#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/18/2211886.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211886_Fobs loop_ _publ_author_name 'Jia, Fang' 'Li, Jian' 'Wang, Xiu-Guang' 'Zhao, Xiao-Jun' _publ_section_title ; Bis(dicyanamido-\kN^1^)bis[4-(1,2,4-triazol-1-yl)phenol-\kN^4^]copper(II) ; _journal_coeditor_code LH2259 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m31 _journal_page_last m33 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.548 _cell_angle_gamma 90.000 _cell_length_a 12.9515 _cell_length_b 7.6960 _cell_length_c 10.3232 _exptl_crystal_F_000 526.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file lh2259Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 61012D in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3271.97 3308.20 26.18 o 3 0 0 399.38 388.08 3.69 o 4 0 0 3693.29 3650.98 28.83 o 5 0 0 2132.68 2127.13 15.42 o 6 0 0 43.70 21.48 1.70 o 7 0 0 5833.39 6220.84 41.47 o 8 0 0 4.78 16.18 5.39 o 9 0 0 41.34 55.65 3.69 o 10 0 0 117.92 120.29 11.41 o 11 0 0 189.81 179.41 9.85 o 12 0 0 9.11 9.55 5.94 o 13 0 0 283.06 316.38 14.52 o 14 0 0 563.63 630.07 19.13 o 15 0 0 388.59 371.04 16.14 o 1 1 0 42.49 33.70 1.62 o 2 1 0 35.23 43.38 0.91 o 3 1 0 2991.47 2998.97 15.59 o 4 1 0 1727.19 1752.15 11.59 o 5 1 0 601.17 647.48 4.34 o 6 1 0 1677.56 1882.16 11.11 o 7 1 0 225.52 265.29 3.01 o 8 1 0 155.34 158.06 2.79 o 9 1 0 1.10 0.93 1.88 o 10 1 0 22.38 20.82 2.63 o 11 1 0 36.41 28.83 3.11 o 12 1 0 27.65 36.21 6.11 o 13 1 0 286.10 274.22 17.84 o 14 1 0 24.63 24.57 11.74 o 15 1 0 43.89 46.47 6.90 o 0 2 0 59.11 49.98 1.31 o 1 2 0 8838.39 8805.99 43.30 o 2 2 0 4611.73 4669.12 23.46 o 3 2 0 41.78 32.56 1.18 o 4 2 0 1086.47 1029.56 6.80 o 5 2 0 4607.65 4536.80 23.84 o 6 2 0 2655.86 2627.29 15.14 o 7 2 0 258.48 227.05 3.40 o 8 2 0 472.55 475.10 5.12 o 9 2 0 3377.18 3396.52 30.46 o 10 2 0 27.28 27.63 2.92 o 11 2 0 117.57 124.75 4.17 o 12 2 0 122.12 131.11 4.81 o 13 2 0 541.44 504.34 11.98 o 14 2 0 102.69 118.41 8.34 o 1 3 0 45.20 45.29 1.16 o 2 3 0 896.56 949.59 5.61 o 3 3 0 464.95 454.74 3.96 o 4 3 0 169.78 195.78 2.96 o 5 3 0 256.30 280.30 3.50 o 6 3 0 203.84 201.79 3.96 o 7 3 0 641.40 635.12 6.00 o 8 3 0 1.73 2.58 1.87 o 9 3 0 45.02 51.28 2.96 o 