#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/17/2211742.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211742_Fobs loop_ _publ_author_name 'Smith, Graham' 'Wermuth, Urs D.' 'Healy, Peter C.' 'White, Jonathan M.' _publ_section_title ; Guanidinium 2-amino-4-nitrobenzoate monohydrate at 130K ; _journal_coeditor_code BT2212 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o7 _journal_page_last o9 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.006 _cell_angle_gamma 90.000 _cell_length_a 16.1223 _cell_length_b 3.7796 _cell_length_c 19.7147 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bt2212Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jmwgs108 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1069.40 1134.33 68.45 o 6 0 0 225.97 207.01 9.18 o 8 0 0 6777.61 7009.34 297.41 o 10 0 0 2153.74 2252.24 95.77 o 12 0 0 21.07 18.26 3.37 o 14 0 0 207.95 192.59 13.88 o 16 0 0 204.51 217.29 15.93 o 18 0 0 115.52 118.26 11.62 o 1 1 0 280.50 268.93 11.17 o 2 1 0 849.33 866.38 16.27 o 3 1 0 482.59 492.23 12.04 o 4 1 0 373.37 341.69 8.20 o 5 1 0 476.97 484.84 11.56 o 6 1 0 1.36 0.22 0.59 o 7 1 0 1148.55 1119.17 25.32 o 8 1 0 465.58 436.93 11.12 o 9 1 0 887.04 876.38 26.93 o 10 1 0 7.04 10.93 2.07 o 11 1 0 54.18 59.59 4.16 o 12 1 0 33.55 32.45 3.42 o 13 1 0 316.06 292.80 14.26 o 14 1 0 6.55 10.73 2.50 o 15 1 0 47.92 39.58 4.20 o 16 1 0 130.34 127.78 7.32 o 17 1 0 101.31 104.68 7.53 o 0 2 0 302.14 237.88 13.22 o 1 2 0 65.32 66.07 3.88 o 2 2 0 4221.40 4242.20 112.03 o 3 2 0 4518.35 4701.67 85.76 o 4 2 0 3783.07 4018.59 91.15 o 5 2 0 250.89 259.55 8.05 o 6 2 0 188.93 199.78 6.21 o 7 2 0 61.95 63.36 3.08 o 8 2 0 22.68 23.17 2.15 o 9 2 0 71.78 76.74 3.65 o 10 2 0 144.09 143.21 5.47 o 11 2 0 279.68 260.78 8.28 o 12 2 0 17.47 22.48 2.52 o 13 2 0 136.82 127.82 9.64 o 14 2 0 28.75 21.50 7.77 o 15 2 0 67.52 65.88 9.74 o 16 2 0 1.86 0.14 2.71 o 1 3 0 155.99 147.22 5.66 o 2 3 0 223.54 190.75 12.24 o 3 3 0 187.32 182.60 5.66 o 4 3 0 5.59 8.32 1.60 o 5 3 0 44.50 40.74 2.95 o 6 3 0 60.86 57.31 4.10 o 7 3 0 416.27 418.15 13.40 o 8 3 0 379.35 351.24 12.09 o 9 3 0 137.52 149.53 6.96 o 10 3 0 0.01 1.39 1.48 o 11 3 0 13.87 15.58 2.84 o 12 3 0 29.64 28.06 5.49 o 13 3 0 3.33 3.97 3.05 o 0 4 0 365.61 338.47 16.35 o 1 4 0 42.50 40.49 