#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/16/2211600.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211600_Fobs loop_ _publ_author_name 'Steyl, Gideon' _publ_section_title ; Chlorobis[diphenyl(p-tolyl)phosphine]copper(I) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3277 _journal_page_last m3278 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.266 _cell_angle_gamma 90.000 _cell_length_a 11.5427 _cell_length_b 18.1087 _cell_length_c 15.4940 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file sg2081Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6GGS2_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 15100.82 15108.36 302.64 o 4 0 0 7.64 -5.57 25.12 o 5 0 0 22374.88 21261.42 607.03 o 6 0 0 63303.23 60106.92 1633.30 o 7 0 0 0.07 -76.50 40.82 o 8 0 0 2014.11 1969.25 129.65 o 9 0 0 26.31 -3.07 48.16 o 10 0 0 2287.30 2012.36 142.92 o 11 0 0 725.06 655.05 104.58 o 12 0 0 2065.49 2215.56 140.94 o 13 0 0 335.66 241.60 101.26 o 14 0 0 653.41 940.56 257.58 o 2 1 0 6227.51 6407.82 94.90 o 3 1 0 419.33 506.42 22.34 o 4 1 0 946.95 824.20 43.95 o 5 1 0 10401.27 10111.25 222.57 o 6 1 0 5897.82 5205.90 142.49 o 7 1 0 9926.66 9207.90 219.95 o 8 1 0 16.73 11.99 32.29 o 9 1 0 4.18 56.87 39.98 o 10 1 0 6201.23 6190.31 148.79 o 11 1 0 232.69 257.78 55.03 o 12 1 0 2656.12 2693.41 118.59 o 13 1 0 648.92 777.55 87.77 o 14 1 0 0.99 16.19 70.14 o 1 2 0 960.66 1133.74 25.10 o 2 2 0 4707.11 4093.98 55.47 o 3 2 0 1577.73 1708.18 38.89 o 4 2 0 1402.87 1466.53 43.35 o 5 2 0 3083.36 2902.28 72.72 o 6 2 0 12137.90 12103.38 221.03 o 7 2 0 24.85 87.28 28.30 o 8 2 0 331.03 333.58 42.01 o 9 2 0 51.10 61.04 38.10 o 10 2 0 50.06 250.96 41.88 o 11 2 0 1214.41 1314.10 84.64 o 12 2 0 1023.11 1112.21 86.53 o 13 2 0 1.97 42.65 69.45 o 14 2 0 56.84 82.08 69.24 o 1 3 0 2755.43 2807.54 50.34 o 2 3 0 3545.31 3592.63 60.00 o 3 3 0 535.27 545.27 25.40 o 4 3 0 2250.04 2348.39 62.61 o 5 3 0 1312.92 1355.31 50.03 o 6 3 0 326.71 258.16 31.45 o 7 3 0 732.04 790.74 62.65 o 8 3 0 135.36 90.82 30.12 o 9 3 0 708.61 697.08 50.41 o 10 3 0 2.90 -4.13 41.76 o 11 3 0 123.31 104.73 49.70 o 12 3 0 229.58 176.05 66.93 o 13 3 0 19.44 29.39 67.27 o 14 3 0 4.33 277.95 89.94 o 1 4 0 294.15 356.23 28.94 o 2 4 0 22.37 14.58 16.43 o 3 4 0 61.41 18.98 24.11 o 4 4 0 182.46 182.86 29.42 o 5 4 0 4630.30 4789.81 144.83 o 6 4 0 243.79 129.71 30.28 o 7 4 0 112.16 142.00 33.67 o 8 4 0 2459.01 2308.40 103.60 o 9 4 0 25.07 52.29 38.68 o 10 4 0 286.86 