10 3 0 67.10 67.64 3.61 o 11 3 0 5.43 6.54 2.78 o 12 3 0 47.08 50.42 4.12 o 13 3 0 5.38 6.59 3.90 o 14 3 0 146.41 156.13 11.80 o 0 4 0 125.81 108.16 3.65 o 1 4 0 11.28 7.71 1.05 o 2 4 0 369.24 362.56 4.75 o 3 4 0 736.14 736.13 5.11 o 4 4 0 2353.58 2375.91 14.99 o 5 4 0 658.93 658.41 5.81 o 6 4 0 438.96 450.53 5.37 o 7 4 0 581.70 573.97 7.78 o 8 4 0 1026.03 1002.07 11.55 o 9 4 0 190.70 183.09 6.40 o 10 4 0 647.22 626.13 9.53 o 11 4 0 996.55 955.94 23.50 o 12 4 0 282.93 276.88 7.79 o 13 4 0 21.73 25.07 5.27 o 1 5 0 110.30 119.49 3.96 o 2 5 0 92.30 105.18 2.67 o 3 5 0 0.61 -0.07 1.63 o 4 5 0 3.24 3.63 2.33 o 5 5 0 42.80 47.36 2.71 o 6 5 0 0.22 0.63 2.20 o 7 5 0 94.21 91.68 4.09 o 8 5 0 322.15 311.41 6.97 o 9 5 0 303.15 285.42 7.20 o 10 5 0 90.82 89.41 4.87 o 11 5 0 21.81 21.65 4.64 o 12 5 0 65.98 59.35 5.46 o 0 6 0 18.04 21.08 3.30 o 1 6 0 106.93 117.00 3.68 o 2 6 0 108.71 105.56 5.02 o 3 6 0 923.69 955.47 11.11 o 4 6 0 19.76 20.10 3.17 o 5 6 0 359.07 352.60 6.95 o 6 6 0 137.11 152.80 4.45 o 7 6 0 58.90 61.78 3.97 o 8 6 0 28.14 25.00 3.62 o 9 6 0 5.53 3.37 3.49 o 10 6 0 557.30 532.83 12.19 o 11 6 0 82.50 78.21 5.48 o 1 7 0 1.38 -0.10 2.60 o 2 7 0 0.39 3.04 3.26 o 3 7 0 2.85 2.19 3.24 o 4 7 0 2.25 2.56 3.08 o 5 7 0 3.60 1.04 3.44 o 6 7 0 23.47 22.64 7.18 o 7 7 0 6.89 2.96 4.54 o 8 7 0 2.71 6.44 4.94 o 9 7 0 50.03 41.68 6.04 o 0 8 0 60.08 67.31 7.02 o 1 8 0 156.53 164.98 6.22 o 2 8 0 16.02 16.99 3.79 o 3 8 0 111.03 105.74 5.29 o 4 8 0 49.16 53.28 5.03 o 5 8 0 9.64 10.62 5.17 o 6 8 0 83.90 79.73 8.39 o 7 8 0 8.77 6.61 6.15 o 1 9 0 3.39 3.33 6.17 o 2 9 0 63.88 65.24 7.22 o -15 1 1 18.98 12.61 5.50 o -14 1 1 119.56 123.32 7.14 o -13 1 1 514.20 553.50 13.78 o -12 1 1 38.01 42.94 3.95 o -11 1 1 116.68 130.50 3.75 o -10 1 1 847.09 859.53 15.35 o -9 1 1 1527.48 1519.22 10.84 o -8 1 1 1143.21 1089.37 8.10 o -7 1 1 3879.88 3921.04 19.46 o -6 1 1 3088.02 3118.24 15.64 o -5 1 1 6000.66 6073.53 30.62 o -4 1 1 8305.12 8243.48 46.47 o -3 1 1 8510.88 8319.50 55.52 o -2 1 1 2321.71 2349.13 12.28 o -1 1 1 506.76 489.08 3.64 o 0 1 1 9203.51 8639.01 71.01 o 1 1 1 1398.80 1408.10 8.76 o 2 1 1 296.33 312.49 3.99 o 3 1 1 809.31 739.26 5.81 o 4 1 1 553.70 459.10 5.09 o 5 1 1 54.57 30.72 1.34 o 6 1 1 218.60 