0 2 4 125233.74 127923.59 852.50 o 1 2 4 12491.12 12939.96 105.43 o 2 2 4 318163.09 326588.56 2157.89 o 3 2 4 71552.38 75629.48 516.26 o -3 3 4 93637.00 102914.83 658.46 o -2 3 4 5695.97 5772.07 58.34 o -1 3 4 30751.46 28366.02 206.24 o 0 3 4 4880.73 4680.09 50.35 o 1 3 4 32051.60 29733.88 206.69 o 2 3 4 5858.66 5832.97 60.79 o 3 3 4 96039.34 106543.41 750.97 o -4 4 4 195108.31 201023.45 2425.81 o -3 4 4 43830.30 47854.50 368.99 o -2 4 4 119925.37 120949.85 747.80 o -1 4 4 78805.05 83616.06 535.71 o 0 4 4 42191.48 43477.22 294.49 o 1 4 4 79490.84 84216.92 535.44 o 2 4 4 111670.49 111759.66 746.53 o 3 4 4 43654.12 47477.64 389.41 o 4 4 4 199924.78 204110.55 3698.36 o 1 0 5 24.48 126.98 12.93 o 2 0 5 55476.61 59602.55 379.80 o 3 0 5 2898.88 2554.34 36.14 o 4 0 5 32347.41 34454.25 246.64 o -4 1 5 27653.25 24868.70 180.99 o -3 1 5 29962.86 30809.20 208.46 o -2 1 5 100678.08 111151.79 708.63 o -1 1 5 10021.55 9920.27 80.11 o 0 1 5 1973.51 2120.10 35.24 o 1 1 5 9899.13 9762.79 82.57 o 2 1 5 97799.99 108205.25 633.40 o 3 1 5 29458.96 30480.77 210.72 o 4 1 5 26123.83 23142.88 175.53 o -4 2 5 3986.64 3939.70 51.75 o -3 2 5 2252.38 1943.34 35.71 o -2 2 5 24243.51 23509.68 174.29 o -1 2 5 38386.68 37134.68 256.24 o 0 2 5 177.81 67.34 16.98 o 1 2 5 39059.43 37698.78 267.16 o 2 2 5 24795.13 23841.33 169.97 o 3 2 5 2289.28 2110.20 35.03 o 4 2 5 3947.24 3851.25 52.21 o -4 3 5 64005.40 64048.64 492.41 o -3 3 5 14253.94 13450.09 118.68 o -2 3 5 95634.33 96847.73 629.51 o -1 3 5 19322.86 20604.39 156.73 o 0 3 5 3711.94 4625.50 52.35 o 1 3 5 19748.89 21058.27 160.70 o 2 3 5 92871.26 93311.90 641.77 o 3 3 5 14517.50 13738.89 129.96 o 4 3 5 65002.41 65014.55 506.03 o -4 4 5 1377.80 1815.17 39.85 o -3 4 5 84608.79 88803.61 663.76 o -2 4 5 13921.09 13339.44 121.70 o -1 4 5 57306.50 60298.79 446.72 o 0 4 5 53307.84 59658.67 424.47 o 1 4 5 56876.27 59269.06 415.83 o 2 4 5 13545.79 12921.68 117.46 o 3 4 5 84621.74 88228.93 680.31 o 4 4 5 1273.50 1779.55 43.60 o -5 5 5 1719.88 2000.08 80.31 o -4 5 5 23107.68 23911.81 200.42 o -3 5 5 19659.48 20713.16 181.59 o -2 5 5 9584.84 9807.73 97.80 o -1 5 5 6632.24 6537.14 71.78 o 0 5 5 17013.38 17463.66 147.59 o 1 5 5 6333.37 6263.73 70.67 o 2 5 5 9091.50 8930.24 97.42 o 3 5 5 19233.04 20142.55 174.05 o 4 5 5 23022.06 