#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/19/2211901.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211901_Fobs loop_ _publ_author_name 'Mtshali, Thato N.' 'Purcell, Walter' 'Visser, Hendrik G.' _publ_section_title ; Tetraphenylphosphonium aquatetracyanonitridorhenate(V) pentahydrate ; _journal_coeditor_code NG2165 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m80 _journal_page_last m82 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.576 _cell_angle_gamma 90.000 _cell_length_a 15.1335 _cell_length_b 19.7216 _cell_length_c 16.7754 _exptl_crystal_F_000 2068.00 _reflns_d_resolution_high 0.7489 _[local]_cod_data_source_file ng2165Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6ftm1_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 523.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 132627.97 126678.31 4539.04 o 4 0 0 14919.42 16982.13 352.23 o 6 0 0 179.62 128.88 37.34 o 8 0 0 1948.52 1951.38 134.34 o 10 0 0 522.94 405.81 111.64 o 12 0 0 14671.86 13303.38 600.94 o 14 0 0 24566.86 23153.27 683.90 o 16 0 0 5327.73 4770.36 315.34 o 18 0 0 4590.52 4807.30 359.08 o 2 1 0 12827.32 13025.36 243.69 o 3 1 0 48421.14 49169.18 502.07 o 4 1 0 39643.51 40191.55 397.94 o 5 1 0 407.22 421.28 36.51 o 6 1 0 18824.10 17310.12 262.90 o 7 1 0 7077.70 7611.39 176.07 o 8 1 0 40452.38 38838.32 600.58 o 9 1 0 5595.89 5476.54 163.17 o 10 1 0 26586.87 26441.33 467.79 o 11 1 0 50.88 138.02 54.29 o 12 1 0 8211.37 7885.96 231.77 o 13 1 0 3448.18 3613.76 172.62 o 14 1 0 4128.61 4099.32 226.41 o 15 1 0 4958.22 4709.58 213.42 o 16 1 0 563.49 443.36 119.96 o 17 1 0 5006.77 4695.40 236.79 o 18 1 0 1345.75 1444.50 161.12 o 19 1 0 3875.77 3620.64 238.97 o 1 2 0 9052.01 9119.78 205.49 o 2 2 0 17830.41 18168.33 182.63 o 3 2 0 35983.54 37132.41 361.29 o 4 2 0 18990.54 19493.21 212.22 o 5 2 0 78587.55 79337.41 872.77 o 6 2 0 3006.43 3089.74 86.78 o 7 2 0 45681.11 44786.83 662.01 o 8 2 0 778.48 762.85 66.93 o 9 2 0 26806.62 25669.57 444.63 o 10 2 0 8508.64 8981.06 286.52 o 11 2 0 19876.50 18879.58 381.17 o 12 2 0 2181.86 2093.42 176.51 o 13 2 0 7979.87 8061.26 318.89 o 14 2 0 1356.77 1418.57 132.81 o 15 2 0 1922.02 2157.21 158.55 o 16 2 0 7993.44 7945.08 280.60 o 17 2 0 151.11 198.88 98.72 o 18 2 0 5034.04 5075.05 256.54 o 19 2 0 1530.35 1717.42 187.83 o 1 3 0 135804.70 126348.66 1371.16 o 2 3 0 408.86 387.94 15.57 o 3 3 0 28493.34 27270.83 273.25 o 4 3 0 21179.67 21564.84 231.03 o 5 3 0 639.08 823.77 