187.70 2.90 o 7 1 1 1829.83 1849.93 10.27 o 8 1 1 1304.90 1291.49 8.12 o 9 1 1 817.46 819.43 8.28 o 10 1 1 191.48 198.79 4.58 o 11 1 1 371.07 385.31 7.60 o 12 1 1 926.97 949.75 26.68 o 13 1 1 997.56 975.65 24.13 o 14 1 1 425.07 423.64 11.69 o 15 1 1 91.22 77.39 7.41 o -15 2 1 19.58 21.44 6.33 o -14 2 1 12.66 14.14 5.13 o -13 2 1 183.23 165.67 9.01 o -12 2 1 133.57 130.29 4.65 o -11 2 1 419.65 410.79 6.66 o -10 2 1 16.39 15.51 2.31 o -9 2 1 1099.41 1147.08 9.17 o -8 2 1 9.77 14.19 1.81 o -7 2 1 209.14 203.19 3.33 o -6 2 1 85.50 91.02 2.29 o -5 2 1 422.54 447.47 4.17 o -4 2 1 282.01 285.49 3.02 o -3 2 1 819.36 918.08 6.39 o -2 2 1 2453.83 2569.32 15.56 o -1 2 1 26720.55 24568.85 152.34 o 0 2 1 30.32 30.05 2.29 o 1 2 1 268.16 274.27 2.39 o 2 2 1 145.80 162.23 3.27 o 3 2 1 4.95 6.35 0.89 o 4 2 1 120.25 128.21 2.05 o 5 2 1 0.03 3.29 1.18 o 6 2 1 405.16 447.63 4.33 o 7 2 1 442.36 477.72 4.79 o 8 2 1 601.06 618.12 6.94 o 9 2 1 44.88 50.27 2.83 o 10 2 1 373.21 344.49 5.69 o 11 2 1 24.02 22.55 3.16 o 12 2 1 241.60 258.86 11.97 o 13 2 1 1.84 2.02 4.82 o 14 2 1 12.13 11.93 7.46 o -14 3 1 446.15 444.87 13.18 o -13 3 1 228.28 241.56 7.51 o -12 3 1 511.12 515.59 8.09 o -11 3 1 514.62 510.56 7.65 o -10 3 1 33.85 31.51 2.89 o -9 3 1 1691.02 1755.97 19.49 o -8 3 1 1293.13 1330.71 9.89 o -7 3 1 24.95 20.13 1.87 o -6 3 1 115.01 114.52 2.98 o -5 3 1 440.89 389.75 4.08 o -4 3 1 1455.85 1489.96 13.71 o -3 3 1 9.46 6.76 1.69 o -2 3 1 5024.33 5005.14 25.80 o -1 3 1 5070.77 4978.48 45.09 o 0 3 1 360.53 329.55 5.20 o 1 3 1 825.30 874.71 6.44 o 2 3 1 8306.16 8309.47 60.25 o 3 3 1 2338.44 2285.54 11.68 o 4 3 1 1867.17 1870.32 14.30 o 5 3 1 1105.45 1063.91 7.54 o 6 3 1 687.92 656.77 5.75 o 7 3 1 270.97 233.07 4.24 o 8 3 1 512.52 517.62 6.50 o 9 3 1 430.18 445.12 9.11 o 10 3 1 263.41 260.19 5.73 o 11 3 1 34.57 43.77 3.67 o 12 3 1 58.09 68.21 4.00 o 13 3 1 176.67 190.22 7.19 o 14 3 1 127.88 128.17 21.19 o -13 4 1 111.84 116.64 6.46 o -12 4 1 143.73 140.24 6.33 o -11 4 1 11.97 7.03 3.44 o -10 4 1 0.44 -0.12 3.16 o -9 4 1 19.77 24.94 3.18 o -8 4 1 15.12 16.96 2.49 o -7 4 1 84.44 84.78 3.35 o -6 4 1 45.00 46.29 2.46 o -5 4 1 328.35 324.27 4.70 o -4 4 1 672.22 712.16 5.92 o -3 4 1 307.84 349.02 4.20 o -2 4 1 216.43 