#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/18/2211892.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2211892_Fobs
loop_
_publ_author_name
'de Souza, M. V. N.'
'Wardell, Solange M. S. V.'
'Wardell, James L.'
'Low, John N.'
'Glidewell, Christopher'
_publ_section_title
;
N-(5-Chloro-2-nitrobenzoyl)-N'-isonicotinoylhydrazine: a
three-dimensional framework containing four types of hydrogen bond
;
_journal_coeditor_code LH2269
_journal_issue 1
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first o230
_journal_page_last o232
_journal_volume 63
_journal_year 2007
_space_group_IT_number 43
_symmetry_space_group_name_Hall 'F 2 -2d'
_symmetry_space_group_name_H-M 'F d d 2'
_cell_angle_alpha 90.000
_cell_angle_beta 90.000
_cell_angle_gamma 90.000
_cell_length_a 67.7860
_cell_length_b 34.6130
_cell_length_c 4.6486
_exptl_crystal_F_000 5248.00
_reflns_d_resolution_high 0.9279
_[local]_cod_data_source_file lh2269Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' 2006src0888 in Fdd2 Fdd2'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 871.67
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x+1/4, y+1/4, z+1/4'
'x+3/4, -y+3/4, z+1/4'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'-x+1/4, y+3/4, z+3/4'
'x+3/4, -y+5/4, z+3/4'
'x+1/2, y, z+1/2'
'-x+1/2, -y, z+1/2'
'-x+3/4, y+1/4, z+3/4'
'x+5/4, -y+3/4, z+3/4'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'-x+3/4, y+3/4, z+1/4'
'x+5/4, -y+5/4, z+1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 0 -4 5187.90 3643.25 1419.23 o
4 0 -4 8099.50 7488.90 850.64 o
8 0 -4 3810.32 3957.24 633.36 o
12 0 -4 7214.26 7310.53 1498.58 o
16 0 -4 2349.25 2147.27 972.81 o
20 0 -4 4933.92 2439.52 1182.82 o
24 0 -4 4248.90 6847.97 2349.94 o
2 2 -4 8676.07 9638.28 881.40 o
4 2 -4 13194.17 13798.77 973.68 o
6 2 -4 55.71 -8.20 466.14 o
8 2 -4 7204.71 6705.46 757.66 o
10 2 -4 856.62 206.03 487.41 o
12 2 -4 4364.87 4598.62 556.33 o
14 2 -4 1285.88 538.11 863.27 o
16 2 -4 8544.43 7599.27 941.20 o
18 2 -4 6125.56 3874.48 858.96 o
20 2 -4 13944.95 11784.68 1469.05 o
22 2 -4 9495.06 7838.82 1847.65 o
24 2 -4 2516.06 1787.29 1313.87 o
26 2 -4 3561.00 949.59 1563.75 o
28 2 -4 7614.59 9376.20 8304.91 o
0 4 -4 25354.81 23964.87 1554.91 o
2 4 -4 1602.45 1571.35 388.52 o
4 4 -4 1881.72 2339.55 387.97 o
6 4 -4 1063.80 1414.12 433.48 o
8 4 -4 3046.14 2785.04 396.25 o
10 4 -4 7739.84 7674.07 635.69 o
12 4 -4 8253.94 7503.56 964.50 o
14 4 -4 17049.85 14603.87 1553.08 o