37.82 o 6 3 0 827.05 832.28 65.42 o 7 3 0 3634.96 4188.68 125.83 o 8 3 0 37.00 14.84 37.53 o 9 3 0 161.40 123.49 48.82 o 10 3 0 68.65 62.45 47.80 o 11 3 0 11840.85 11581.56 276.09 o 12 3 0 2681.29 2806.15 143.78 o 13 3 0 15497.89 15472.44 359.92 o 14 3 0 689.95 796.28 170.35 o 15 3 0 13774.17 13352.28 414.89 o 16 3 0 28.71 96.62 87.83 o 17 3 0 10672.29 11114.76 483.40 o 18 3 0 16.42 -45.09 94.02 o 19 3 0 8523.19 9142.03 367.15 o 0 4 0 7873.58 7985.04 153.05 o 1 4 0 3688.00 3936.13 51.89 o 2 4 0 17930.91 18240.69 175.33 o 3 4 0 3469.65 3559.97 56.87 o 4 4 0 318.40 303.24 23.39 o 5 4 0 15136.43 14704.18 205.05 o 6 4 0 1926.32 1860.99 73.36 o 7 4 0 35738.98 33776.00 463.14 o 8 4 0 45.50 72.97 37.47 o 9 4 0 57622.22 56973.20 846.61 o 10 4 0 747.75 654.51 94.92 o 11 4 0 21330.35 20854.76 563.63 o 12 4 0 336.56 281.22 68.71 o 13 4 0 7788.50 8205.34 249.60 o 14 4 0 2102.34 2221.91 149.39 o 15 4 0 1296.03 1151.69 153.63 o 16 4 0 8563.49 8726.02 296.15 o 17 4 0 358.31 337.72 108.55 o 18 4 0 4421.55 4435.67 319.45 o 19 4 0 347.07 28.76 114.30 o 1 5 0 56648.53 56838.61 578.66 o 2 5 0 36620.41 37028.96 356.62 o 3 5 0 3043.45 2968.22 48.96 o 4 5 0 9377.64 9059.36 151.65 o 5 5 0 809.63 941.10 43.47 o 6 5 0 25173.16 25120.13 325.56 o 7 5 0 826.26 706.53 49.03 o 8 5 0 25842.47 24369.53 414.13 o 9 5 0 159.22 143.12 49.20 o 10 5 0 24872.59 23683.06 431.88 o 11 5 0 15982.45 15840.22 338.14 o 12 5 0 2738.90 2585.41 139.85 o 13 5 0 6330.39 5515.07 220.90 o 14 5 0 226.80 188.04 79.73 o 15 5 0 2195.76 2198.08 160.17 o 16 5 0 7.62 -7.10 84.82 o 17 5 0 1178.59 1109.41 170.00 o 18 5 0 150.40 80.54 107.40 o 19 5 0 2782.58 3158.12 268.28 o 0 6 0 88096.63 89102.13 1676.64 o 1 6 0 61275.98 62982.12 644.00 o 2 6 0 51081.66 51273.50 484.22 o 3 6 0 1968.21 1978.76 52.29 o 4 6 0 16697.44 16078.22 183.15 o 5 6 0 450.64 307.34 29.58 o 6 6 0 4132.92 4354.74 118.41 o 7 6 0 7581.65 7726.35 146.61 o 8 6 0 2029.71 2227.95 100.69 o 9 6 0 246.51 261.92 53.22 o 10 6 0 6346.68 6440.80 188.92 o 11 6 0 452.92 366.71 68.84 o 12 6 0 12156.96 12049.97 297.38 o 13 6 0 33.24 43.35 63.88 o 14 6 0 14368.39 14217.33 355.30 o 15 6 0 613.56 667.89 107.19 o 16 6 0 20997.81 22609.47 507.16 o 17 6 0 155.85 175.80 98.80 o 18 6 0 14568.67 15327.63 511.70 o 19 6 0 564.16 384.96 166.08 o 1 7 0 15308.79 15732.40 194.29 o 2 7 0 6294.21 6099.37 86.28 o 3 7 0 8912.32 9061.25 119.38 o 4 7 0 24129.17 23755.49 272.24 o 5 7 0 2014.78 2123.45 63.37 o 6 7 0 17759.90 17167.54 