#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/18/2211843.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211843_Fobs loop_ _publ_author_name 'Meijboom, Reinout' _publ_section_title ; Iodotris(tri-p-tolylphosphine)silver(I) ; _journal_coeditor_code HG2143 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m78 _journal_page_last m79 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.292 _cell_angle_beta 92.174 _cell_angle_gamma 106.196 _cell_length_a 11.0426 _cell_length_b 11.5665 _cell_length_c 23.2431 _exptl_crystal_F_000 1172.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file hg2143Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ipt2ac_m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 263.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10905.62 10926.08 165.62 o 2 0 0 9060.89 9452.56 144.23 o 3 0 0 12833.20 13351.78 204.13 o 4 0 0 6834.85 7017.25 114.38 o 5 0 0 9864.79 10616.31 226.59 o 6 0 0 1.19 -10.00 15.59 o 7 0 0 8773.85 8451.28 113.10 o 8 0 0 4000.70 3816.36 62.45 o 9 0 0 425.17 478.75 23.35 o 10 0 0 77.16 74.76 16.73 o 11 0 0 1514.81 1483.56 42.35 o 12 0 0 106.51 131.52 22.91 o 13 0 0 117.54 166.19 56.50 o -14 1 0 19.58 -10.54 45.70 o -13 1 0 44.62 23.25 24.46 o -12 1 0 529.29 538.19 30.84 o -11 1 0 11.37 27.75 18.31 o -10 1 0 770.37 690.94 29.03 o -9 1 0 7.51 -5.43 14.63 o -8 1 0 6266.81 6393.28 92.29 o -7 1 0 442.08 379.13 38.77 o 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7 0 1.42 14.63 39.80 o 9 7 0 389.30 330.24 53.16 o 10 7 0 57.49 55.81 52.74 o -14 8 0 49.81 38.41 32.01 o -13 8 0 9.33 3.92 32.00 o -12 8 0 360.03 383.34 50.06 o -11 8 0 335.55 376.77 30.65 o -10 8 0 0.61 -31.13 20.00 o -9 8 0 139.34 142.60 39.86 o -8 8 0 1703.36 1740.58 46.02 o -7 8 0 451.08 448.04 26.29 o -6 8 0 242.51 236.65 15.03 o -5 8 0 372.65 363.58 20.13 o -4 8 0 3045.05 3028.87 46.39 o -3 8 0 727.57 690.22 41.72 o -2 8 0 448.06 438.25 37.09 o -1 8 0 387.92 460.83 37.21 o 0 8 0 97.97 134.74 25.05 o 1 8 0 1017.73 1066.16 52.02 o 2 8 0 5.24 18.84 24.26 o 3 8 0 332.56 343.48 29.68 o 4 8 0 3.69 -23.44 18.23 o 5 8 0 51.91 50.45 34.74 o 6 8 0 43.55 32.09 34.44 o 7 8 0 12.66 35.34 41.48 o 8 8 0 223.95 296.64 54.01 o 9 8 0 22.68 32.69 53.34 o -13 9 0 5.65 2.88 30.44 o -12 9 0 634.36 657.62 41.48 o -11 9 0 63.83 26.84 26.91 o -10 9 0 11.02 4.94 20.70 o -9 9 0 213.30 226.06 23.67 o -8 9 0 286.50 309.24 36.37 o -7 9 0 542.42 531.60 23.68 o -6 9 0 55.90 74.26 13.44 o -5 9 0 2811.50 2850.65 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