#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211553.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211553_Fobs loop_ _publ_author_name 'Meijboom, Reinout' _publ_section_title ; Di-\m-iodo-tris(tri-p-tolylphosphine)-1\kP,2\k^2^P-dicopper(I) ; _journal_coeditor_code NG2164 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3511 _journal_page_last m3513 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.812 _cell_angle_beta 90.643 _cell_angle_gamma 108.538 _cell_length_a 11.0334 _cell_length_b 13.7572 _cell_length_c 20.7319 _exptl_crystal_F_000 1300.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ng2164Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 344.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4254.63 4492.78 110.28 o 2 0 0 22529.98 22056.18 504.95 o 3 0 0 45644.98 44953.84 1013.80 o 4 0 0 36272.45 34430.81 791.91 o 5 0 0 3522.64 3406.01 122.87 o 6 0 0 10.58 9.69 38.32 o 7 0 0 5365.29 5493.66 186.47 o 8 0 0 2437.14 2078.96 127.77 o 9 0 0 188.25 205.41 71.07 o 10 0 0 312.35 350.67 84.55 o 11 0 0 290.07 425.19 95.69 o 12 0 0 20.12 96.58 95.24 o 13 0 0 220.56 379.41 117.08 o -13 1 0 15.62 -114.40 104.38 o -12 1 0 297.72 232.26 97.36 o -11 1 0 90.76 36.65 81.65 o -10 1 0 26.04 27.74 69.06 o -9 1 0 77.70 11.47 59.60 o -7 1 0 1291.03 1219.55 89.00 o -6 1 0 1729.68 1573.34 87.67 o -5 1 0 5554.25 5546.46 167.43 o -4 1 0 18815.25 17766.60 308.56 o -3 1 0 2876.17 3044.77 66.75 o -2 1 0 8388.09 8484.52 200.78 o -1 1 0 59879.96 60398.75 802.82 o 0 1 0 5.80 17.38 5.57 o 1 1 0 8141.68 8370.32 196.95 o 2 1 0 14864.53 15404.46 359.14 o 3 1 0 144.31 129.22 26.51 o 4 1 0 8231.25 8344.70 223.46 o 5 1 0 9039.53 7962.95 224.46 o 6 1 0 5928.03 5771.03 183.58 o 7 1 0 13.91 45.56 48.57 o 8 1 0 3175.75 2873.76 144.92 o 9 1 0 6655.43 6687.14 238.61 o 10 1 0 388.48 398.68 86.11 o 11 1 0 350.10 266.12 94.24 o 12 1 0 1645.33 1568.89 155.73 o 13 1 0 263.54 69.40 120.08 o -14 2 0 132.96 236.27 126.88 o -13 2 0 169.03 267.68 115.52 o -12 2 0 221.58 202.85 95.24 o -11 2 0 771.07 848.38 106.49 o -10 2 0 1783.07 1767.39 127.99 o -9 2 0 0.78 -5.12 52.13 o -8 2 0 159.34 156.84 58.04 o -7 2 0 3714.28 3669.01 139.69 o -6 2 0 5410.01 5279.85 129.27 o -5 2 0 2232.16 2243.87 65.97 o -4 2 0 2236.72 2233.38 46.60 o -3 2 0 8816.26 8996.56 128.70 o -2 2 0 3305.27 3324.25 52.40 o -1 2 0 1055.83 1091.47 46.17 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95.43 o 7 3 0 1886.58 1662.48 74.53 o 8 3 0 385.92 429.91 49.45 o 9 3 0 927.23 830.76 65.65 o 10 3 0 848.46 1046.22 112.29 o 11 3 0 440.89 486.91 108.94 o 12 3 0 17.86 -101.37 109.72 o -14 4 0 24.18 -42.11 112.95 o -13 4 0 1187.56 1327.27 145.26 o -12 4 0 821.54 803.60 111.95 o -11 4 0 137.60 124.32 79.76 o -10 4 0 757.42 756.37 92.35 o -9 4 0 6151.41 6015.30 267.40 o -8 4 0 