152.87 46.99 o 11 4 0 2235.70 2049.15 125.93 o 12 4 0 593.27 814.86 101.75 o 13 4 0 24.63 137.92 76.47 o 14 4 0 954.62 1260.80 128.53 o 1 5 0 1512.61 1607.07 44.55 o 2 5 0 170.78 94.16 24.31 o 3 5 0 0.54 -40.94 20.47 o 4 5 0 313.47 368.38 35.68 o 5 5 0 4825.64 5083.73 137.08 o 6 5 0 717.28 616.70 49.98 o 7 5 0 483.66 518.50 47.68 o 8 5 0 1034.61 977.77 63.14 o 9 5 0 203.22 89.62 41.77 o 10 5 0 517.21 492.11 60.33 o 11 5 0 168.14 202.64 54.84 o 12 5 0 570.99 784.22 89.67 o 13 5 0 37.90 75.65 73.87 o 14 5 0 151.32 196.81 88.29 o 1 6 0 1212.29 1342.25 59.84 o 2 6 0 2594.31 2590.35 74.00 o 3 6 0 8158.67 8103.43 172.42 o 4 6 0 19.64 40.28 27.31 o 5 6 0 8045.05 8734.50 190.82 o 6 6 0 61.81 8.29 31.84 o 7 6 0 78.71 188.95 36.84 o 8 6 0 1665.04 1545.92 76.90 o 9 6 0 2912.97 2746.67 105.27 o 10 6 0 139.38 82.61 46.55 o 11 6 0 1070.62 1163.20 85.22 o 12 6 0 211.84 103.58 82.91 o 13 6 0 30.16 -13.78 71.68 o 1 7 0 587.53 436.35 34.55 o 2 7 0 2233.40 1992.22 82.75 o 3 7 0 280.11 352.36 40.98 o 4 7 0 548.41 451.78 41.13 o 5 7 0 41.89 103.24 33.07 o 6 7 0 71.02 146.69 39.55 o 7 7 0 514.69 656.48 60.33 o 8 7 0 889.32 887.40 124.22 o 9 7 0 1302.40 1519.59 102.32 o 10 7 0 230.99 235.54 53.23 o 11 7 0 94.60 25.01 47.69 o 12 7 0 7.74 -24.83 71.01 o 13 7 0 451.40 642.82 131.59 o 0 8 0 11596.09 12257.43 311.80 o 1 8 0 979.66 895.90 46.89 o 2 8 0 7249.24 6580.01 165.78 o 3 8 0 22044.50 20696.63 433.76 o 4 8 0 976.32 1030.65 57.49 o 5 8 0 1950.82 2026.25 78.74 o 6 8 0 1375.39 1365.30 93.06 o 7 8 0 478.56 548.46 59.90 o 8 8 0 4552.58 4143.37 146.91 o 9 8 0 5407.91 5771.58 185.20 o 10 8 0 70.55 183.17 59.17 o 11 8 0 54.93 95.97 67.97 o 12 8 0 106.37 101.48 107.99 o 13 8 0 179.57 139.17 147.69 o 1 9 0 2384.11 2243.87 75.63 o 2 9 0 8028.65 7233.55 161.20 o 3 9 0 850.59 836.97 58.73 o 4 9 0 18416.46 18277.49 397.22 o 5 9 0 2444.83 2522.14 100.02 o 6 9 0 1309.23 1377.97 81.47 o 7 9 0 3656.95 3577.18 131.05 o 8 9 0 1086.12 1086.27 83.63 o 9 9 0 2648.38 2595.66 124.96 o 10 9 0 4969.17 4926.23 178.69 o 11 9 0 4.99 -49.47 57.44 o 12 9 0 556.81 611.56 129.26 o 13 9 0 1573.28 2029.31 199.82 o 0 10 0 10877.52 12726.17 400.42 o 1 10 0 943.16 914.81 52.23 o 2 10 0 865.81 790.49 62.76 o 3 10 0 11624.33 11492.79 294.08 o 4 10 0 149.64 211.69 46.46 o 5 10 0 639.77 580.88 60.77 o 6 10 0 561.18 719.22 67.39 o 7 10 0 32.91 71.31 46.63 o 8 10 0 2632.51 2712.08 161.12 o 9 10 0 2298.50 2443.81 124.28 o 10 10 0 290.80 243.44 68.30 o 11 10 0 72.96 126.20 74.06 