16 4 -4 2568.77 1657.79 745.66 o
18 4 -4 4172.13 3598.95 889.28 o
20 4 -4 6874.31 5983.98 1019.95 o
22 4 -4 4037.42 2585.56 1863.77 o
24 4 -4 90.81 -249.46 1126.67 o
26 4 -4 6295.83 2390.00 1908.54 o
2 6 -4 7065.55 6951.16 713.22 o
4 6 -4 778.09 948.55 396.61 o
6 6 -4 218.79 -231.18 400.53 o
8 6 -4 1600.14 2114.27 603.04 o
10 6 -4 3050.13 3179.36 437.88 o
12 6 -4 217.36 303.86 433.87 o
14 6 -4 3732.98 2690.47 932.87 o
16 6 -4 9688.26 7346.06 1188.05 o
18 6 -4 9414.48 5719.64 1085.56 o
20 6 -4 8363.14 6446.57 1187.68 o
22 6 -4 6966.92 7951.23 1755.64 o
24 6 -4 2299.44 383.28 1818.22 o
26 6 -4 2612.69 874.94 2043.63 o
0 8 -4 17330.86 19555.23 2842.34 o
2 8 -4 10519.48 8529.52 785.03 o
4 8 -4 864.24 142.48 520.11 o
6 8 -4 1506.16 1921.42 628.65 o
8 8 -4 2508.67 1626.44 651.78 o
10 8 -4 10882.53 10081.63 702.45 o
12 8 -4 1302.90 1252.06 641.67 o
14 8 -4 6650.08 5105.33 793.89 o
16 8 -4 1526.24 1090.11 982.08 o
18 8 -4 2807.26 1676.83 1204.59 o
20 8 -4 1760.87 1854.32 1167.95 o
22 8 -4 7317.69 3626.27 1180.32 o
24 8 -4 3924.59 5255.95 2045.99 o
2 10 -4 1146.29 1315.76 579.45 o
4 10 -4 7337.15 7588.44 886.82 o
6 10 -4 8724.54 8267.39 756.48 o
8 10 -4 3981.26 3283.35 605.22 o
10 10 -4 1823.35 1205.21 490.08 o
12 10 -4 339.86 -55.56 550.75 o
14 10 -4 6613.35 8017.33 802.91 o
16 10 -4 6251.93 4504.65 980.17 o
18 10 -4 5324.57 4223.59 1078.43 o
20 10 -4 2221.35 660.09 1025.52 o
22 10 -4 871.34 2197.24 1251.39 o
0 12 -4 22821.94 26579.19 2445.19 o
2 12 -4 1153.44 518.94 629.81 o
4 12 -4 702.69 221.34 574.88 o
6 12 -4 9626.97 8766.72 944.65 o
8 12 -4 13839.29 12616.37 968.26 o
10 12 -4 15220.37 12352.17 1361.48 o
12 12 -4 13149.37 12951.45 1297.04 o
14 12 -4 5527.79 4084.13 876.70 o
16 12 -4 2551.24 1895.32 1035.97 o
18 12 -4 3913.18 4524.00 1361.75 o
20 12 -4 9216.83 9431.97 2257.26 o
22 12 -4 1767.50 1895.19 2056.20 o
2 14 -4 598.42 1142.41 1171.62 o
4 14 -4 4249.41 1043.85 1137.12 o
6 14 -4 17908.67 16553.11 1493.59 o
8 14 -4 2564.34 2328.60 814.02 o
10 14 -4 6555.28 4451.17 958.97 o
12 14 -4 3314.27 3833.84 1175.47 o
14 14 -4 6064.25 6190.21 1252.38 o
16 14 -4 5217.36 3494.28 1785.23 o
18 14 -4 194.37 3539.05 2100.18 o
20 14 -4 3286.36 -2145.74 2145.74 o
0 16 -4 23743.06 25079.66 3630.94 o
2 16 -4 12823.88 10107.42 2780.35 o
4 16 -4 427.18 -177.47 1018.23 o
6 16 -4 9708.58 10982.99 1595.34 o
8 16 -4 7470.78 6052.16 1330.61 o
10 16 -4 2175.08 1028.72 849.59 o
12 16 -4 944.60 352.28 877.54 o
