#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:23:50 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181037 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/17/2211754.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211754_Fobs loop_ _publ_author_name 'van Blerk, Charmaine' 'Kruger, Gert J.' _publ_section_title ; Butane-1,4-diammonium dibromide ; _journal_coeditor_code CF2076 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o342 _journal_page_last o344 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.037 _cell_angle_gamma 90.000 _cell_length_a 4.7107 _cell_length_b 8.5491 _cell_length_c 11.2286 _exptl_crystal_F_000 244.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file cf2076Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6ccvb2_s in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1187.95 1598.90 14.52 o 2 0 0 379.09 378.74 7.37 o 3 0 0 809.14 982.79 16.11 o 4 0 0 2588.69 3101.85 36.22 o 5 0 0 318.45 345.81 14.05 o 6 0 0 122.98 112.82 12.62 o 1 1 0 3196.71 3794.48 49.86 o 2 1 0 2043.48 2471.37 16.91 o 3 1 0 1122.75 1158.54 45.73 o 4 1 0 80.42 90.59 7.53 o 5 1 0 87.17 94.18 10.30 o 6 1 0 34.66 30.21 6.36 o 0 2 0 397.71 440.92 5.77 o 1 2 0 1430.80 1584.20 45.71 o 2 2 0 3.24 5.81 1.69 o 3 2 0 163.68 185.32 7.16 o 4 2 0 127.27 142.21 12.39 o 5 2 0 74.96 76.16 15.30 o 6 2 0 0.93 -2.52 4.10 o 1 3 0 5090.41 5182.10 121.40 o 2 3 0 3975.34 4408.27 21.49 o 3 3 0 2755.22 3219.48 23.08 o 4 3 0 35.43 34.40 3.67 o 5 3 0 63.47 66.33 4.77 o 6 3 0 149.85 145.65 9.20 o 0 4 0 4964.79 4176.36 93.31 o 1 4 0 2597.85 2737.92 42.73 o 2 4 0 55.16 69.95 3.83 o 3 4 0 461.23 526.09 7.64 o 4 4 0 703.44 761.78 9.89 o 5 4 0 261.39 257.66 12.29 o 1 5 0 3.63 3.57 1.92 o 2 5 0 1.29 5.86 2.43 o 3 5 0 3.61 6.85 3.20 o 4 5 0 3.95 3.64 4.90 o 5 5 0 0.02 -5.46 5.46 o 0 6 0 2157.18 2088.05 56.97 o 1 6 0 1571.64 1436.23 22.33 o 2 6 0 27.23 30.47 4.31 o 3 6 0 356.84 400.37 10.15 o 4 6 0 383.93 472.01 12.30 o 5 6 0 174.45 188.01 10.56 o 1 7 0 646.60 570.16 12.34 o 2 7 0 1803.14 1964.12 56.15 o 3 7 0 484.75 566.37 12.69 o 4 7 0 37.80 43.45 6.99 o 0 8 0 3.18 -4.14 6.44 o 1 8 0 291.59 256.70 8.03 o 2 8 0 2.95 -4.20 4.90 o 3 8 0 20.76 28.32 6.26 o 4 8 0 0.48 -6.47 6.47 o 1 9 0 179.02 168.68 11.29 o 2 9 