#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:23:50 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181037 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/17/2211757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211757_Fobs loop_ _publ_author_name 'Sukanya, Duraiswamy' 'Natarajan, Karuppannan' 'Dobosh, Brian' 'Zeller, Matthias' _publ_section_title ; Carbonyl(5-carboxypyridine-2-carboxylato-\k^2^N,O^2^)chlorobis(triphenylphosphine-\kP)ruthenium(II) 0.345-hydrate benzene sesquisolvate ; _journal_coeditor_code CI2218 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m135 _journal_page_last m137 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.678 _cell_angle_beta 96.295 _cell_angle_gamma 115.790 _cell_length_a 9.9570 _cell_length_b 11.0361 _cell_length_c 22.9009 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file ci2218Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 06bd001m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7520.80 7422.81 134.60 o 2 0 0 804.22 711.15 10.14 o 3 0 0 10046.58 11180.38 207.70 o 4 0 0 386.08 244.29 4.92 o 5 0 0 2642.45 2909.57 39.87 o 6 0 0 527.41 624.81 10.90 o 7 0 0 127.85 127.83 4.48 o 8 0 0 91.97 94.69 3.95 o 9 0 0 17.19 19.00 2.81 o 10 0 0 290.95 234.00 13.71 o 11 0 0 893.69 966.23 33.34 o -12 1 0 0.24 13.21 5.41 o -11 1 0 30.90 59.88 7.42 o -10 1 0 577.88 555.56 21.81 o -9 1 0 1.13 5.17 1.93 o -8 1 0 52.82 52.26 4.01 o -7 1 0 2299.62 2465.46 35.08 o -6 1 0 724.96 695.87 12.00 o -5 1 0 2658.22 2616.72 53.59 o -4 1 0 116.06 94.05 5.41 o -3 1 0 322.20 272.80 11.27 o -2 1 0 28038.24 29035.02 378.29 o -1 1 0 23038.45 23511.79 433.36 o 0 1 0 1.34 14.82 0.81 o 1 1 0 16211.94 16896.57 221.26 o 2 1 0 688.40 686.68 13.78 o 3 1 0 2041.36 2170.16 29.60 o 4 1 0 53.77 68.23 2.44 o 5 1 0 1496.03 1671.84 24.28 o 6 1 0 675.74 634.56 11.30 o 7 1 0 118.52 117.49 6.97 o 8 1 0 92.85 72.47 6.79 o 9 1 0 2818.58 2795.67 49.51 o 10 1 0 383.30 417.21 19.25 o 11 1 0 421.62 444.81 21.64 o -12 2 0 73.73 61.10 8.09 o -11 2 0 178.67 150.46 11.20 o -10 2 0 304.67 299.75 10.48 o -9 2 0 91.37 102.77 12.52 o -8 2 0 2625.45 2615.48 37.37 o -7 2 0 4873.02 4955.49 66.79 o -6 2 0 889.75 933.00 14.67 o -5 2 0 3393.92 3454.76 46.51 o -4 2 0 3522.09 3717.24 49.39 o -3 2 0 51.85 10.15 3.59 