234.14 4.18 o -1 4 1 181.87 192.51 3.32 o 0 4 1 95.45 92.36 2.33 o 1 4 1 23.01 25.48 2.39 o 2 4 1 401.12 442.70 3.74 o 3 4 1 1631.08 1721.98 9.63 o 4 4 1 206.32 191.30 2.66 o 5 4 1 113.28 122.56 3.77 o 6 4 1 5.34 3.56 1.63 o 7 4 1 1.41 -0.13 2.13 o 8 4 1 962.03 990.54 11.01 o 9 4 1 1274.84 1239.60 21.39 o 10 4 1 69.60 74.84 4.56 o 11 4 1 211.61 207.71 6.51 o 12 4 1 10.95 10.99 3.84 o 13 4 1 13.39 6.32 5.52 o -12 5 1 65.54 52.96 4.97 o -11 5 1 234.30 232.87 8.36 o -10 5 1 825.66 802.73 11.45 o -9 5 1 2.01 2.94 3.39 o -8 5 1 123.78 129.89 4.16 o -7 5 1 402.34 401.61 6.14 o -6 5 1 160.86 147.36 4.09 o -5 5 1 150.20 153.37 3.85 o -4 5 1 8.18 5.60 1.97 o -3 5 1 1380.02 1411.76 9.90 o -2 5 1 31.42 30.59 1.89 o -1 5 1 49.59 51.08 2.47 o 0 5 1 314.29 297.07 5.45 o 1 5 1 1794.07 1844.17 15.38 o 2 5 1 76.77 75.55 3.46 o 3 5 1 596.57 603.88 6.64 o 4 5 1 777.96 778.60 7.74 o 5 5 1 537.27 506.60 6.26 o 6 5 1 518.89 535.16 11.64 o 7 5 1 364.65 379.59 7.13 o 8 5 1 724.63 740.50 10.16 o 9 5 1 102.84 98.11 4.85 o 10 5 1 34.24 33.56 4.45 o 11 5 1 535.11 520.05 11.68 o 12 5 1 54.61 59.05 5.11 o -11 6 1 153.30 144.68 6.85 o -10 6 1 7.26 7.60 4.16 o -9 6 1 37.27 44.03 4.22 o -8 6 1 0.78 2.00 3.16 o -7 6 1 2.46 3.40 2.79 o -6 6 1 25.49 24.52 2.94 o -5 6 1 17.53 18.91 2.71 o -4 6 1 142.83 143.78 5.01 o -3 6 1 31.54 28.00 3.07 o -2 6 1 1.32 1.20 2.31 o -1 6 1 8.69 10.88 2.27 o 0 6 1 119.26 126.24 7.05 o 1 6 1 7.08 6.26 2.21 o 2 6 1 1.52 -0.42 2.10 o 3 6 1 12.53 15.68 2.74 o 4 6 1 78.94 70.87 23.93 o 5 6 1 13.03 12.63 3.19 o 6 6 1 0.04 -2.09 3.60 o 7 6 1 29.37 22.80 3.61 o 8 6 1 0.33 0.35 3.40 o 9 6 1 91.14 90.86 5.20 o 10 6 1 8.93 6.10 4.17 o 11 6 1 18.54 16.54 5.12 o -9 7 1 31.79 38.14 5.93 o -8 7 1 40.03 47.98 5.87 o -7 7 1 51.10 59.82 5.82 o -6 7 1 51.95 49.44 4.24 o -5 7 1 68.35 62.29 4.94 o -4 7 1 73.86 84.16 5.92 o -3 7 1 67.67 82.34 4.42 o -2 7 1 107.43 113.40 4.77 o -1 7 1 61.81 59.89 3.47 o 0 7 1 97.12 107.77 4.01 o 1 7 1 35.31 33.65 3.05 o 2 7 1 324.02 340.29 6.98 o 3 7 1 155.25 156.05 5.48 o 4 7 1 19.90 19.88 3.61 o 5 7 1 60.92 60.84 5.48 o 6 7 1 256.75 233.52 8.53 o 7 7 1 178.20 174.60 7.94 o 8 7 1 9.85 7.89 5.03 o 9 7 1 70.44 58.22 6.47 o -7 8 1 28.52 20.46 5.81 o -6 8 1 0.01 -0.71 5.04 o -5 8 