#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/16/2211608.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211608_Fobs loop_ _publ_author_name 'Stibrany, Robert T.' 'Potenza, Joseph A.' _publ_section_title ; A structure with trigonally and tetrahedrally coordinated Cu^I^ cations: rac-(acetonitrile)[2,2'-bis(1-propyl-1H-benzimidazol-2-yl)biphenyl]copper(I) bis(acetonitrile)[2,2'-bis(1-propyl-1H-benzimidazol-2-yl)biphenyl]copper(I) bis(perchlorate) ; _journal_coeditor_code SG2094 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3425 _journal_page_last m3428 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.424 _cell_angle_beta 87.901 _cell_angle_gamma 88.588 _cell_length_a 8.8593 _cell_length_b 17.4072 _cell_length_c 22.7595 _exptl_crystal_F_000 1444.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file sg2094Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' prpnut2 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 296.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 274.24 171.97 5.88 o 2 0 0 19048.63 21223.05 228.57 o 3 0 0 642.00 474.58 19.89 o 4 0 0 5731.81 5817.55 64.65 o 5 0 0 1454.32 1549.85 27.34 o 6 0 0 27.98 11.63 11.80 o 7 0 0 5.23 9.17 17.63 o 8 0 0 12.68 -20.30 25.45 o 9 0 0 4.56 -7.81 28.92 o 10 0 0 1245.12 1340.09 65.77 o -10 1 0 106.05 117.34 34.18 o -9 1 0 615.88 598.85 50.33 o -8 1 0 921.62 931.50 38.74 o -7 1 0 135.32 107.40 26.49 o -6 1 0 748.78 629.80 21.07 o -5 1 0 2535.51 1970.55 30.88 o -4 1 0 6811.84 7164.78 77.15 o -3 1 0 1978.00 1904.11 25.31 o -2 1 0 32248.24 33462.65 320.47 o -1 1 0 53.83 61.08 9.48 o 1 1 0 9280.97 9929.06 100.21 o 2 1 0 14165.90 15792.02 132.79 o 3 1 0 151.32 86.52 36.91 o 4 1 0 2518.30 2812.82 42.25 o 5 1 0 764.85 561.64 14.67 o 6 1 0 127.40 32.55 12.78 o 7 1 0 1937.85 1525.42 32.77 o 8 1 0 339.65 357.44 23.98 o 9 1 0 1113.53 1164.70 45.37 o 10 1 0 298.91 364.12 59.22 o -10 2 0 3.95 14.06 32.85 o -9 2 0 295.67 331.81 53.55 o -8 2 0 837.09 835.58 38.21 o -7 2 0 85.81 70.73 24.58 o -6 2 0 651.28 623.92 22.83 o -5 2 0 863.86 847.33 68.21 o -4 2 0 1813.44 1668.75 28.82 o -3 2 0 477.70 452.80 32.03 o -2 2 0 14174.35 13782.28 164.96 o -1 2 0 12796.06 14312.56 168.60 o 0 2 0 399.37 196.89 12.26 o 1 2 0 7606.61 8327.17 104.57 o 2 2 0 45785.31 51927.12 426.92 o 3 2 0 1774.15 1504.80 22.82 o 4 2 0 8667.92 10023.76 96.78 o 5 2 0 400.04 557.58 14.85 o 6 2 0 332.40 337.47 20.65 o 7 2 0 61.76 13.32 45.05 o 8 2 0 752.49 698.56 53.12 o 9 2 0 