#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/19/2211938.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211938_Fobs loop_ _publ_author_name 'Rosli, Mohd Mustaqim' 'Karthikeyan, Mari Sithambaram' 'Fun, Hoong-Kun' 'Razak, Ibrahim Abdul' 'Patil, P. S.' _publ_section_title ; N-(3-Chloro-4-fluorophenyl)thiourea ; _journal_coeditor_code SJ2176 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o67 _journal_page_last o68 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.228 _cell_angle_beta 94.455 _cell_angle_gamma 95.321 _cell_length_a 5.4642 _cell_length_b 8.3919 _cell_length_c 9.6469 _exptl_crystal_F_000 208.00 _reflns_d_resolution_high 0.6614 _[local]_cod_data_source_file sj2176Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil54b_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 42.30 42.51 0.73 o 2 0 0 2468.86 2265.45 38.32 o 3 0 0 59.23 72.93 1.01 o 4 0 0 77.34 87.89 1.04 o 5 0 0 195.85 206.11 2.66 o 6 0 0 56.67 50.53 1.12 o 7 0 0 0.83 0.73 0.24 o 8 0 0 0.57 1.11 0.31 o -8 1 0 11.16 11.79 0.69 o -7 1 0 98.77 101.56 1.91 o -6 1 0 15.68 15.53 0.74 o -5 1 0 182.16 181.98 1.99 o -4 1 0 0.12 0.20 0.16 o -3 1 0 10.23 13.41 0.29 o -2 1 0 1167.52 1170.51 19.79 o -1 1 0 371.49 389.64 8.91 o 0 1 0 2.82 2.66 0.18 o 1 1 0 132.59 134.57 2.56 o 2 1 0 117.86 134.47 2.00 o 3 1 0 589.77 575.50 5.49 o 4 1 0 22.60 22.54 0.49 o 5 1 0 37.82 33.29 0.67 o 6 1 0 20.21 20.11 0.80 o 7 1 0 31.23 33.33 2.60 o 8 1 0 62.21 65.61 2.12 o -8 2 0 49.03 52.28 1.33 o -7 2 0 24.39 23.58 0.80 o -6 2 0 22.92 22.74 0.71 o -5 2 0 55.09 54.61 0.87 o -4 2 0 555.75 560.87 5.84 o -3 2 0 28.37 27.52 0.55 o -2 2 0 562.05 563.89 12.95 o -1 2 0 250.21 265.76 6.22 o 0 2 0 1345.16 1330.95 30.25 o 1 2 0 4388.01 3686.72 94.21 o 2 2 0 135.51 160.09 2.85 o 3 2 0 470.92 459.80 4.40 o 4 2 0 20.63 16.65 0.41 o 5 2 0 1.84 0.49 0.15 o 6 2 0 316.95 299.74 7.43 o 7 2 0 23.87 25.61 0.82 o -8 3 0 86.65 87.54 1.86 o -7 3 0 61.31 57.18 1.32 o -6 3 0 12.44 12.96 0.48 o -5 3 0 0.58 1.10 0.15 o -4 3 0 285.85 273.28 3.03 o -3 3 0 0.43 1.01 0.19 o -2 3 0 11.42 13.11 0.32 o -1 3 0 1224.00 1182.63 25.60 o 0 3 0 276.19 294.88 4.77 o 1 3 0 993.01 961.64 21.51 o 2 3 0 697.42 730.70 14.14 o 3 3 0 22.03 23.03 0.57 o 4 3 0 207.74 179.12 2.23 o 5 3 0 69.72 58.23 0.95 o 6 3 0 23.72 25.62 0.81 o 7 3 0 82.98 84.49 3.25 