5.53 o 2 4 0 12.55 10.49 2.94 o 3 4 0 63.21 62.89 5.40 o 4 4 0 4.20 3.17 3.06 o 5 4 0 118.01 111.44 8.79 o 6 4 0 170.99 143.65 10.38 o 7 4 0 236.76 229.83 20.09 o 8 4 0 27.65 31.40 5.80 o -17 0 1 11.21 15.65 4.97 o -15 0 1 173.37 157.08 12.49 o -13 0 1 12.44 11.41 3.58 o -9 0 1 40.66 39.92 3.67 o -7 0 1 2234.26 2249.06 81.00 o -5 0 1 644.73 592.12 22.30 o -3 0 1 15.77 12.38 1.70 o -1 0 1 365.58 306.65 18.50 o 1 0 1 1120.69 1064.39 47.03 o 9 0 1 260.08 256.69 12.00 o 11 0 1 1.68 0.76 1.54 o 13 0 1 28.19 31.27 5.32 o 15 0 1 277.93 265.85 17.98 o 17 0 1 135.43 104.14 10.57 o -17 1 1 8.10 10.82 3.15 o -16 1 1 56.09 51.41 5.38 o -15 1 1 25.25 19.71 3.13 o -14 1 1 66.10 73.20 5.18 o -13 1 1 247.01 238.45 10.05 o -12 1 1 91.36 93.51 5.41 o -11 1 1 9.66 7.52 1.93 o -10 1 1 152.20 154.78 8.78 o -9 1 1 204.01 208.52 6.40 o -8 1 1 153.63 151.84 4.99 o -7 1 1 3329.09 3645.60 83.74 o -6 1 1 124.96 161.14 5.15 o -5 1 1 938.96 1015.20 24.05 o -4 1 1 24.27 21.17 1.48 o -3 1 1 130.66 116.02 3.69 o -2 1 1 3947.45 4331.53 78.74 o -1 1 1 5674.47 5726.42 176.79 o 0 1 1 9021.67 8595.86 264.68 o 1 1 1 11086.01 11225.57 231.68 o 2 1 1 33904.49 33493.11 907.17 o 3 1 1 18642.79 18897.02 367.82 o 4 1 1 10.53 11.13 1.23 o 5 1 1 3.94 2.26 0.61 o 6 1 1 737.34 724.23 18.20 o 7 1 1 676.34 681.23 16.08 o 8 1 1 766.95 789.14 21.75 o 9 1 1 136.82 142.04 6.38 o 10 1 1 1081.15 1073.10 32.52 o 11 1 1 577.77 568.59 18.93 o 12 1 1 112.45 111.94 6.12 o 13 1 1 7.83 12.38 2.57 o 14 1 1 7.41 3.27 1.84 o 15 1 1 34.29 28.96 3.80 o 16 1 1 83.54 88.65 8.12 o 17 1 1 0.84 2.44 2.12 o -16 2 1 72.26 76.11 10.57 o -15 2 1 24.33 27.13 6.14 o -14 2 1 81.19 74.83 9.52 o -13 2 1 42.33 36.47 3.16 o -12 2 1 3.05 3.00 1.39 o -11 2 1 5.35 8.50 1.75 o -10 2 1 9.31 11.99 1.86 o -9 2 1 148.03 151.50 5.52 o -8 2 1 170.08 173.10 5.85 o -7 2 1 949.06 936.45 23.42 o -6 2 1 5.25 4.88 1.28 o -5 2 1 3086.77 3268.94 75.21 o -4 2 1 110.19 127.47 4.70 o -3 2 1 110.91 116.23 3.48 o -2 2 1 846.34 850.78 20.82 o -1 2 1 126.69 116.91 5.59 o 0 2 1 159.66 156.67 6.80 o 1 2 1 1227.00 1142.62 37.32 o 2 2 1 41.85 36.00 1.63 o 3 2 1 406.75 441.21 8.87 o 4 2 1 118.58 142.27 4.67 o 5 2 1 873.97 920.22 21.17 o 6 2 1 211.65 218.83 6.50 o 7 2 1 45.29 51.21 2.75 o 8 2 1 6.01 4.66 1.17 o 9 2 1 10.98 15.96 1.94 o 10 2 1 164.13 