#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/15/2211598.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211598_Fobs loop_ _publ_author_name 'Kowalewski, Markus' 'Mayer, Peter' 'Schulz, Axel' 'Villinger, Alexander' _publ_section_title ; Reinvestigation of hydrazinium tetrafluoroborate ; _journal_coeditor_code SG2079 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i248 _journal_page_last i249 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.885 _cell_angle_gamma 90.000 _cell_length_a 13.8644 _cell_length_b 5.3233 _cell_length_c 12.2334 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file sg2079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jn509 in C2/c (15) shelxs97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.02 9.95 1.99 o 4 0 0 11117.73 10110.32 190.80 o 6 0 0 3644.76 4047.25 74.33 o 8 0 0 1048.02 1006.75 20.24 o 10 0 0 1052.13 976.56 22.23 o 12 0 0 0.02 4.65 1.99 o 14 0 0 0.00 0.00 4.31 o 16 0 0 85.72 100.21 17.92 o 1 1 0 2536.58 2744.85 44.61 o 3 1 0 14.27 4.48 0.66 o 5 1 0 799.94 917.92 14.43 o 7 1 0 142.59 111.66 5.97 o 9 1 0 690.06 723.37 11.70 o 11 1 0 2.15 0.00 1.41 o 13 1 0 912.56 982.91 30.02 o 15 1 0 8.34 12.43 3.56 o 0 2 0 5124.89 5230.77 108.64 o 2 2 0 4096.54 3851.88 51.05 o 4 2 0 903.87 883.88 11.61 o 6 2 0 3623.17 3789.57 58.64 o 8 2 0 259.18 258.82 4.69 o 10 2 0 69.89 63.07 2.35 o 12 2 0 5.36 2.18 1.35 o 14 2 0 19.39 7.78 3.15 o 1 3 0 776.12 833.05 12.23 o 3 3 0 1263.20 1300.14 46.95 o 5 3 0 13.85 26.55 1.17 o 7 3 0 111.53 108.86 3.15 o 9 3 0 0.79 1.00 0.70 o 11 3 0 105.32 99.05 3.31 o 13 3 0 31.65 40.63 5.15 o 0 4 0 880.25 800.36 23.56 o 2 4 0 102.70 91.71 4.81 o 4 4 0 281.10 306.09 9.29 o 6 4 0 250.03 209.42 10.12 o 8 4 0 42.01 25.33 5.48 o 10 4 0 326.78 351.16 25.55 o 12 4 0 18.63 19.78 6.80 o 1 5 0 253.18 245.55 6.97 o 3 5 0 422.45 412.65 12.11 o 5 5 0 211.44 244.55 6.93 o 7 5 0 79.73 76.99 4.31 o 9 5 0 69.23 48.56 5.48 o 11 5 0 6.61 8.81 5.63 o 0 6 0 426.46 406.48 23.89 o 2 6 0 12.49 17.25 2.65 o 4 6 0 235.25 297.91 48.61 o 6 6 0 209.59 236.25 20.08 o 8 6 0 91.67 91.59 10.89 o -15 1 1 1.80 3.98 2.31 o -13 1 1 4.03 2.81 1.41 o -11 1 1 54.49 52.48 2.65 o -9 1 1 356.54 359.14 6.75 o -7 1 1 252.55 238.51 