14 16 -4 8251.79 6516.53 2361.72 o
16 16 -4 5555.38 9097.38 2649.97 o
6 18 -4 9144.77 8358.31 1829.22 o
8 18 -4 252.35 -968.41 1409.81 o
10 18 -4 239.23 89.54 1061.09 o
12 18 -4 1181.44 607.12 1031.24 o
2 20 -4 3303.34 6105.76 2325.59 o
4 20 -4 768.09 1501.70 1658.00 o
6 20 -4 2641.61 3555.54 1362.68 o
8 20 -4 160.44 -984.90 1101.93 o
10 20 -4 9149.11 7631.03 1767.17 o
12 20 -4 356.81 731.22 1407.45 o
2 22 -4 578.54 521.63 896.91 o
4 22 -4 3662.51 3628.59 1496.99 o
6 22 -4 1573.42 1013.18 1562.18 o
1 1 -3 27262.22 27859.32 1502.43 o
3 1 -3 35634.31 38069.57 1876.68 o
5 1 -3 8090.02 8522.18 682.45 o
7 1 -3 5930.25 5635.01 622.48 o
9 1 -3 196.93 233.44 179.83 o
11 1 -3 6684.21 6807.82 411.51 o
13 1 -3 14121.69 11860.02 1143.36 o
15 1 -3 944.59 257.59 560.23 o
17 1 -3 7866.61 8503.39 387.03 o
19 1 -3 17239.76 16280.75 724.77 o
21 1 -3 17793.09 18090.31 939.43 o
23 1 -3 12149.62 12102.06 679.36 o
25 1 -3 1018.38 1122.18 370.20 o
27 1 -3 5225.98 4920.84 494.36 o
29 1 -3 3013.35 3793.26 568.68 o
31 1 -3 2233.87 2734.93 434.03 o
33 1 -3 6340.19 6564.73 800.99 o
35 1 -3 6550.44 4760.45 870.85 o
37 1 -3 24626.22 23886.77 2046.90 o
39 1 -3 2654.42 1414.34 582.58 o
41 1 -3 27836.58 26337.55 3300.51 o
43 1 -3 16478.46 18694.72 3854.39 o
1 3 -3 2736.46 3046.44 441.73 o
3 3 -3 7371.52 7496.10 537.46 o
5 3 -3 7070.19 7023.60 583.13 o
7 3 -3 10570.20 9977.71 543.71 o
9 3 -3 24650.80 25260.81 1030.00 o
11 3 -3 18828.64 19389.69 813.64 o
13 3 -3 11037.62 11769.51 541.59 o
15 3 -3 11717.05 12752.62 398.22 o
17 3 -3 1025.05 949.71 203.02 o
19 3 -3 933.23 884.09 290.19 o
21 3 -3 14396.41 16009.46 770.89 o
23 3 -3 12854.18 13008.49 741.33 o
25 3 -3 9946.41 10526.79 662.53 o
27 3 -3 16887.88 17728.55 1030.06 o
29 3 -3 6521.01 6943.90 644.32 o
31 3 -3 9148.19 7872.16 786.71 o
33 3 -3 24969.47 30995.81 1842.75 o
35 3 -3 7820.61 5792.11 883.38 o
37 3 -3 218.41 -151.99 724.07 o
39 3 -3 12469.20 14673.09 1501.51 o
41 3 -3 244.94 662.58 1658.19 o
43 3 -3 12594.06 13260.85 2941.29 o
1 5 -3 1810.30 1771.69 271.46 o
3 5 -3 110.14 270.38 222.07 o
5 5 -3 3659.40 3373.70 401.95 o
7 5 -3 3012.69 3905.26 331.96 o
9 5 -3 19545.76 18851.76 672.26 o
11 5 -3 452.73 359.47 161.20 o
13 5 -3 6430.46 6176.47 317.47 o
15 5 -3 653.27 970.98 199.56 o
17 5 -3 625.87 954.52 235.34 o
19 5 -3 475.29 728.83 267.22 o
21 5 -3 5888.93 5657.22 530.28 o
23 5 -3 3828.33 3197.54 327.02 o
25 5 -3 197.45 417.67 322.24 o
27 5 -3 8124.01 9170.08 577.59 o
29 5 -3 5403.58 5348.81 464.88 o