o -2 2 0 1147.88 1194.41 39.24 o -1 2 0 2700.36 2885.58 52.15 o 0 2 0 182.83 308.13 7.30 o 1 2 0 104.18 144.37 8.39 o 2 2 0 65.54 50.53 4.21 o 3 2 0 1436.02 1169.41 17.07 o 4 2 0 584.23 503.02 8.86 o 5 2 0 0.29 4.32 1.78 o 6 2 0 1808.19 1793.23 26.68 o 7 2 0 1899.24 1890.03 28.54 o 8 2 0 1146.78 1210.60 24.58 o 9 2 0 2.21 8.78 3.21 o 10 2 0 2030.88 2270.25 63.49 o -12 3 0 28.69 34.93 7.38 o -11 3 0 405.46 372.09 17.61 o -10 3 0 1666.23 1756.43 35.22 o -9 3 0 403.69 385.60 11.61 o -8 3 0 41.00 53.50 2.94 o -7 3 0 2641.65 2528.79 35.62 o -6 3 0 1459.27 1290.89 24.59 o -5 3 0 757.99 863.06 13.19 o -4 3 0 1005.29 1041.90 15.20 o -3 3 0 10799.74 12327.76 159.56 o -2 3 0 1247.32 1234.10 17.24 o -1 3 0 1458.89 1535.92 21.02 o 0 3 0 4239.44 4848.35 63.52 o 1 3 0 4.54 31.66 1.72 o 2 3 0 526.86 415.52 7.24 o 3 3 0 393.21 397.92 7.39 o 4 3 0 6042.38 5803.72 77.32 o 5 3 0 2165.57 2220.93 32.02 o 6 3 0 715.92 644.70 12.08 o 7 3 0 134.41 138.65 6.46 o 8 3 0 291.39 288.35 10.00 o 9 3 0 3154.98 3293.34 58.62 o 10 3 0 210.58 231.57 14.89 o -12 4 0 1753.86 1787.82 52.04 o -11 4 0 949.50 931.41 34.62 o -10 4 0 67.21 61.64 5.14 o -9 4 0 3343.32 3394.18 60.53 o -8 4 0 524.65 513.98 9.77 o -7 4 0 276.05 278.47 6.18 o -6 4 0 1856.21 1947.92 27.72 o -5 4 0 13.11 9.78 1.76 o -4 4 0 3489.38 3676.29 92.98 o -3 4 0 2981.82 3074.94 41.23 o -2 4 0 156.09 127.80 3.04 o -1 4 0 5377.19 5607.43 73.44 o 0 4 0 468.43 387.18 10.90 o 1 4 0 9802.95 10929.04 199.34 o 2 4 0 11040.20 11604.06 151.02 o 3 4 0 7495.31 7783.97 102.53 o 4 4 0 89.07 98.14 4.87 o 5 4 0 695.79 673.37 19.61 o 6 4 0 173.36 185.77 7.10 o 7 4 0 576.98 593.45 15.02 o 8 4 0 811.51 875.71 20.40 o 9 4 0 40.63 35.14 4.73 o -13 5 0 45.78 56.11 8.43 o -12 5 0 23.60 47.15 5.56 o -11 5 0 10.40 17.44 3.57 o -10 5 0 3.22 6.15 2.69 o -9 5 0 8.76 10.92 2.67 o -8 5 0 222.92 210.56 7.77 o -7 5 0 2869.60 2748.77 38.54 o -6 5 0 665.20 702.29 11.74 o -5 5 0 669.60 688.80 18.37 o -4 5 0 6009.43 6142.87 80.92 o -3 5 0 5044.80 5129.21 121.64 o -2 5 0 1432.94 1412.53 20.20 o -1 5 0 4.15 2.99 0.87 o 0 5 0 4129.39 4153.73 55.49 o 1 5 0 4061.91 4185.12 56.18 o 2 5 0 856.18 718.12 12.01 o 3 5 0 759.81 800.89 13.87 o 4 5 0 2184.15 2231.85 48.34 o 5 5 0 177.29 171.71 6.69 o 6 5 0 79.34 91.78 5.35 o 7 5 0 11.36 12.67 3.11 o 8 