3.87 o -5 1 1 312.40 297.73 4.22 o -3 1 1 13.94 29.72 0.94 o -1 1 1 1949.23 1960.89 32.57 o 1 1 1 5.44 16.14 0.55 o 3 1 1 3090.67 2883.10 40.05 o 5 1 1 356.64 408.18 6.79 o 7 1 1 191.12 213.42 3.97 o 9 1 1 348.01 342.85 6.92 o 11 1 1 20.94 20.61 1.59 o 13 1 1 30.25 27.58 2.22 o 15 1 1 21.95 18.35 6.80 o -16 2 1 7.29 10.61 6.57 o -14 2 1 33.97 39.09 4.65 o -12 2 1 32.90 38.06 2.55 o -10 2 1 2.70 1.63 1.33 o -8 2 1 510.00 500.95 7.56 o -6 2 1 1101.07 1047.37 13.69 o -4 2 1 13430.22 12836.57 194.71 o -2 2 1 122.89 146.33 6.97 o 0 2 1 6.28 9.34 0.80 o 2 2 1 2562.63 2518.66 34.21 o 4 2 1 538.12 582.76 8.74 o 6 2 1 2658.84 2595.24 36.02 o 8 2 1 498.71 528.46 10.62 o 10 2 1 15.87 9.80 1.83 o 12 2 1 10.13 11.52 1.51 o 14 2 1 0.18 -2.99 3.65 o -15 3 1 14.48 17.01 7.65 o -13 3 1 4.95 7.26 2.40 o -11 3 1 34.98 38.90 4.81 o -9 3 1 0.31 1.63 1.16 o -7 3 1 28.43 19.77 1.27 o -5 3 1 2834.38 2783.10 65.87 o -3 3 1 1571.39 1738.78 27.86 o -1 3 1 134.19 113.46 2.56 o 1 3 1 234.81 241.41 4.21 o 3 3 1 272.76 242.29 4.01 o 5 3 1 189.83 206.03 3.56 o 7 3 1 873.15 962.56 17.62 o 9 3 1 299.46 288.91 6.80 o 11 3 1 53.93 62.31 5.48 o 13 3 1 5.87 6.54 4.70 o -12 4 1 6.33 12.26 4.91 o -10 4 1 348.72 328.20 10.55 o -8 4 1 0.38 0.55 1.04 o -6 4 1 5.08 1.99 0.64 o -4 4 1 392.88 391.10 10.12 o -2 4 1 1479.80 1528.13 28.41 o 0 4 1 1146.81 1187.88 52.59 o 2 4 1 1485.75 1515.61 46.62 o 4 4 1 799.72 743.58 19.08 o 6 4 1 6.14 6.05 2.65 o 8 4 1 26.77 17.54 1.53 o 10 4 1 0.00 1.31 1.66 o 12 4 1 2.88 1.70 3.63 o -11 5 1 4.17 -1.14 6.30 o -9 5 1 14.05 19.86 4.01 o -7 5 1 14.92 12.55 2.58 o -5 5 1 78.55 60.40 6.30 o -3 5 1 66.24 82.14 3.47 o -1 5 1 323.78 395.20 9.62 o 1 5 1 70.99 68.02 3.32 o 3 5 1 55.29 57.99 5.31 o 5 5 1 0.80 5.48 1.98 o 7 5 1 22.77 27.79 2.81 o 9 5 1 0.06 -1.81 3.50 o -8 6 1 9.18 2.80 4.66 o -6 6 1 19.61 17.59 5.48 o -4 6 1 35.63 31.90 6.97 o -2 6 1 0.03 -1.66 1.99 o 0 6 1 23.99 25.55 2.99 o 2 6 1 1.49 1.33 2.65 o 4 6 1 2.06 4.76 2.07 o 6 6 1 9.85 4.14 3.56 o -16 0 2 186.69 233.60 20.24 o -14 0 2 5.12 5.97 1.66 o -12 0 2 158.71 172.22 6.30 o -10 0 2 106.09 108.51 3.98 o -8 0 2 3443.50 3301.97 69.02 o -6 0 2 5305.10 5126.67 99.22 o -4 0 2 3190.77 3078.99 72.34 o -2 0 2 522.09 653.03 