0 238.40 271.04 10.33 o 3 9 0 100.25 107.88 12.82 o 0 10 0 637.65 587.54 19.77 o 1 10 0 262.84 227.23 8.49 o 2 10 0 12.98 13.81 8.70 o 3 10 0 75.88 72.63 11.65 o 1 11 0 13.33 9.47 5.60 o -6 1 1 86.91 90.40 7.58 o -5 1 1 25.24 27.85 5.02 o -4 1 1 629.92 756.07 34.84 o -3 1 1 2697.53 3066.61 28.51 o -2 1 1 3917.27 5002.54 87.43 o -1 1 1 7.42 14.00 3.28 o 0 1 1 1257.56 1276.13 44.88 o 1 1 1 9554.07 10566.79 347.00 o 2 1 1 4648.86 5220.55 112.13 o 3 1 1 383.35 405.30 9.43 o 4 1 1 49.86 61.99 16.10 o 5 1 1 417.15 503.41 17.81 o 6 1 1 113.30 116.12 9.05 o -6 2 1 152.40 145.55 9.41 o -5 2 1 612.06 615.34 30.92 o -4 2 1 665.03 697.61 10.35 o -3 2 1 0.10 1.31 2.13 o -2 2 1 2157.03 2463.14 23.49 o -1 2 1 12592.78 12885.91 94.82 o 0 2 1 7676.96 7047.61 117.51 o 1 2 1 796.31 955.53 17.60 o 2 2 1 689.20 822.22 9.14 o 3 2 1 3184.69 3691.56 50.82 o 4 2 1 1227.33 1397.26 23.42 o 5 2 1 201.30 223.50 29.34 o 6 2 1 2.35 -2.20 4.77 o -6 3 1 8.30 0.43 8.91 o -5 3 1 0.05 -2.18 3.93 o -4 3 1 199.40 212.91 6.44 o -3 3 1 49.34 58.02 3.58 o -2 3 1 914.24 1025.67 7.78 o -1 3 1 20.68 29.49 2.40 o 0 3 1 727.48 678.68 10.14 o 1 3 1 68.41 76.00 2.44 o 2 3 1 900.62 1084.61 11.42 o 3 3 1 33.05 34.49 3.23 o 4 3 1 12.16 9.21 3.45 o 5 3 1 20.60 17.71 4.09 o 6 3 1 19.74 13.06 5.20 o -5 4 1 185.30 197.40 9.17 o -4 4 1 128.41 146.93 6.64 o -3 4 1 116.20 137.52 10.56 o -2 4 1 1929.33 2023.48 34.75 o -1 4 1 766.91 693.76 6.87 o 0 4 1 2700.68 2371.05 35.14 o 1 4 1 841.30 862.69 15.44 o 2 4 1 1316.43 1532.05 41.07 o 3 4 1 165.22 188.84 5.94 o 4 4 1 808.50 851.86 10.48 o 5 4 1 19.82 18.90 4.43 o -5 5 1 10.17 8.64 6.43 o -4 5 1 368.25 413.65 14.00 o -3 5 1 2650.32 2986.56 123.97 o -2 5 1 1291.34 1421.24 10.24 o -1 5 1 284.08 271.35 6.89 o 0 5 1 1469.15 1254.59 8.49 o 1 5 1 5043.25 5215.77 36.94 o 2 5 1 2395.62 2744.87 24.67 o 3 5 1 423.41 460.82 7.90 o 4 5 1 70.40 83.56 6.88 o 5 5 1 254.90 244.02 9.90 o -5 6 1 107.58 114.88 8.67 o -4 6 1 66.09 70.15 6.92 o -3 6 1 0.02 1.19 4.76 o -2 6 1 361.85 374.43 10.10 o -1 6 1 1031.69 919.41 15.99 o 0 6 1 769.74 700.62 14.70 o 1 6 1 145.05 137.06 3.96 o 2 6 1 192.58 201.26 7.27 o 3 6 1 254.22 301.18 20.46 o 4 6 1 240.15 269.09 18.43 o 5 6 1 24.57 25.17 6.45 o -4 7 1 11.35 13.16 6.51 o -3 7 1 109.03 147.19 10.27 