153.87 5.68 o 11 2 1 696.94 675.27 17.25 o 12 2 1 9.54 8.59 3.08 o 13 2 1 21.71 12.15 3.54 o 14 2 1 36.07 23.65 7.76 o 15 2 1 14.59 17.09 4.74 o -13 3 1 26.24 21.62 3.30 o -12 3 1 1.42 2.60 2.37 o -11 3 1 30.68 30.51 3.67 o -10 3 1 199.01 219.76 9.05 o -9 3 1 1.77 2.64 1.57 o -8 3 1 51.35 51.23 4.14 o -7 3 1 22.55 22.55 2.50 o -6 3 1 14.16 13.35 2.02 o -5 3 1 516.50 520.35 15.27 o -4 3 1 57.45 53.01 2.75 o -3 3 1 485.54 499.09 20.55 o -2 3 1 8.79 9.90 1.59 o -1 3 1 4.92 3.12 1.05 o 0 3 1 19.65 18.73 2.43 o 1 3 1 4.77 4.21 1.11 o 2 3 1 304.33 288.37 7.35 o 3 3 1 422.15 424.08 10.83 o 4 3 1 318.63 280.61 9.69 o 5 3 1 2169.50 1998.74 51.40 o 6 3 1 876.05 855.43 24.07 o 7 3 1 72.72 71.67 4.55 o 8 3 1 8.13 7.48 2.02 o 9 3 1 0.83 3.51 2.38 o 10 3 1 0.16 2.68 2.38 o 11 3 1 0.01 1.43 2.48 o 12 3 1 62.34 51.22 12.78 o 13 3 1 211.52 259.86 20.77 o -8 4 1 83.29 86.54 10.99 o -7 4 1 188.62 152.22 20.02 o -6 4 1 6.77 8.32 3.11 o -5 4 1 0.15 1.18 1.69 o -4 4 1 49.20 43.44 13.58 o -3 4 1 9.44 4.39 2.63 o -2 4 1 1.23 0.16 3.91 o -1 4 1 5.19 8.24 3.10 o 0 4 1 211.96 186.82 10.24 o 1 4 1 0.03 0.92 1.68 o 2 4 1 144.23 141.43 9.67 o 3 4 1 0.05 2.88 2.29 o 4 4 1 24.46 27.83 5.88 o 5 4 1 4.73 7.77 4.24 o 6 4 1 30.51 32.21 6.87 o 7 4 1 58.77 60.92 13.11 o -18 0 2 5.40 4.83 3.34 o -16 0 2 80.45 73.95 8.21 o -14 0 2 0.26 0.00 2.02 o -12 0 2 166.78 165.76 15.08 o -10 0 2 91.00 89.92 7.48 o -8 0 2 35.41 44.26 3.53 o -6 0 2 298.32 289.22 15.34 o -4 0 2 11586.41 11650.17 507.10 o -2 0 2 3.18 4.53 0.49 o 8 0 2 185.00 180.86 13.48 o 10 0 2 1006.90 1040.40 60.31 o 12 0 2 363.89 374.73 33.84 o 14 0 2 98.99 88.11 8.87 o 16 0 2 40.65 33.46 6.47 o -18 1 2 76.93 84.99 7.43 o -17 1 2 0.21 1.36 2.49 o -16 1 2 66.24 56.67 9.89 o -15 1 2 55.27 58.21 9.47 o -14 1 2 4.36 8.70 2.21 o -13 1 2 12.09 15.25 2.70 o -12 1 2 0.35 1.63 1.40 o -11 1 2 136.45 125.23 7.26 o -10 1 2 59.12 55.75 3.74 o -9 1 2 390.66 383.44 10.87 o -8 1 2 1229.81 1241.70 30.02 o -7 1 2 47.00 38.30 2.34 o -6 1 2 67.56 59.77 2.71 o -5 1 2 949.95 955.54 22.86 o -4 1 2 55.27 66.41 2.69 o -3 1 2 2563.05 2542.97 58.00 o -2 1 2 1250.54 1319.26 24.67 o -1 1 2 494.47 549.12 16.04 o 0 1 2 636.01 632.00 18.16 o 1 1 2 0.36 0.29 0.29 o 2 1 2 76.95 82.60 2.80 o 3 1 2 2556.83 2495.81 49.18 o 4 1 2 265.53 271.87 6.39 o 