o 12 10 0 244.83 205.61 108.49 o 1 11 0 7.97 7.62 29.01 o 2 11 0 205.59 249.46 45.68 o 3 11 0 12.05 84.56 34.21 o 4 11 0 3729.72 3595.23 126.83 o 5 11 0 219.10 112.85 44.60 o 6 11 0 172.97 170.64 66.99 o 7 11 0 667.14 610.77 70.56 o 8 11 0 509.00 559.76 71.10 o 9 11 0 653.34 730.77 83.03 o 10 11 0 281.61 231.80 79.52 o 11 11 0 15.83 -48.01 69.49 o 12 11 0 144.78 123.58 96.81 o 0 12 0 942.93 865.14 86.79 o 1 12 0 50.63 41.95 31.44 o 2 12 0 209.95 244.25 40.59 o 3 12 0 8370.93 8206.36 191.06 o 4 12 0 10.96 -16.86 40.39 o 5 12 0 371.19 378.15 58.23 o 6 12 0 711.20 676.30 71.63 o 7 12 0 8.10 64.05 49.58 o 8 12 0 626.84 677.39 81.06 o 9 12 0 1954.34 1913.44 119.15 o 10 12 0 3.70 -98.49 58.64 o 11 12 0 589.39 742.58 110.39 o 12 12 0 41.50 -25.58 101.28 o 1 13 0 76.19 82.43 34.91 o 2 13 0 1785.25 1807.38 80.15 o 3 13 0 5.89 69.49 36.06 o 4 13 0 190.83 144.06 53.06 o 5 13 0 10.54 -46.78 46.70 o 6 13 0 979.60 1046.68 85.65 o 7 13 0 1101.34 1067.68 131.30 o 8 13 0 825.31 859.14 89.43 o 9 13 0 361.62 518.02 92.50 o 10 13 0 29.28 42.09 73.16 o 11 13 0 39.99 29.89 98.80 o 0 14 0 1361.33 1361.86 114.56 o 1 14 0 19.66 13.34 36.46 o 2 14 0 1677.79 1572.47 93.41 o 3 14 0 5247.01 4925.32 142.83 o 4 14 0 271.68 325.08 52.23 o 5 14 0 4.36 -39.41 41.59 o 6 14 0 871.31 922.58 85.18 o 7 14 0 186.72 310.06 67.38 o 8 14 0 2206.09 2216.56 146.10 o 9 14 0 620.83 577.62 96.44 o 10 14 0 63.05 73.84 80.36 o 11 14 0 268.90 208.55 183.92 o 1 15 0 157.89 95.39 44.37 o 2 15 0 2607.62 2808.90 107.77 o 3 15 0 655.81 645.31 62.56 o 4 15 0 253.03 147.06 46.78 o 5 15 0 164.99 157.21 47.43 o 6 15 0 386.16 363.04 69.65 o 7 15 0 345.69 205.25 66.66 o 8 15 0 384.98 456.44 94.76 o 9 15 0 261.10 358.97 91.38 o 10 15 0 95.33 102.66 83.97 o 0 16 0 7492.20 6916.18 287.92 o 1 16 0 739.92 830.80 74.53 o 2 16 0 54.85 41.84 42.74 o 3 16 0 49.16 52.38 42.08 o 4 16 0 8.64 16.95 41.37 o 5 16 0 2037.56 1961.04 109.90 o 6 16 0 2178.08 2006.57 126.25 o 7 16 0 138.29 191.41 78.68 o 8 16 0 131.23 92.16 72.37 o 9 16 0 58.36 91.70 80.72 o 10 16 0 2.08 -1.46 102.56 o 1 17 0 3156.70 3248.73 134.50 o 2 17 0 7.88 10.91 44.03 o 3 17 0 60.86 3.83 44.70 o 4 17 0 1492.35 1444.81 91.34 o 5 17 0 2754.46 2787.38 121.95 o 6 17 0 299.25 391.89 74.99 o 7 17 0 1914.64 2268.98 133.70 o 8 17 0 136.33 305.41 91.28 o 9 17 0 194.26 54.91 78.72 o 0 18 0 10938.19 10848.22 409.90 o 1 18 0 1647.44 1608.75 101.52 o 2 18 0 251.28 321.00 62.76 o 3 18 0 366.66 332.78 60.03 o 4 18 0 8.50 -7.51 