#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:23:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181036 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/16/2211617.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211617_Fobs loop_ _publ_author_name 'Hu, Xue-Lei' 'Qiu, Li' 'Sun, Wen-Bing' 'Chen, Zhong' _publ_section_title ; Tetra-\m-acetato-\k^4^O:O';\k^3^O,O':O';\k^3^O:O,O'-bis[(acetato-\k^2^O,O')(1,10-phenanthroline-\k^2^N,N')holmium(III)] ; _journal_coeditor_code SJ2149 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3213 _journal_page_last m3214 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 103.318 _cell_angle_beta 109.007 _cell_angle_gamma 98.380 _cell_length_a 8.7171 _cell_length_b 8.9262 _cell_length_c 12.9138 _exptl_crystal_F_000 508.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file sj2149Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 060919am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 206.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 42637.64 42821.61 834.61 o 2 0 0 2236.91 1948.59 59.47 o 3 0 0 6729.59 6714.35 216.66 o 4 0 0 7744.97 8521.50 253.44 o 5 0 0 1812.20 1673.13 85.65 o 6 0 0 1286.47 1463.02 199.74 o 7 0 0 868.85 1003.07 119.47 o 8 0 0 769.44 959.90 266.87 o 9 0 0 91.04 0.00 157.18 o -10 1 0 554.66 614.89 143.68 o -9 1 0 1077.30 1237.24 156.28 o -8 1 0 2183.94 2473.11 165.33 o -7 1 0 2845.17 3150.18 294.59 o -6 1 0 3138.97 2998.38 185.92 o -5 1 0 4108.24 4021.39 127.02 o -4 1 0 11046.03 11167.92 234.62 o -3 1 0 8196.55 8171.72 173.31 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