#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/15/2211597.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211597_Fobs loop_ _publ_author_name 'Kyzio\/l, Janusz B.' 'Nog\/ly, Przemys\/law' 'Daszkiewicz, Zdzis\/law' 'Zaleski, Jacek' _publ_section_title ; 1,5-Dimethyl-2-nitrimino-1,2-dihydropyridine ; _journal_coeditor_code SG2078 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5485 _journal_page_last o5487 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.586 _cell_angle_gamma 90.000 _cell_length_a 14.3053 _cell_length_b 7.6741 _cell_length_c 15.7895 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file sg20781sup2.hkl _[local]_cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 4286.97 4237.23 19.44 o 6 0 0 3700.28 3879.78 20.99 o 8 0 0 842.95 927.25 14.72 o 10 0 0 1.94 5.78 3.73 o 12 0 0 331.31 362.30 18.66 o 14 0 0 292.94 306.32 19.44 o 16 0 0 82.28 95.63 16.33 o 1 1 0 1460.14 1450.76 7.00 o 3 1 0 7392.77 6742.23 66.71 o 5 1 0 24.54 22.00 1.81 o 7 1 0 30.86 47.79 2.96 o 9 1 0 59.28 40.82 4.40 o 11 1 0 1137.89 1153.99 19.10 o 13 1 0 97.75 104.18 9.52 o 15 1 0 185.30 196.70 11.95 o 0 2 0 16543.38 15840.90 234.41 o 2 2 0 2461.19 2252.01 28.84 o 4 2 0 346.25 340.50 4.12 o 6 2 0 344.80 331.06 10.15 o 8 2 0 9.35 5.05 2.47 o 10 2 0 0.19 4.59 2.93 o 12 2 0 172.71 159.33 7.62 o 14 2 0 870.31 926.38 18.59 o 16 2 0 145.85 132.27 10.07 o 1 3 0 59.28 77.96 2.78 o 3 3 0 864.37 874.97 19.09 o 5 3 0 923.81 936.72 11.39 o 7 3 0 28.15 22.80 2.60 o 9 3 0 5.61 12.13 3.44 o 11 3 0 3.21 2.49 2.59 o 13 3 0 402.55 393.90 13.45 o 15 3 0 138.73 146.16 18.66 o 0 4 0 6740.10 6493.84 175.83 o 2 4 0 1.13 3.48 1.82 o 4 4 0 3348.92 3507.23 38.29 o 6 4 0 197.67 194.75 6.30 o 8 4 0 366.91 392.77 12.64 o 10 4 0 56.73 47.47 5.29 o 12 4 0 624.96 648.80 25.66 o 14 4 0 378.39 364.63 21.77 o 1 5 0 1479.61 1435.04 28.55 o 3 5 0 1810.75 1797.25 18.71 o 5 5 0 129.82 118.00 7.69 o 7 5 0 28.05 29.64 4.46 o 9 5 0 264.89 224.41 8.64 o 11 5 0 314.70 356.44 11.80 o 13 5 0 121.07 108.67 10.95 o 0 6 0 194.39 190.09 12.09 o 2 6 0 788.19 806.39 30.97 o 4 6 0 1503.70 1588.16 16.07 o 6 6 0 0.30 3.38 2.37 o 8 6 0 24.42 10.29 3.52 o 10 6 0 404.55 335.37 12.58 o 12 6 0 15.47 19.81 7.89 o 1 7 0 82.51 84.11 7.97 o 3 7 0 0.76 1.89 2.56 o 5 7 