o -2 7 1 234.79 219.71 6.28 o -1 7 1 13.05 10.87 3.05 o 0 7 1 1.35 4.04 3.05 o 1 7 1 467.25 459.74 9.88 o 2 7 1 109.52 131.52 7.65 o 3 7 1 10.10 10.23 5.53 o 4 7 1 0.22 5.36 10.05 o -4 8 1 185.28 212.85 11.75 o -3 8 1 0.45 -4.27 5.47 o -2 8 1 411.21 405.83 8.05 o -1 8 1 1183.16 1127.03 16.59 o 0 8 1 1202.54 993.92 14.78 o 1 8 1 86.85 83.78 5.58 o 2 8 1 128.20 137.64 13.17 o 3 8 1 509.59 549.72 18.60 o 4 8 1 254.26 285.38 17.45 o -3 9 1 261.29 276.83 16.27 o -2 9 1 180.71 191.33 9.34 o -1 9 1 17.33 8.97 5.22 o 0 9 1 168.64 165.81 9.53 o 1 9 1 517.26 480.97 10.12 o 2 9 1 303.62 296.79 15.93 o 3 9 1 49.88 50.98 10.83 o -3 10 1 2.22 2.30 9.73 o -2 10 1 0.47 -5.80 5.80 o -1 10 1 9.56 15.26 5.27 o 0 10 1 0.24 2.17 5.48 o 1 10 1 1.68 -0.35 5.05 o 2 10 1 0.19 -3.91 8.39 o -1 11 1 8.81 9.67 5.44 o 0 11 1 101.74 107.27 11.28 o 1 11 1 115.98 120.41 8.13 o -6 0 2 229.50 257.92 15.00 o -5 0 2 509.44 570.20 16.69 o -4 0 2 22.70 26.60 5.61 o -3 0 2 756.09 776.80 13.10 o -2 0 2 8479.60 9942.07 69.54 o -1 0 2 13968.42 15631.84 104.29 o 0 0 2 277.62 295.51 5.72 o 1 0 2 68.22 87.37 4.73 o 2 0 2 7582.44 8740.86 68.25 o 3 0 2 3720.95 4004.38 39.65 o 4 0 2 548.87 601.12 16.55 o 5 0 2 56.51 59.51 9.48 o -6 1 2 11.17 18.76 6.58 o -5 1 2 233.39 256.26 9.28 o -4 1 2 344.16 380.99 8.60 o -3 1 2 1388.98 1625.62 38.02 o -2 1 2 328.45 398.74 18.80 o -1 1 2 2890.97 2999.43 20.22 o 0 1 2 357.19 444.77 15.23 o 1 1 2 8475.08 8721.23 233.90 o 2 1 2 437.41 440.89 7.17 o 3 1 2 34.69 34.10 3.74 o 4 1 2 198.34 221.19 9.63 o 5 1 2 320.32 335.80 11.27 o 6 1 2 27.17 33.14 9.17 o -6 2 2 11.42 12.83 6.46 o -5 2 2 93.40 100.35 6.08 o -4 2 2 0.39 -0.81 2.95 o -3 2 2 42.37 50.43 4.66 o -2 2 2 692.10 743.74 6.14 o -1 2 2 1036.66 975.90 20.23 o 0 2 2 195.31 197.94 4.57 o 1 2 2 55.90 57.16 4.89 o 2 2 2 422.47 465.41 8.69 o 3 2 2 340.97 349.79 7.99 o 4 2 2 93.16 83.64 5.80 o 5 2 2 1.82 0.89 7.88 o 6 2 2 4.05 10.24 6.16 o -6 3 2 0.16 4.03 10.13 o -5 3 2 158.21 161.69 6.68 o -4 3 2 1592.02 1723.16 13.62 o -3 3 2 1554.26 1847.44 13.02 o -2 3 2 1092.36 1262.04 35.44 o -1 3 2 1826.93 1729.35 10.91 o 0 3 2 8163.94 7515.88 133.29 o 1 3 2 4832.76 4536.56 216.24 o 2 3 2 2525.12 2890.41 32.51 o 3 3 2 124.87 144.96 7.21 o 4 3 2 555.10 568.44 11.33 o 5 3 2 502.34 