o -8 4 0 22.24 22.91 0.86 o -7 4 0 198.92 191.89 3.12 o -6 4 0 383.86 378.13 4.65 o -5 4 0 177.59 182.80 2.49 o -4 4 0 0.80 0.89 0.21 o -3 4 0 345.97 349.23 4.86 o -2 4 0 0.01 0.86 0.14 o -1 4 0 944.45 958.11 10.73 o 0 4 0 203.01 189.99 2.28 o 1 4 0 11.38 9.85 0.43 o 2 4 0 698.50 745.43 11.98 o 3 4 0 3.49 3.28 0.28 o 4 4 0 429.93 426.14 5.92 o 5 4 0 67.01 63.21 1.67 o 6 4 0 19.93 18.55 0.87 o 7 4 0 21.98 22.84 1.56 o -7 5 0 105.04 105.83 2.00 o -6 5 0 17.47 17.66 0.71 o -5 5 0 1.01 1.30 0.21 o -4 5 0 1.71 1.71 0.22 o -3 5 0 562.71 553.06 7.50 o -2 5 0 1.12 0.21 0.08 o -1 5 0 0.23 0.31 0.16 o 0 5 0 323.27 328.56 3.36 o 1 5 0 24.57 24.92 0.41 o 2 5 0 784.87 775.96 10.15 o 3 5 0 45.67 44.87 0.96 o 4 5 0 16.37 18.55 0.62 o 5 5 0 10.47 10.52 0.53 o 6 5 0 11.92 11.02 0.74 o 7 5 0 3.99 3.49 0.75 o -7 6 0 74.81 71.70 2.21 o -6 6 0 22.73 22.44 0.81 o -5 6 0 519.89 516.22 7.30 o -4 6 0 6.28 6.18 0.48 o -3 6 0 7.97 8.29 0.35 o -2 6 0 0.13 0.45 0.36 o -1 6 0 166.52 173.40 1.95 o 0 6 0 787.29 792.28 7.77 o 1 6 0 824.85 798.20 8.68 o 2 6 0 81.46 79.58 1.36 o 3 6 0 6.22 7.37 0.36 o 4 6 0 19.24 16.24 1.97 o 5 6 0 210.03 209.35 4.24 o 6 6 0 57.89 58.74 1.82 o -7 7 0 12.90 13.62 0.92 o -6 7 0 51.91 48.23 1.46 o -5 7 0 0.35 0.24 0.18 o -4 7 0 57.33 52.14 1.11 o -3 7 0 49.96 44.73 0.89 o -2 7 0 614.52 601.04 8.20 o -1 7 0 0.18 0.64 0.15 o 0 7 0 311.57 308.75 3.65 o 1 7 0 59.21 58.25 1.72 o 2 7 0 4.83 5.74 0.38 o 3 7 0 276.82 272.97 5.08 o 4 7 0 15.56 16.50 0.86 o 5 7 0 21.36 19.35 0.99 o 6 7 0 1.63 2.22 0.48 o -6 8 0 20.17 19.19 1.10 o -5 8 0 22.53 22.88 0.69 o -4 8 0 128.50 127.64 2.97 o -3 8 0 62.22 59.95 2.44 o -2 8 0 113.72 122.24 2.17 o -1 8 0 4.45 4.83 0.28 o 0 8 0 0.90 1.11 0.19 o 1 8 0 1166.06 1118.67 17.42 o 2 8 0 39.44 39.63 1.02 o 3 8 0 190.09 193.26 3.95 o 4 8 0 14.49 10.76 1.17 o 5 8 0 20.08 21.36 1.21 o -6 9 0 21.76 20.87 1.67 o -5 9 0 7.48 6.50 1.02 o -4 9 0 115.89 113.89 4.04 o -3 9 0 51.56 47.82 2.24 o -2 9 0 40.04 39.63 1.94 o -1 9 0 121.73 121.66 1.80 o 0 9 0 113.38 114.05 1.73 o 1 9 0 2.13 2.44 0.37 o 2 9 0 3.51 2.91 0.35 o 3 9 0 42.29 44.82 1.31 o 4 9 0 30.30 28.89 1.02 o -5 10 0 59.68 59.49 2.91 o -4 10 0 24.01 26.31 1.81 o -3 10 0 82.63 88.31 3.46 o -2 10 0 5.62 5.37 0.86 o -1 10 0 117.35 122.49 2.67 o 0 10 0 119.64 115.49 2.09 o 1 10 0 3.51 4.32 0.56 o 2 10 0 