0 0.40 2.03 2.06 o 7 7 0 0.22 2.59 3.14 o 9 7 0 445.39 474.50 15.16 o 11 7 0 167.78 154.72 17.10 o 0 8 0 0.23 5.11 3.73 o 2 8 0 353.99 375.35 11.65 o 4 8 0 542.17 540.58 12.55 o 6 8 0 10.70 10.48 5.59 o 8 8 0 17.44 16.57 5.14 o 1 9 0 355.71 346.98 11.65 o 3 9 0 371.99 362.93 12.10 o 5 9 0 3.73 6.24 4.38 o -15 1 1 1.67 4.66 4.10 o -13 1 1 33.51 35.32 6.86 o -11 1 1 0.01 4.66 2.59 o -9 1 1 39.14 33.49 2.89 o -7 1 1 1007.14 1017.39 6.48 o -5 1 1 489.84 614.35 13.28 o -3 1 1 22.82 34.32 4.75 o -1 1 1 2714.52 2671.40 10.11 o 1 1 1 28.35 44.08 5.09 o 3 1 1 518.24 447.91 11.42 o 5 1 1 263.99 278.57 6.73 o 7 1 1 231.29 271.59 6.10 o 9 1 1 498.14 446.82 11.60 o 11 1 1 53.91 47.05 10.89 o 13 1 1 622.36 691.60 15.05 o 15 1 1 84.72 94.17 10.71 o -16 2 1 1.10 7.93 5.18 o -14 2 1 65.90 42.36 6.30 o -12 2 1 0.94 3.37 2.69 o -10 2 1 41.90 56.39 5.40 o -8 2 1 581.58 603.41 10.02 o -6 2 1 5496.08 5783.11 53.95 o -4 2 1 455.12 415.41 3.32 o -2 2 1 79557.55 75363.00 829.43 o 0 2 1 21268.16 21594.82 299.50 o 2 2 1 812.09 869.44 6.20 o 4 2 1 2032.59 2073.61 15.82 o 6 2 1 1037.29 1178.88 17.84 o 8 2 1 22.26 20.95 4.48 o 10 2 1 899.11 868.15 17.11 o 12 2 1 2444.94 2559.87 58.31 o 14 2 1 225.45 230.20 12.61 o -15 3 1 53.46 45.09 12.44 o -13 3 1 226.19 236.40 11.27 o -11 3 1 338.01 260.37 9.64 o -9 3 1 23.25 35.31 4.70 o -7 3 1 429.50 403.62 4.47 o -5 3 1 326.52 288.28 3.82 o -3 3 1 8297.97 8272.35 63.73 o -1 3 1 2731.12 2830.84 20.76 o 1 3 1 4891.91 4560.74 37.09 o 3 3 1 1319.25 1306.75 13.31 o 5 3 1 21.25 33.41 2.87 o 7 3 1 70.07 55.53 5.05 o 9 3 1 2089.81 2033.52 16.94 o 11 3 1 34.37 20.73 5.01 o 13 3 1 2829.08 3140.99 37.32 o 15 3 1 67.05 59.87 16.33 o -14 4 1 389.18 399.75 15.05 o -12 4 1 106.79 92.09 10.40 o -10 4 1 23.40 10.52 5.20 o -8 4 1 15.68 12.01 5.72 o -6 4 1 1054.49 1080.38 9.84 o -4 4 1 615.67 591.87 13.18 o -2 4 1 480.81 453.73 5.32 o 0 4 1 63.53 69.98 2.40 o 2 4 1 5.16 4.24 1.80 o 4 4 1 540.53 575.74 8.41 o 6 4 1 134.78 115.62 5.59 o 8 4 1 79.92 67.16 5.73 o 10 4 1 84.27 90.57 5.84 o 12 4 1 366.11 359.29 23.32 o 14 4 1 281.54 283.78 18.66 o -13 5 1 9.83 12.36 6.07 o -11 5 1 668.70 690.94 13.48 o -9 5 1 13.04 12.54 3.85 o -7 5 1 34.90 39.70 4.16 o -5 5 1 406.26 458.85 18.00 o -3 5 1 230.16 269.42 6.34 o -1 5 1 797.63 