23268.81 228.77 o 5 5 5 1480.65 1767.43 83.23 o 0 0 6 5690.32 5750.28 82.97 o 1 0 6 5175.59 6371.05 62.40 o 2 0 6 324327.06 332471.84 2058.29 o 3 0 6 66109.89 62457.21 434.30 o 4 0 6 38229.68 39252.76 299.08 o 5 0 6 488.06 215.46 25.76 o -5 1 6 52737.79 53650.33 400.56 o -4 1 6 49552.05 51638.30 365.52 o -3 1 6 4942.71 4452.85 55.06 o -2 1 6 7157.99 8274.22 79.02 o -1 1 6 6726.74 7030.20 71.26 o 0 1 6 865.26 695.84 22.92 o 1 1 6 6690.21 6893.63 68.49 o 2 1 6 7425.64 8522.54 71.70 o 3 1 6 4642.06 4145.21 52.29 o 4 1 6 50149.95 51328.76 391.57 o 5 1 6 52151.38 53760.17 408.92 o -5 2 6 3377.09 4689.43 63.87 o -4 2 6 189758.38 198548.59 1326.25 o -3 2 6 18036.94 17968.46 145.33 o -2 2 6 36485.00 39798.18 322.60 o -1 2 6 4366.67 3829.89 52.23 o 0 2 6 280535.59 280903.38 1986.31 o 1 2 6 4504.20 3952.70 50.39 o 2 2 6 40591.55 44249.31 301.51 o 3 2 6 18494.27 18371.32 146.19 o 4 2 6 185886.19 190780.67 1460.96 o 5 2 6 3409.77 4484.18 63.17 o -5 3 6 36648.07 38016.78 302.49 o -4 3 6 14545.37 14000.82 129.18 o -3 3 6 2403.25 2348.85 47.35 o -2 3 6 6099.66 5949.61 74.57 o -1 3 6 13856.60 16409.72 142.24 o 0 3 6 47070.07 49766.45 368.38 o 1 3 6 14664.45 17252.33 148.57 o 2 3 6 6262.43 6066.68 69.87 o 3 3 6 2410.18 2313.76 44.67 o 4 3 6 14326.17 13863.40 138.11 o 5 3 6 37128.87 38296.54 326.39 o -5 4 6 2215.05 3021.38 50.92 o -4 4 6 50067.58 50125.22 376.59 o -3 4 6 9156.62 8386.59 90.96 o -2 4 6 154074.70 158268.45 1117.31 o -1 4 6 19448.12 20642.49 173.07 o 0 4 6 833.17 1126.41 36.21 o 1 4 6 18383.82 19603.97 176.68 o 2 4 6 149348.05 152473.81 1172.88 o 3 4 6 9023.17 8147.48 98.23 o 4 4 6 50144.86 50722.20 431.28 o 5 4 6 2364.34 3122.55 60.56 o -5 5 6 57161.94 59751.18 444.24 o -4 5 6 11716.15 12431.08 125.97 o -3 5 6 77964.98 79197.45 597.95 o -2 5 6 13909.68 14148.65 140.10 o -1 5 6 2351.32 2947.85 53.68 o 0 5 6 5836.91 6094.84 79.91 o 1 5 6 2288.93 2682.13 49.66 o 2 5 6 14300.37 14901.25 142.01 o 3 5 6 77955.63 77487.30 611.79 o 4 5 6 11305.38 11989.31 134.62 o 5 5 6 58057.98 59676.37 561.08 o -6 6 6 35050.05 37152.48 514.64 o -5 6 6 19217.54 20579.25 189.52 o -4 6 6 46525.87 43864.68 360.08 o -3 6 6 10170.91 10639.96 117.66 o -2 6 6 76408.13 75762.50 579.16 o -1 6 6 19285.22 20082.04 181.19 o 0 6 6 8996.26 7872.70 91.68 o 1 6 6 