474.86 476.92 47.15 o 10 2 0 75.41 104.08 52.87 o -10 3 0 11.51 13.94 32.54 o -9 3 0 594.97 718.13 41.44 o -8 3 0 56.00 58.62 27.49 o -7 3 0 327.78 305.55 28.66 o -6 3 0 634.30 633.30 20.24 o -5 3 0 9563.60 9062.57 123.12 o -4 3 0 370.07 278.74 67.19 o -3 3 0 34606.74 35116.26 410.01 o -2 3 0 4930.97 5649.30 73.87 o -1 3 0 2328.76 2405.14 34.66 o 0 3 0 2288.06 1563.48 18.88 o 1 3 0 483.61 647.19 35.18 o 2 3 0 2135.04 1902.93 33.00 o 3 3 0 3.06 12.80 12.12 o 4 3 0 863.44 672.30 21.41 o 5 3 0 1872.28 1745.72 29.46 o 6 3 0 67.65 148.20 28.60 o 7 3 0 2341.33 2314.70 40.61 o 8 3 0 1474.71 1434.86 37.96 o 9 3 0 15.77 41.14 48.47 o 10 3 0 802.43 944.79 72.51 o -10 4 0 16.30 47.76 34.22 o -9 4 0 427.33 405.58 36.43 o -8 4 0 11.14 -22.29 26.48 o -7 4 0 1848.53 1727.16 74.37 o -6 4 0 1309.98 1186.71 64.30 o -5 4 0 453.50 397.87 37.87 o -4 4 0 6496.70 6474.93 90.89 o -3 4 0 3330.66 3053.82 61.37 o -2 4 0 4714.09 5041.31 178.93 o -1 4 0 4669.62 4694.51 130.31 o 0 4 0 710.13 470.81 18.50 o 1 4 0 7388.71 8160.34 105.76 o 2 4 0 2328.36 2162.79 37.22 o 3 4 0 1648.99 1157.14 27.34 o 4 4 0 16898.83 18363.83 182.40 o 5 4 0 838.91 778.53 20.00 o 6 4 0 8458.54 8221.31 93.43 o 7 4 0 72.59 66.07 29.14 o 8 4 0 347.78 335.41 80.67 o 9 4 0 59.15 -10.43 77.59 o 10 4 0 6.98 5.57 54.04 o -10 5 0 19.85 26.92 34.99 o -9 5 0 844.22 945.29 45.08 o -8 5 0 321.42 285.84 31.86 o -7 5 0 484.76 509.58 57.51 o -6 5 0 148.36 111.12 23.52 o -5 5 0 977.15 1130.41 49.79 o -4 5 0 1147.31 1137.00 43.29 o -3 5 0 41.28 33.46 19.30 o -2 5 0 1472.76 1388.94 27.55 o -1 5 0 5539.47 6102.28 196.04 o 0 5 0 1464.95 1829.06 23.93 o 1 5 0 5802.39 6111.79 121.18 o 2 5 0 81.64 17.79 17.93 o 3 5 0 72.91 31.07 14.37 o 4 5 0 223.36 235.92 28.05 o 5 5 0 58.59 85.05 19.77 o 6 5 0 150.86 163.90 22.30 o 7 5 0 870.30 924.59 38.04 o 8 5 0 19.37 -30.98 30.98 o 9 5 0 308.87 255.81 84.97 o 10 5 0 2.82 24.63 53.75 o -9 6 0 5.45 17.78 31.39 o -8 6 0 1167.28 1294.81 106.03 o -7 6 0 2275.92 2108.88 92.20 o -6 6 0 2750.22 2687.02 56.94 o -5 6 0 466.86 518.58 66.79 o -4 6 0 2309.54 2211.15 44.41 o -3 6 0 1273.14 1425.20 32.66 o -2 6 0 1319.69 1338.09 24.31 o -1 6 0 4273.24 3721.31 83.75 o 0 6 0 983.45 1088.72 26.32 o 1 6 0 1575.30 1909.86 28.51 o 2 6 0 1091.18 1285.16 43.54 o 3 6 0 48.35 37.41 14.80 o 4 6 0 1272.85 1669.41 38.85 o 5 6 0 224.57 220.38 21.64 o 6 6 0 450.19 385.68 28.82 o 7 6 0 457.00 453.07 32.01 o 8 6 0 128.67 54.65 64.94 o 9 6 0 1091.40 1112.68 57.80 o 10 6 0 4.18 17.95 