56.44 56.56 1.38 o 3 10 0 8.23 9.47 0.72 o -4 11 0 6.53 8.17 1.14 o -3 11 0 76.78 79.43 3.36 o -2 11 0 28.88 31.60 1.89 o -1 11 0 0.12 0.03 0.28 o 0 11 0 8.90 8.98 0.55 o 1 11 0 0.12 0.57 0.26 o 2 11 0 66.08 65.12 1.57 o -2 12 0 6.29 7.07 1.06 o -1 12 0 8.63 7.95 0.70 o 0 12 0 93.13 91.88 3.15 o -1 -12 1 32.34 34.52 1.16 o 0 -12 1 5.30 7.72 0.90 o 1 -12 1 85.33 88.53 2.29 o 2 -12 1 11.98 14.19 1.36 o 3 -12 1 50.56 55.97 2.79 o -3 -11 1 17.05 16.83 0.79 o -2 -11 1 119.72 118.63 2.28 o -1 -11 1 19.83 20.05 0.78 o 0 -11 1 41.20 39.45 1.32 o 1 -11 1 0.53 0.75 0.34 o 2 -11 1 55.12 54.85 2.56 o 3 -11 1 2.64 3.18 0.82 o 4 -11 1 13.76 15.03 1.45 o -4 -10 1 30.76 32.04 1.09 o -3 -10 1 9.18 10.42 0.91 o -2 -10 1 2.60 2.63 0.36 o -1 -10 1 28.99 31.23 0.93 o 0 -10 1 378.63 376.38 5.25 o 1 -10 1 6.88 7.71 0.62 o 2 -10 1 0.28 0.42 0.33 o 3 -10 1 2.87 3.12 0.71 o 4 -10 1 130.78 134.91 4.69 o 5 -10 1 111.40 109.17 4.19 o -5 -9 1 23.46 21.70 1.14 o -4 -9 1 0.02 -0.29 0.21 o -3 -9 1 3.91 4.32 0.43 o -2 -9 1 162.33 162.57 2.67 o -1 -9 1 47.20 47.06 3.40 o 0 -9 1 115.40 116.18 2.00 o 1 -9 1 26.30 25.17 0.64 o 2 -9 1 20.29 19.55 0.90 o 3 -9 1 269.58 262.64 5.15 o 4 -9 1 0.44 0.79 0.35 o 5 -9 1 11.67 10.62 0.84 o 6 -9 1 0.01 -0.38 0.47 o -5 -8 1 23.90 24.57 1.15 o -4 -8 1 158.80 151.77 3.36 o -3 -8 1 15.51 15.48 1.20 o -2 -8 1 57.40 57.92 1.25 o -1 -8 1 0.55 0.50 0.46 o 0 -8 1 798.60 797.48 8.85 o 1 -8 1 333.92 340.79 4.05 o 2 -8 1 256.34 252.83 4.79 o 3 -8 1 43.38 35.35 1.76 o 4 -8 1 3.36 2.80 0.43 o 5 -8 1 4.18 5.26 0.58 o 6 -8 1 176.65 168.44 2.87 o -6 -7 1 5.85 5.88 0.64 o -5 -7 1 1.34 0.73 0.55 o -4 -7 1 114.18 113.94 2.64 o -3 -7 1 14.75 15.72 0.84 o -2 -7 1 10.49 9.98 0.46 o -1 -7 1 129.94 125.97 2.38 o 0 -7 1 3.76 3.98 0.21 o 1 -7 1 77.48 78.40 1.23 o 2 -7 1 6.30 7.70 0.51 o 3 -7 1 98.21 89.51 2.13 o 4 -7 1 286.26 276.46 4.08 o 5 -7 1 15.63 16.15 0.60 o 6 -7 1 72.88 70.84 1.57 o 7 -7 1 0.71 1.25 0.43 o -6 -6 1 62.26 60.74 1.84 o -5 -6 1 66.26 61.70 2.11 o -4 -6 1 20.79 17.88 0.84 o -3 -6 1 153.28 148.06 2.98 o -2 -6 1 0.66 0.45 0.20 o -1 -6 1 556.89 569.79 5.66 o 0 -6 1 239.84 232.62 2.49 o 1 -6 1 287.76 290.40 2.82 o 2 -6 1 41.13 41.23 2.36 o 3 -6 1 170.53 154.44 2.38 o 4 -6 1 355.71 339.32 4.37 o 5 -6 1 29.56 28.29 0.83 o 6 -6 1 12.84 13.17 0.62 o 7 -6 1 286.63 276.86 4.49 o -7 -5 1 174.40 169.30 5.39 o -6 -5 1 169.60 164.51 3.51 o -5 -5 1 0.17 0.31 0.24 o -4 -5 1 45.53 33.81 1.46 o -3 -5 1 270.85 232.57 5.07 o -2 -5 1 0.55 0.47 0.14 o -1 -5 1 205.24 232.56 2.43 o 0 -5 1 164.76 160.88 1.76 o 1 -5 1 166.14 174.06 1.94 o 2 -5 1 566.66 567.60 7.61 o 3 -5 1 2.26 2.95 0.33 o 4 -5 1 15.04 14.22 0.46 o 5 -5 1 101.73 97.83 1.63 o 6 -5 1 68.52 69.66 1.55 o 7 -5 1 2.83 2.77 0.35 o -7 -4 1 130.88 124.26 4.23 o -6 -4 1 22.72 24.97 1.01 o -5 -4 1 729.29 683.12 11.34 o -4 -4 1 64.70 73.35 1.38 o -3 -4 1 51.44 50.59 6.45 o -2 -4 1 0.12 0.34 0.10 o -1 -4 1 2.70 1.99 0.16 o 0 -4 1 1287.38 1252.89 16.09 o 1 -4 1 384.83 401.10 4.75 o 2 -4 1 0.91 2.04 0.15 o 3 -4 1 29.53 32.39 0.73 o 4 -4 1 257.21 255.45 3.35 o 5 -4 1 458.76 444.65 8.27 o 6 -4 1 0.19 0.32 0.18 o 7 -4 1 1.05 0.42 0.24 o 8 -4 1 3.49 4.54 1.27 o -7 -3 1 183.33 177.56 5.43 o -6 -3 1 20.01 19.04 0.84 o -5 -3 1 303.11 285.86 4.20 o -3 -3 1 0.72 1.63 0.17 o -2 -3 1 164.94 136.31 3.36 o -1 -3 1 898.17 1018.45 22.91 o 0 -3 1 48.23 59.02 1.61 o 1 -3 1 910.62 1004.11 24.72 o 2 -3 1 129.01 113.19 1.70 o 3 -3 1 482.50 466.45 5.63 o 4 -3 1 42.13 39.06 0.86 o 5 -3 1 33.70 32.64 0.64 o 6 -3 1 64.61 64.69 1.25 o 7 -3 1 1.04 1.46 0.28 o 8 -3 1 80.92 79.24 1.74 o -7 -2 1 15.78 17.08 0.62 o -6 -2 1 0.69 1.87 0.26 o -5 -2 1 156.71 140.44 1.88 o -4 -2 1 386.74 406.06 4.65 o -3 -2 1 129.56 158.54 1.93 o -2 -2 1 1406.91 1171.76 26.02 o 1 -2 1 12695.44 7999.36 178.90 o 2 -2 1 1.26 1.86 0.17 o 3 -2 1 733.25 773.29 9.24 o 4 -2 1 0.31 1.46 0.27 o 5 -2 1 166.07 169.37 2.06 o 6 -2 1 209.57 207.72 3.18 o 7 -2 1 1.17 2.02 0.31 o 8 -2 1 46.84 48.79 1.27 o -8 -1 1 0.42 0.29 0.24 o -7 -1 1 0.32 0.28 0.19 o -6 -1 1 194.17 197.34 3.53 o -5 -1 1 45.46 43.60 0.79 o -4 -1 1 846.77 870.57 8.06 o -3 -1 1 200.21 210.68 3.22 o -2 -1 1 11.14 11.31 0.42 o 0 -1 1 182.21 183.35 3.97 o 1 -1 1 47.17 51.55 1.56 o 2 -1 1 0.60 0.30 0.11 o 3 -1 1 172.33 182.43 2.03 o 4 -1 1 394.42 396.87 3.86 o 5 -1 1 25.50 27.77 0.77 o 6 -1 1 80.68 78.34 1.51 o 7 -1 1 9.05 9.33 0.51 o 8 -1 1 6.52 6.33 0.63 o -8 0 1 75.27 79.13 1.90 o -7 0 1 14.48 14.84 0.69 o -6 0 1 278.68 280.89 4.85 o -5 0 1 93.70 90.16 1.37 o -4 0 1 0.00 0.01 0.07 o -3 0 1 407.36 440.52 7.42 o 0 0 1 79.82 70.26 1.94 o 1 0 1 3793.63 2910.79 106.63 o 2 0 1 2470.09 2394.70 40.71 o 3 0 1 864.30 