19334.25 19728.94 178.67 o 2 6 6 71601.62 70169.35 570.76 o 3 6 6 9718.19 10256.01 114.83 o 4 6 6 48036.93 45509.56 403.94 o 5 6 6 18723.08 20057.18 224.36 o 6 6 6 35513.91 37414.94 673.82 o 1 0 7 9472.79 8398.96 93.72 o 2 0 7 15713.53 16179.76 150.56 o 3 0 7 31047.23 33437.16 266.68 o 4 0 7 4890.33 4470.20 66.15 o 5 0 7 11064.76 10632.00 124.26 o 6 0 7 12142.62 12366.54 137.36 o -6 1 7 6061.80 4684.13 70.85 o -5 1 7 12897.69 13782.00 149.16 o -4 1 7 10602.82 11085.98 121.91 o -3 1 7 764.99 687.20 29.21 o -2 1 7 15992.27 17162.91 160.59 o -1 1 7 8754.32 9866.63 104.31 o 0 1 7 47401.20 48039.33 398.85 o 1 1 7 8650.65 9630.32 104.59 o 2 1 7 16993.10 17959.78 142.02 o 3 1 7 666.24 615.02 24.23 o 4 1 7 10319.47 10739.26 109.30 o 5 1 7 12738.16 13484.38 142.72 o 6 1 7 5376.03 4126.02 70.00 o -6 2 7 4198.30 4531.07 77.02 o -5 2 7 9772.30 10552.07 120.20 o -4 2 7 16280.55 16361.67 148.80 o -3 2 7 24487.20 24735.38 221.85 o -2 2 7 83989.18 89695.56 707.72 o -1 2 7 1499.66 1806.99 40.74 o 0 2 7 64.96 119.63 20.95 o 1 2 7 1510.85 1849.03 41.07 o 2 2 7 84380.92 88391.84 669.83 o 3 2 7 25663.51 25776.46 209.21 o 4 2 7 16400.68 16495.11 156.71 o 5 2 7 10185.51 10869.08 119.25 o 6 2 7 4525.53 4704.24 68.91 o -6 3 7 25193.75 26886.77 247.25 o -5 3 7 9253.60 8017.55 98.49 o -4 3 7 970.92 1652.51 51.29 o -3 3 7 10861.04 11647.47 123.39 o -2 3 7 9111.14 10217.22 110.26 o -1 3 7 3518.51 3387.82 57.30 o 0 3 7 844.22 810.82 34.84 o 1 3 7 3313.93 3053.68 59.45 o 2 3 7 7968.25 9104.73 94.67 o 3 3 7 11438.41 12091.70 124.86 o 4 3 7 1360.33 2138.59 48.56 o 5 3 7 9519.51 8570.69 107.09 o 6 3 7 25157.05 26680.77 252.87 o -6 4 7 17490.40 16822.75 173.93 o -5 4 7 17324.44 17773.40 170.26 o -4 4 7 5486.76 5314.65 73.13 o -3 4 7 10379.56 9738.81 110.18 o -2 4 7 30801.43 30847.37 264.27 o -1 4 7 890.64 945.48 33.64 o 0 4 7 47227.33 44520.76 354.67 o 1 4 7 1024.70 1134.73 38.60 o 2 4 7 30573.20 30622.72 262.87 o 3 4 7 9636.65 8858.45 103.03 o 4 4 7 5331.83 5298.23 80.66 o 5 4 7 16174.30 16736.46 178.62 o 6 4 7 17747.19 17072.60 176.36 o -6 5 7 21962.20 22467.28 204.46 o -5 5 7 10610.64 12822.82 133.30 o -4 5 7 10266.54 10376.57 116.41 o -3 5 7 26002.54 24552.28 227.89 o -2 5 7 1077.48 1398.82 40.76 o -1 5 7 3892.45 4194.31 65.43 o 0 5 7 22763.60 21931.17 201.01 o 1 