14.27 o 0 0 2 1166.22 1192.24 26.55 o 2 0 2 6601.94 6698.18 134.72 o 4 0 2 24440.06 23196.77 638.43 o 6 0 2 316.49 291.34 6.97 o 8 0 2 1206.02 1199.87 22.23 o 10 0 2 2047.90 2102.76 46.46 o 12 0 2 87.13 83.29 3.65 o 14 0 2 340.10 386.24 24.22 o -17 1 2 51.70 38.21 14.10 o -15 1 2 114.55 113.49 11.12 o -13 1 2 83.74 86.93 5.31 o -11 1 2 61.27 75.12 2.93 o -9 1 2 2732.42 2756.06 65.54 o -7 1 2 339.24 362.23 5.74 o -5 1 2 9095.12 9038.53 138.08 o -3 1 2 13751.56 12951.94 208.15 o -1 1 2 961.37 840.45 13.99 o 1 1 2 13012.60 11497.80 220.66 o 3 1 2 35.58 56.31 1.04 o 5 1 2 68.72 71.71 4.48 o 7 1 2 83.68 84.32 2.22 o 9 1 2 599.09 583.50 11.10 o 11 1 2 30.38 28.76 2.08 o 13 1 2 0.14 0.30 2.10 o 15 1 2 1.54 4.75 5.66 o -16 2 2 10.15 3.34 3.16 o -14 2 2 138.66 117.04 5.31 o -12 2 2 310.52 341.37 17.42 o -10 2 2 47.26 56.71 2.46 o -8 2 2 49.87 51.94 1.88 o -6 2 2 1516.70 1496.64 20.27 o -4 2 2 1602.60 1597.84 22.35 o -2 2 2 966.67 911.74 12.43 o 0 2 2 27.08 23.98 1.00 o 2 2 2 1157.12 1171.79 18.05 o 4 2 2 173.00 146.67 2.55 o 6 2 2 312.15 316.43 7.96 o 8 2 2 38.17 57.74 1.98 o 10 2 2 1371.31 1345.03 65.87 o 12 2 2 0.93 -0.83 1.83 o 14 2 2 21.21 8.45 3.53 o -15 3 2 15.47 31.66 11.28 o -13 3 2 2.34 2.01 2.46 o -11 3 2 76.67 87.51 4.98 o -9 3 2 141.93 126.97 3.15 o -7 3 2 15.24 13.22 2.65 o -5 3 2 2.27 4.95 0.94 o -3 3 2 398.47 436.43 10.45 o -1 3 2 314.47 316.08 5.64 o 1 3 2 28.53 22.43 1.99 o 3 3 2 31.25 39.17 3.65 o 5 3 2 78.35 65.80 2.65 o 7 3 2 634.71 636.65 12.20 o 9 3 2 4.51 7.07 3.65 o 11 3 2 21.74 8.19 2.01 o 13 3 2 6.52 4.99 5.04 o -14 4 2 1.90 -7.12 7.12 o -12 4 2 109.42 78.17 11.95 o -10 4 2 54.35 59.74 2.79 o -8 4 2 73.53 65.81 2.46 o -6 4 2 483.62 461.94 10.95 o -4 4 2 31.73 33.06 2.65 o -2 4 2 273.30 289.35 10.12 o 0 4 2 493.99 501.20 9.60 o 2 4 2 205.52 225.34 7.30 o 4 4 2 483.57 476.14 8.40 o 6 4 2 2.45 1.64 1.83 o 8 4 2 1.08 1.61 1.66 o 10 4 2 96.12 73.50 5.38 o 12 4 2 12.69 21.18 5.98 o -11 5 2 17.28 25.03 5.88 o -9 5 2 357.30 402.64 19.14 o -7 5 2 25.68 23.89 3.65 o -5 5 2 2.12 4.31 1.59 o -3 5 2 380.23 357.72 19.91 o -1 5 2 98.57 96.23 3.65 o 1 5 2 1069.58 1124.96 31.69 o 3 5 2 255.63 273.67 10.29 o 5 5 2 70.82 76.46 6.47 o 7 5 2 139.83 140.25 7.08 o 9 5 2 0.00 