335.98 o 7 7 0 1015.69 1269.48 90.19 o 8 7 0 37218.51 36688.46 468.96 o 9 7 0 1960.83 2050.40 105.51 o 10 7 0 30401.61 30120.52 629.02 o 11 7 0 677.87 588.01 80.54 o 12 7 0 10519.71 10423.51 273.32 o 13 7 0 1924.64 1807.86 138.44 o 14 7 0 722.69 682.00 101.42 o 15 7 0 1599.07 1396.94 138.94 o 16 7 0 145.56 96.01 92.58 o 17 7 0 445.78 578.13 147.56 o 18 7 0 233.76 55.41 122.08 o 19 7 0 790.86 1355.08 204.47 o 0 8 0 157664.00 156125.08 2374.48 o 1 8 0 660.09 721.52 25.55 o 2 8 0 27326.36 27441.42 299.06 o 3 8 0 6717.69 6807.80 86.63 o 4 8 0 21907.82 22519.34 284.22 o 5 8 0 18621.43 18385.17 248.29 o 6 8 0 128.38 229.01 33.40 o 7 8 0 25502.13 25825.29 342.59 o 8 8 0 2258.34 2284.75 83.05 o 9 8 0 23114.56 22762.06 368.78 o 10 8 0 16915.52 16475.02 333.73 o 11 8 0 29715.64 29485.64 522.65 o 12 8 0 5055.98 4859.00 181.69 o 13 8 0 4878.33 4785.14 191.10 o 14 8 0 3381.37 3175.05 171.51 o 15 8 0 775.21 703.29 111.08 o 16 8 0 1772.93 1614.94 188.43 o 17 8 0 294.23 192.99 226.00 o 18 8 0 988.80 844.76 170.87 o 1 9 0 53005.84 52322.44 589.11 o 2 9 0 4488.39 4741.83 74.25 o 3 9 0 9533.53 9094.98 146.44 o 4 9 0 1465.95 1389.22 58.92 o 5 9 0 7648.37 7339.73 127.33 o 6 9 0 2064.17 1881.07 66.59 o 7 9 0 7227.43 7213.56 143.47 o 8 9 0 30.50 13.72 31.94 o 9 9 0 840.48 1028.78 74.85 o 10 9 0 1036.81 1066.72 90.21 o 11 9 0 3354.40 3453.88 153.44 o 12 9 0 1626.95 1799.54 123.12 o 13 9 0 20230.21 19929.98 465.00 o 14 9 0 92.07 90.16 74.94 o 15 9 0 15014.51 15323.93 776.67 o 16 9 0 274.26 214.61 114.80 o 17 9 0 14491.38 15243.92 492.28 o 18 9 0 19.74 34.89 124.77 o 0 10 0 5794.19 6140.52 193.50 o 1 10 0 12661.62 12836.29 170.75 o 2 10 0 5735.89 6097.11 112.12 o 3 10 0 21275.17 21134.77 288.94 o 4 10 0 3405.97 3398.23 88.96 o 5 10 0 25082.87 23842.86 342.83 o 6 10 0 85.46 69.53 27.35 o 7 10 0 47201.27 45916.61 560.78 o 8 10 0 3546.71 3679.34 164.44 o 9 10 0 40010.33 38967.23 566.66 o 10 10 0 21.98 25.89 50.06 o 11 10 0 20282.32 19945.76 395.00 o 12 10 0 108.49 104.74 62.84 o 13 10 0 6500.19 6291.44 215.81 o 14 10 0 4713.00 4668.55 241.53 o 15 10 0 555.31 271.60 168.82 o 16 10 0 2052.03 2169.78 204.51 o 17 10 0 396.22 290.57 134.93 o 18 10 0 1966.49 2439.72 237.86 o 1 11 0 72241.24 72906.34 894.47 o 2 11 0 2937.75 3248.37 95.77 o 3 11 0 29458.30 29719.35 349.45 o 4 11 0 1853.51 1918.00 118.16 o 5 11 0 4727.46 4624.51 93.19 o 6 11 0 13675.42 13800.04 235.94 o 7 11 0 116.99 160.79 35.14 o 8 11 0 18703.18 18910.91 285.41 o 9 11 0 