5 1 2 672.03 665.44 15.16 o 6 1 2 33.02 48.48 2.21 o 7 1 2 860.77 936.90 27.78 o 8 1 2 572.51 576.29 16.39 o 9 1 2 294.36 297.26 18.82 o 10 1 2 99.92 99.47 5.34 o 11 1 2 73.85 64.34 4.34 o 12 1 2 264.95 231.55 9.80 o 13 1 2 264.61 245.94 10.39 o 14 1 2 260.69 228.95 10.11 o 15 1 2 3.69 10.12 2.59 o 16 1 2 102.67 98.82 8.78 o -16 2 2 21.10 25.60 3.85 o -15 2 2 0.18 1.92 1.71 o -14 2 2 33.02 36.99 4.28 o -13 2 2 2.07 2.74 1.53 o -12 2 2 5.68 4.33 1.44 o -11 2 2 185.95 183.84 6.60 o -10 2 2 242.92 239.45 7.63 o -9 2 2 0.57 1.22 1.00 o -8 2 2 7.06 8.30 1.55 o -7 2 2 163.41 169.21 6.05 o -6 2 2 365.12 380.60 10.80 o -5 2 2 253.68 277.96 7.63 o -4 2 2 216.45 255.88 6.66 o -3 2 2 105.03 114.86 3.27 o -2 2 2 324.37 345.43 8.86 o -1 2 2 82.39 86.44 4.04 o 0 2 2 2.43 1.87 0.89 o 1 2 2 178.75 152.18 5.83 o 2 2 2 159.21 148.30 4.29 o 3 2 2 331.90 324.62 8.41 o 4 2 2 4453.32 4600.23 97.84 o 5 2 2 1625.66 1687.34 37.32 o 6 2 2 588.39 590.75 19.12 o 7 2 2 137.55 136.08 4.78 o 8 2 2 16.27 18.12 1.93 o 9 2 2 5.42 6.03 1.39 o 10 2 2 21.22 18.14 3.96 o 11 2 2 39.68 36.89 8.52 o 12 2 2 205.84 198.05 15.86 o 13 2 2 251.17 233.25 18.02 o 14 2 2 6.63 11.28 4.18 o 15 2 2 6.12 10.67 4.38 o -13 3 2 14.89 15.06 4.26 o -12 3 2 13.31 16.64 3.03 o -11 3 2 54.69 54.53 4.64 o -10 3 2 2.07 2.99 1.64 o -9 3 2 3.94 3.79 1.51 o -8 3 2 4.28 4.00 1.57 o -7 3 2 81.35 81.61 4.39 o -6 3 2 57.13 57.51 3.83 o -5 3 2 665.96 621.40 17.07 o -4 3 2 0.52 0.98 0.95 o -3 3 2 290.33 288.78 7.44 o -2 3 2 182.76 180.25 6.01 o -1 3 2 27.44 28.95 2.90 o 0 3 2 53.39 60.47 3.91 o 1 3 2 85.63 85.60 3.62 o 2 3 2 1.29 4.73 1.53 o 3 3 2 465.41 487.74 14.56 o 4 3 2 3.27 1.93 1.37 o 5 3 2 17.27 17.62 2.43 o 6 3 2 107.60 119.51 5.67 o 7 3 2 98.21 107.94 8.38 o 8 3 2 97.34 91.43 7.91 o 9 3 2 27.86 22.56 5.29 o 10 3 2 157.12 154.25 11.88 o 11 3 2 87.39 71.74 17.08 o 12 3 2 15.52 11.11 3.89 o -8 4 2 79.31 86.22 12.58 o -7 4 2 52.62 47.22 6.24 o -6 4 2 5.25 6.06 2.81 o -5 4 2 2.26 2.19 2.75 o -4 4 2 29.78 22.93 5.36 o -3 4 2 13.06 13.39 3.86 o -2 4 2 40.39 42.78 6.02 o -1 4 2 2.49 5.25 2.12 o 0 4 2 2.59 2.80 1.78 o 1 4 2 4.39 8.87 3.58 o 2 4 2 17.46 18.52 4.12 o 3 4 2 5.54 6.13 2.86 o 4 4 2 69.46 62.12 6.94 o 5 4 2 39.46 34.32 5.62 o 6 4 2 346.78 307.18 17.36 o 7 4 2 170.41 140.78 14.23 o -17 0 3 