5 0 622.24 659.36 17.28 o 9 5 0 226.70 306.44 11.44 o -13 6 0 553.11 627.48 25.92 o -12 6 0 70.48 61.56 5.53 o -11 6 0 18.36 20.90 3.78 o -10 6 0 35.13 25.80 3.86 o -9 6 0 1156.75 1179.01 25.22 o -8 6 0 1841.14 1704.50 120.35 o -7 6 0 118.38 95.93 4.25 o -6 6 0 2670.91 2609.07 36.57 o -5 6 0 3883.34 3875.94 104.79 o -4 6 0 2782.68 2911.47 39.93 o -3 6 0 2874.07 2908.93 39.85 o -2 6 0 4390.36 4438.99 59.38 o -1 6 0 56.51 121.46 3.43 o 0 6 0 537.00 562.45 9.75 o 1 6 0 453.08 475.93 8.84 o 2 6 0 371.80 352.72 7.42 o 3 6 0 520.92 449.10 9.15 o 4 6 0 315.27 290.23 8.89 o 5 6 0 73.36 57.37 6.10 o 6 6 0 27.72 31.70 3.78 o 7 6 0 35.92 39.56 4.95 o 8 6 0 62.08 32.98 4.63 o -13 7 0 0.39 0.03 5.49 o -12 7 0 133.12 128.97 7.69 o -11 7 0 77.32 57.68 5.33 o -10 7 0 78.24 111.62 16.21 o -9 7 0 138.41 145.17 7.05 o -8 7 0 632.51 649.59 53.51 o -7 7 0 3952.50 3948.11 133.24 o -6 7 0 508.41 463.30 9.01 o -5 7 0 485.73 474.30 11.57 o -4 7 0 6645.46 7022.62 105.36 o -3 7 0 823.92 887.53 14.24 o -2 7 0 1760.83 1781.28 25.84 o -1 7 0 36.28 41.84 2.23 o 0 7 0 356.65 415.79 8.17 o 1 7 0 1303.81 1366.31 21.00 o 2 7 0 4.84 1.41 1.42 o 3 7 0 1970.13 2133.26 31.66 o 4 7 0 532.64 530.63 13.48 o 5 7 0 15.01 12.40 2.95 o 6 7 0 602.95 675.11 17.12 o 7 7 0 571.58 592.91 16.28 o -13 8 0 277.79 276.54 16.27 o -12 8 0 0.28 0.42 2.88 o -11 8 0 161.26 114.99 7.04 o -10 8 0 748.20 791.87 19.81 o -9 8 0 1005.83 1068.92 23.83 o -8 8 0 4.69 13.10 3.06 o -7 8 0 138.18 166.55 5.08 o -6 8 0 1857.40 1781.28 26.54 o -5 8 0 410.11 468.55 9.12 o -4 8 0 1.53 4.36 2.23 o -3 8 0 1601.55 1665.99 24.74 o -2 8 0 107.55 114.54 3.85 o -1 8 0 481.45 548.08 10.23 o 0 8 0 0.47 1.74 1.57 o 1 8 0 361.63 403.32 8.64 o 2 8 0 1939.83 1806.73 36.58 o 3 8 0 64.74 49.84 4.44 o 4 8 0 736.64 805.23 18.52 o 5 8 0 655.25 688.37 25.37 o 6 8 0 20.93 41.56 7.38 o -12 9 0 184.57 232.28 17.19 o -11 9 0 96.14 159.60 8.27 o -10 9 0 46.40 40.36 4.45 o -9 9 0 1.25 6.62 2.81 o -8 9 0 541.50 567.80 14.87 o -7 9 0 384.02 393.79 11.26 o -6 9 0 168.12 209.89 11.40 o -5 9 0 1518.82 1553.90 23.79 o -4 9 0 3086.92 3045.47 56.84 o -3 9 0 38.72 42.06 3.60 o -2 9 0 455.93 457.56 24.31 o -1 9 0 1833.88 2029.07 30.09 o 0 9 0 1266.41 1279.44 26.35 o 1 9 0 2.53 1.34 2.25 o 2 9 0 1370.72 1488.28 42.40 o 3 9 0 1494.88 1535.00 