#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:24:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181040 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/20/2212059.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212059_Fobs loop_ _publ_author_name 'Fu, Wei-Wei' 'Chen, Zhong-Ning' _publ_section_title ; catena-Poly[[[acetonitrilebis[\m-bis(diphenylphosphino)methane-\k^2^P:P']dicopper(I)]-\m-(1,2-dicyanoethylene-1,2-dithiolato)-[(1,2-dicyanoethylene-1,2-dithiolato)tungstate(IV)]-\m-(1,2-dicyanoethylene-1,2-dithiolato)] diethyl ether disolvate acetonitrile solvate] ; _journal_coeditor_code BT2238 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m482 _journal_page_last m483 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.502 _cell_angle_gamma 90.000 _cell_length_a 17.3530 _cell_length_b 21.8357 _cell_length_c 21.2915 _exptl_crystal_F_000 3496.00 _reflns_d_resolution_high 0.8408 _cod_data_source_file bt2238Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' x in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 684.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46900.23 49268.07 1249.53 o 4 0 0 132951.09 116235.98 2939.52 o 6 0 0 11139.99 11000.12 336.78 o 8 0 0 8815.11 7745.54 281.72 o 10 0 0 25166.28 25068.54 729.53 o 12 0 0 34995.81 33948.90 979.43 o 14 0 0 724.10 877.57 226.05 o 16 0 0 9632.34 10379.79 461.88 o 18 0 0 2812.68 3102.25 394.59 o 20 0 0 3732.08 3995.12 456.38 o 1 1 0 35898.09 4206.43 6310.04 o 2 1 0 274500.38 255103.58 4522.74 o 3 1 0 40766.21 38459.50 1056.21 o 4 1 0 23397.36 22821.08 430.14 o 5 1 0 1089.48 991.49 69.44 o 6 1 0 2398.82 2831.70 99.94 o 7 1 0 14872.15 13637.92 327.29 o 8 1 0 18285.85 18232.83 380.10 o 9 1 0 83.97 20.72 113.48 o 10 1 0 30954.11 29283.12 589.18 o 11 1 0 225.66 235.98 109.32 o 12 1 0 1260.38 1298.98 150.15 o 13 1 0 2676.08 2426.29 177.43 o 14 1 0 13079.45 13268.99 361.14 o 15 1 0 1472.82 1477.63 305.58 o 16 1 0 157.57 337.96 164.39 o 17 1 0 184.50 -163.19 163.19 o 18 1 0 8343.93 9247.78 348.66 o 19 1 0 1962.48 2159.79 263.61 o 20 1 0 429.23 454.53 244.40 o 0 2 0 402057.47 290779.78 28247.88 o 1 2 0 35729.41 35949.15 647.12 o 2 2 0 25370.75 24665.93 539.58 o 3 2 0 93788.81 89954.27 1609.09 o 4 2 0 8232.09 8173.88 466.01 o 5 2 0 11470.80 11452.89 239.00 o 6 2 0 164.10 265.71 97.42 o 7 2 0 485.28 640.81 77.03 o 8 2 0 7549.00 6689.03 185.59 o 9 2 0 25467.93 23251.91 476.37 o 10 2 0 6998.46 6705.30 204.11 o 11 2 0 10979.09 10586.55 285.05 o 12 2 0 17473.77 17557.73 406.84 o 13 2 0 1463.47 1512.16 167.08 o 14 2 0 546.91 363.41 266.73 o 15 2 0 595.11 199.73 156.52 o 16 2 0 7718.69 7496.66 295.57 o 17 2 0 7671.91 7795.94 312.71 o 18 2 0 1407.15 1615.76 232.61 o 19 2 0 905.08 890.62 225.99 o 20 2 0 955.74 875.13 379.29 o 1 3 0 42609.84 42310.71 