#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212054.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212054_Fobs loop_ _publ_author_name 'Hay, Michael T.' 'Geib, Steven J.' _publ_section_title ; Tetrabutylammonium isobutyl silsesquioxane monochloroferrate(III) ; _journal_coeditor_code BT2233 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m445 _journal_page_last m446 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.586 _cell_angle_gamma 90.000 _cell_length_a 23.6451 _cell_length_b 32.1149 _cell_length_c 18.3528 _exptl_crystal_F_000 4856.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file bt2233Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hay712s in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 886.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 613591.56 698864.06 12862.11 o 4 0 0 310477.75 328391.56 4375.71 o 6 0 0 292793.94 326660.56 3557.23 o 8 0 0 53524.18 53867.32 1295.96 o 10 0 0 3570.90 2703.24 132.01 o 12 0 0 380.10 359.83 84.83 o 14 0 0 6564.27 6168.96 220.78 o 16 0 0 11174.28 9951.42 471.74 o 18 0 0 16.00 36.96 194.15 o 20 0 0 11447.76 10759.78 541.62 o 22 0 0 2777.12 3225.47 369.94 o 24 0 0 51.73 0.00 191.65 o 26 0 0 889.10 952.30 278.60 o 3 1 0 6561.98 8071.49 116.22 o 5 1 0 284442.72 313237.47 2405.27 o 7 1 0 73132.02 77074.46 680.68 o 9 1 0 2134.43 2240.33 83.92 o 11 1 0 75800.80 82083.09 813.26 o 13 1 0 108995.98 106174.02 976.49 o 15 1 0 5703.97 6254.13 271.41 o 17 1 0 3033.99 3012.82 231.84 o 19 1 0 1064.19 1205.58 200.49 o 21 1 0 258.37 311.05 169.55 o 23 1 0 306.72 173.35 156.38 o 25 1 0 9.24 153.71 194.26 o 2 2 0 9052.92 8969.19 104.67 o 4 2 0 476.14 114.41 44.61 o 6 2 0 4198.07 5454.84 126.38 o 8 2 0 1324.21 2104.55 134.32 o 10 2 0 2428.88 3148.32 163.96 o 12 2 0 27719.73 26328.86 337.86 o 14 2 0 68424.43 65179.39 738.56 o 16 2 0 3071.56 2979.96 236.44 o 18 2 0 6800.15 6264.36 289.43 o 20 2 0 4184.47 3778.88 254.27 o 22 2 0 82.13 0.00 159.79 o 24 2 0 15.84 139.11 159.20 o 26 2 0 126.41 577.16 180.72 o 1 3 0 58276.16 67734.60 706.97 o 3 3 0 4726.47 7676.90 110.87 o 5 3 0 288194.34 338177.66 5009.01 o 7 3 0 73509.62 74792.82 668.31 o 9 3 0 501.09 322.32 59.86 o 11 3 0 17973.75 19071.09 270.22 o 13 3 0 34594.85 35673.09 429.16 o 15 3 0 14978.17 13752.17 295.56 o 17 3 0 1476.99 1570.42 211.00 o 19 3 0 93.09 238.25 155.52 o 21 3 0 60.51 178.28 154.91 o 23 3 0 51.72 0.00 142.84 o 25 3 0 1733.89 1805.09 239.01 o 0 4 0 156237.52 177916.50 3317.81 o 2 4 0 