2046.87 1958.66 99.36 o -7 4 0 1.64 8.89 30.20 o -6 4 0 2224.16 2280.91 55.34 o -5 4 0 15027.01 15140.82 216.57 o -4 4 0 2296.78 2491.30 52.26 o -3 4 0 13043.99 13142.03 235.44 o -2 4 0 1223.84 1307.35 30.05 o -1 4 0 5804.39 6452.66 171.44 o 0 4 0 28024.43 29779.24 541.32 o 1 4 0 1500.18 1501.34 60.99 o 2 4 0 1197.99 1144.27 41.75 o 3 4 0 427.50 367.24 40.10 o 4 4 0 9774.46 9988.82 189.06 o 5 4 0 24.71 86.83 31.25 o 6 4 0 201.51 281.51 40.49 o 7 4 0 29.03 5.17 38.38 o 8 4 0 133.26 104.81 44.53 o 9 4 0 105.48 42.57 49.06 o 10 4 0 159.10 316.27 63.62 o 11 4 0 391.14 351.23 108.83 o 12 4 0 113.21 -12.70 120.42 o -14 5 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7 0 4376.44 4263.42 146.82 o 1 7 0 17957.20 17336.87 298.29 o 2 7 0 67.53 23.31 28.63 o 3 7 0 3.85 50.50 29.52 o 4 7 0 2731.26 2657.32 88.31 o 5 7 0 171.25 92.94 137.13 o 6 7 0 525.80 440.95 54.73 o 7 7 0 50.09 47.06 49.74 o 8 7 0 38.56 53.16 58.08 o 9 7 0 187.69 244.72 83.49 o 10 7 0 235.34 299.68 82.90 o -14 8 0 58.52 102.59 128.55 o -13 8 0 194.04 238.61 82.81 o -12 8 0 87.13 174.05 69.02 o -11 8 0 224.89 235.84 94.02 o -10 8 0 59.34 78.43 48.30 o -9 8 0 1653.04 1758.46 87.45 o -8 8 0 579.44 698.89 43.56 o -7 8 0 9.78 -9.73 27.32 o -6 8 0 136.31 112.42 27.85 o -5 8 0 5642.28 5450.29 99.25 o -4 8 0 1073.80 1025.65 41.24 o -3 8 0 731.41 756.37 69.06 o -2 8 0 1276.21 1268.12 83.99 o -1 8 0 1270.93 1193.04 83.43 o 0 8 0 45.37 40.44 41.77 o 1 8 0 171.11 110.41 26.49 o 2 8 0 1791.73 1829.87 103.60 o 3 8 0 773.04 792.82 54.66 o 4 8 0 1090.92 1144.71 66.63 o 5 8 0 957.14 907.52 150.33 o 6 8 0 977.72 957.31 69.66 o 7 8 0 675.93 816.52 72.92 o 8 8 0 83.12 92.65 61.83 o 9 8 0 167.44 159.29 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131.75 106.38 85.89 o -1 15 0 604.04 443.69 99.36 o 0 15 0 96.49 170.77 103.37 o 1 15 0 753.67 702.68 121.09 o 2 15 0 7.72 61.94 102.26 o 3 15 0 515.81 277.15 124.09 o -10 16 0 2.56 116.30 116.63 o -9 16 0 26.33 11.47 111.39 o -8 16 0 18.03 -69.84 102.59 o -7 16 0 504.05 526.81 78.47 o -6 16 0 126.75 104.09 104.15 o -5 16 0 192.47 168.46 70.79 o -4 16 0 192.96 334.08 71.39 o -3 16 0 1216.21 1068.50 134.56 o -2 16 0 10.43 -80.65 95.35 o -1 16 0 25.06 19.72 94.02 o 0 16 0 1145.02 1105.71 138.80 o 1 16 0 319.71 402.69 126.43 o -8 17 0 326.52 202.52 119.42 o -7 17 0 580.12 732.64 136.24 o -6 17 0 1.86 -9.61 106.16 o -5 17 0 16.61 -53.33 73.18 o -4 17 0 444.03 440.51 82.15 o -3 17 0 50.57 139.13 112.06 o -2 17 0 17.73 158.96 109.06 o -1 17 0 42.38 103.49 114.96 o 1 -17 1 59.07 65.28 109.50 o 2 -17 1 60.18 78.98 105.83 o 3 -17 1 507.97 617.35 119.42 o 4 -17 1 138.42 88.70 78.76 o 5 -17 1 39.03 -71.48 159.57 o 6 -17 1 70.88 62.76 77.31 o 7 -17 1 111.48 214.10 111.51 o 8 -17 1 12.97 -6.13 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