1819.26 1850.51 84.87 o 10 11 0 15065.08 15398.11 296.00 o 11 11 0 5529.70 5433.26 171.73 o 12 11 0 9678.14 9725.87 283.44 o 13 11 0 2006.25 2097.77 195.04 o 14 11 0 3295.24 3540.01 214.17 o 15 11 0 3022.09 3496.32 225.21 o 16 11 0 113.78 -2.79 104.26 o 17 11 0 858.29 1193.53 190.46 o 0 12 0 50128.25 50573.68 1034.65 o 1 12 0 95.15 75.10 25.02 o 2 12 0 71920.41 70296.01 871.56 o 3 12 0 563.52 620.79 45.40 o 4 12 0 9626.77 9056.53 185.51 o 5 12 0 511.16 532.57 41.82 o 6 12 0 7873.74 8042.55 141.81 o 7 12 0 365.83 405.41 51.66 o 8 12 0 6310.58 6107.14 141.08 o 9 12 0 2207.27 2127.93 99.55 o 10 12 0 60.12 -9.55 47.18 o 11 12 0 1207.67 1337.78 174.15 o 12 12 0 18041.94 17704.07 405.32 o 13 12 0 665.66 824.57 121.82 o 14 12 0 9887.80 9960.55 312.50 o 15 12 0 969.80 1082.01 139.42 o 16 12 0 11383.53 12272.91 545.30 o 17 12 0 35.50 -49.86 104.33 o 1 13 0 102.78 97.57 24.50 o 2 13 0 2435.41 2445.96 71.56 o 3 13 0 392.38 410.71 46.54 o 4 13 0 31330.96 30766.93 413.58 o 5 13 0 6382.27 6541.07 160.83 o 6 13 0 43876.21 43711.21 585.75 o 7 13 0 6216.31 6152.94 127.01 o 8 13 0 17235.62 16593.38 335.90 o 9 13 0 680.25 870.15 127.21 o 10 13 0 10679.09 10762.11 276.47 o 11 13 0 13.67 77.90 68.15 o 12 13 0 6103.83 5816.18 313.71 o 13 13 0 675.53 786.20 111.87 o 14 13 0 2641.15 2418.14 170.28 o 15 13 0 1206.82 1263.19 167.14 o 16 13 0 32.71 30.66 107.14 o 17 13 0 1134.98 1272.67 188.22 o 0 14 0 24698.14 25451.97 976.17 o 1 14 0 1121.81 1196.04 97.26 o 2 14 0 7436.15 7337.73 230.76 o 3 14 0 82.08 80.33 70.43 o 4 14 0 7411.36 7106.63 163.14 o 5 14 0 1185.14 1036.61 70.07 o 6 14 0 1661.35 1705.28 111.95 o 7 14 0 19263.32 19755.18 362.28 o 8 14 0 55.86 8.36 49.24 o 9 14 0 24704.52 24495.43 457.62 o 10 14 0 1543.02 1519.74 114.90 o 11 14 0 7993.64 7906.80 245.95 o 12 14 0 5056.05 5017.87 301.00 o 13 14 0 5723.82 5399.25 298.88 o 14 14 0 3725.61 4147.12 370.15 o 15 14 0 1528.12 1429.69 263.37 o 16 14 0 7438.03 7233.39 342.48 o 1 15 0 31505.79 30866.63 490.66 o 2 15 0 8033.42 7752.55 208.09 o 3 15 0 9550.64 9759.65 193.14 o 4 15 0 3057.95 2804.74 100.74 o 5 15 0 1335.52 1420.00 79.86 o 6 15 0 140.99 135.17 71.98 o 7 15 0 1415.64 1621.46 121.61 o 8 15 0 1236.18 1256.71 124.94 o 9 15 0 105.63 143.21 67.63 o 10 15 0 1582.38 1338.94 126.48 o 11 15 0 3902.63 3605.19 272.74 o 12 15 0 1665.99 1739.61 156.81 o 13 15 0 8285.56 8851.99 327.74 o 14 15 0 19.35 58.99 100.44 o 15 15 0 11389.40 11712.72 662.12 o 16 15 0 23.82 -10.15 112.90 o 0 