0.39 3.91 o -8 6 2 22.34 27.78 16.92 o -6 6 2 8.81 3.21 2.79 o -4 6 2 24.53 21.13 2.39 o -2 6 2 14.11 12.94 2.99 o 0 6 2 145.18 154.96 7.96 o 2 6 2 48.88 38.16 4.31 o 4 6 2 61.27 36.83 4.65 o 6 6 2 109.06 138.72 20.57 o -17 1 3 0.03 0.26 5.22 o -15 1 3 5.03 8.34 2.39 o -13 1 3 361.94 366.33 18.42 o -11 1 3 11.99 16.11 1.71 o -9 1 3 433.59 414.10 7.73 o -7 1 3 12.67 7.15 1.27 o -5 1 3 427.12 372.00 9.79 o -3 1 3 1031.05 975.80 15.23 o -1 1 3 1882.36 1803.78 26.23 o 1 1 3 420.60 449.84 9.29 o 3 1 3 756.72 795.38 21.90 o 5 1 3 1200.87 1225.62 19.44 o 7 1 3 177.98 187.46 5.14 o 9 1 3 0.17 0.69 1.49 o 11 1 3 52.65 60.54 2.87 o 13 1 3 42.81 52.26 3.82 o -16 2 3 11.08 16.07 3.73 o -14 2 3 89.69 76.68 4.15 o -12 2 3 100.86 94.55 3.87 o -10 2 3 910.71 925.73 19.20 o -8 2 3 174.18 166.11 3.63 o -6 2 3 63.47 61.03 2.99 o -4 2 3 479.76 505.81 7.86 o -2 2 3 4729.03 4412.00 65.89 o 0 2 3 10241.60 9738.50 144.46 o 2 2 3 107.54 112.97 2.21 o 4 2 3 179.62 181.27 3.01 o 6 2 3 1539.73 1484.40 41.81 o 8 2 3 798.86 876.40 16.14 o 10 2 3 488.85 540.70 12.51 o 12 2 3 163.17 127.78 4.44 o 14 2 3 0.39 -1.08 6.14 o -15 3 3 63.66 78.21 8.64 o -13 3 3 300.06 319.71 11.50 o -11 3 3 64.22 63.75 2.51 o -9 3 3 13.59 7.50 1.49 o -7 3 3 1158.69 1273.68 22.63 o -5 3 3 12.10 6.52 0.80 o -3 3 3 2982.36 3131.38 44.48 o -1 3 3 513.87 462.72 7.62 o 1 3 3 33.41 35.25 3.15 o 3 3 3 752.90 740.04 11.87 o 5 3 3 356.72 337.58 8.63 o 7 3 3 42.23 43.49 2.32 o 9 3 3 64.25 62.19 2.94 o 11 3 3 3.89 6.76 2.01 o 13 3 3 2.47 7.26 5.95 o -14 4 3 4.44 11.22 6.19 o -12 4 3 8.54 1.97 2.82 o -10 4 3 0.12 0.27 1.27 o -8 4 3 243.59 241.25 5.77 o -6 4 3 436.46 419.36 8.80 o -4 4 3 0.37 0.90 0.62 o -2 4 3 92.35 86.00 2.35 o 0 4 3 11.72 13.94 1.04 o 2 4 3 666.34 726.94 12.41 o 4 4 3 68.86 47.97 2.08 o 6 4 3 1384.46 1429.93 29.96 o 8 4 3 3.93 7.54 1.55 o 10 4 3 70.93 45.18 6.47 o -11 5 3 5.72 16.39 6.57 o -9 5 3 84.14 104.89 5.85 o -7 5 3 4.82 2.99 1.75 o -5 5 3 1.59 4.18 1.66 o -3 5 3 21.49 17.18 2.65 o -1 5 3 8.52 13.38 3.65 o 1 5 3 163.80 207.26 5.33 o 3 5 3 11.19 16.39 3.15 o 5 5 3 140.02 135.32 5.97 o 7 5 3 0.83 0.13 4.31 o 9 5 3 17.01 10.55 5.04 o -8 6 3 45.24 42.13 6.09 o -6 6 3 8.42 7.34 2.69 o -4 6 3 57.14 43.66 3.31 