31 5 -3 15356.49 15102.54 948.24 o
33 5 -3 5825.60 5533.55 509.62 o
35 5 -3 4181.45 4329.54 781.64 o
37 5 -3 711.03 576.82 659.32 o
39 5 -3 5256.99 5359.40 715.50 o
41 5 -3 25024.07 28176.44 3462.55 o
43 5 -3 904.38 -306.12 2734.73 o
1 7 -3 38613.28 40735.00 1507.13 o
3 7 -3 23129.40 24512.20 1107.07 o
5 7 -3 11018.18 10818.31 640.03 o
7 7 -3 14961.09 14342.69 704.98 o
9 7 -3 1566.20 1512.32 242.05 o
11 7 -3 13079.87 13336.59 764.48 o
13 7 -3 9064.87 8098.03 447.13 o
15 7 -3 7454.80 7161.01 441.62 o
17 7 -3 1550.91 1576.75 313.19 o
19 7 -3 19385.70 21260.35 817.26 o
21 7 -3 5992.44 6077.41 738.81 o
23 7 -3 35130.62 37857.05 1418.34 o
25 7 -3 9980.05 10418.67 620.13 o
27 7 -3 5053.15 4966.16 575.27 o
29 7 -3 7669.95 8393.30 634.22 o
31 7 -3 7984.16 6474.71 883.48 o
33 7 -3 39890.50 40614.00 1834.38 o
35 7 -3 16418.54 15227.91 1440.87 o
37 7 -3 437.09 -752.41 817.01 o
39 7 -3 5104.79 4587.86 1378.91 o
41 7 -3 5335.56 5776.76 1174.95 o
1 9 -3 2215.14 1697.07 523.23 o
3 9 -3 3398.90 3710.90 416.87 o
5 9 -3 1947.22 1792.62 361.79 o
7 9 -3 4413.98 4117.69 361.42 o
9 9 -3 11684.66 13317.54 759.38 o
11 9 -3 9421.99 9280.16 639.61 o
13 9 -3 6411.43 6921.89 505.20 o
15 9 -3 210.10 752.66 309.14 o
17 9 -3 1953.26 1189.16 328.84 o
19 9 -3 12810.83 13253.20 679.17 o
21 9 -3 24097.28 26566.37 1101.67 o
23 9 -3 966.64 1166.25 360.33 o
25 9 -3 5199.02 5457.73 499.92 o
27 9 -3 2992.79 3182.81 430.45 o
29 9 -3 9494.94 10765.70 889.15 o
31 9 -3 1465.37 743.86 460.01 o
33 9 -3 17253.50 17947.34 1213.13 o
35 9 -3 16136.38 16465.33 2730.71 o
37 9 -3 2414.33 1724.84 761.83 o
39 9 -3 15733.79 16581.53 1749.81 o
41 9 -3 5038.07 4319.76 924.88 o
1 11 -3 10028.99 9243.73 691.90 o
3 11 -3 114.44 593.92 336.28 o
5 11 -3 3707.09 3579.28 743.29 o
7 11 -3 10879.81 10758.76 605.74 o
9 11 -3 6876.95 6349.19 487.03 o
11 11 -3 40306.02 42011.27 1407.59 o
13 11 -3 10747.70 10596.38 675.09 o
15 11 -3 17687.58 18256.19 778.73 o
17 11 -3 16662.86 17454.65 797.54 o
19 11 -3 24539.58 23987.72 965.89 o
21 11 -3 6823.41 6801.10 562.97 o
23 11 -3 45179.32 48462.28 2018.19 o
25 11 -3 12960.24 11259.20 859.13 o
27 11 -3 4632.72 3271.75 683.46 o
29 11 -3 7326.42 5434.97 666.21 o
31 11 -3 7247.34 6216.78 813.03 o
33 11 -3 4483.84 4170.29 1165.73 o
35 11 -3 9284.46 8869.86 1209.46 o
37 11 -3 12356.52 10832.19 1322.00 o
39 11 -3 1760.00 1391.19 785.33 o
41 11 -3 232.45 0.00 769.70 o
1 13 -3 673.97 1072.88 353.12 o
3 13 -3 5752.26 6131.02 610.08 o