756.11 9.99 o 1 5 1 68.60 64.27 4.90 o 3 5 1 54.42 49.04 3.93 o 5 5 1 3.96 16.58 7.26 o 7 5 1 42.92 39.06 4.99 o 9 5 1 36.49 18.44 3.68 o 11 5 1 54.08 56.57 7.66 o 13 5 1 492.45 594.59 17.02 o -12 6 1 1.96 5.57 4.90 o -10 6 1 13.34 4.00 3.83 o -8 6 1 0.33 3.85 2.28 o -6 6 1 3.36 3.89 2.99 o -4 6 1 0.03 2.94 2.89 o -2 6 1 200.46 185.72 8.44 o 0 6 1 554.36 538.98 9.94 o 2 6 1 2.83 2.64 2.59 o 4 6 1 1.74 3.33 2.75 o 6 6 1 187.51 166.55 8.57 o 8 6 1 3.66 2.56 2.69 o 10 6 1 44.09 36.96 7.00 o 12 6 1 308.97 288.02 13.61 o -11 7 1 38.81 20.25 8.94 o -9 7 1 75.71 63.72 10.50 o -7 7 1 20.34 15.86 4.44 o -5 7 1 309.57 287.56 9.79 o -3 7 1 1343.65 1403.90 27.83 o -1 7 1 11.93 4.98 3.16 o 1 7 1 1198.23 1242.37 20.35 o 3 7 1 54.10 45.16 6.98 o 5 7 1 7.62 7.44 3.83 o 7 7 1 1.14 3.27 3.29 o 9 7 1 725.50 799.92 16.94 o 11 7 1 296.12 272.12 21.77 o -8 8 1 1.35 2.38 4.30 o -6 8 1 230.67 229.00 9.81 o -4 8 1 19.69 11.14 4.04 o -2 8 1 482.36 524.07 11.61 o 0 8 1 1.02 2.18 2.47 o 2 8 1 36.19 41.36 6.25 o 4 8 1 50.57 42.19 5.60 o 6 8 1 0.00 1.03 2.82 o 8 8 1 16.85 6.59 5.20 o -5 9 1 8.24 9.45 5.24 o -3 9 1 50.71 40.56 6.61 o -1 9 1 235.06 219.47 11.05 o 1 9 1 112.63 101.62 8.96 o 3 9 1 23.90 12.55 4.53 o 5 9 1 70.96 60.07 8.80 o -16 0 2 89.98 60.64 11.66 o -14 0 2 99.53 83.97 13.22 o -12 0 2 69.60 52.87 12.44 o -10 0 2 94.74 93.52 5.55 o -8 0 2 4782.04 5149.50 176.77 o -6 0 2 13454.65 13122.64 260.84 o -4 0 2 4419.73 4238.93 85.13 o 0 0 2 81.80 14.77 1.55 o 2 0 2 1381.31 1314.05 37.23 o 4 0 2 1.66 2.90 3.89 o 6 0 2 192.11 234.62 33.04 o 8 0 2 535.47 547.42 15.94 o 10 0 2 5636.35 5575.92 106.13 o 12 0 2 4095.53 4173.70 78.14 o 14 0 2 139.98 167.93 16.33 o -17 1 2 24.69 15.27 6.86 o -15 1 2 26.07 17.70 5.75 o -13 1 2 140.14 102.80 8.40 o -11 1 2 101.15 116.84 7.15 o -9 1 2 485.11 493.85 5.85 o -7 1 2 2191.95 2372.01 38.10 o -5 1 2 14.00 23.98 1.76 o -3 1 2 23394.43 22492.14 328.08 o -1 1 2 5480.84 5325.40 36.70 o 1 1 2 961.76 979.50 7.85 o 3 1 2 317.89 286.02 8.19 o 5 1 2 157.83 138.58 5.72 o 7 1 2 886.72 888.71 18.86 o 9 1 2 56.39 47.24 5.29 o 11 1 2 3292.90 3366.80 31.10 o 13 1 2 574.28 604.10 12.65 o 15 1 2 105.20 128.28 11.51 o -16 2 2 16.85 11.46 5.83 o -14 2 2 197.64 163.61 10.40 o -12 2 2 33.36 22.36 4.22 o -10 2 2 2.29 4.09 2.62 