64978.10 81348.19 727.46 o 4 4 0 9201.61 6356.59 115.78 o 6 4 0 194973.80 224253.91 1767.03 o 8 4 0 15482.15 14491.15 214.36 o 10 4 0 9969.44 8682.37 170.90 o 12 4 0 3217.97 3548.70 170.10 o 14 4 0 4488.26 3770.91 132.97 o 16 4 0 1698.16 1772.94 213.12 o 18 4 0 3971.36 4426.04 262.94 o 20 4 0 2342.00 2508.66 366.31 o 22 4 0 757.16 915.69 204.09 o 24 4 0 47.81 266.94 223.25 o 1 5 0 6891.44 6779.97 101.50 o 3 5 0 43736.72 50341.00 453.01 o 5 5 0 16332.79 20937.08 249.82 o 7 5 0 1059.25 1243.17 84.28 o 9 5 0 24921.83 28827.44 347.18 o 11 5 0 3575.58 3159.58 113.43 o 13 5 0 6956.52 6560.14 166.62 o 15 5 0 3163.63 3479.79 170.76 o 17 5 0 1376.32 1473.31 204.89 o 19 5 0 14222.98 13917.58 536.63 o 21 5 0 2394.86 2849.04 276.00 o 23 5 0 625.44 787.13 192.25 o 25 5 0 582.23 950.79 196.77 o 0 6 0 26.36 608.97 72.35 o 4 6 0 34345.27 37410.31 374.92 o 6 6 0 49688.16 49294.07 483.09 o 8 6 0 39636.13 42593.60 453.28 o 10 6 0 13514.67 11959.07 212.56 o 12 6 0 40509.56 39894.41 611.42 o 14 6 0 5769.83 6086.76 168.80 o 16 6 0 48.95 0.00 256.56 o 18 6 0 3170.52 2582.82 259.88 o 20 6 0 6856.09 5990.90 303.12 o 22 6 0 2295.59 2357.09 265.46 o 24 6 0 601.12 888.78 192.63 o 1 7 0 30330.03 37537.05 358.36 o 3 7 0 20097.11 22595.80 259.34 o 5 7 0 13168.58 15035.47 215.08 o 7 7 0 2485.87 2132.43 101.75 o 9 7 0 18.82 0.00 59.86 o 11 7 0 9614.70 8058.44 182.87 o 13 7 0 612.42 711.05 97.02 o 15 7 0 6254.74 5996.67 214.43 o 17 7 0 13407.31 12715.32 395.01 o 19 7 0 2051.35 2114.39 283.00 o 21 7 0 423.69 320.47 166.55 o 23 7 0 2021.62 1683.46 236.62 o 25 7 0 1932.15 2967.84 273.49 o 0 8 0 1628.65 958.23 96.23 o 2 8 0 90466.92 110497.36 917.41 o 4 8 0 1870.24 1978.71 87.73 o 6 8 0 55049.62 56993.24 604.05 o 8 8 0 21829.66 20112.52 284.45 o 10 8 0 77.04 0.00 94.51 o 12 8 0 17.67 182.86 93.54 o 14 8 0 438.90 514.87 96.44 o 16 8 0 9952.95 9129.07 458.89 o 18 8 0 5341.50 4881.75 276.09 o 20 8 0 1750.57 1881.02 243.92 o 22 8 0 7470.55 6791.55 335.60 o 24 8 0 843.72 1309.38 494.80 o 1 9 0 892.51 853.79 71.41 o 3 9 0 1271.77 1561.09 83.59 o 5 9 0 5902.72 6919.67 180.07 o 7 9 0 5356.37 6873.67 162.34 o 9 9 0 7889.21 6927.02 169.90 o 11 9 0 2909.03 2241.11 118.51 o 13 9 0 1957.79 1618.09 130.48 o 15 9 0 4370.99 3338.27 185.08 o 17 9 0 2654.63 2409.27 246.29 o 19 9 0 4175.18 4671.55 284.93 o 21 9 0 3745.07 4094.39 288.72 o 23 9 0 869.02 1170.96 201.92 o 25 9 0 46.41 9.45 150.03 o 0 10 0 612.15 1400.33 120.73 o 2 10 0 955.15 1010.34 80.89 o 4 10 0 126.45 306.65 70.13 