949.24 8.69 o 4 0 1 693.76 690.82 5.98 o 5 0 1 30.18 25.90 0.61 o 6 0 1 37.15 33.75 0.78 o 7 0 1 138.60 133.92 2.75 o 8 0 1 6.71 6.01 0.51 o -8 1 1 15.10 14.07 0.73 o -7 1 1 59.78 66.56 2.02 o -6 1 1 36.94 36.53 1.05 o -5 1 1 0.26 1.23 1.08 o -4 1 1 0.50 0.99 0.11 o -3 1 1 1458.09 1401.67 15.11 o -2 1 1 315.08 340.51 5.47 o 1 1 1 127.30 142.16 2.74 o 2 1 1 61.42 51.45 0.87 o 3 1 1 352.34 378.08 3.38 o 4 1 1 0.66 1.29 0.13 o 5 1 1 252.14 236.12 3.59 o 6 1 1 127.97 123.57 2.09 o 7 1 1 127.28 133.17 2.29 o -8 2 1 34.75 35.53 1.06 o -7 2 1 20.28 20.74 0.75 o -6 2 1 174.19 175.17 2.77 o -5 2 1 854.99 859.56 9.93 o -4 2 1 581.23 587.06 6.10 o -3 2 1 79.67 86.99 1.05 o -2 2 1 0.37 0.41 0.09 o -1 2 1 8.89 10.57 0.50 o 1 2 1 470.71 508.09 13.15 o 2 2 1 21.57 23.79 0.35 o 3 2 1 145.99 152.12 1.72 o 4 2 1 167.39 174.40 2.01 o 5 2 1 524.03 510.92 5.87 o 6 2 1 0.16 0.02 0.18 o 7 2 1 7.63 8.68 0.44 o -8 3 1 0.20 0.15 0.27 o -7 3 1 119.43 121.46 2.21 o -6 3 1 252.21 254.23 3.76 o -5 3 1 299.32 299.83 3.76 o -4 3 1 83.53 89.00 1.29 o -3 3 1 22.53 26.75 0.59 o -2 3 1 786.17 760.67 17.15 o -1 3 1 9.79 6.99 0.23 o 0 3 1 7.76 7.63 0.27 o 1 3 1 40.78 41.06 0.58 o 2 3 1 67.44 58.86 2.17 o 3 3 1 719.59 707.52 7.14 o 4 3 1 4.30 5.26 0.24 o 5 3 1 20.41 22.36 0.53 o 6 3 1 5.59 6.32 0.33 o 7 3 1 59.62 58.58 1.82 o -8 4 1 12.49 13.08 0.80 o -7 4 1 152.41 141.35 2.48 o -6 4 1 183.05 180.85 2.85 o -5 4 1 0.62 1.13 0.36 o -4 4 1 1575.70 1544.74 19.48 o -3 4 1 187.92 178.38 2.31 o -2 4 1 333.57 332.43 3.94 o -1 4 1 958.80 1010.49 11.30 o 0 4 1 85.86 99.72 1.31 o 1 4 1 267.43 285.06 3.82 o 2 4 1 385.59 374.22 4.35 o 3 4 1 68.21 62.84 1.72 o 4 4 1 0.27 0.54 0.48 o 5 4 1 63.59 65.37 1.73 o 6 4 1 213.20 208.51 3.70 o 7 4 1 18.17 19.64 1.02 o -7 5 1 7.92 5.73 0.90 o -6 5 1 56.42 55.50 1.22 o -5 5 1 32.90 34.21 1.12 o -4 5 1 183.37 177.44 2.42 o -3 5 1 249.27 236.93 3.00 o -2 5 1 0.44 -0.04 0.05 o -1 5 1 326.45 330.08 3.37 o 0 5 1 6.81 7.34 0.24 o 1 5 1 340.05 337.20 3.80 o 2 5 1 12.31 13.66 0.77 o 3 5 1 20.28 20.25 0.66 o 4 5 1 183.28 174.50 2.80 o 5 5 1 4.49 4.54 0.37 o 6 5 1 62.99 62.56 1.47 o -7 6 1 11.16 11.78 0.79 o -6 6 1 79.97 79.68 2.08 o -5 6 1 51.16 50.46 1.43 o -4 6 1 23.68 25.15 0.64 o -3 6 1 183.17 176.75 2.37 o -2 6 1 138.57 129.72 1.56 o -1 6 1 792.99 827.29 7.39 o 0 6 1 130.71 123.33 