16 0 19389.92 18674.22 463.80 o 1 16 0 723.15 1000.10 59.96 o 2 16 0 608.98 779.69 108.79 o 3 16 0 8718.92 8810.79 247.61 o 4 16 0 5461.48 5541.97 167.04 o 5 16 0 10481.02 10933.81 360.46 o 6 16 0 1552.54 1529.87 147.23 o 7 16 0 17216.33 16383.79 632.47 o 8 16 0 1209.04 1095.94 148.91 o 9 16 0 20501.34 19920.83 445.99 o 10 16 0 256.96 279.02 81.80 o 11 16 0 22238.36 22630.75 537.22 o 12 16 0 7.36 9.29 84.74 o 13 16 0 9217.01 8911.57 398.50 o 14 16 0 532.78 340.68 119.73 o 15 16 0 432.72 221.76 123.08 o 1 17 0 5597.21 5689.82 150.84 o 2 17 0 4392.46 4225.92 169.38 o 3 17 0 9759.34 9924.75 232.97 o 4 17 0 2837.14 2759.89 169.46 o 5 17 0 3413.52 3351.94 453.17 o 6 17 0 4767.71 4133.19 226.43 o 7 17 0 2300.24 2436.25 190.90 o 8 17 0 2642.73 2549.79 204.12 o 9 17 0 1182.65 1258.36 266.44 o 10 17 0 5884.15 5941.07 323.59 o 11 17 0 1413.91 1204.65 132.60 o 12 17 0 8362.17 8308.79 544.78 o 13 17 0 6404.38 5595.94 260.61 o 14 17 0 908.98 935.39 146.90 o 15 17 0 6673.37 6562.20 362.47 o 0 18 0 47773.92 47790.60 1034.42 o 1 18 0 336.76 448.51 48.49 o 2 18 0 31843.69 31203.12 635.61 o 3 18 0 114.63 119.98 70.02 o 4 18 0 7198.40 7002.81 282.27 o 5 18 0 8291.66 7920.23 432.06 o 6 18 0 1967.40 2157.70 235.45 o 7 18 0 7614.34 7491.44 324.52 o 8 18 0 2.89 55.35 125.71 o 9 18 0 799.46 984.10 159.13 o 10 18 0 195.86 29.29 109.91 o 11 18 0 712.71 956.85 176.24 o 12 18 0 4345.68 4466.74 317.64 o 13 18 0 595.05 344.52 158.07 o 14 18 0 11242.57 11270.40 946.54 o 1 19 0 77.63 41.46 73.69 o 2 19 0 3332.00 3476.81 165.08 o 3 19 0 15.58 199.13 95.26 o 4 19 0 2702.53 2535.80 173.75 o 5 19 0 4.63 -13.59 74.65 o 6 19 0 10169.51 9910.39 372.13 o 7 19 0 1884.49 1773.50 177.42 o 8 19 0 14813.81 14818.63 954.52 o 9 19 0 162.16 327.46 126.91 o 10 19 0 17303.14 16746.90 581.89 o 11 19 0 785.52 702.17 164.86 o 12 19 0 13348.36 13048.80 536.91 o 13 19 0 108.18 136.70 143.43 o 0 20 0 6579.89 6774.46 544.78 o 1 20 0 1516.44 1671.09 172.79 o 2 20 0 18354.75 18382.71 530.30 o 3 20 0 4519.28 4497.56 215.89 o 4 20 0 4446.09 4585.90 269.01 o 5 20 0 6721.73 6115.03 279.91 o 6 20 0 5263.24 5275.89 271.70 o 7 20 0 8102.99 8385.85 356.95 o 8 20 0 518.35 471.11 128.72 o 9 20 0 5174.83 4918.89 298.62 o 10 20 0 1577.31 1268.82 233.28 o 11 20 0 2759.75 2929.40 267.35 o 12 20 0 3123.66 3404.26 419.48 o 1 21 0 9843.72 10244.78 290.42 o 2 21 0 1507.41 1403.57 125.98 o 3 21 0 5275.11 5835.60 253.75 o 4 21 0 2393.98 2221.90 230.04 o 5 21 0 3376.73 3040.60 346.14 