#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/18/2211824.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211824_Fobs loop_ _publ_author_name 'Dornhaus, Franz' 'Bolte, Michael' _publ_section_title ; Bis(12-crown-4)lithium(I) bis[(N,N-diisopropylamino)borohydride(1--)]lithium(I) ; _journal_coeditor_code HB2217 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m41 _journal_page_last m42 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 116.790 _cell_angle_beta 105.314 _cell_angle_gamma 94.850 _cell_length_a 10.2918 _cell_length_b 14.5424 _cell_length_c 14.8057 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8006 _[local]_cod_data_source_file hb2217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa523 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 389.88 360.22 45.24 o 3 0 0 57.45 51.14 39.43 o 4 0 0 257.73 290.32 36.61 o 5 0 0 266.30 352.57 34.98 o 6 0 0 494.89 616.78 35.45 o 7 0 0 6.55 17.94 44.47 o 8 0 0 15.39 65.80 34.38 o 9 0 0 129.92 129.60 40.31 o 10 0 0 188.05 115.25 37.10 o 11 0 0 16.95 57.21 42.51 o -12 1 0 98.21 69.03 43.52 o -11 1 0 12.74 52.62 41.91 o -10 1 0 116.47 163.66 55.74 o -9 1 0 202.93 173.80 37.03 o -8 1 0 24.44 19.19 37.42 o -7 1 0 110.99 87.09 43.63 o -6 1 0 154.02 173.64 47.23 o -5 1 0 156.40 205.20 34.91 o -4 1 0 170.67 141.06 35.39 o -3 1 0 1793.82 1634.69 52.29 o -2 1 0 169.94 69.94 44.98 o 2 1 0 81.63 99.90 46.68 o 3 1 0 869.24 734.45 44.55 o 4 1 0 18.60 15.34 33.72 o 5 1 0 60.40 87.15 32.71 o 6 1 0 64.16 67.26 32.63 o 7 1 0 204.11 180.63 34.98 o 8 1 0 267.90 227.26 30.43 o 9 1 0 7.83 58.21 34.02 o 10 1 0 69.94 69.41 37.26 o 11 1 0 129.14 142.48 58.27 o -12 2 0 25.14 14.20 39.83 o -11 2 0 61.93 15.33 51.58 o -10 2 0 135.30 105.12 35.47 o -9 2 0 22.03 32.66 32.09 o -8 2 0 52.64 76.69 35.82 o -7 2 0 118.06 75.38 32.28 o -6 2 0 471.52 531.01 34.75 o -5 2 0 1090.09 1058.71 42.08 o -4 2 0 0.58 11.31 31.73 o -3 2 0 54.78 50.79 37.03 o -2 2 0 14007.65 14091.92 270.51 o 1 2 0 334.28 255.68 42.73 o 2 2 0 16834.44 18505.10 655.71 o 3 2 0 267.23 235.35 39.57 o 4 2 0 842.20 899.88 38.38 o 5 2 0 163.11 193.16 31.42 o 6 2 0 225.38 197.37 58.10 o 7 2 0 136.05 164.28 38.07 o 8 2 0 0.13 10.03 36.89 o 9 2 0 53.65 39.35 35.07 o 10 2 0 17.21 11.29 40.25 o 11 2 0 8.70 -16.50 41.52 o -12 3 0 150.73 129.22 42.06 o -11 3 0 15.38 -23.23 41.14 o -10 3 0 13.31 21.83 32.57 o -9 3 0 104.82 121.07 30.63 o -8 3 0 66.84 72.21 39.20 o -7 3 0 1033.02 1040.78 40.56 o -6 3 0 618.67 622.39 32.81 o -5 3 0 43.91 17.57 