80.12 65.08 8.59 o -15 0 3 204.27 206.51 15.06 o -13 0 3 48.71 47.06 6.50 o -11 0 3 4.36 5.97 2.11 o -9 0 3 327.00 302.75 17.18 o -7 0 3 502.40 457.15 23.20 o -5 0 3 1203.28 1206.17 54.85 o -3 0 3 991.44 1041.80 25.74 o -1 0 3 481.41 394.86 7.80 o 7 0 3 4.93 7.49 1.92 o 9 0 3 1013.18 1148.67 58.07 o 11 0 3 0.46 3.71 4.14 o 13 0 3 179.42 177.99 10.66 o 15 0 3 549.53 571.00 32.21 o 17 0 3 103.17 98.09 10.54 o -18 1 3 2.25 5.17 2.54 o -17 1 3 3.34 4.00 2.26 o -16 1 3 91.85 100.04 6.36 o -15 1 3 10.42 9.16 2.37 o -14 1 3 44.53 48.28 4.41 o -13 1 3 17.72 20.97 2.98 o -12 1 3 1.16 1.54 1.26 o -11 1 3 10.44 9.89 1.65 o -10 1 3 12.11 13.67 1.83 o -9 1 3 131.56 122.28 4.79 o -8 1 3 6.08 5.66 1.45 o -7 1 3 884.95 885.33 21.74 o -6 1 3 5.65 10.03 1.29 o -5 1 3 0.76 1.47 0.78 o -4 1 3 2313.96 2379.74 54.40 o -3 1 3 216.04 212.70 4.88 o -2 1 3 2711.17 2580.93 58.71 o 0 1 3 83.40 76.91 2.96 o 1 1 3 356.20 335.72 7.72 o 2 1 3 143.04 98.55 5.12 o 3 1 3 161.02 132.63 4.23 o 4 1 3 176.58 167.30 4.47 o 5 1 3 3.02 2.50 0.65 o 6 1 3 197.65 182.71 11.96 o 7 1 3 9.70 11.22 1.60 o 8 1 3 304.43 276.56 8.98 o 9 1 3 95.75 96.40 4.53 o 10 1 3 1.94 1.42 1.19 o 11 1 3 2.61 1.44 1.36 o 12 1 3 0.43 1.22 1.42 o 13 1 3 150.82 145.96 7.73 o 14 1 3 197.29 183.14 15.15 o 15 1 3 35.11 43.64 9.51 o 16 1 3 132.54 134.63 10.25 o -16 2 3 54.81 63.69 7.67 o -15 2 3 8.48 8.02 2.39 o -14 2 3 22.82 20.62 2.70 o -13 2 3 76.09 77.45 4.32 o -12 2 3 6.80 8.63 1.87 o -11 2 3 45.50 41.41 3.37 o -10 2 3 66.65 60.84 3.71 o -9 2 3 3.60 4.89 1.38 o -8 2 3 55.04 50.95 3.23 o -7 2 3 28.64 33.89 3.58 o -6 2 3 455.59 458.25 12.63 o -5 2 3 337.83 338.33 11.16 o -4 2 3 0.00 0.94 0.64 o -3 2 3 2.15 2.21 0.74 o -2 2 3 27.17 26.37 1.76 o -1 2 3 954.08 912.35 26.89 o 0 2 3 77.93 78.10 3.70 o 1 2 3 242.18 245.08 6.46 o 2 2 3 4.13 3.93 0.75 o 3 2 3 0.96 0.00 0.62 o 4 2 3 22.26 21.19 1.67 o 5 2 3 726.80 754.74 17.70 o 6 2 3 20.68 22.34 1.84 o 7 2 3 177.14 151.24 5.13 o 8 2 3 40.19 44.56 3.70 o 9 2 3 91.31 96.43 4.77 o 10 2 3 255.10 222.90 13.16 o 11 2 3 1.68 4.58 2.80 o 12 2 3 485.03 496.81 30.26 o 13 2 3 0.33 0.00 2.97 o 14 2 3 2.28 3.93 3.10 o 15 2 3 0.21 2.03 2.79 o -14 3 3 0.21 3.17 1.98 o -13 3 3 13.65 21.18 3.22 o -12 3 3 0.33 0.00 1.60 o -11 3 3 4.05 5.43 2.02 o -10 3 3 18.51 16.66 2.37 o -9 3 3 