44.37 o 4 9 0 423.21 439.61 19.21 o 5 9 0 16.38 35.94 6.84 o -12 10 0 112.69 123.14 13.82 o -11 10 0 361.25 430.02 25.60 o -10 10 0 32.01 36.72 4.39 o -9 10 0 484.42 436.72 18.70 o -8 10 0 3.00 4.97 2.48 o -7 10 0 393.62 350.50 10.71 o -6 10 0 1708.96 1869.22 28.40 o -5 10 0 258.94 272.56 6.95 o -4 10 0 606.35 551.74 57.77 o -3 10 0 1540.74 1578.77 31.30 o -2 10 0 123.69 108.84 5.95 o -1 10 0 312.69 318.12 10.46 o 0 10 0 786.34 862.77 20.20 o 1 10 0 431.65 457.35 18.87 o 2 10 0 491.36 443.13 19.12 o 3 10 0 500.49 548.68 22.65 o 4 10 0 82.91 77.33 9.10 o -12 11 0 26.89 20.34 3.89 o -11 11 0 8.73 6.84 3.29 o -10 11 0 6.42 3.93 3.56 o -9 11 0 435.36 351.84 13.72 o -8 11 0 704.49 717.13 28.98 o -7 11 0 88.02 101.36 10.57 o -6 11 0 1472.85 1513.80 30.74 o -5 11 0 1704.71 1717.55 34.07 o -4 11 0 826.84 883.75 20.48 o -3 11 0 686.05 726.18 17.98 o -2 11 0 643.88 674.21 17.93 o -1 11 0 95.01 65.20 5.13 o 0 11 0 176.64 206.58 8.70 o 1 11 0 348.01 312.46 15.98 o 2 11 0 0.37 -0.75 4.45 o 3 11 0 441.76 342.95 17.91 o -11 12 0 266.06 274.84 19.00 o -10 12 0 481.56 583.57 28.26 o -9 12 0 0.63 22.73 6.71 o -8 12 0 196.65 168.08 13.29 o -7 12 0 185.94 214.58 14.85 o -6 12 0 88.03 102.07 6.14 o -5 12 0 133.96 100.44 6.19 o -4 12 0 1007.65 966.23 22.51 o -3 12 0 254.15 294.09 10.67 o -2 12 0 2.50 3.38 2.45 o -1 12 0 2.53 -0.14 2.16 o 0 12 0 43.99 68.73 8.09 o 1 12 0 683.31 612.88 24.49 o 2 12 0 357.18 392.47 19.79 o -10 13 0 336.74 334.48 21.72 o -9 13 0 233.24 296.65 18.75 o -8 13 0 128.22 133.69 12.25 o -7 13 0 4.51 1.72 4.57 o -6 13 0 12.08 16.90 5.75 o -5 13 0 536.95 581.05 16.33 o -4 13 0 282.35 280.17 14.64 o -3 13 0 95.52 105.93 6.85 o -2 13 0 326.81 337.01 12.21 o -1 13 0 361.48 358.38 17.74 o 0 13 0 0.82 -3.40 3.40 o -9 14 0 1.20 4.74 4.61 o -8 14 0 10.10 0.46 4.11 o -7 14 0 192.93 164.30 14.05 o -6 14 0 429.67 548.09 26.29 o -5 14 0 6.27 11.91 4.34 o -4 14 0 984.04 1048.21 25.50 o -3 14 0 276.74 305.03 11.94 o -2 14 0 17.47 -0.63 4.32 o 2 -14 1 373.29 500.37 21.89 o 3 -14 1 499.61 473.16 20.49 o 4 -14 1 87.74 96.62 12.87 o 5 -14 1 457.88 567.46 16.67 o 6 -14 1 6.01 3.90 4.95 o 7 -14 1 20.10 38.87 8.14 o 8 -14 1 76.47 103.62 10.95 o 9 -14 1 115.60 128.80 12.98 o 0 -13 1 377.20 395.45 19.21 o 1 -13 1 114.45 92.76 9.73 o 2 -13 1 55.68 