5 7 3575.17 3779.09 64.61 o 2 5 7 780.22 971.95 37.30 o 3 5 7 25551.91 24166.81 218.33 o 4 5 7 10152.48 10060.25 125.13 o 5 5 7 10874.46 13030.82 150.32 o 6 5 7 22115.52 22160.89 237.14 o -6 6 7 4696.39 5327.86 79.74 o -5 6 7 41566.76 46561.86 379.85 o -4 6 7 788.20 730.97 37.10 o -3 6 7 38680.77 39744.26 345.80 o -2 6 7 1106.59 1000.84 37.12 o -1 6 7 37877.40 39446.07 341.50 o 0 6 7 1202.67 1889.43 52.15 o 1 6 7 38178.09 38669.25 339.73 o 2 6 7 988.16 842.34 35.31 o 3 6 7 38797.42 39164.63 352.55 o 4 6 7 740.86 684.51 35.80 o 5 6 7 41764.38 46952.40 426.13 o 6 6 7 4422.96 5005.66 101.31 o -7 7 7 381.35 378.30 74.33 o -6 7 7 2671.89 2278.73 57.86 o -5 7 7 2244.34 1966.06 52.05 o -4 7 7 18624.27 20212.83 198.70 o -3 7 7 19700.86 21828.14 261.40 o -2 7 7 6092.13 5734.80 89.66 o -1 7 7 6122.61 5734.86 83.79 o 0 7 7 30449.24 32317.15 282.66 o 1 7 7 6192.70 5781.46 82.28 o 2 7 7 5558.12 5145.41 79.88 o 3 7 7 19429.26 21706.36 210.11 o 4 7 7 17932.53 19161.21 206.69 o 5 7 7 2172.23 1823.37 57.82 o 6 7 7 2483.15 1950.17 63.05 o 7 7 7 410.11 307.37 119.59 o 0 0 8 51919.75 48862.66 558.35 o 1 0 8 22475.42 22769.39 209.25 o 2 0 8 34790.49 38235.10 318.51 o 3 0 8 192.65 581.27 27.99 o 4 0 8 143612.08 140533.14 1108.21 o 5 0 8 5398.98 8439.86 103.26 o 6 0 8 59845.96 62397.98 537.32 o 7 0 8 90.11 -27.59 27.59 o -7 1 8 947.21 858.03 38.57 o -6 1 8 4105.10 4428.49 79.27 o -5 1 8 16814.19 17437.45 170.65 o -4 1 8 5917.37 6543.88 89.78 o -3 1 8 4105.68 4068.41 66.19 o -2 1 8 1420.10 1597.97 41.23 o -1 1 8 14784.49 15931.90 160.65 o 0 1 8 6602.53 7002.11 94.51 o 1 1 8 15067.72 16204.90 165.30 o 2 1 8 1351.47 1488.27 34.40 o 3 1 8 4439.79 4403.77 57.17 o 4 1 8 6073.24 6668.29 81.55 o 5 1 8 16333.95 17181.46 165.58 o 6 1 8 4221.69 4600.33 77.04 o 7 1 8 861.32 693.44 40.71 o -7 2 8 897.01 1109.92 47.84 o -6 2 8 113199.48 112931.35 981.02 o -5 2 8 4352.10 6049.38 81.88 o -4 2 8 53695.91 54866.91 455.06 o -3 2 8 1903.43 2202.43 53.83 o -2 2 8 39144.59 35939.14 346.56 o -1 2 8 10410.24 10842.15 130.70 o 0 2 8 53417.28 56678.76 538.64 o 1 2 8 9839.90 10134.66 125.81 o 2 2 8 40244.36 36644.82 304.78 o 3 2 8 1634.05 1830.83 40.38 o 4 2 8 52651.40 53710.29 425.87 o 5 2 8 4344.27 6201.01 83.82 o 6 2 8 112643.84 110245.88 886.27 o 7 2 8 1045.93 1192.74 40.66 