3.46 3.26 1.46 o -8 3 3 105.90 119.27 5.55 o -7 3 3 6.71 7.24 1.80 o -6 3 3 12.47 11.77 2.05 o -5 3 3 3.29 2.72 1.43 o -4 3 3 0.58 0.47 0.98 o -3 3 3 0.00 0.04 0.93 o -2 3 3 16.84 14.32 1.78 o -1 3 3 18.64 15.13 2.22 o 0 3 3 24.96 17.64 3.23 o 1 3 3 66.49 56.97 3.42 o 2 3 3 7.72 10.00 1.84 o 3 3 3 36.15 35.00 4.89 o 4 3 3 176.27 154.24 9.79 o 5 3 3 11.04 8.62 2.94 o 6 3 3 624.92 557.56 28.66 o 7 3 3 69.89 54.26 10.89 o 8 3 3 31.10 33.12 5.37 o 9 3 3 82.42 68.65 21.67 o 10 3 3 148.27 145.15 11.02 o 11 3 3 67.94 56.07 19.95 o 12 3 3 0.29 1.30 2.73 o -8 4 3 6.57 7.41 5.58 o -7 4 3 0.01 2.10 2.40 o -6 4 3 8.48 10.50 3.79 o -5 4 3 0.62 0.00 2.57 o -4 4 3 12.86 14.92 3.93 o -3 4 3 178.01 196.69 7.21 o -2 4 3 0.10 0.00 1.54 o -1 4 3 37.57 35.51 4.16 o 0 4 3 23.28 23.89 7.46 o 1 4 3 0.25 2.05 2.78 o 2 4 3 33.19 33.92 5.62 o 3 4 3 5.32 8.75 3.19 o 4 4 3 3.20 9.57 4.66 o 5 4 3 0.01 0.00 2.03 o 6 4 3 0.27 2.27 2.86 o 7 4 3 1.01 6.38 3.18 o -18 0 4 3.23 2.54 2.96 o -16 0 4 3.22 3.30 2.85 o -14 0 4 191.33 171.58 13.15 o -12 0 4 284.55 286.33 18.78 o -10 0 4 205.45 198.61 12.87 o -8 0 4 413.13 383.66 20.49 o -6 0 4 1.60 2.43 0.92 o -4 0 4 5505.30 5801.59 139.57 o -2 0 4 989.51 888.64 26.35 o 0 0 4 3847.00 3294.65 272.11 o 6 0 4 1.58 1.07 1.09 o 8 0 4 36.42 48.91 4.43 o 10 0 4 340.34 351.69 40.16 o 12 0 4 47.15 42.79 5.20 o 14 0 4 30.11 35.65 6.26 o 16 0 4 251.00 234.61 17.25 o -18 1 4 128.34 126.69 8.71 o -17 1 4 334.92 312.28 14.98 o -16 1 4 30.09 26.99 3.76 o -15 1 4 111.99 107.74 6.41 o -14 1 4 220.07 207.58 9.34 o -13 1 4 17.97 19.81 2.98 o -12 1 4 54.31 52.81 4.74 o -11 1 4 94.67 98.75 4.51 o -10 1 4 22.39 22.81 2.26 o -9 1 4 0.50 0.44 0.82 o -8 1 4 389.55 334.65 9.60 o -7 1 4 174.12 168.69 5.60 o -6 1 4 186.53 184.72 6.83 o -5 1 4 156.00 133.88 4.00 o -4 1 4 31.17 30.09 1.82 o -3 1 4 60.67 62.04 2.85 o -2 1 4 389.07 391.93 9.91 o -1 1 4 95.18 86.83 3.08 o 0 1 4 196.66 202.55 8.88 o 3 1 4 28.87 25.38 1.26 o 4 1 4 53.87 56.77 2.83 o 5 1 4 42.05 43.81 2.58 o 6 1 4 8.82 5.69 1.47 o 7 1 4 148.62 137.01 25.97 o 8 1 4 40.87 38.29 2.96 o 9 1 4 15.33 13.21 1.96 o 10 1 4 0.00 0.05 1.16 o 11 1 4 177.99 177.67 8.88 o 12 1 4 6.99 4.94 2.80 o 13 1 4 59.25 54.70 6.32 o 14 1 4 116.99 125.98 11.15 o 15 1 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