o 6 10 0 1117.57 874.26 97.36 o 8 10 0 9810.84 8526.81 187.84 o 10 10 0 5449.22 5459.26 161.14 o 12 10 0 7102.43 6340.57 185.26 o 14 10 0 13452.56 12801.29 265.41 o 16 10 0 11337.90 9776.40 290.57 o 18 10 0 27.89 0.00 148.07 o 20 10 0 369.12 326.04 249.78 o 22 10 0 81.70 186.83 155.97 o 24 10 0 23.43 556.77 168.21 o 1 11 0 1631.49 1121.08 83.16 o 3 11 0 2391.41 2407.98 99.70 o 5 11 0 20705.87 22330.65 298.83 o 7 11 0 19486.21 19997.64 389.65 o 9 11 0 629.02 601.72 92.23 o 11 11 0 1145.67 1491.73 130.77 o 13 11 0 1887.41 1692.53 133.28 o 15 11 0 13183.74 13336.33 365.50 o 17 11 0 5370.26 5087.65 275.64 o 19 11 0 234.82 29.83 154.54 o 21 11 0 4304.88 4295.87 286.84 o 23 11 0 253.27 418.68 168.48 o 25 11 0 95.51 334.64 204.64 o 0 12 0 17614.19 17003.66 337.48 o 2 12 0 13317.24 15422.42 275.25 o 4 12 0 34159.10 40109.63 441.48 o 6 12 0 842.72 1491.98 111.01 o 8 12 0 312.07 888.37 98.45 o 10 12 0 1005.67 1623.79 122.79 o 12 12 0 4.03 0.00 82.22 o 14 12 0 17163.00 15372.02 305.09 o 16 12 0 11234.53 12469.16 330.46 o 18 12 0 3621.61 3848.93 247.65 o 20 12 0 1472.39 2114.89 269.39 o 22 12 0 3111.70 3065.07 257.14 o 24 12 0 1189.75 1794.02 230.28 o 1 13 0 14325.77 14486.03 226.13 o 3 13 0 8852.05 7330.45 165.03 o 5 13 0 1609.10 1845.60 108.76 o 7 13 0 145.99 173.94 77.28 o 9 13 0 7893.26 7895.51 195.52 o 11 13 0 6957.77 7548.86 203.62 o 13 13 0 1025.53 1143.98 131.30 o 15 13 0 222.64 429.09 152.63 o 17 13 0 19.28 28.51 136.05 o 19 13 0 4249.76 4359.11 279.33 o 21 13 0 6234.63 6214.01 320.06 o 23 13 0 953.29 1092.93 207.09 o 0 14 0 70551.18 69525.83 944.00 o 2 14 0 15745.98 16305.64 253.88 o 4 14 0 4224.64 5239.67 184.19 o 6 14 0 16730.37 14045.71 264.53 o 8 14 0 35513.48 31810.74 554.82 o 10 14 0 16361.53 15970.36 292.24 o 12 14 0 433.56 516.92 106.52 o 14 14 0 123.96 114.63 102.34 o 16 14 0 754.98 845.67 156.78 o 18 14 0 57.54 195.40 204.21 o 20 14 0 973.86 1000.00 190.42 o 22 14 0 186.90 90.50 152.58 o 24 14 0 50.61 153.29 149.48 o 1 15 0 3833.50 4545.28 140.01 o 3 15 0 385.28 357.21 76.14 o 5 15 0 15046.73 14116.29 249.81 o 7 15 0 23029.33 19627.60 339.97 o 9 15 0 8191.41 8797.49 217.18 o 11 15 0 6708.07 6238.90 195.60 o 13 15 0 5573.89 4672.14 186.74 o 15 15 0 6674.04 5310.27 233.34 o 17 15 0 110.45 129.32 184.74 o 19 15 0 1322.86 1178.38 199.72 o 21 15 0 1.39 0.00 234.78 o 23 15 0 1096.04 1066.44 211.68 o 0 16 0 7879.16 8162.70 257.92 o 2 16 0 1430.75 1345.51 108.93 o 4 16 0 4294.51 4761.94 151.23 o 6 16 0 20009.17 16967.54 