71.53 5.62 o 3 -13 1 508.93 551.48 16.08 o 4 -13 1 272.93 277.48 10.61 o 5 -13 1 81.74 86.40 8.30 o 6 -13 1 124.76 140.73 11.99 o 7 -13 1 825.26 853.93 33.80 o 8 -13 1 261.37 237.90 16.06 o 9 -13 1 22.19 5.75 4.11 o 10 -13 1 112.01 149.92 15.05 o -2 -12 1 135.14 125.22 11.20 o -1 -12 1 16.06 20.76 5.75 o 0 -12 1 15.68 8.26 4.74 o 1 -12 1 268.48 277.49 14.43 o 2 -12 1 260.16 284.89 10.58 o 3 -12 1 236.04 238.74 9.42 o 4 -12 1 604.47 688.58 17.70 o 5 -12 1 949.68 993.38 40.72 o 6 -12 1 428.54 384.84 19.79 o 7 -12 1 42.01 43.32 7.93 o 8 -12 1 193.33 244.57 15.85 o 9 -12 1 1106.98 1133.89 42.06 o 10 -12 1 548.08 566.88 27.51 o 11 -12 1 163.23 134.91 13.75 o -3 -11 1 199.76 173.78 12.96 o -2 -11 1 435.53 420.86 19.46 o -1 -11 1 275.50 314.98 15.81 o 0 -11 1 145.77 155.54 10.57 o 1 -11 1 340.42 327.40 14.66 o 2 -11 1 1.48 -1.26 2.13 o 3 -11 1 1265.25 1364.77 28.56 o 4 -11 1 2281.88 2239.58 44.93 o 5 -11 1 325.13 307.31 10.22 o 6 -11 1 220.98 211.58 8.30 o 7 -11 1 349.29 378.13 11.56 o 8 -11 1 2.78 4.22 2.75 o 9 -11 1 80.91 45.97 4.69 o 10 -11 1 73.09 93.85 6.35 o 11 -11 1 180.04 193.07 9.85 o 12 -11 1 272.50 235.77 13.75 o -4 -10 1 370.73 382.95 18.87 o -3 -10 1 568.16 505.32 21.30 o -2 -10 1 576.27 587.64 22.73 o -1 -10 1 3.16 8.43 3.77 o 0 -10 1 89.75 90.73 5.65 o 1 -10 1 1422.66 1412.85 28.97 o 2 -10 1 2117.14 2141.85 40.40 o 3 -10 1 103.79 131.36 4.80 o 4 -10 1 992.97 1047.80 24.85 o 5 -10 1 1673.18 1641.38 25.36 o 6 -10 1 26.72 25.61 2.55 o 7 -10 1 532.97 497.08 17.99 o 8 -10 1 38.13 31.98 3.85 o 9 -10 1 97.39 91.68 5.94 o 10 -10 1 175.69 122.70 7.34 o 11 -10 1 0.22 14.65 3.70 o 12 -10 1 77.06 90.69 6.82 o -5 -9 1 361.20 334.60 17.15 o -4 -9 1 981.91 1065.82 34.55 o -3 -9 1 153.69 151.13 10.90 o -2 -9 1 287.77 283.08 12.52 o -1 -9 1 949.46 1004.78 17.29 o 0 -9 1 969.33 986.31 21.48 o 1 -9 1 16.97 27.26 2.40 o 2 -9 1 682.89 745.90 13.26 o 3 -9 1 997.66 1068.73 17.54 o 4 -9 1 429.30 429.91 27.40 o 5 -9 1 804.18 797.66 13.92 o 6 -9 1 2542.62 2619.19 53.08 o 7 -9 1 137.05 159.63 10.34 o 8 -9 1 503.69 460.47 20.28 o 9 -9 1 74.39 105.59 6.34 o 10 -9 1 162.28 173.86 8.25 o 11 -9 1 395.49 410.75 13.69 o 12 -9 1 4.13 8.99 3.49 o -6 -8 1 621.84 668.82 25.62 o -5 -8 1 228.59 258.50 9.59 o -4 -8 1 155.04 170.03 8.05 o -3 -8 1 1369.45 1352.25 