60.34 o 5 18 0 2241.32 2592.07 213.29 o 6 18 0 4628.55 4906.55 225.27 o 7 18 0 0.32 12.47 71.48 o 8 18 0 118.43 146.37 77.36 o 9 18 0 74.16 240.89 201.07 o 1 19 0 2016.45 1916.08 113.54 o 2 19 0 24.84 34.87 53.90 o 3 19 0 10.31 -34.01 56.45 o 4 19 0 346.80 264.85 68.80 o 5 19 0 816.99 688.93 86.60 o 6 19 0 294.24 266.66 72.17 o 7 19 0 535.91 632.33 177.87 o 8 19 0 13.24 -45.27 98.57 o 0 20 0 1617.68 1596.84 157.94 o 1 20 0 11.66 27.96 64.90 o 2 20 0 7.41 7.40 61.22 o 3 20 0 610.65 727.43 98.05 o 4 20 0 9.25 -21.09 65.42 o 5 20 0 186.71 203.04 166.41 o 6 20 0 1671.56 1608.38 207.85 o 7 20 0 26.35 81.84 79.32 o 1 21 0 1128.16 701.32 118.73 o 2 21 0 62.65 -61.78 75.26 o 3 21 0 205.65 154.62 90.77 o 4 21 0 101.32 -48.07 125.39 o 5 21 0 581.96 645.34 110.54 o 6 21 0 4.92 -92.18 71.42 o 0 22 0 1957.40 2355.47 265.00 o 1 22 0 3.40 153.11 92.05 o 2 22 0 46.06 70.15 85.11 o 3 22 0 5.88 -72.16 122.77 o 4 22 0 74.60 47.64 86.89 o 1 23 0 244.19 246.89 104.43 o -14 1 1 143.52 77.75 68.57 o -13 1 1 471.46 773.10 87.65 o -12 1 1 11.89 139.01 58.76 o -11 1 1 235.65 219.48 49.48 o -10 1 1 2021.69 1976.63 111.83 o -9 1 1 179.08 160.52 39.35 o -8 1 1 3396.72 3417.40 89.48 o -7 1 1 826.31 882.95 55.67 o -6 1 1 19.69 273.98 36.25 o -5 1 1 829.66 975.40 44.36 o -4 1 1 601.05 711.92 32.01 o -3 1 1 10352.97 10719.45 166.02 o -2 1 1 147.83 355.02 13.46 o -1 1 1 27.11 41.90 10.21 o 1 1 1 105.05 217.04 10.63 o 2 1 1 2727.50 1973.54 39.26 o 3 1 1 6330.72 7593.85 116.52 o 4 1 1 2273.71 2346.31 79.72 o 5 1 1 409.97 468.05 39.34 o 6 1 1 4067.41 3812.88 118.03 o 7 1 1 1375.83 1452.42 72.00 o 8 1 1 1260.56 1295.03 82.18 o 9 1 1 102.71 133.42 50.37 o 10 1 1 53.01 112.15 48.31 o 11 1 1 100.54 34.87 45.21 o 12 1 1 680.72 617.44 72.54 o 13 1 1 8.95 28.38 63.72 o 14 1 1 283.76 326.55 81.58 o -14 2 1 491.83 707.29 96.73 o -13 2 1 470.04 401.82 74.37 o -12 2 1 1521.18 1569.95 122.81 o -11 2 1 32.78 86.87 63.76 o -10 2 1 3722.30 3572.30 119.13 o -9 2 1 61.93 79.94 35.76 o -8 2 1 0.90 -24.71 29.72 o -7 2 1 3880.69 4007.01 104.64 o -6 2 1 3007.24 2620.73 74.73 o -5 2 1 155.22 120.34 24.41 o -4 2 1 55431.56 59787.01 900.97 o -3 2 1 11636.14 11902.77 173.84 o -2 2 1 1740.16 1632.37 30.88 o -1 2 1 12.77 42.71 7.58 o 0 2 1 245.65 239.87 11.41 o 1 2 1 428.49 297.98 13.27 o 2 2 1 133510.70 144476.75 1798.42 o 3 2 1 288.81 517.07 24.17 o 4 2 1 2432.58 1987.29 67.61 o 5 2 1 26.65 38.15 28.83 o 6 2 1 0.01 8.16 26.93 o 7 2 1 7915.93 7265.73 185.30 o 8 2 1 856.23 