287.27 o 8 16 0 10287.55 10946.47 239.70 o 10 16 0 52.55 0.00 76.62 o 12 16 0 6968.74 7157.89 214.89 o 14 16 0 1864.68 2238.84 165.85 o 16 16 0 19.02 114.83 148.77 o 18 16 0 4.53 0.21 129.36 o 20 16 0 92.43 158.41 143.90 o 22 16 0 3.50 255.41 173.91 o 1 17 0 7165.47 8594.20 223.94 o 3 17 0 9443.56 9773.43 210.46 o 5 17 0 840.28 618.40 109.72 o 7 17 0 541.61 631.52 96.72 o 9 17 0 1539.00 1303.51 123.83 o 11 17 0 7037.92 6751.17 208.59 o 13 17 0 572.57 574.74 120.25 o 15 17 0 2525.90 2130.07 173.03 o 17 17 0 926.69 1478.13 202.00 o 19 17 0 1250.17 1817.91 222.18 o 21 17 0 1036.21 1116.97 237.69 o 23 17 0 333.46 733.05 246.76 o 0 18 0 531.77 280.96 121.61 o 2 18 0 14.73 212.31 81.95 o 4 18 0 244.29 174.08 79.67 o 6 18 0 2042.09 2102.28 125.55 o 8 18 0 382.12 611.93 95.77 o 10 18 0 449.61 591.42 105.91 o 12 18 0 4797.54 5150.01 194.61 o 14 18 0 1884.25 2174.24 162.20 o 16 18 0 806.61 1269.63 166.32 o 18 18 0 4.98 262.83 185.04 o 20 18 0 1956.61 2061.02 382.32 o 22 18 0 798.04 1136.93 250.23 o 1 19 0 200.79 189.07 85.26 o 3 19 0 739.23 780.55 104.40 o 5 19 0 16.10 21.44 96.22 o 7 19 0 2153.45 2286.16 162.81 o 9 19 0 176.64 215.00 87.63 o 11 19 0 71.00 142.34 150.43 o 13 19 0 3264.07 3249.61 172.33 o 15 19 0 1091.92 832.52 140.48 o 17 19 0 913.91 1283.28 170.25 o 19 19 0 284.43 276.61 149.66 o 21 19 0 2.32 148.37 193.70 o 0 20 0 576.87 949.01 168.14 o 2 20 0 1336.31 1795.34 132.66 o 4 20 0 5241.27 5037.48 176.78 o 6 20 0 57.74 100.21 81.82 o 8 20 0 3010.02 2940.64 165.87 o 10 20 0 9399.27 9528.49 246.12 o 12 20 0 1415.52 1505.78 150.71 o 14 20 0 450.17 687.33 120.45 o 16 20 0 1494.26 1369.04 191.46 o 18 20 0 1.90 536.73 164.73 o 20 20 0 35.09 14.34 203.65 o 22 20 0 29.30 0.00 190.89 o 1 21 0 8553.73 9451.97 227.64 o 3 21 0 10446.50 10689.97 243.03 o 5 21 0 3449.92 3351.94 151.47 o 7 21 0 2.99 0.00 123.72 o 9 21 0 4.63 53.41 84.19 o 11 21 0 10550.73 9343.77 251.62 o 13 21 0 114.10 70.88 96.35 o 15 21 0 191.95 455.82 126.02 o 17 21 0 3117.59 3332.67 332.42 o 19 21 0 13.75 211.57 202.54 o 21 21 0 168.26 400.66 288.49 o 0 22 0 54067.88 54709.22 893.34 o 2 22 0 10861.74 10590.39 248.27 o 4 22 0 6680.63 6422.67 204.89 o 6 22 0 9395.43 8841.04 236.31 o 8 22 0 1253.66 1709.31 165.27 o 10 22 0 9582.85 9596.82 257.14 o 12 22 0 169.92 363.46 148.91 o 14 22 0 11.93 124.32 154.41 o 16 22 0 230.63 328.03 196.22 o 18 22 0 486.45 722.55 220.00 o 20 22 0 45.30 378.90 216.58 o 1 23 0 496.05 590.78 119.40 o 3 23 0 68.75 182.54 99.10 o 5 23 0 