o -2 6 3 4.92 3.98 2.32 o 0 6 3 4.67 7.63 3.32 o 2 6 3 6.11 1.92 1.66 o 4 6 3 7.76 7.50 3.32 o 6 6 3 16.41 8.01 5.57 o -16 0 4 164.21 150.98 11.95 o -14 0 4 4.91 2.65 1.66 o -12 0 4 72.28 49.44 2.65 o -10 0 4 1308.25 1261.26 25.88 o -8 0 4 110.74 153.63 3.98 o -6 0 4 1132.71 1064.82 24.22 o -4 0 4 8104.49 7884.78 157.95 o -2 0 4 12732.97 12678.63 248.54 o 0 0 4 1652.95 1677.70 31.52 o 2 0 4 649.02 767.51 15.26 o 4 0 4 5004.85 4847.27 103.53 o 6 0 4 505.02 507.03 9.95 o 8 0 4 22.39 27.21 1.99 o 10 0 4 190.81 156.95 5.97 o 12 0 4 7.32 13.94 1.99 o 14 0 4 74.86 98.55 11.95 o -17 1 4 26.77 19.73 5.57 o -15 1 4 314.45 359.21 13.69 o -13 1 4 83.68 96.50 6.47 o -11 1 4 170.46 177.20 4.48 o -9 1 4 15.17 10.10 4.31 o -7 1 4 254.89 250.11 4.48 o -5 1 4 1552.43 1670.92 27.32 o -3 1 4 741.14 781.01 10.91 o -1 1 4 1464.54 1419.56 20.16 o 1 1 4 6408.06 6762.62 90.75 o 3 1 4 358.91 432.07 7.63 o 5 1 4 3253.86 3261.57 49.94 o 7 1 4 1190.91 1143.06 18.76 o 9 1 4 11.60 5.32 1.66 o 11 1 4 534.64 507.75 13.47 o 13 1 4 2.89 6.14 3.43 o -16 2 4 51.43 34.65 6.30 o -14 2 4 26.95 15.18 3.65 o -12 2 4 257.30 304.92 8.61 o -10 2 4 114.03 115.38 3.98 o -8 2 4 437.04 472.88 8.09 o -6 2 4 313.12 273.30 4.57 o -4 2 4 97.83 71.53 3.65 o -2 2 4 549.35 501.19 7.03 o 0 2 4 574.72 509.21 7.39 o 2 2 4 2394.67 2403.75 33.79 o 4 2 4 10.02 11.31 2.16 o 6 2 4 178.17 181.66 4.65 o 8 2 4 223.15 216.03 5.97 o 10 2 4 120.08 84.87 3.52 o 12 2 4 6.26 -2.94 3.82 o -15 3 4 10.39 8.96 4.98 o -13 3 4 94.23 98.55 4.77 o -11 3 4 68.44 55.17 3.48 o -9 3 4 41.16 48.50 3.48 o -7 3 4 3.39 10.49 1.04 o -5 3 4 250.17 241.90 4.34 o -3 3 4 341.00 340.99 5.51 o -1 3 4 6.82 13.08 2.82 o 1 3 4 35.10 29.54 1.17 o 3 3 4 129.54 122.63 2.55 o 5 3 4 160.55 143.50 3.26 o 7 3 4 336.05 388.77 29.53 o 9 3 4 2.26 7.57 1.99 o 11 3 4 19.04 26.39 3.71 o -14 4 4 6.72 3.41 6.47 o -12 4 4 4.23 7.87 2.65 o -10 4 4 5.25 2.23 1.66 o -8 4 4 4.49 1.70 1.04 o -6 4 4 125.29 99.77 3.02 o -4 4 4 2.85 5.65 1.10 o -2 4 4 96.56 79.31 2.35 o 0 4 4 527.06 504.57 9.29 o 2 4 4 103.00 126.97 3.71 o 4 4 4 33.39 15.15 1.99 o 6 4 4 0.02 5.54 1.41 o 8 4 4 128.29 136.10 6.30 o 10 4 4 0.08 -2.59 4.78 o -11 5 4 37.06 21.57 9.03 o -9 5 4 99.70 88.49 9.79 o -7 5 4 10.86 