440.59 31.84 o -5 4 2 169.36 210.21 10.52 o -4 4 2 9.37 15.51 3.50 o -3 4 2 346.44 378.62 6.33 o -2 4 2 2970.30 3297.59 77.38 o -1 4 2 3017.01 2833.85 29.44 o 0 4 2 988.18 918.07 8.59 o 1 4 2 314.98 324.10 6.68 o 2 4 2 1900.64 1983.64 47.40 o 3 4 2 1282.55 1447.66 19.66 o 4 4 2 391.19 405.05 9.76 o 5 4 2 0.01 -2.43 4.15 o -5 5 2 1.76 -0.05 6.07 o -4 5 2 15.90 25.52 5.53 o -3 5 2 12.19 14.15 4.30 o -2 5 2 46.21 47.46 3.86 o -1 5 2 1.07 3.24 2.06 o 0 5 2 35.80 30.95 2.73 o 1 5 2 5.88 7.64 1.92 o 2 5 2 20.48 24.47 3.11 o 3 5 2 7.89 8.92 3.36 o 4 5 2 0.02 3.03 3.75 o 5 5 2 0.14 -4.57 4.76 o -5 6 2 169.28 182.55 10.91 o -4 6 2 10.07 7.92 5.92 o -3 6 2 249.62 270.89 17.25 o -2 6 2 1169.54 1086.63 15.94 o -1 6 2 2379.47 2089.07 44.12 o 0 6 2 391.42 346.36 11.92 o 1 6 2 165.73 177.62 4.42 o 2 6 2 856.89 956.18 10.33 o 3 6 2 1018.50 1175.75 15.34 o 4 6 2 173.83 182.13 9.45 o 5 6 2 0.01 3.44 5.84 o -4 7 2 543.58 628.30 14.28 o -3 7 2 519.45 576.64 12.25 o -2 7 2 73.65 68.21 3.98 o -1 7 2 96.87 95.87 5.40 o 0 7 2 2578.43 2453.71 60.86 o 1 7 2 1273.05 1348.59 21.71 o 2 7 2 452.64 524.69 12.02 o 3 7 2 0.74 0.24 5.20 o 4 7 2 292.78 341.91 11.58 o -4 8 2 1.85 0.58 6.59 o -3 8 2 41.97 44.63 6.34 o -2 8 2 66.29 58.60 4.46 o -1 8 2 34.03 27.48 3.98 o 0 8 2 86.77 69.18 5.85 o 1 8 2 93.90 94.83 7.26 o 2 8 2 4.39 4.89 7.40 o 3 8 2 55.53 73.24 12.07 o 4 8 2 29.02 51.88 11.72 o -3 9 2 154.26 205.42 15.58 o -2 9 2 52.35 53.63 6.22 o -1 9 2 102.34 100.05 7.86 o 0 9 2 146.83 141.32 9.19 o 1 9 2 476.25 466.66 14.21 o 2 9 2 44.86 44.45 9.25 o 3 9 2 1.76 -5.36 8.86 o -2 10 2 282.14 282.65 23.21 o -1 10 2 445.45 393.79 11.97 o 0 10 2 115.23 106.64 8.92 o 1 10 2 44.93 44.92 6.07 o 2 10 2 207.25 216.70 15.99 o -1 11 2 9.40 11.98 6.28 o 0 11 2 67.82 64.60 6.20 o 1 11 2 110.19 107.78 7.44 o -6 1 3 60.16 69.44 7.75 o -5 1 3 295.60 324.59 17.95 o -4 1 3 1196.57 1370.23 14.01 o -3 1 3 491.75 555.61 11.60 o -2 1 3 500.21 527.93 10.67 o -1 1 3 2534.85 2543.29 12.52 o 0 1 3 13144.21 9557.15 399.93 o 1 1 3 2044.10 2216.96 18.79 o 2 1 3 29.37 32.74 5.67 o 3 1 3 732.51 729.02 23.70 o 4 1 3 1259.45 1201.94 16.90 o 5 1 3 198.09 189.37 9.83 o 6 1 3 28.02 49.89 12.17 o -6 2 3 89.69 101.29 8.59 o -5 2 3 74.81 81.82 6.46 o -4 2 3 150.59 156.14 5.84 o -3 