5 13 -3 498.64 548.36 376.86 o
7 13 -3 2879.60 3439.23 563.71 o
9 13 -3 10998.69 10575.11 725.91 o
11 13 -3 3413.86 2919.45 454.36 o
13 13 -3 21787.98 22888.39 1012.17 o
15 13 -3 5153.76 5135.99 565.94 o
17 13 -3 18244.83 17318.71 1059.99 o
19 13 -3 4568.19 4121.22 558.49 o
21 13 -3 3107.63 3047.32 496.11 o
23 13 -3 9377.06 7881.39 846.53 o
25 13 -3 24018.71 24052.65 1383.84 o
27 13 -3 7432.74 6948.02 1100.88 o
29 13 -3 13762.02 14520.01 1793.98 o
31 13 -3 15035.13 15684.73 1631.23 o
33 13 -3 1909.13 2433.31 1037.21 o
35 13 -3 29602.52 35991.63 2306.59 o
37 13 -3 5298.47 6290.33 2055.23 o
39 13 -3 4428.22 3284.58 1273.15 o
41 13 -3 785.32 2390.00 1062.66 o
1 15 -3 8315.34 8736.51 547.12 o
3 15 -3 22575.61 23185.87 975.96 o
5 15 -3 6089.00 5459.94 535.39 o
7 15 -3 3726.08 3695.06 583.58 o
9 15 -3 26911.83 28722.22 1391.03 o
11 15 -3 6454.02 6408.94 663.58 o
13 15 -3 4732.60 3824.29 804.54 o
15 15 -3 1369.48 2541.14 658.73 o
17 15 -3 10917.54 9543.69 737.86 o
19 15 -3 5504.49 5555.41 830.64 o
21 15 -3 16.83 1615.30 723.80 o
23 15 -3 17187.91 15117.80 1680.58 o
25 15 -3 10737.24 11431.95 1577.57 o
27 15 -3 2276.95 2018.10 728.66 o
29 15 -3 8069.32 8584.04 1220.05 o
31 15 -3 2749.46 3221.96 1919.15 o
33 15 -3 4681.71 6191.52 1475.00 o
35 15 -3 3903.11 4298.54 1060.30 o
37 15 -3 3433.58 2912.29 1127.06 o
39 15 -3 62.49 3736.19 1372.11 o
41 15 -3 4919.05 7550.13 1742.82 o
1 17 -3 20829.30 22435.55 1026.33 o
3 17 -3 17450.18 17097.85 845.54 o
5 17 -3 35368.48 35332.55 1484.78 o
7 17 -3 21693.16 21320.72 1108.85 o
9 17 -3 12328.00 14029.99 1106.72 o
11 17 -3 17763.47 17855.79 1255.17 o
13 17 -3 15175.62 18431.35 1548.76 o
15 17 -3 3203.45 1509.75 742.98 o
17 17 -3 12077.76 11996.09 2716.43 o
19 17 -3 25429.22 23274.90 2512.26 o
21 17 -3 15026.48 14219.82 1165.90 o
23 17 -3 42493.89 37591.27 2553.22 o
25 17 -3 12780.89 13980.76 1945.06 o
27 17 -3 11640.24 17708.60 2924.07 o
29 17 -3 3540.23 2855.20 945.85 o
31 17 -3 6847.90 8318.41 1221.72 o
33 17 -3 3870.94 4717.16 1696.48 o
35 17 -3 1722.94 4296.18 1319.49 o
37 17 -3 3744.43 2709.66 1218.95 o
39 17 -3 2124.11 1178.11 1306.13 o
1 19 -3 17930.76 18759.97 1304.59 o
3 19 -3 6009.70 6246.39 682.13 o
5 19 -3 1600.24 1894.21 653.40 o
7 19 -3 1115.83 1801.21 704.65 o
9 19 -3 4050.16 4225.11 675.38 o
11 19 -3 3060.70 4542.00 946.28 o
13 19 -3 30721.35 36862.29 3147.99 o
15 19 -3 8530.66 8141.14 1446.64 o
17 19 -3 2153.87 1936.45 824.23 o
19 19 -3 5928.80 5653.21 1039.76 o