32.65 o -4 3 0 2121.47 2141.11 44.40 o -3 3 0 1074.16 1147.10 57.90 o -2 3 0 31.30 27.03 67.27 o -1 3 0 11999.23 13529.57 314.12 o 0 3 0 114.85 81.38 34.12 o 1 3 0 7552.68 7553.52 103.72 o 2 3 0 11.64 9.82 36.91 o 3 3 0 1735.72 1740.18 45.32 o 4 3 0 88.46 96.35 35.98 o 5 3 0 11.85 34.74 33.74 o 6 3 0 15.95 9.65 33.05 o 7 3 0 183.55 169.84 30.76 o 8 3 0 184.75 180.96 56.78 o 9 3 0 19.99 3.49 53.34 o 10 3 0 6.42 31.60 38.02 o 11 3 0 7.90 -10.52 42.47 o -12 4 0 0.10 -37.04 37.04 o -11 4 0 20.53 28.65 37.93 o -10 4 0 24.23 35.58 32.74 o -9 4 0 0.55 27.59 32.07 o -8 4 0 41.95 16.73 30.13 o -7 4 0 17.67 -13.43 33.05 o -6 4 0 177.92 206.88 38.54 o -5 4 0 1862.88 1977.29 130.57 o -4 4 0 0.60 17.03 33.21 o -3 4 0 401.12 389.92 48.52 o -1 4 0 63.76 87.71 51.32 o 0 4 0 2284.38 2060.80 47.11 o 1 4 0 988.54 865.22 38.42 o 2 4 0 1752.66 1688.24 131.59 o 3 4 0 49.75 79.11 37.85 o 4 4 0 1326.97 1417.02 39.39 o 5 4 0 26.25 -7.62 34.10 o 6 4 0 72.35 80.49 38.78 o 7 4 0 120.25 108.54 32.30 o 8 4 0 0.58 -35.29 35.29 o 9 4 0 242.04 206.14 37.75 o 10 4 0 5.19 58.68 42.48 o -12 5 0 31.21 70.30 40.61 o -11 5 0 10.75 -38.41 39.39 o -10 5 0 90.46 122.56 32.99 o -9 5 0 251.68 252.36 31.88 o -8 5 0 14.45 12.79 29.70 o -7 5 0 993.67 993.20 37.22 o -6 5 0 1.00 -1.79 32.11 o -5 5 0 535.52 593.17 34.60 o -4 5 0 631.25 609.90 50.71 o -3 5 0 973.59 1012.45 60.16 o -2 5 0 755.51 887.24 86.23 o -1 5 0 87.87 39.09 40.59 o 0 5 0 395.35 408.32 27.64 o 1 5 0 22.94 38.76 30.08 o 2 5 0 0.04 1.42 31.10 o 3 5 0 3554.49 3500.85 69.02 o 4 5 0 320.36 329.12 63.22 o 5 5 0 275.10 309.23 37.56 o 6 5 0 782.28 695.96 37.05 o 7 5 0 18.70 87.02 33.44 o 8 5 0 762.96 670.04 35.72 o 9 5 0 1.18 63.18 38.96 o 10 5 0 4.25 34.52 44.65 o -12 6 0 3.24 -7.90 42.85 o -11 6 0 14.47 3.22 47.73 o -10 6 0 67.02 72.04 46.00 o -9 6 0 2.59 52.66 34.18 o -8 6 0 34.36 49.81 43.81 o -7 6 0 41.80 18.30 30.84 o -6 6 0 111.70 140.54 43.96 o -5 6 0 73.74 123.54 43.80 o -4 6 0 997.78 971.08 56.02 o -3 6 0 1949.34 2143.52 207.73 o -2 6 0 66.38 89.38 46.91 o -1 6 0 16.76 13.96 37.75 o 0 6 0 1.78 26.46 25.45 o 1 6 0 295.69 261.34 33.33 o 2 6 0 427.81 413.92 31.86 o 3 6 0 133.51 191.24 28.98 o 4 6 0 371.89 354.63 34.56 o 5 6 0 1438.07 1480.39 49.52 o 6 6 0 26.59 -8.23 32.22 o 7 6 0 56.72 104.52 35.18 o 8 6 0 7.73 76.50 66.66 o 9 6 0 18.71 48.24 49.82 o 10 6 0 6.07 -12.19 42.41 o -12 7 0 9.09 29.31 32.28 o -11 7 0 6.04 -1.50 44.85 o -10 7 0 1.31 -48.97 48.97 o -9 7 0 145.08 145.77 53.53 o -8 7 0 348.20 293.84 45.64 o -7 7 0 548.33 