o -8 2 2 637.47 682.19 18.23 o -6 2 2 2882.12 3002.38 18.71 o -4 2 2 6338.71 6522.43 41.15 o -2 2 2 19498.07 19101.26 48.02 o 0 2 2 489.25 474.09 10.21 o 2 2 2 580.44 604.25 19.75 o 4 2 2 310.65 291.58 4.48 o 6 2 2 55.52 73.65 4.54 o 8 2 2 102.11 99.25 5.81 o 10 2 2 2.18 1.72 2.22 o 12 2 2 13.41 7.48 3.80 o 14 2 2 34.07 31.46 10.88 o -15 3 2 10.20 4.66 5.44 o -13 3 2 427.37 407.85 13.71 o -11 3 2 205.78 207.20 7.97 o -9 3 2 27.25 25.21 4.20 o -7 3 2 651.92 673.91 6.08 o -5 3 2 1939.02 2000.61 26.08 o -3 3 2 427.65 450.04 14.12 o -1 3 2 800.09 799.61 8.13 o 1 3 2 3286.72 3203.62 36.70 o 3 3 2 1905.12 1831.92 37.22 o 5 3 2 138.09 151.11 8.78 o 7 3 2 8.87 13.98 3.22 o 9 3 2 72.52 58.15 8.87 o 11 3 2 512.19 467.31 21.27 o 13 3 2 576.27 650.74 24.10 o -14 4 2 46.99 32.21 9.06 o -12 4 2 327.66 252.68 11.54 o -10 4 2 52.34 46.81 10.85 o -8 4 2 16.79 24.64 4.16 o -6 4 2 55.16 52.97 4.01 o -4 4 2 4379.85 4579.98 39.05 o -2 4 2 8881.44 8983.02 39.73 o 0 4 2 2523.22 2522.34 26.72 o 2 4 2 639.31 626.53 10.52 o 4 4 2 495.16 508.27 9.89 o 6 4 2 6.67 3.85 2.00 o 8 4 2 2.41 7.72 3.18 o 10 4 2 1100.81 1130.66 13.35 o 12 4 2 1180.11 1296.65 28.77 o 14 4 2 21.78 10.88 10.88 o -13 5 2 27.55 16.33 5.87 o -11 5 2 7.65 3.61 3.27 o -9 5 2 2.43 4.19 3.04 o -7 5 2 2.53 1.86 1.91 o -5 5 2 1212.75 1225.04 16.83 o -3 5 2 2329.13 2409.82 10.91 o -1 5 2 1199.48 1167.44 24.56 o 1 5 2 2561.65 2520.06 64.39 o 3 5 2 106.73 103.92 5.58 o 5 5 2 0.59 4.98 2.81 o 7 5 2 2556.80 2507.62 44.81 o 9 5 2 2126.58 2161.43 21.19 o 11 5 2 31.14 33.43 7.29 o 13 5 2 13.73 11.24 5.97 o -12 6 2 36.50 16.33 6.41 o -10 6 2 25.38 10.53 4.31 o -8 6 2 7.02 5.29 2.80 o -6 6 2 122.55 124.27 11.03 o -4 6 2 180.78 194.72 8.09 o -2 6 2 2.79 7.82 2.92 o 0 6 2 899.40 897.28 17.57 o 2 6 2 1752.41 1867.95 26.10 o 4 6 2 91.73 71.37 9.57 o 6 6 2 51.16 52.71 11.58 o 8 6 2 16.92 24.75 4.61 o 10 6 2 2.40 1.85 3.16 o 12 6 2 30.08 40.53 9.71 o -11 7 2 64.87 58.46 23.71 o -9 7 2 35.70 42.67 9.33 o -7 7 2 11.96 9.59 4.04 o -5 7 2 42.36 25.84 5.05 o -3 7 2 473.50 478.38 15.04 o -1 7 2 255.56 267.36 8.51 o 1 7 2 32.37 28.61 5.07 o 3 7 2 113.38 95.58 7.89 o 5 7 2 0.04 4.15 3.16 o 7 7 2 963.51 978.44 18.47 o 9 7 2 70.01 61.78 10.16 o -10 8 2 92.69 114.83 13.06 o -8 8 2 0.56 3.42 3.88 o -6 