21 19 -3 7859.34 5951.34 1415.33 o
23 19 -3 17345.43 16032.54 1850.42 o
25 19 -3 1033.90 1218.45 709.33 o
27 19 -3 3832.32 5100.61 1206.33 o
29 19 -3 2514.17 -351.08 1209.53 o
31 19 -3 620.31 -139.02 1117.64 o
33 19 -3 25888.49 25634.15 2182.65 o
35 19 -3 22056.14 17435.28 2630.33 o
37 19 -3 2398.51 3254.73 1442.01 o
39 19 -3 1345.27 3218.60 1202.46 o
1 21 -3 9979.82 10801.44 1074.25 o
3 21 -3 761.74 1439.47 708.80 o
5 21 -3 9428.53 9343.20 929.94 o
7 21 -3 4537.51 4756.79 884.24 o
9 21 -3 1699.83 2639.50 736.24 o
11 21 -3 1485.02 2209.72 703.43 o
13 21 -3 3331.28 1052.43 692.83 o
15 21 -3 3619.04 4057.48 1242.53 o
17 21 -3 13510.54 10790.18 1280.36 o
19 21 -3 16463.81 15880.27 1833.95 o
21 21 -3 3174.92 4688.60 1258.42 o
23 21 -3 1557.90 2786.63 1581.81 o
25 21 -3 10321.36 11594.20 1862.99 o
27 21 -3 1423.27 1821.36 1401.95 o
29 21 -3 4011.17 3939.61 1564.53 o
31 21 -3 291.90 14.14 1380.75 o
33 21 -3 17619.58 23140.48 3135.35 o
35 21 -3 1667.42 1859.06 1328.13 o
37 21 -3 4328.48 2847.10 1263.72 o
39 21 -3 479.29 1011.61 1580.24 o
1 23 -3 2953.46 2375.87 598.61 o
3 23 -3 8684.09 7749.49 1138.65 o
5 23 -3 8285.57 9213.46 868.52 o
7 23 -3 8546.11 9230.29 891.79 o
9 23 -3 2052.33 2164.05 750.32 o
11 23 -3 5806.58 5101.94 801.93 o
13 23 -3 1324.79 1185.53 826.76 o
15 23 -3 4411.62 6994.85 1815.08 o
17 23 -3 2360.64 2302.03 1321.06 o
19 23 -3 2667.77 1980.80 1558.25 o
21 23 -3 2619.66 3049.74 1442.01 o
23 23 -3 2706.98 3290.08 1650.93 o
25 23 -3 5543.08 6289.55 1859.06 o
27 23 -3 1968.63 -387.99 1460.07 o
29 23 -3 7542.00 7616.10 2217.21 o
31 23 -3 235.00 -1587.31 1655.64 o
33 23 -3 833.13 -219.91 1488.35 o
35 23 -3 137.66 460.25 1454.58 o
1 25 -3 929.71 1096.52 564.52 o
3 25 -3 5542.05 4428.17 943.65 o
5 25 -3 1095.78 1129.92 1001.39 o
7 25 -3 3323.05 3936.23 970.37 o
9 25 -3 3667.74 3701.89 1194.76 o
11 25 -3 375.09 -132.00 1060.27 o
13 25 -3 4908.05 5045.46 1666.64 o
15 25 -3 6252.14 6453.70 1921.89 o
17 25 -3 14824.54 15899.02 2484.25 o
19 25 -3 5509.25 5316.43 1597.52 o
21 25 -3 1679.87 910.29 1140.41 o
23 25 -3 2550.27 4147.74 2050.70 o
25 25 -3 2198.09 1560.61 1785.23 o
27 25 -3 1286.08 3575.96 1921.89 o
29 25 -3 1838.86 305.52 1387.82 o
31 25 -3 797.62 2935.86 2123.74 o
1 27 -3 3520.69 2358.31 1383.10 o
3 27 -3 523.22 11.28 812.07 o
5 27 -3 4533.28 4843.70 1236.24 o
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43 17 3 2715.82 4449.84 1443.76 o
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