68.31 o -9 7 0 641.73 695.16 42.72 o -8 7 0 79.91 25.72 29.72 o -7 7 0 3378.69 3215.05 68.46 o -6 7 0 115.56 109.84 25.16 o -5 7 0 3120.98 3069.34 58.98 o -4 7 0 3780.28 3258.91 57.19 o -3 7 0 1394.91 1448.58 33.73 o -2 7 0 2320.92 2382.93 32.61 o -1 7 0 1550.17 1609.46 50.62 o 0 7 0 75.79 229.98 14.90 o 1 7 0 15046.69 15510.32 228.91 o 2 7 0 41.12 -0.50 14.34 o 3 7 0 3529.25 2739.17 50.98 o 4 7 0 854.76 1002.73 61.71 o 5 7 0 1307.76 1589.85 52.92 o 6 7 0 191.48 255.51 27.85 o 7 7 0 4.36 -33.37 33.37 o 8 7 0 4.50 -70.21 70.21 o 9 7 0 672.38 684.28 58.98 o -9 8 0 426.34 450.88 42.36 o -8 8 0 4.11 0.64 53.60 o -7 8 0 379.82 380.31 34.44 o -6 8 0 32.74 16.22 32.54 o -5 8 0 1405.30 1372.64 39.84 o -4 8 0 840.90 706.14 28.67 o -3 8 0 79.92 81.29 29.37 o -2 8 0 4772.37 4387.05 52.53 o -1 8 0 1013.43 1018.37 20.35 o 0 8 0 9235.91 9729.22 101.48 o 1 8 0 852.05 887.60 17.52 o 2 8 0 6.71 -14.26 16.13 o 3 8 0 581.50 560.33 26.00 o 4 8 0 190.26 207.17 27.02 o 5 8 0 728.80 842.69 45.00 o 6 8 0 395.18 361.70 30.54 o 7 8 0 664.75 603.24 36.41 o 8 8 0 259.85 182.42 32.90 o 9 8 0 95.20 93.40 44.37 o -9 9 0 7.68 19.31 40.95 o -8 9 0 78.31 30.10 32.05 o -7 9 0 63.40 100.70 55.80 o -6 9 0 23.62 36.27 25.11 o -5 9 0 147.09 182.74 63.47 o -4 9 0 197.33 247.82 23.65 o -3 9 0 614.73 528.81 21.34 o -2 9 0 1062.80 1184.82 23.89 o -1 9 0 597.87 665.58 18.59 o 0 9 0 142.78 274.80 14.02 o 1 9 0 101.06 104.70 23.78 o 2 9 0 6929.18 7265.08 106.94 o 3 9 0 5954.05 6176.14 96.21 o 4 9 0 3788.82 3345.22 65.33 o 5 9 0 748.52 811.71 35.96 o 6 9 0 2634.91 2767.04 63.31 o 7 9 0 569.50 558.06 37.27 o 8 9 0 3.52 -30.69 30.69 o 9 9 0 277.61 227.76 36.63 o -9 10 0 268.44 283.59 51.11 o -8 10 0 1549.90 1540.57 54.25 o -7 10 0 121.98 127.35 29.30 o -6 10 0 1390.69 1286.59 49.99 o -5 10 0 132.77 183.24 47.20 o -4 10 0 7153.01 6852.98 139.50 o -3 10 0 329.57 369.58 17.57 o -2 10 0 7799.46 7449.51 84.16 o -1 10 0 627.36 681.31 19.46 o 0 10 0 7192.77 6767.27 76.64 o 1 10 0 2785.74 3261.13 107.92 o 2 10 0 1249.19 1475.19 39.37 o 3 10 0 685.62 567.86 38.06 o 4 10 0 365.59 364.20 27.78 o 5 10 0 158.63 255.45 28.33 o 6 10 0 2885.74 2795.42 65.25 o 7 10 0 2027.50 1863.70 56.27 o 8 10 0 834.96 754.25 42.83 o 9 10 0 414.08 417.18 61.42 o -8 11 0 200.59 180.79 33.30 o -7 11 0 859.31 930.79 42.99 o -6 11 0 784.39 768.21 36.77 o -5 11 0 6387.38 6407.04 102.83 o -4 11 0 123.26 94.15 23.88 o -3 11 0 931.57 952.01 71.29 o -2 11 0 428.40 332.63 18.42 o -1 11 0 592.08 556.55 