494.97 54.10 o -6 7 0 0.35 35.35 43.30 o -5 7 0 14.77 33.69 42.28 o -4 7 0 22.93 48.97 34.51 o -3 7 0 1435.05 1564.84 90.86 o -2 7 0 7.79 70.60 37.81 o -1 7 0 148.51 65.95 36.92 o 0 7 0 665.84 634.42 27.46 o 1 7 0 1.12 18.90 28.96 o 2 7 0 11.45 33.24 28.51 o 3 7 0 253.45 294.41 29.71 o 4 7 0 0.34 -3.58 30.06 o 5 7 0 384.37 400.72 30.93 o 6 7 0 530.70 479.34 39.77 o 7 7 0 2.81 60.14 39.95 o 8 7 0 46.35 70.51 42.99 o 9 7 0 6.18 13.18 40.48 o -11 8 0 16.29 41.39 42.34 o -10 8 0 4.82 30.64 49.30 o -9 8 0 28.50 8.15 52.77 o -8 8 0 1.68 46.41 46.10 o -7 8 0 22.38 6.72 45.54 o -6 8 0 2.57 -29.04 36.55 o -5 8 0 188.42 181.59 35.61 o -4 8 0 813.21 822.12 103.27 o -3 8 0 39.77 -15.35 41.94 o -2 8 0 59.88 112.15 35.75 o -1 8 0 189.23 200.12 37.29 o 0 8 0 337.96 293.92 29.41 o 1 8 0 220.79 240.99 26.68 o 2 8 0 33.99 66.75 26.95 o 3 8 0 115.16 123.86 29.94 o 4 8 0 113.78 135.04 31.68 o 5 8 0 49.20 81.94 30.27 o 6 8 0 117.12 94.73 29.38 o 7 8 0 0.95 47.94 32.13 o 8 8 0 0.15 0.39 32.97 o 9 8 0 43.34 75.20 61.38 o -11 9 0 0.03 -40.36 40.36 o -10 9 0 3.73 3.86 36.45 o -9 9 0 5.52 51.30 33.83 o -8 9 0 62.33 42.18 34.12 o -7 9 0 375.62 379.14 39.99 o -6 9 0 683.92 697.12 64.58 o -5 9 0 137.25 164.37 37.44 o -4 9 0 398.88 417.30 31.09 o -3 9 0 72.00 74.80 37.91 o -2 9 0 548.44 482.83 55.49 o -1 9 0 10.41 29.28 38.71 o 0 9 0 403.76 393.70 30.72 o 1 9 0 102.98 119.55 28.06 o 2 9 0 19.65 30.30 29.91 o 3 9 0 7.47 8.70 27.75 o 4 9 0 342.55 278.38 31.25 o 5 9 0 191.24 242.41 32.33 o 6 9 0 4.22 36.73 32.22 o 7 9 0 58.30 48.48 32.81 o 8 9 0 60.95 104.94 36.02 o -11 10 0 11.62 38.53 41.44 o -10 10 0 0.01 -7.64 37.21 o -9 10 0 70.26 87.48 36.60 o -8 10 0 28.68 -8.06 35.29 o -7 10 0 23.94 64.39 35.68 o -6 10 0 75.05 69.05 37.89 o -5 10 0 187.42 241.00 31.33 o -4 10 0 0.62 38.84 31.00 o -3 10 0 447.16 418.12 51.59 o -2 10 0 512.25 484.68 48.45 o -1 10 0 961.40 1050.11 90.98 o 0 10 0 189.14 147.42 47.51 o 1 10 0 27.55 11.29 27.41 o 2 10 0 4.36 39.67 28.05 o 3 10 0 1.33 13.08 27.61 o 4 10 0 90.57 95.37 26.91 o 5 10 0 34.29 3.01 26.83 o 6 10 0 77.50 99.67 43.47 o 7 10 0 6.44 -11.04 35.22 o -10 11 0 12.89 21.99 39.94 o -9 11 0 1.12 -34.32 45.23 o -8 11 0 99.19 110.68 37.24 o -7 11 0 1.83 11.33 41.76 o -6 11 0 95.59 44.52 35.82 o -5 11 0 20.72 37.37 29.36 o -4 11 0 64.89 75.78 28.46 o -3 11 0 12.29 -31.88 37.97 o -2 11 0 51.20 40.45 37.49 o -1 11 0 14.59 14.54 38.69 o 0 11 0 11.83 64.28 47.87 o 1 11 0 0.79 16.47 31.28 o 2 11 0 6.18 7.57 25.68 o 3 11 0 0.33 18.90 27.26 o 4 11 0 