3664.99 3249.93 164.03 o 7 23 0 3836.78 3790.20 185.94 o 9 23 0 898.92 807.87 125.34 o 11 23 0 7975.65 6961.12 227.19 o 13 23 0 10528.63 9466.45 389.42 o 15 23 0 29.69 333.20 166.36 o 17 23 0 7341.63 6812.94 322.26 o 19 23 0 927.33 1138.87 271.71 o 21 23 0 36.20 0.00 206.78 o 0 24 0 10311.05 9920.50 356.97 o 2 24 0 807.33 1092.29 135.93 o 4 24 0 16786.90 15459.97 316.14 o 6 24 0 1120.62 1523.98 143.24 o 8 24 0 626.33 842.91 130.90 o 10 24 0 1522.27 1922.44 203.07 o 12 24 0 10065.71 9153.81 312.13 o 14 24 0 8615.34 8411.87 308.48 o 16 24 0 874.39 993.74 202.62 o 18 24 0 237.58 538.27 278.43 o 20 24 0 484.39 883.83 273.56 o 1 25 0 551.27 444.28 127.87 o 3 25 0 16.84 190.93 107.18 o 5 25 0 4859.61 4921.90 197.04 o 7 25 0 5169.96 4877.68 253.51 o 9 25 0 347.05 292.01 128.17 o 11 25 0 19.89 85.55 143.44 o 13 25 0 12.50 69.81 207.34 o 15 25 0 56.35 200.33 160.57 o 17 25 0 9.96 273.39 166.38 o 19 25 0 1944.88 3548.44 435.08 o 0 26 0 3678.54 4097.38 269.81 o 2 26 0 1.09 168.21 134.77 o 4 26 0 1146.70 1479.70 157.73 o 6 26 0 13.46 0.00 110.65 o 8 26 0 415.03 253.97 132.73 o 10 26 0 3796.35 4182.17 231.49 o 12 26 0 235.93 272.26 137.34 o 14 26 0 2675.21 3749.87 257.27 o 16 26 0 1226.14 1664.12 236.73 o 18 26 0 6030.60 5779.03 384.45 o 1 27 0 1221.39 1378.16 154.05 o 3 27 0 2379.92 2466.59 187.90 o 5 27 0 440.01 752.74 149.63 o 7 27 0 1943.90 1859.47 204.68 o 9 27 0 9876.94 8413.57 304.48 o 11 27 0 8993.02 9831.64 333.71 o 13 27 0 923.78 1309.57 192.60 o 15 27 0 2.03 3.29 177.01 o 17 27 0 3200.76 3210.79 302.34 o 19 27 0 3177.93 2436.98 463.81 o 0 28 0 78.24 0.00 150.48 o 2 28 0 360.82 506.36 136.21 o 4 28 0 1706.62 1546.30 187.15 o 6 28 0 3291.85 3581.12 225.29 o 8 28 0 2664.25 2739.71 217.80 o 10 28 0 537.04 856.56 164.70 o 12 28 0 2115.69 1672.99 211.44 o 14 28 0 1013.98 1135.17 185.26 o 16 28 0 436.33 611.82 239.81 o 18 28 0 118.65 287.81 323.21 o 1 29 0 1181.22 1342.32 168.43 o 3 29 0 5948.09 4956.38 232.93 o 5 29 0 5643.13 4954.35 238.48 o 7 29 0 89.37 32.41 127.91 o 9 29 0 1454.12 1397.20 215.78 o 11 29 0 585.11 349.57 148.83 o 13 29 0 451.93 534.61 214.13 o 15 29 0 354.02 365.81 235.55 o 17 29 0 280.73 204.27 211.80 o 0 30 0 73.65 91.70 258.78 o 2 30 0 220.40 450.50 134.44 o 4 30 0 65.82 0.00 215.91 o 6 30 0 2405.08 2622.82 243.87 o 8 30 0 4059.29 3931.15 259.93 o 10 30 0 42.08 0.00 125.86 o 12 30 0 789.04 630.02 201.08 o 14 30 0 6.24 0.00 181.13 o 16 30 0 346.58 688.08 255.29 o 1 31 0 5.72 202.80 133.59 o 3 31 0 163.65 303.47 