26.86 o 0 11 0 2737.23 2846.74 41.29 o 1 11 0 1371.32 1345.38 36.21 o 2 11 0 284.45 243.12 26.04 o 3 11 0 34.94 44.13 24.56 o 4 11 0 141.65 157.48 26.69 o 5 11 0 147.56 134.20 27.60 o 6 11 0 798.50 1057.87 43.98 o 7 11 0 394.46 483.84 38.85 o 8 11 0 1305.89 1388.30 53.45 o -8 12 0 44.79 101.13 31.51 o -7 12 0 0.39 -23.63 28.22 o -6 12 0 339.94 367.27 31.89 o -5 12 0 613.89 648.77 34.59 o -4 12 0 1582.17 1448.03 43.10 o -3 12 0 1001.27 939.64 34.04 o -2 12 0 485.14 445.49 21.21 o -1 12 0 742.66 559.32 21.43 o 0 12 0 1333.29 1187.52 26.86 o 1 12 0 1487.97 1304.94 26.76 o 2 12 0 4157.78 4234.24 77.39 o 3 12 0 1731.16 1634.85 91.37 o 4 12 0 4014.39 4146.66 81.48 o 5 12 0 28.78 -0.53 41.34 o 6 12 0 703.57 943.21 49.89 o 7 12 0 206.50 291.27 46.61 o 8 12 0 15.88 -4.77 50.62 o -7 13 0 1251.48 1234.68 61.96 o -6 13 0 228.98 262.75 30.83 o -5 13 0 2434.52 2380.55 58.02 o -4 13 0 1278.36 1277.72 40.81 o -3 13 0 96.56 47.31 23.45 o -2 13 0 396.24 363.46 21.71 o -1 13 0 290.97 174.85 18.72 o 0 13 0 544.70 737.94 23.86 o 1 13 0 2.12 -23.63 24.69 o 2 13 0 319.76 314.91 32.98 o 3 13 0 1464.50 1480.47 48.05 o 4 13 0 63.33 39.83 29.47 o 5 13 0 388.83 439.32 37.66 o 6 13 0 583.61 671.96 40.86 o 7 13 0 63.42 86.30 32.68 o 8 13 0 310.52 233.46 53.94 o -7 14 0 21.59 27.56 30.42 o -6 14 0 856.21 891.90 42.05 o -5 14 0 272.17 232.79 28.74 o -4 14 0 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1010.95 47.33 o 4 16 0 374.07 346.98 44.07 o 5 16 0 776.17 709.69 46.43 o 6 16 0 103.27 105.61 38.39 o -5 17 0 0.97 11.40 27.68 o -4 17 0 7.64 -23.04 25.86 o -3 17 0 182.33 170.93 28.18 o -2 17 0 767.50 722.74 50.87 o -1 17 0 1603.31 1839.85 82.97 o 0 17 0 2002.19 1885.54 56.24 o 1 17 0 1083.05 989.95 45.92 o 2 17 0 974.43 968.53 47.07 o 3 17 0 143.88 164.50 46.08 o 4 17 0 1201.29 1183.22 83.85 o 5 17 0 145.19 220.00 40.46 o -4 18 0 966.99 1133.08 46.00 o -3 18 0 490.06 425.40 33.37 o -2 18 0 614.50 746.41 63.13 o -1 18 0 245.78 282.23 50.52 o 0 18 0 2309.67 2216.10 62.67 o 1 18 0 130.56 229.87 35.89 o 2 18 0 412.92 369.73 40.21 o 3 18 0 527.87 584.27 45.74 o 4 18 0 46.70 60.04 37.52 o -2 19 0 124.70 110.13 49.45 o -1 19 0 38.02 29.81 49.45 o 0 19 0 159.65 263.76 50.62 o 1 19 0 17.82 21.28 33.22 o 2 19 0 824.91 869.16 50.69 o -2 -19 1 1091.95 1274.86 55.75 o -1 -19 1 543.12 518.35 42.48 o 0 -19 1 882.11 802.61 65.28 o 1 -19 1 1398.94 1376.63 79.25 o -4 -18 1 61.70 59.12 56.39 o -3 -18 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