26.68 o -2 -8 1 176.22 180.19 5.60 o -1 -8 1 601.58 559.11 10.82 o 0 -8 1 1331.27 1398.14 21.64 o 1 -8 1 186.11 222.21 5.65 o 2 -8 1 6.19 8.92 1.55 o 3 -8 1 1414.85 1509.63 22.77 o 4 -8 1 2735.70 2713.79 38.24 o 5 -8 1 689.18 698.42 12.23 o 6 -8 1 105.38 127.07 4.19 o 7 -8 1 1774.13 1837.56 38.01 o 8 -8 1 1575.91 1748.45 34.50 o 9 -8 1 92.74 84.55 5.59 o 10 -8 1 6.93 11.80 3.35 o 11 -8 1 240.98 260.48 10.48 o 12 -8 1 624.73 619.30 18.03 o 13 -8 1 58.87 58.28 6.22 o -7 -7 1 79.90 89.57 6.37 o -6 -7 1 262.90 296.45 10.44 o -5 -7 1 365.35 403.61 11.80 o -4 -7 1 421.57 469.38 18.41 o -3 -7 1 273.41 241.03 7.99 o -2 -7 1 933.39 978.15 16.25 o -1 -7 1 70.99 66.66 3.06 o 0 -7 1 212.27 182.25 4.81 o 1 -7 1 278.49 328.76 9.22 o 2 -7 1 1233.76 1280.73 19.40 o 3 -7 1 3231.41 3273.31 51.46 o 4 -7 1 767.51 893.48 14.39 o 5 -7 1 3049.14 3033.75 55.13 o 6 -7 1 6950.25 7005.59 93.08 o 7 -7 1 2444.43 2607.37 47.31 o 8 -7 1 1158.36 1177.16 24.85 o 9 -7 1 767.05 790.33 19.01 o 10 -7 1 263.66 255.34 9.79 o 11 -7 1 69.30 55.23 5.30 o 12 -7 1 0.66 2.66 2.95 o 13 -7 1 623.41 700.71 20.14 o -8 -6 1 146.19 214.52 9.34 o -7 -6 1 251.65 262.80 9.84 o -6 -6 1 26.63 24.24 4.34 o -5 -6 1 652.26 719.80 16.75 o -4 -6 1 965.12 913.06 19.22 o -3 -6 1 227.01 234.07 5.19 o -2 -6 1 787.00 736.71 12.65 o -1 -6 1 29.95 58.61 2.78 o 0 -6 1 396.20 414.29 7.81 o 1 -6 1 609.38 535.50 14.36 o 2 -6 1 280.89 204.11 4.73 o 3 -6 1 3264.58 3306.88 44.90 o 4 -6 1 2460.76 2339.89 32.68 o 5 -6 1 6910.01 7100.61 93.67 o 6 -6 1 291.99 233.81 5.41 o 7 -6 1 1489.74 1411.82 21.43 o 8 -6 1 130.70 124.30 6.07 o 9 -6 1 89.09 77.09 5.31 o 10 -6 1 62.25 39.89 4.28 o 11 -6 1 131.66 107.06 6.67 o 12 -6 1 544.80 599.75 22.08 o 13 -6 1 104.92 103.75 10.48 o -9 -5 1 28.47 34.17 4.84 o -8 -5 1 238.63 263.55 11.74 o -7 -5 1 1005.00 1086.53 23.54 o -6 -5 1 1043.32 1035.58 22.02 o -5 -5 1 137.09 144.95 6.12 o -4 -5 1 159.95 186.69 5.32 o -3 -5 1 2431.92 2361.19 33.62 o -2 -5 1 3475.74 3308.81 45.32 o -1 -5 1 1872.40 1974.07 27.86 o 0 -5 1 43.71 37.33 2.83 o 1 -5 1 2787.49 2799.03 40.76 o 2 -5 1 1336.64 1293.32 18.67 o 3 -5 1 1886.86 1677.86 23.67 o 4 -5 1 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19.33 o -3 2 30 616.97 573.55 23.86 o -2 2 30 371.98 425.77 19.63 o -1 2 30 26.45 65.21 5.13 o