143.18 o 5 31 0 1979.80 2439.84 229.03 o 7 31 0 567.88 527.22 149.86 o 9 31 0 1230.15 2039.18 207.42 o 11 31 0 1144.39 1480.04 248.20 o 13 31 0 2.21 6.36 181.32 o 15 31 0 62.42 38.67 252.62 o 0 32 0 319.14 590.20 257.95 o 2 32 0 2.62 35.26 145.80 o 4 32 0 1528.58 1643.02 213.13 o 6 32 0 2781.26 2752.25 217.99 o 8 32 0 2953.33 2986.89 243.25 o 10 32 0 191.06 71.84 178.18 o 12 32 0 1.33 197.86 240.84 o 14 32 0 159.60 0.00 195.12 o 1 33 0 1120.41 991.93 199.17 o 3 33 0 7.91 200.90 153.92 o 5 33 0 539.54 460.35 196.47 o 7 33 0 533.30 587.60 170.95 o 9 33 0 22.72 116.32 244.88 o 11 33 0 29.79 180.84 190.35 o 13 33 0 131.11 61.09 182.71 o 0 34 0 348.95 449.82 253.27 o 2 34 0 96.58 353.04 177.12 o 4 34 0 1404.69 1915.03 261.33 o 6 34 0 24.97 234.79 205.28 o 8 34 0 827.95 1171.45 268.40 o 10 34 0 8.75 0.00 186.81 o 12 34 0 166.24 73.30 191.18 o 1 35 0 3468.96 3783.84 293.56 o 3 35 0 12393.01 11818.20 425.50 o 5 35 0 1663.97 1857.85 308.91 o 7 35 0 558.55 848.06 260.36 o 9 35 0 2784.66 3075.87 366.14 o 11 35 0 1467.45 1792.43 352.77 o 0 36 0 3083.92 3355.15 451.76 o 2 36 0 2826.15 2877.96 357.05 o 4 36 0 1838.50 2575.61 744.87 o 6 36 0 25.57 0.00 199.71 o 8 36 0 2500.61 2369.53 335.94 o 10 36 0 7289.65 7946.30 708.39 o 1 37 0 1552.05 1640.03 308.18 o 3 37 0 5104.58 4944.14 436.14 o 5 37 0 6044.67 5355.35 390.93 o 7 37 0 1138.52 1412.00 287.78 o 9 37 0 39.67 552.64 250.38 o 0 38 0 6093.03 4882.86 722.39 o 2 38 0 397.47 773.34 520.56 o 4 38 0 219.72 641.48 265.97 o 6 38 0 1507.39 1869.08 461.74 o 1 39 0 0.45 32.97 434.63 o 3 39 0 2938.10 2676.75 493.88 o -25 1 1 50.41 299.70 163.07 o -23 1 1 769.94 1041.62 196.43 o -21 1 1 1297.59 1247.20 208.20 o -19 1 1 994.93 1181.91 200.29 o -17 1 1 390.99 374.87 150.47 o -15 1 1 2299.00 2381.71 112.27 o -13 1 1 50246.25 50238.60 547.75 o -11 1 1 10087.40 11167.73 198.53 o -9 1 1 25510.60 26007.74 312.59 o -7 1 1 190239.67 205804.39 1788.67 o -5 1 1 11133.40 14278.18 178.03 o -3 1 1 5246.83 6246.23 88.09 o 1 1 1 7544.52 7396.37 122.33 o 3 1 1 51730.37 59298.74 624.93 o 5 1 1 72037.05 74686.87 713.14 o 7 1 1 31916.08 32163.86 383.93 o 9 1 1 1584.62 2707.40 103.16 o 11 1 1 90815.43 92623.13 952.21 o 13 1 1 70248.52 68475.45 929.67 o 15 1 1 8486.51 8138.65 303.86 o 17 1 1 1734.12 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8 21 1262.20 1361.48 188.21 o -4 8 21 19.18 196.83 388.67 o -19 9 21 28.69 403.41 209.94 o -17 9 21 445.82 375.46 215.98 o -15 9 21 1.00 173.05 173.54 o -13 9 21 10.60 