8 2 237.40 229.69 9.57 o -4 8 2 1033.15 1110.44 15.63 o -2 8 2 2.44 3.80 2.50 o 0 8 2 26.01 20.85 6.16 o 2 8 2 244.11 263.42 10.85 o 4 8 2 29.54 19.33 4.53 o 6 8 2 9.90 5.41 5.75 o 8 8 2 0.53 6.22 4.40 o -7 9 2 64.34 41.92 10.27 o -5 9 2 744.50 806.53 25.72 o -3 9 2 171.99 203.86 11.50 o -1 9 2 28.01 25.43 6.62 o 1 9 2 1.28 3.06 3.99 o 3 9 2 98.33 78.61 7.74 o 5 9 2 19.38 17.19 9.61 o -17 1 3 63.08 54.11 8.03 o -15 1 3 16.61 3.89 3.85 o -13 1 3 537.37 495.13 10.20 o -11 1 3 1.74 1.89 2.26 o -9 1 3 988.51 1092.52 17.79 o -7 1 3 6382.19 6314.91 64.56 o -5 1 3 538.01 475.23 5.27 o -3 1 3 4664.47 4438.62 42.07 o -1 1 3 2390.91 2451.11 40.96 o 1 1 3 4148.52 3989.06 28.32 o 3 1 3 227.36 234.80 6.28 o 5 1 3 37.01 28.48 3.17 o 7 1 3 252.72 243.53 14.25 o 9 1 3 4.20 5.36 2.68 o 11 1 3 143.97 158.59 8.64 o 13 1 3 42.08 40.04 5.83 o 15 1 3 182.68 212.10 12.44 o -16 2 3 44.98 40.15 9.61 o -14 2 3 544.05 457.65 10.55 o -12 2 3 1282.86 1167.67 25.50 o -10 2 3 523.87 585.28 9.55 o -8 2 3 440.61 413.36 5.11 o -6 2 3 491.96 457.22 6.83 o -4 2 3 284.22 311.73 3.13 o -2 2 3 3244.25 2977.49 32.39 o 0 2 3 699.85 641.99 10.55 o 2 2 3 538.30 461.30 7.83 o 4 2 3 150.54 147.71 8.42 o 6 2 3 445.81 421.85 18.16 o 8 2 3 802.63 777.62 19.53 o 10 2 3 7409.54 7583.14 91.74 o 12 2 3 714.51 693.89 10.59 o 14 2 3 224.67 249.10 14.77 o -15 3 3 8.12 3.11 4.66 o -13 3 3 211.96 231.05 12.83 o -11 3 3 57.51 32.78 5.65 o -9 3 3 243.95 292.62 7.22 o -7 3 3 1010.77 992.09 10.73 o -5 3 3 5861.70 5769.36 60.65 o -3 3 3 1440.61 1426.66 16.69 o -1 3 3 2517.87 2423.63 28.28 o 1 3 3 220.78 182.78 3.82 o 3 3 3 6.54 21.69 2.78 o 5 3 3 1369.95 1398.15 10.26 o 7 3 3 909.54 950.39 35.69 o 9 3 3 50.41 38.87 4.19 o 11 3 3 13.10 6.64 3.22 o 13 3 3 359.21 430.72 21.77 o -16 4 3 43.34 16.33 9.33 o -14 4 3 19.88 7.77 5.50 o -12 4 3 162.94 124.80 16.33 o -10 4 3 0.48 5.34 3.53 o -8 4 3 298.61 283.17 7.39 o -6 4 3 1152.22 1138.28 25.74 o -4 4 3 9089.33 9497.92 34.11 o -2 4 3 32.01 22.38 2.55 o 0 4 3 3410.37 3659.01 39.16 o 2 4 3 124.60 102.33 4.07 o 4 4 3 19.35 24.01 2.85 o 6 4 3 16.08 9.56 2.98 o 8 4 3 90.86 78.67 5.81 o 10 4 3 286.63 305.59 15.57 o 12 4 3 163.52 188.41 11.95 o -15 5 3 232.05 214.37 11.62 o -13 5 3 159.24 160.58 8.28 o -11 5 3 121.24 110.69 9.83 o -9 5 3 