1.45 o 1 6 1 92.26 90.26 1.25 o 2 6 1 887.34 862.71 11.34 o 3 6 1 5.70 7.38 0.38 o 4 6 1 271.08 271.68 5.00 o 5 6 1 20.16 18.35 0.71 o 6 6 1 20.19 20.45 1.04 o -7 7 1 19.92 19.20 0.97 o -6 7 1 3.95 3.67 0.45 o -5 7 1 18.00 17.16 0.76 o -4 7 1 53.83 54.16 1.38 o -3 7 1 453.69 431.95 5.98 o -2 7 1 260.03 239.49 3.52 o -1 7 1 12.64 15.68 0.45 o 0 7 1 19.91 20.92 0.59 o 1 7 1 363.82 356.50 4.09 o 2 7 1 16.32 17.75 0.55 o 3 7 1 0.16 0.36 0.24 o 4 7 1 19.09 21.97 0.73 o 5 7 1 29.82 26.60 1.19 o -6 8 1 4.40 5.44 0.49 o -5 8 1 120.02 119.58 2.56 o -4 8 1 133.97 135.55 2.69 o -3 8 1 6.00 5.23 0.50 o -2 8 1 16.07 14.31 1.10 o -1 8 1 9.29 6.99 0.34 o 0 8 1 208.94 207.24 2.69 o 1 8 1 188.37 183.14 3.38 o 2 8 1 14.75 15.10 0.61 o 3 8 1 25.24 25.74 0.86 o 4 8 1 23.39 22.65 1.08 o 5 8 1 113.34 111.11 2.85 o -6 9 1 50.06 48.72 1.23 o -5 9 1 2.25 1.78 0.71 o -4 9 1 38.22 39.40 2.11 o -3 9 1 4.64 4.33 0.52 o -2 9 1 221.72 212.01 4.23 o -1 9 1 108.53 106.95 2.04 o 0 9 1 20.03 19.97 0.60 o 1 9 1 88.24 83.78 1.67 o 2 9 1 8.17 8.15 0.52 o 3 9 1 10.07 11.58 0.92 o 4 9 1 26.61 31.14 1.06 o -5 10 1 96.37 92.42 3.80 o -4 10 1 162.13 168.61 5.56 o -3 10 1 177.28 183.92 5.78 o -2 10 1 16.67 17.38 0.91 o -1 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156.71 158.20 2.20 o 2 2 9 106.39 105.43 1.65 o 3 2 9 19.24 19.22 0.60 o 4 2 9 1.78 1.79 0.29 o 5 2 9 1.26 1.36 0.38 o -6 3 9 129.54 131.60 3.48 o -5 3 9 144.09 144.19 2.85 o -4 3 9 19.21 22.14 0.67 o -3 3 9 6.43 7.76 0.37 o -2 3 9 26.63 27.17 0.67 o -1 3 9 86.13 84.49 1.69 o 0 3 9 321.05 324.26 4.79 o 1 3 9 5.92 5.53 0.43 o 2 3 9 3.42 2.71 0.42 o 3 3 9 16.90 14.68 0.53 o 4 3 9 69.69 65.41 1.64 o -5 4 9 0.57 0.54 0.24 o -4 4 9 44.13 47.05 1.00 o -3 4 9 179.56 179.00 2.49 o -2 4 9 298.89 305.56 5.04 o -1 4 9 301.95 308.44 4.64 o 0 4 9 48.69 43.45 1.16 o 1 4 9 83.69 87.88 1.83 o 2 4 9 88.40 94.39 1.95 o 3 4 9 44.28 46.37 1.26 o 4 4 9 21.46 22.53 1.09 o -5 5 9 13.17 13.34 0.61 o -4 5 9 138.25 136.22 2.37 o -3 5 9 10.87 11.08 0.47 o -2 5 9 15.14 16.76 0.72 o -1 5 9 9.16 9.70 0.64 o 0 5 9 127.23 133.35 2.47 o 1 5 9 161.18 166.96 2.94 o 2 5 9 27.60 30.62 1.01 o 3 5 9 11.05 11.38 0.79 o -4 6 9 136.96 140.68 2.48 o -3 6 9 0.08 0.22 0.18 o -2 6 9 84.89 89.73 2.89 o -1 6 9 17.78 15.37 0.70 o 0 6 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