18.89 3.82 o -5 5 4 827.38 881.58 32.27 o -3 5 4 36.59 32.79 2.65 o -1 5 4 32.46 25.08 1.41 o 1 5 4 246.25 220.41 6.48 o 3 5 4 64.82 71.04 9.46 o 5 5 4 200.98 235.32 8.64 o 7 5 4 2.07 -3.05 3.05 o -8 6 4 14.71 5.93 4.77 o -6 6 4 0.39 2.92 3.32 o -4 6 4 2.18 1.80 1.83 o -2 6 4 0.31 1.66 2.99 o 0 6 4 11.83 4.02 3.20 o 2 6 4 6.03 13.00 3.82 o 4 6 4 8.40 6.64 3.19 o -17 1 5 8.27 2.29 4.91 o -15 1 5 79.49 94.76 4.53 o -13 1 5 19.50 12.27 2.82 o -11 1 5 107.19 98.94 3.11 o -9 1 5 1300.73 1364.60 19.57 o -7 1 5 690.57 688.21 9.97 o -5 1 5 1954.51 2096.74 47.95 o -3 1 5 3541.12 3447.82 48.95 o -1 1 5 53.65 63.09 1.66 o 1 1 5 323.83 353.49 5.97 o 3 1 5 1029.09 1074.25 24.39 o 5 1 5 104.41 111.19 2.69 o 7 1 5 1056.50 1097.47 22.73 o 9 1 5 0.10 1.99 1.27 o 11 1 5 9.25 8.81 1.66 o 13 1 5 29.49 13.16 5.21 o -16 2 5 45.78 50.08 14.77 o -14 2 5 118.66 100.89 4.93 o -12 2 5 14.52 4.50 2.49 o -10 2 5 10.53 9.08 1.51 o -8 2 5 875.23 829.08 12.54 o -6 2 5 2455.01 2408.78 39.77 o -4 2 5 420.06 427.92 8.30 o -2 2 5 13.74 6.90 0.94 o 0 2 5 5.16 4.35 1.33 o 2 2 5 560.54 625.66 9.11 o 4 2 5 1271.18 1223.45 30.36 o 6 2 5 57.80 61.09 3.48 o 8 2 5 0.75 2.05 0.93 o 10 2 5 102.67 104.68 6.64 o 12 2 5 50.08 55.93 5.31 o -15 3 5 47.94 49.26 5.33 o -13 3 5 447.69 495.11 15.06 o -11 3 5 0.16 -1.28 1.51 o -9 3 5 2907.09 3060.53 54.99 o -7 3 5 27.75 33.49 2.16 o -5 3 5 306.84 272.82 4.93 o -3 3 5 3591.84 3615.11 58.28 o -1 3 5 150.16 151.69 3.28 o 1 3 5 2644.41 2808.27 47.84 o 3 3 5 648.53 683.96 13.13 o 5 3 5 107.04 101.39 6.47 o 7 3 5 1068.93 1094.64 44.46 o 9 3 5 93.13 77.61 5.26 o 11 3 5 64.77 64.45 6.54 o -14 4 5 6.70 11.79 5.04 o -12 4 5 118.63 99.19 6.48 o -10 4 5 26.68 21.65 3.48 o -8 4 5 7.64 7.86 2.32 o -6 4 5 197.56 203.55 4.86 o -4 4 5 272.44 256.06 5.48 o -2 4 5 3.03 1.83 1.49 o 0 4 5 98.86 96.35 5.64 o 2 4 5 342.36 367.59 12.61 o 4 4 5 0.01 -0.83 1.41 o 6 4 5 43.03 26.64 2.21 o 8 4 5 5.01 -1.99 3.98 o 10 4 5 50.22 57.71 13.11 o -11 5 5 26.93 27.52 4.37 o -9 5 5 16.81 17.49 2.99 o -7 5 5 3.33 8.07 1.83 o -5 5 5 183.85 190.39 5.16 o -3 5 5 36.14 24.60 1.51 o -1 5 5 0.41 0.71 0.80 o 1 5 5 9.14 6.18 1.04 o 3 5 5 141.89 143.82 5.33 o 5 5 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