o 6 21 0 4229.66 4227.69 252.01 o 7 21 0 952.56 861.28 153.72 o 8 21 0 3904.57 3277.62 248.83 o 9 21 0 15.50 19.56 109.67 o 10 21 0 2281.88 2137.28 321.10 o 11 21 0 731.16 549.47 286.33 o 0 22 0 136.99 437.88 241.94 o 1 22 0 235.87 296.14 208.12 o 2 22 0 79.57 139.10 196.48 o 3 22 0 1259.07 1373.70 179.16 o 4 22 0 1.26 -147.67 233.42 o 5 22 0 5681.75 5812.94 284.10 o 6 22 0 37.26 27.26 98.01 o 7 22 0 9382.94 9661.17 738.28 o 8 22 0 246.15 304.09 133.96 o 9 22 0 18853.14 18906.96 634.91 o 10 22 0 56.43 69.59 125.94 o 1 23 0 11391.68 11527.56 553.24 o 2 23 0 1962.47 1824.06 371.58 o 3 23 0 6300.12 6730.35 621.64 o 4 23 0 1158.21 1552.07 369.68 o 5 23 0 2703.18 2745.29 522.05 o 6 23 0 1471.60 1335.33 220.02 o 7 23 0 348.86 240.73 123.50 o 8 23 0 2042.16 1578.77 198.81 o 9 23 0 4.76 5.42 200.40 o 0 24 0 7702.56 6619.12 626.24 o 1 24 0 605.67 444.65 255.75 o 2 24 0 4717.58 4361.77 532.06 o 3 24 0 1102.54 1594.29 381.59 o 4 24 0 2022.45 2483.59 444.65 o 5 24 0 1047.68 1185.37 355.61 o 6 24 0 3822.05 4294.12 556.15 o 7 24 0 1299.43 1570.97 190.11 o 8 24 0 3942.52 3771.04 372.66 o 1 25 0 917.26 938.55 340.18 o 2 25 0 71.68 46.55 246.28 o 3 25 0 262.54 56.56 235.99 o 4 25 0 3886.42 3900.35 548.84 o 5 25 0 411.80 480.10 300.40 o 6 25 0 8067.43 8199.34 755.60 o 0 26 0 12768.64 11378.72 832.73 o 1 26 0 60.68 -56.29 220.84 o 2 26 0 7774.24 7152.26 699.31 o 3 26 0 88.39 -3.52 244.38 o -19 0 1 1253.04 1565.53 476.85 o -17 0 1 12.76 -92.48 121.37 o -15 0 1 1464.40 1857.94 211.00 o -13 0 1 15751.15 15782.58 512.38 o -11 0 1 25648.40 25550.51 664.48 o -9 0 1 39426.73 37729.94 848.90 o -7 0 1 35637.24 34987.48 759.73 o -5 0 1 9450.27 9175.29 177.90 o -3 0 1 32222.54 33181.00 529.00 o 1 0 1 187.74 212.68 20.26 o 3 0 1 50482.82 52642.17 709.30 o 5 0 1 106568.78 108132.84 1647.51 o 7 0 1 120348.39 121974.25 3436.62 o 9 0 1 37560.50 34916.10 817.44 o 11 0 1 31298.08 30499.04 1336.92 o 13 0 1 9900.21 9665.49 387.47 o 15 0 1 46.87 -69.08 105.68 o 17 0 1 1085.15 731.03 181.15 o 19 0 1 1935.11 1871.97 450.47 o -19 1 1 10334.95 11220.34 569.61 o -18 1 1 202.54 199.18 110.35 o -17 1 1 14040.96 13319.28 430.39 o -16 1 1 1160.44 1279.34 137.01 o -15 1 1 14464.17 14830.50 406.99 o -14 1 1 2636.43 2914.12 163.86 o -13 1 1 6170.99 6225.26 214.89 o -12 1 1 8159.02 8260.20 314.61 o -11 1 1 1177.27 1111.41 99.53 o -10 1 1 15970.29 16191.47 330.65 o -9 1 1 2900.92 2622.58 176.91 o -8 1 1 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