0.00 150.95 o -11 9 21 4.41 0.00 125.59 o -9 9 21 92.77 0.00 129.54 o -7 9 21 648.29 858.92 179.10 o -5 9 21 1405.69 1601.36 429.39 o -18 10 21 19.60 92.95 183.70 o -16 10 21 401.68 691.31 224.69 o -14 10 21 435.24 534.07 181.45 o -12 10 21 20.31 227.88 155.58 o -10 10 21 474.11 290.65 233.63 o -8 10 21 805.22 786.62 169.82 o -6 10 21 416.81 367.97 151.14 o -17 11 21 3585.19 3830.14 337.49 o -15 11 21 151.30 135.40 162.09 o -13 11 21 3264.20 3623.09 273.23 o -11 11 21 1944.87 2046.07 247.39 o -9 11 21 180.06 342.64 147.33 o -7 11 21 334.92 652.32 162.32 o -16 12 21 52.62 279.64 179.47 o -14 12 21 1403.35 1377.50 234.54 o -12 12 21 3856.49 3845.38 274.46 o -10 12 21 1157.04 1486.15 237.81 o -8 12 21 637.68 602.60 157.81 o -15 13 21 669.76 831.97 203.42 o -13 13 21 401.41 305.88 181.28 o -11 13 21 122.34 484.59 164.95 o -9 13 21 256.96 268.38 159.63 o -14 14 21 3287.89 3868.32 378.16 o -12 14 21 150.39 101.39 156.24 o -10 14 21 142.14 288.67 187.46 o -18 0 22 22.20 203.83 302.74 o -16 0 22 9382.44 9085.30 781.34 o -14 0 22 16023.62 14846.24 1473.25 o -12 0 22 2169.35 2975.35 336.58 o -10 0 22 1925.65 2121.03 336.39 o -8 0 22 8696.53 8596.58 483.54 o -17 1 22 62.25 336.17 221.39 o -15 1 22 20.04 188.81 189.20 o -13 1 22 27.64 78.58 146.23 o -11 1 22 14.32 154.13 134.89 o -9 1 22 1762.03 1915.21 203.67 o -7 1 22 182.16 596.42 148.95 o -18 2 22 1.80 0.00 189.89 o -16 2 22 2.83 0.00 186.95 o -14 2 22 206.52 582.08 203.65 o -12 2 22 8.96 7.51 136.09 o -10 2 22 9.18 0.00 133.06 o -8 2 22 1935.59 2309.04 219.49 o -17 3 22 26.57 110.29 180.07 o -15 3 22 8.99 0.00 165.06 o -13 3 22 230.88 16.89 158.38 o -11 3 22 226.29 38.44 152.28 o -9 3 22 256.17 368.50 155.11 o -7 3 22 3202.21 3340.73 238.53 o -18 4 22 94.91 0.00 221.97 o -16 4 22 1084.08 1099.62 245.28 o -14 4 22 1181.64 1189.35 313.37 o -12 4 22 130.11 322.78 207.02 o -10 4 22 1534.43 1663.89 245.70 o -8 4 22 1775.41 2064.19 262.03 o -17 5 22 24.77 0.00 174.12 o -15 5 22 127.68 0.00 169.75 o -13 5 22 426.92 304.20 193.24 o -11 5 22 93.16 104.46 147.84 o -9 5 22 2.51 26.25 147.20 o -16 6 22 774.06 1251.20 256.23 o -14 6 22 247.91 316.33 182.64 o -12 6 22 46.41 237.71 169.54 o -10 6 22 107.25 254.66 163.24 o -8 6 22 469.52 377.06 162.87 o -15 7 22 32.99 90.75 164.52 o -13 7 22 5.86 0.00 172.62 o -11 7 22 143.30 0.00 137.25 o -9 7 22 275.61 513.08 159.80 o -14 8 22 1259.80 1815.44 355.14 o -12 8 22 542.18 338.89 170.42 o -10 8 22 3.51 34.69 138.29 o -13 9 22 49.92 117.61 192.95 o