1 4.46 3.39 3.91 o -4 8 1 11.29 5.47 4.31 o -3 8 1 0.59 -0.42 3.80 o -2 8 1 82.61 75.08 4.82 o -1 8 1 1.94 1.86 3.65 o 0 8 1 0.06 0.06 3.23 o 1 8 1 2.21 2.57 3.67 o 2 8 1 29.67 24.77 4.14 o 3 8 1 2.95 1.54 4.01 o 4 8 1 0.94 0.50 4.71 o 5 8 1 13.70 12.66 5.26 o 6 8 1 0.59 0.54 5.16 o 7 8 1 25.12 15.65 5.87 o -2 9 1 3.18 4.19 4.36 o -1 9 1 84.57 78.75 6.67 o 0 9 1 24.54 20.73 7.66 o 1 9 1 163.50 160.70 11.43 o 2 9 1 9.33 6.22 4.63 o -15 0 2 239.27 249.38 14.99 o -14 0 2 671.89 637.16 18.76 o -13 0 2 990.92 1035.54 21.33 o -12 0 2 674.68 673.24 11.84 o -11 0 2 9.61 10.52 3.78 o -10 0 2 5012.86 5122.44 63.46 o -9 0 2 1509.58 1499.96 13.59 o -8 0 2 328.84 284.61 5.08 o -7 0 2 3925.04 3879.73 27.44 o -6 0 2 6568.32 6612.01 43.61 o -5 0 2 1825.88 1756.70 13.46 o -4 0 2 622.12 770.92 6.91 o -3 0 2 207.52 251.80 4.11 o -2 0 2 394.74 391.69 4.77 o -1 0 2 88.70 88.13 2.77 o 0 0 2 13383.75 12327.37 136.15 o 1 0 2 7186.43 6929.00 54.26 o 2 0 2 227.62 184.18 2.77 o 3 0 2 28.26 15.77 1.46 o 4 0 2 2405.45 2356.23 20.03 o 5 0 2 1369.32 1242.07 19.86 o 6 0 2 2330.21 2330.35 20.97 o 7 0 2 1072.05 1067.09 14.23 o 8 0 2 4548.69 4562.51 58.24 o 9 0 2 1667.49 1597.76 18.05 o 10 0 2 191.45 171.33 9.78 o 11 0 2 66.69 59.10 7.61 o 12 0 2 1326.21 1231.04 26.22 o 13 0 2 300.27 323.22 14.69 o 14 0 2 304.39 307.40 15.34 o -15 1 2 0.16 -1.06 5.65 o -14 1 2 49.98 42.91 6.06 o -13 1 2 105.80 93.96 5.09 o -12 1 2 52.61 52.56 4.75 o -11 1 2 329.27 324.27 5.17 o -10 1 2 190.08 206.44 4.04 o -9 1 2 2.82 1.26 1.81 o -8 1 2 174.88 191.85 2.95 o -7 1 2 297.76 318.69 3.43 o -6 1 2 122.64 141.78 2.22 o -5 1 2 298.97 293.15 3.53 o -4 1 2 1214.21 1279.30 8.02 o -3 1 2 2116.68 2106.69 11.69 o -2 1 2 4790.57 4872.68 29.03 o -1 1 2 8649.44 8515.19 54.19 o 0 1 2 1533.86 1563.84 11.29 o 1 1 2 417.21 439.20 4.22 o 2 1 2 143.86 173.75 3.65 o 3 1 2 98.30 100.66 3.56 o 4 1 2 55.88 52.63 2.53 o 5 1 2 924.44 1025.02 9.15 o 6 1 2 2739.57 2989.50 21.87 o 7 1 2 21.96 28.69 1.87 o 8 1 2 60.54 70.73 4.04 o 9 1 2 29.87 30.23 2.63 o 10 1 2 122.37 128.38 5.01 o 11 1 2 2.13 3.80 2.97 o 12 1 2 122.28 119.28 6.91 o 13 1 2 12.80 9.95 5.26 o 14 1 2 29.04 30.71 6.23 o -14 2 2 294.40 298.93 10.82 o -13 2 2 198.48 192.43 6.33 o -12 2 2 395.74 409.82 