0.02 33.70 28.20 o 5 11 0 0.14 30.09 29.22 o 6 11 0 4.44 86.31 32.29 o -10 12 0 4.18 -35.60 44.89 o -9 12 0 11.08 34.83 45.67 o -8 12 0 15.11 -15.02 39.27 o -7 12 0 0.47 31.75 32.93 o -6 12 0 179.75 137.39 30.15 o -5 12 0 888.99 810.05 30.59 o -4 12 0 4.72 26.03 36.44 o -3 12 0 159.45 160.73 39.02 o -2 12 0 45.82 106.65 39.97 o -1 12 0 56.48 95.23 41.05 o 0 12 0 70.64 130.53 52.88 o 1 12 0 180.06 176.33 51.89 o 2 12 0 23.85 30.36 27.88 o 3 12 0 0.10 -16.23 28.18 o 4 12 0 29.74 38.63 25.84 o 5 12 0 14.97 29.38 28.94 o -9 13 0 17.60 26.14 37.18 o -8 13 0 37.35 62.94 30.62 o -7 13 0 98.30 117.24 31.43 o -6 13 0 15.22 15.41 33.20 o -5 13 0 24.01 -19.54 33.29 o -4 13 0 10.14 39.23 36.94 o -3 13 0 30.29 40.79 47.40 o -2 13 0 6.23 -38.73 38.73 o -1 13 0 44.86 62.98 40.47 o 0 13 0 18.27 10.23 51.18 o 1 13 0 2.66 50.15 48.69 o 2 13 0 5.53 -9.10 39.56 o 3 13 0 20.79 50.56 28.12 o 4 13 0 3.88 15.45 30.31 o -8 14 0 26.09 70.81 33.50 o -7 14 0 40.33 42.17 33.55 o -6 14 0 41.62 80.00 33.09 o -5 14 0 78.83 67.17 32.64 o -4 14 0 103.29 91.67 40.92 o -3 14 0 170.42 167.83 61.57 o -2 14 0 48.87 103.41 41.38 o -1 14 0 14.46 50.15 50.56 o 0 14 0 103.96 99.50 51.01 o 1 14 0 11.38 45.71 50.28 o 2 14 0 16.44 -6.54 62.07 o 3 14 0 6.31 16.80 36.25 o -7 15 0 31.19 36.16 34.08 o -6 15 0 8.63 15.65 43.66 o -5 15 0 25.74 59.49 35.77 o -4 15 0 0.40 13.46 34.07 o -3 15 0 31.03 58.84 43.48 o -2 15 0 0.20 -13.92 44.54 o -1 15 0 93.21 175.92 55.70 o 0 15 0 25.85 83.76 55.79 o 1 15 0 5.45 1.44 55.07 o -4 16 0 32.52 62.35 36.04 o -3 16 0 0.26 14.80 46.60 o 0 -16 1 4.22 -64.99 64.99 o 1 -16 1 40.46 76.67 56.10 o 2 -16 1 59.37 97.48 44.83 o 3 -16 1 2.91 -59.13 59.74 o 4 -16 1 32.75 94.03 34.33 o 5 -16 1 1.94 68.81 35.76 o -2 -15 1 13.18 -5.95 54.30 o -1 -15 1 4.96 77.58 53.89 o 0 -15 1 73.49 119.32 60.18 o 1 -15 1 40.89 38.85 59.61 o 2 -15 1 11.99 27.67 46.00 o 3 -15 1 151.33 119.21 41.65 o 4 -15 1 10.66 33.33 32.42 o 5 -15 1 19.83 13.55 33.44 o 6 -15 1 22.00 -1.12 33.35 o 7 -15 1 0.00 11.49 33.82 o -4 -14 1 0.00 0.98 30.87 o -3 -14 1 3.36 -3.17 31.57 o -2 -14 1 0.89 -16.02 47.94 o -1 -14 1 54.76 79.16 50.00 o 0 -14 1 0.14 12.18 58.48 o 1 -14 1 21.65 62.97 40.50 o 2 -14 1 22.33 31.16 40.18 o 3 -14 1 62.61 51.77 40.10 o 4 -14 1 64.89 70.13 30.90 o 5 -14 1 78.54 103.86 32.44 o 6 -14 1 17.18 18.31 30.54 o 7 -14 1 3.19 -28.70 28.70 o 8 -14 1 17.97 9.44 35.76 o -5 -13 1 5.67 19.88 32.12 o -4 -13 1 3.57 -2.25 30.99 o -3 -13 1 34.93 49.85 28.22 o -2 -13 1 28.19 21.11 34.51 o -1 -13 1 3.80 