2 3 3208.66 3733.51 20.69 o -2 2 3 3402.71 3563.59 17.23 o -1 2 3 4459.52 4188.76 52.72 o 0 2 3 98.08 107.65 2.10 o 1 2 3 5601.48 5385.27 185.38 o 2 2 3 4296.04 4449.91 58.23 o 3 2 3 1969.20 1989.61 18.77 o 4 2 3 30.85 29.33 4.85 o 5 2 3 121.31 134.62 9.46 o -5 3 3 46.61 45.81 5.85 o -4 3 3 53.51 55.59 3.97 o -3 3 3 171.24 196.72 5.14 o -2 3 3 504.62 552.44 16.48 o -1 3 3 5.80 3.32 2.06 o 0 3 3 1172.26 1107.27 23.21 o 1 3 3 668.45 679.56 20.72 o 2 3 3 153.35 158.67 4.82 o 3 3 3 1.32 1.18 3.54 o 4 3 3 242.18 237.18 9.08 o 5 3 3 14.58 23.32 9.68 o -5 4 3 22.98 20.61 9.36 o -4 4 3 52.51 67.10 6.04 o -3 4 3 585.65 630.29 9.59 o -2 4 3 1478.14 1492.86 9.59 o -1 4 3 906.38 822.46 19.91 o 0 4 3 57.85 53.30 3.38 o 1 4 3 929.17 980.42 13.31 o 2 4 3 1217.60 1307.55 11.31 o 3 4 3 758.89 823.70 10.98 o 4 4 3 2.13 -0.36 5.38 o 5 4 3 17.05 12.48 4.44 o -5 5 3 302.82 348.75 18.41 o -4 5 3 899.99 980.18 15.05 o -3 5 3 165.02 173.30 7.41 o -2 5 3 15.94 15.04 2.57 o -1 5 3 3776.23 3499.19 73.50 o 0 5 3 4243.11 4153.25 44.35 o 1 5 3 1661.01 1757.19 17.37 o 2 5 3 105.29 106.72 5.18 o 3 5 3 1105.48 1169.94 19.11 o 4 5 3 500.67 484.20 31.10 o 5 5 3 288.63 251.26 9.02 o -5 6 3 0.15 0.54 7.16 o -4 6 3 46.96 47.85 6.33 o -3 6 3 228.87 248.58 9.08 o -2 6 3 970.14 796.12 21.96 o -1 6 3 72.50 60.33 3.98 o 0 6 3 2.94 2.96 2.70 o 1 6 3 588.49 615.21 6.96 o 2 6 3 691.56 777.12 9.78 o 3 6 3 179.54 185.87 7.06 o 4 6 3 16.10 14.74 12.04 o 5 6 3 27.70 28.77 6.35 o -4 7 3 59.29 67.33 7.28 o -3 7 3 46.85 58.38 6.08 o -2 7 3 11.65 13.87 3.45 o -1 7 3 53.64 52.59 3.98 o 0 7 3 479.36 463.48 18.69 o 1 7 3 61.66 61.51 4.09 o 2 7 3 1.50 7.06 7.37 o 3 7 3 18.22 24.15 5.50 o 4 7 3 89.28 98.24 8.33 o -4 8 3 55.01 74.78 8.12 o -3 8 3 361.98 365.68 15.74 o -2 8 3 862.48 834.92 10.82 o -1 8 3 490.12 476.34 9.34 o 0 8 3 41.21 47.84 5.56 o 1 8 3 443.47 456.91 11.31 o 2 8 3 1004.55 1076.36 24.28 o 3 8 3 271.73 318.78 16.91 o 4 8 3 6.16 15.70 9.78 o -3 9 3 55.18 57.71 11.63 o -2 9 3 18.88 21.02 5.59 o -1 9 3 482.26 415.76 27.77 o 0 9 3 349.92 305.30 9.99 o 1 9 3 296.57 307.55 9.57 o 2 9 3 0.25 3.97 8.90 o 3 9 3 87.78 103.60 13.47 o -2 10 3 1.90 -5.36 5.36 o -1 10 3 7.95 4.43 6.09 o 0 10 3 6.45 4.29 5.02 o 1 10 3 12.73 16.36 5.47 o 2 10 3 3.14 2.44 9.02 o -1 11 3 74.89 74.27 6.54 o 0 11 3 226.75 204.79 8.67 o -6 0 4 34.39 39.50 10.43 o -5 0 4 10.02 12.38 7.44 o -4 0 4 1332.16 1573.47 23.76 o -3 0 4 3021.53 3419.90 20.98 o -2 0 4 3082.56 2959.87 26.97 o -1 0 4 191.86 204.67 6.44 o 0 0 4 5793.48 4861.40 45.69 o 1 0 4 7346.98 7778.69 65.53 o 2 0 4 4642.55 4622.50 44.32 o 3 0 4 353.90 351.54 12.96 o 4 0 4 169.92 153.74 11.71 o 5 0 4 483.65 448.76 18.45 o -6 1 4 73.31 80.39 8.01 o -5 1 4 170.63 200.43 9.30 o -4 1 4 229.75 268.96 8.48 o -3 1 4 32.49 33.10 2.54 o -2 1 4 1053.66 1018.75 14.78 o -1 1 4 2398.67 2149.60 55.06 o 0 1 4 3911.74 3487.41 73.20 o 1 1 4 45.90 50.26 3.47 o 2 1 4 108.32 101.69 5.71 o 3 1 4 1075.43 1054.22 13.67 o 4 1 4 523.76 478.25 14.22 o 5 1 4 5.02 5.72 5.95 o -6 2 4 20.23 30.47 11.58 o -5 2 4 40.67 48.97 6.21 o -4 2 4 2.86 3.17 4.12 o -3 2 4 697.34 733.55 28.04 o -2 2 4 148.25 140.90 3.37 o -1 2 4 2.15 6.14 1.21 o 0 2 4 3.77 2.62 1.26 o 1 2 4 2127.55 2097.54 97.78 o 2 2 4 71.62 59.90 4.43 o 3 2 4 96.30 90.50 6.50 o 4 2 4 15.48 13.79 4.90 o 5 2 4 58.56 53.08 6.90 o -5 3 4 419.25 502.54 19.01 o -4 3 4 398.39 470.74 14.82 o -3 3 4 1.94 3.36 2.62 o -2 3 4 2599.40 2467.90 17.67 o -1 3 4 5136.65 5127.27 35.84 o 0 3 4 4224.59 4109.52 60.30 o 1 3 4 521.52 502.60 37.12 o 2 3 4 1430.87 1378.07 14.21 o 3 3 4 1504.17 1456.58 41.02 o 4 3 4 980.78 888.76 50.98 o 5 3 4 85.23 92.38 7.91 o -5 4 4 19.36 27.49 10.19 o -4 4 4 438.06 521.20 25.50 o -3 4 4 1359.17 1503.89 72.36 o -2 4 4 933.71 846.19 17.88 o -1 4 4 31.19 26.66 2.38 o 0 4 4 1619.15 1571.76 21.82 o 1 4 4 2903.57 2895.22 40.96 o 2 4 4 1499.58 1590.25 13.27 o 3 4 4 175.00 168.89 6.07 o 4 4 4 102.14 103.54 6.25 o 5 4 4 153.40 127.50 8.50 o -5 5 4 0.33 -5.84 9.28 o -4 5 4 0.48 4.79 5.12 o -3 5 4 53.93 59.58 4.94 o -2 5 4 60.45 52.89 3.52 o -1 5 4 30.33 33.38 2.88 o 0 5 4 29.76 36.40 2.74 o 1 5 4 14.00 15.97 2.56 o 2 5 4 26.22 29.57 3.52 o 3 5 4 21.01 14.56 3.69 o 4 5 4 15.89 15.41 4.41 o 5 5 4 0.37 1.13 4.21 o -5 6 4 28.07 30.65 11.02 o -4 6 4 112.55 127.90 9.35 o -3 6 4 1133.45 1199.96 38.86 o -2 6 4 654.75 544.20 15.72 o -1 6 4 8.56 8.92 3.02 o 0 6 4 254.67 247.77 6.04 o 1 6 4 2309.19 2411.92 24.13 o 2 6 4 811.88 901.26 10.66 o 3 6 4 80.19 73.31 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