920.62 57.27 o 9 2 1 1023.31 1025.99 61.42 o 10 2 1 3674.79 3727.10 111.89 o 11 2 1 215.00 195.12 51.24 o 12 2 1 409.84 324.31 71.11 o 13 2 1 660.30 885.17 109.37 o 14 2 1 1.05 25.62 70.44 o -14 3 1 323.45 311.41 78.36 o -13 3 1 283.90 182.89 76.78 o -12 3 1 71.94 53.50 55.75 o -11 3 1 673.36 691.36 67.80 o -10 3 1 2423.11 2260.36 97.14 o -9 3 1 159.24 214.21 69.85 o -8 3 1 1364.67 1388.22 67.70 o -7 3 1 309.90 292.98 37.80 o -6 3 1 1153.90 1076.50 59.50 o -5 3 1 286.70 163.84 28.54 o -4 3 1 2735.22 2686.46 62.94 o -3 3 1 6117.82 6465.10 103.63 o -2 3 1 6011.89 5739.61 85.55 o -1 3 1 1016.64 890.68 23.89 o 0 3 1 1881.90 1797.49 31.67 o 1 3 1 12.96 56.52 12.84 o 2 3 1 1564.87 1517.15 47.47 o 3 3 1 14377.32 14437.25 227.78 o 4 3 1 3202.59 3168.54 76.55 o 5 3 1 45.57 146.40 26.66 o 6 3 1 2583.73 2524.01 77.39 o 7 3 1 3233.67 3210.97 89.74 o 8 3 1 216.72 298.35 38.45 o 9 3 1 941.16 1056.05 60.49 o 10 3 1 347.77 462.93 50.12 o 11 3 1 63.53 88.13 47.88 o 12 3 1 785.50 838.48 80.02 o 13 3 1 82.39 44.12 72.19 o 14 3 1 240.37 254.04 92.12 o -14 4 1 108.25 41.08 76.42 o -13 4 1 217.45 396.70 88.19 o -12 4 1 110.01 239.78 70.44 o -11 4 1 9.66 25.35 43.30 o -10 4 1 1745.10 1838.31 89.93 o -9 4 1 32.37 -34.99 32.50 o -8 4 1 2.88 62.97 31.91 o -7 4 1 3354.47 3148.58 96.39 o -6 4 1 1649.44 1848.84 68.15 o -5 4 1 502.75 516.51 38.37 o -4 4 1 6267.02 6382.17 116.19 o -3 4 1 314.03 391.17 28.23 o -2 4 1 53.91 30.25 18.60 o -1 4 1 4277.15 4070.66 70.40 o 0 4 1 4409.60 4497.14 66.38 o 1 4 1 115.17 91.20 16.92 o 2 4 1 11871.80 12658.60 202.30 o 3 4 1 2093.78 2104.57 60.52 o 4 4 1 1535.85 1684.33 55.22 o 5 4 1 111.12 293.96 31.80 o 6 4 1 876.89 976.30 48.30 o 7 4 1 1201.26 1252.51 56.71 o 8 4 1 3005.99 3203.28 95.46 o 9 4 1 79.39 80.81 38.00 o 10 4 1 299.60 227.22 52.23 o 11 4 1 463.35 687.12 71.21 o 12 4 1 17.88 2.77 48.30 o 13 4 1 487.45 784.62 106.81 o 14 4 1 182.17 173.39 148.15 o -14 5 1 338.38 306.47 95.53 o -13 5 1 305.97 271.89 83.62 o -12 5 1 1.10 142.68 72.53 o -11 5 1 1162.70 1327.65 101.85 o -10 5 1 445.13 439.96 57.13 o -9 5 1 44.91 12.68 41.81 o -8 5 1 239.81 241.72 41.75 o -7 5 1 486.61 466.30 68.29 o -6 5 1 2561.88 2709.25 85.10 o -5 5 1 5055.05 4399.93 100.47 o -4 5 1 486.94 516.27 34.28 o -3 5 1 980.02 1086.84 47.47 o -2 5 1 41.59 33.48 19.37 o -1 5 1 53.82 22.46 18.77 o 0 5 1 27.27 43.25 19.79 o 1 5 1 11832.15 11952.41 205.14 o 2 5 1 1181.20 1409.52 47.38 o 3 5 1 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