7.06 o -11 2 2 732.18 748.02 8.77 o -10 2 2 83.10 99.81 5.87 o -9 2 2 434.76 430.40 6.54 o -8 2 2 3616.38 3623.34 21.01 o -7 2 2 1232.65 1161.74 14.98 o -6 2 2 2405.66 2378.69 14.18 o -5 2 2 3345.90 3298.08 18.19 o -4 2 2 756.78 668.48 5.13 o -3 2 2 1024.08 972.74 6.78 o -2 2 2 324.79 370.21 6.25 o -1 2 2 24214.64 22435.86 301.79 o 0 2 2 472.25 434.57 3.77 o 1 2 2 263.93 221.59 2.29 o 2 2 2 317.02 396.37 5.45 o 3 2 2 2242.01 2197.03 26.25 o 4 2 2 1129.24 1036.75 18.27 o 5 2 2 159.14 124.07 2.32 o 6 2 2 1308.81 1324.40 10.32 o 7 2 2 918.00 901.57 8.78 o 8 2 2 1073.89 1062.96 9.55 o 9 2 2 498.12 484.01 9.60 o 10 2 2 1626.74 1587.34 13.34 o 11 2 2 538.53 536.65 21.47 o 12 2 2 55.73 67.51 4.95 o 13 2 2 505.18 487.97 12.20 o 14 2 2 429.89 416.08 22.89 o -14 3 2 3.85 1.26 5.59 o -13 3 2 181.42 178.44 6.77 o -12 3 2 104.55 99.05 5.20 o -11 3 2 430.46 444.26 7.06 o -10 3 2 543.43 545.04 8.45 o -9 3 2 339.12 351.47 5.05 o -8 3 2 21.72 26.88 2.15 o -7 3 2 0.91 0.39 1.63 o -6 3 2 493.34 500.01 5.01 o -5 3 2 220.46 261.26 3.76 o -4 3 2 278.82 311.04 3.64 o -3 3 2 749.49 823.04 8.97 o -2 3 2 100.43 96.61 2.30 o -1 3 2 266.94 277.21 4.17 o 0 3 2 11.46 12.46 1.26 o 1 3 2 76.09 87.56 2.06 o 2 3 2 36.88 40.91 1.40 o 3 3 2 226.48 245.86 3.19 o 4 3 2 256.85 268.14 3.25 o 5 3 2 0.13 1.37 1.27 o 6 3 2 32.46 35.44 2.16 o 7 3 2 26.61 26.81 2.33 o 8 3 2 11.19 11.93 2.42 o 9 3 2 44.19 47.71 3.18 o 10 3 2 90.73 83.47 3.82 o 11 3 2 116.22 135.05 4.57 o 12 3 2 104.33 105.27 5.49 o 13 3 2 2.98 2.27 4.50 o 14 3 2 21.36 13.73 6.69 o -13 4 2 37.59 45.80 5.12 o -12 4 2 175.64 191.99 7.01 o -11 4 2 296.55 290.16 8.80 o -10 4 2 97.70 105.79 4.18 o -9 4 2 295.35 296.66 5.57 o -8 4 2 40.54 47.74 3.03 o -7 4 2 168.96 168.80 4.20 o -6 4 2 696.69 661.72 7.41 o -5 4 2 750.42 742.16 7.60 o -4 4 2 1325.98 1428.65 9.69 o -3 4 2 1031.48 946.33 7.21 o -2 4 2 4562.70 4622.97 32.61 o -1 4 2 194.48 158.91 3.17 o 0 4 2 185.65 186.08 2.66 o 1 4 2 998.64 981.33 6.33 o 2 4 2 1272.46 1282.71 7.75 o 3 4 2 133.11 118.42 2.24 o 4 4 2 1714.22 1727.52 21.73 o 5 4 2 1396.87 1389.52 9.61 o 6 4 2 117.08 113.94 3.47 o 7 4 2 28.55 31.48 2.61 o 8 4 2 481.54 476.02 8.01 o 9 4 2 166.09 168.80 4.74 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