o -7 3 8 14445.61 14084.42 162.08 o -6 3 8 14789.16 15432.10 165.07 o -5 3 8 1130.03 1270.12 39.98 o -4 3 8 1516.45 1299.12 42.22 o -3 3 8 6964.10 6281.16 92.40 o -2 3 8 14005.73 15103.40 159.98 o -1 3 8 58763.01 58649.63 518.90 o 0 3 8 8469.06 8924.32 114.46 o 1 3 8 60162.01 59456.33 503.23 o 2 3 8 14226.67 15114.11 142.24 o 3 3 8 6883.97 5921.01 77.08 o 4 3 8 1628.09 1505.87 39.67 o 5 3 8 1453.43 1525.64 44.30 o 6 3 8 14584.92 15057.36 159.97 o 7 3 8 14139.33 13544.18 155.53 o -7 4 8 676.91 783.49 42.92 o -6 4 8 27928.26 30068.56 286.34 o -5 4 8 9141.22 9019.86 135.31 o -4 4 8 141372.61 145672.55 1134.20 o -3 4 8 16103.67 18188.61 187.39 o -2 4 8 90621.87 92961.02 716.35 o -1 4 8 11236.97 10516.75 128.10 o 0 4 8 12085.96 10734.77 122.80 o 1 4 8 10907.57 10199.77 122.06 o 2 4 8 89048.71 90670.91 758.35 o 3 4 8 16541.36 18293.42 178.86 o 4 4 8 141155.88 142457.52 1129.62 o 5 4 8 9650.19 9767.67 116.72 o 6 4 8 28513.54 30921.08 299.24 o 7 4 8 657.21 752.89 43.24 o -7 5 8 48459.67 50480.71 422.34 o -6 5 8 10001.64 11840.98 138.17 o -5 5 8 32214.45 32256.49 272.25 o -4 5 8 468.76 424.21 34.76 o -3 5 8 8241.79 7920.41 104.91 o -2 5 8 2238.14 2738.21 61.59 o -1 5 8 6870.84 5096.42 81.94 o 0 5 8 9.98 49.97 23.52 o 1 5 8 6366.24 4810.55 80.09 o 2 5 8 2479.68 2894.08 57.33 o 3 5 8 8717.48 8328.12 103.21 o 4 5 8 564.77 593.62 34.51 o 5 5 8 32777.18 32999.27 304.58 o 6 5 8 9535.17 11357.64 134.47 o 7 5 8 48167.64 49278.05 456.56 o -7 6 8 4448.99 4876.16 88.84 o -6 6 8 35514.49 28943.25 268.99 o -5 6 8 950.16 1197.43 41.75 o -4 6 8 48396.85 45887.12 376.22 o -3 6 8 5276.24 5266.70 88.15 o -2 6 8 50207.85 50877.54 429.13 o -1 6 8 14254.07 14661.03 162.36 o 0 6 8 22155.09 19958.71 206.48 o 1 6 8 13578.39 14073.82 154.53 o 2 6 8 49194.97 49084.13 436.24 o 3 6 8 5356.33 5268.70 85.29 o 4 6 8 45491.23 42691.82 393.30 o 5 6 8 836.64 1095.96 46.49 o 6 6 8 37713.32 30785.50 306.42 o 7 6 8 4644.19 5123.29 101.98 o -7 7 8 6378.02 6894.08 103.26 o -6 7 8 3215.90 3718.83 70.77 o -5 7 8 4177.18 5020.55 80.89 o -4 7 8 12130.93 12716.38 164.54 o -3 7 8 36616.00 37484.64 383.71 o -2 7 8 8433.11 8901.01 126.31 o -1 7 8 3638.78 5008.92 89.16 o 0 7 8 25599.50 25122.76 240.56 o 1 7 8 3245.49 4271.67 77.85 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