86.59 60.11 6.75 o -7 5 3 36.96 31.28 4.18 o -5 5 3 113.05 122.58 12.65 o -3 5 3 105.09 89.26 4.15 o -1 5 3 823.29 769.22 26.87 o 1 5 3 787.24 783.53 22.21 o 3 5 3 63.82 61.32 4.70 o 5 5 3 668.28 667.70 9.17 o 7 5 3 349.68 350.58 7.31 o 9 5 3 21.56 16.34 4.69 o 11 5 3 22.43 16.33 4.97 o -14 6 3 6.17 5.70 3.75 o -12 6 3 234.91 237.38 10.17 o -10 6 3 52.28 34.77 6.18 o -8 6 3 85.49 72.31 9.16 o -6 6 3 332.99 363.20 19.64 o -4 6 3 265.31 247.82 8.81 o -2 6 3 661.01 657.36 21.88 o 0 6 3 4.14 4.35 3.36 o 2 6 3 12.95 11.69 4.08 o 4 6 3 12.27 12.56 4.06 o 6 6 3 6.85 5.59 3.16 o 8 6 3 2.41 4.03 3.69 o 10 6 3 53.91 48.08 6.93 o -11 7 3 3.04 3.61 4.46 o -9 7 3 19.00 16.48 10.88 o -7 7 3 494.12 472.39 10.73 o -5 7 3 1338.32 1431.21 37.59 o -3 7 3 15.70 9.09 3.89 o -1 7 3 414.90 408.35 10.70 o 1 7 3 12.48 14.21 5.14 o 3 7 3 174.39 162.88 7.87 o 5 7 3 135.49 114.79 10.63 o 7 7 3 495.76 505.22 15.66 o 9 7 3 155.65 153.01 12.36 o -10 8 3 64.25 55.21 10.16 o -8 8 3 36.43 33.20 7.62 o -6 8 3 74.16 67.04 11.22 o -4 8 3 661.00 717.24 24.91 o -2 8 3 61.35 56.71 7.32 o 0 8 3 518.28 523.82 12.27 o 2 8 3 2.72 2.53 2.52 o 4 8 3 11.49 8.70 5.75 o 6 8 3 41.43 34.27 8.03 o 8 8 3 14.28 6.90 6.72 o -7 9 3 174.86 158.11 15.16 o -5 9 3 309.02 309.99 16.44 o -3 9 3 996.71 1068.12 25.44 o -1 9 3 254.23 235.81 10.62 o 1 9 3 11.61 7.96 5.09 o 3 9 3 12.37 15.62 9.06 o -16 0 4 861.21 837.34 26.43 o -14 0 4 2533.83 2519.01 31.88 o -12 0 4 563.57 567.12 19.05 o -10 0 4 409.86 421.80 9.61 o -8 0 4 11.06 9.68 2.07 o -6 0 4 1912.58 1940.56 43.54 o -2 0 4 665.37 604.50 49.37 o 0 0 4 9834.14 9407.97 331.59 o 2 0 4 751.57 824.62 23.39 o 4 0 4 4173.33 4368.63 141.11 o 6 0 4 1136.69 1223.94 17.88 o 8 0 4 9535.48 9102.66 376.30 o 10 0 4 5094.73 5237.27 211.47 o 12 0 4 14.35 6.22 4.17 o 14 0 4 0.47 0.78 7.00 o -17 1 4 3.63 3.80 4.59 o -15 1 4 1028.96 1064.01 33.04 o -13 1 4 21.30 15.35 4.08 o -11 1 4 5.73 20.88 3.29 o -9 1 4 5142.13 5254.77 55.66 o -7 1 4 599.09 646.12 6.28 o -5 1 4 56.95 37.18 3.92 o -3 1 4 9268.16 9003.48 39.11 o -1 1 4 5372.00 5005.30 54.65 o 1 1 4 135.88 138.69 4.07 o 3 1 4 38.84 55.03 4.80 o 5 1 4 118.05 101.26 7.29 o 7 1 4 2568.19 2555.19 58.37 o 9 1 4 4788.33 4720.73 123.89 o 11 1 4 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