5.38 53.12 o 0 -13 1 0.29 -25.36 54.28 o 1 -13 1 355.55 363.29 38.53 o 2 -13 1 224.96 235.81 36.42 o 3 -13 1 20.51 78.41 43.79 o 4 -13 1 23.01 14.19 29.20 o 5 -13 1 74.39 47.50 30.27 o 6 -13 1 134.34 88.68 29.78 o 7 -13 1 0.03 -4.76 33.08 o 8 -13 1 7.23 61.30 42.40 o 9 -13 1 7.96 -18.07 48.33 o -6 -12 1 78.77 62.84 31.60 o -5 -12 1 15.98 42.91 30.47 o -4 -12 1 23.00 31.19 28.39 o 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44.13 27.13 o -5 -10 1 0.77 -28.52 28.52 o -4 -10 1 7.20 41.92 27.04 o -3 -10 1 18.55 20.54 28.05 o -2 -10 1 155.66 156.89 33.17 o -1 -10 1 344.53 320.79 28.97 o 0 -10 1 688.24 793.70 41.63 o 1 -10 1 31.22 41.80 36.73 o 2 -10 1 372.10 335.35 37.93 o 3 -10 1 4.79 55.52 35.83 o 4 -10 1 0.94 -27.22 29.22 o 5 -10 1 9.01 61.49 40.39 o 6 -10 1 149.31 115.37 37.40 o 7 -10 1 152.92 149.92 39.57 o 8 -10 1 0.18 15.51 34.27 o 9 -10 1 30.14 -24.73 52.47 o 10 -10 1 17.37 35.16 54.52 o 11 -10 1 27.91 66.35 98.37 o -8 -9 1 82.72 99.52 33.20 o -7 -9 1 12.12 25.56 33.33 o -6 -9 1 22.92 21.29 30.27 o -5 -9 1 138.46 129.97 32.98 o -4 -9 1 332.29 322.56 28.77 o -3 -9 1 183.71 188.17 27.42 o -2 -9 1 22.87 47.29 25.91 o -1 -9 1 12.96 11.25 25.77 o 0 -9 1 5.60 40.19 33.36 o 1 -9 1 549.13 481.42 37.40 o 2 -9 1 41.75 61.83 39.56 o 3 -9 1 481.81 466.38 37.74 o 4 -9 1 4.94 34.95 40.59 o 5 -9 1 871.38 872.76 115.30 o 6 -9 1 673.86 619.65 73.69 o 7 -9 1 251.50 249.25 37.94 o 8 -9 1 6.06 -15.28 33.71 o 9 -9 1 4.99 -12.56 37.08 o 10 -9 1 15.61 44.97 58.14 o 11 -9 1 1.64 48.14 37.02 o -9 -8 1 59.39 58.14 31.68 o -8 -8 1 15.08 35.05 35.48 o -7 -8 1 4.50 89.72 31.53 o -6 -8 1 16.74 26.34 30.78 o -5 -8 1 105.17 100.07 30.15 o -4 -8 1 466.34 410.15 33.68 o -3 -8 1 386.12 401.41 40.25 o -2 -8 1 2.53 18.87 24.95 o -1 -8 1 738.06 717.58 29.64 o 0 -8 1 12.25 2.04 32.26 o 1 -8 1 47.11 66.41 35.71 o 2 -8 1 61.69 43.74 32.66 o 3 -8 1 21.35 7.48 36.27 o 4 -8 1 48.91 64.52 34.43 o 5 -8 1 235.54 240.30 34.80 o 6 -8 1 13.49 -11.08 45.71 o 7 -8 1 0.01 22.38 34.41 o 8 -8 1 188.14 203.44 39.78 o 9 -8 1 35.65 40.75 34.59 o 10 -8 1 98.55 133.77 38.93 o 11 -8 1 23.64 49.81 42.37 o -9 -7 1 0.00 2.38 64.24 o -8 -7 1 38.93 31.23 35.51 o -7 -7 1 56.44 55.63 35.22 o -6 -7 1 24.09 50.11 36.33 o -5 -7 1 22.62 49.61 30.49 o -4 -7 1 114.28 96.18 30.23 o -3 -7 1 5.99 59.89 28.91 o -2 -7 1 358.65 372.28 26.45 o -1 -7 1 149.51 171.10 24.94 o 0 -7 1 18.43 30.33 29.96 o 1 -7 1 83.98 100.99 37.33 o 2 -7 1 556.35 548.24 34.80 o 3 -7 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