2715.77 o 2 3 0 2918.63 2645.85 54.62 o 3 3 0 45540.00 40778.87 1152.72 o 4 3 0 16127.33 14736.69 896.23 o 5 3 0 2997.70 2850.98 94.68 o 6 3 0 3391.32 3265.30 127.25 o 7 3 0 46747.84 45347.10 1152.26 o 8 3 0 4951.39 4723.20 318.88 o 9 3 0 27453.21 25833.01 522.50 o 10 3 0 3362.02 3358.42 451.79 o 11 3 0 3950.68 4399.11 182.82 o 12 3 0 2703.70 2537.84 172.75 o 13 3 0 8511.88 7844.28 258.98 o 14 3 0 4922.73 5036.32 361.86 o 15 3 0 6909.46 7554.77 275.60 o 16 3 0 17.60 -368.59 368.59 o 17 3 0 601.11 504.67 338.46 o 18 3 0 98.07 -174.21 308.02 o 19 3 0 7362.08 8051.11 531.01 o 20 3 0 841.73 247.76 367.06 o 0 4 0 10384.29 12604.29 1217.72 o 1 4 0 9145.70 10278.29 620.02 o 2 4 0 14614.08 13521.15 367.36 o 3 4 0 550.79 509.98 40.14 o 4 4 0 474.31 359.69 46.26 o 5 4 0 37919.95 34182.28 637.22 o 6 4 0 3118.31 2646.48 190.11 o 7 4 0 19867.95 18926.57 399.63 o 8 4 0 1154.85 1103.98 101.42 o 9 4 0 36045.00 36401.78 706.02 o 10 4 0 563.14 372.51 100.67 o 11 4 0 30769.65 30212.64 618.82 o 12 4 0 27.16 -61.51 61.51 o 13 4 0 356.77 605.73 399.48 o 14 4 0 186.26 -114.26 114.26 o 15 4 0 33.56 -124.93 124.93 o 16 4 0 892.88 413.35 171.45 o 17 4 0 8293.80 8370.25 527.80 o 18 4 0 45.92 -207.69 207.69 o 19 4 0 560.00 852.80 326.68 o 20 4 0 275.86 -273.46 273.46 o 1 5 0 10849.14 12349.84 194.52 o 2 5 0 71805.48 75234.25 1357.35 o 3 5 0 224313.72 221715.98 3218.72 o 4 5 0 7155.54 7478.81 160.30 o 5 5 0 22683.77 22843.98 438.30 o 6 5 0 2232.88 2261.50 96.99 o 7 5 0 24211.41 21651.63 755.83 o 8 5 0 2550.85 2557.48 124.52 o 9 5 0 29216.71 27911.92 560.34 o 10 5 0 14409.20 14389.20 332.81 o 11 5 0 526.68 326.77 105.54 o 12 5 0 52.18 82.29 199.28 o 13 5 0 6955.07 7124.69 247.97 o 14 5 0 1872.27 1187.61 216.26 o 15 5 0 7331.93 7197.88 313.53 o 16 5 0 285.42 4.61 149.52 o 17 5 0 1113.83 1052.54 332.80 o 18 5 0 723.79 511.43 296.09 o 19 5 0 6706.87 6819.33 499.50 o 20 5 0 467.41 338.31 336.78 o 0 6 0 13310.74 15341.42 544.93 o 1 6 0 1192.61 1485.17 43.52 o 2 6 0 91815.62 92080.82 2451.95 o 3 6 0 45546.94 47101.25 869.74 o 4 6 0 1833.03 2008.15 98.04 o 5 6 0 62462.79 60625.29 1105.08 o 6 6 0 1178.34 1477.34 101.25 o 7 6 0 59545.33 56735.64 1049.41 o 8 6 0 3509.05 3384.01 134.44 o 9 6 0 1566.45 1760.47 193.62 o 10 6 0 274.95 290.69 96.27 o 11 6 0 11019.51 10443.98 501.95 o 12 6 0 22654.74 22084.36 789.79 o 13 6 0 426.27 138.78 314.14 o 14 6 0 8.12 278.42 359.41 o 15 6 0 2706.09 3127.34 338.61 o 16 6 0 1846.61 1312.84 296.71 o 17 6 0 6927.36 6876.22 469.53 o 18 6 0 5.57 -77.08 260.61 o 19 6 0 32.94 260.61 297.62 o 1 7 0 1664.49 1654.06 62.65 o 2 7 0 4971.99 4881.80 267.03 o 3 7 0 127594.35 127750.26 2514.35 o 4 7 0 8323.89 8849.16 263.06 o 5 7 0 9213.90 8540.83 189.00 o 6 7 0 12634.23 12034.21 357.42 o 7 7 0 98.69 49.06 60.43 o 8 7 0 873.79 993.91 250.67 o 9 7 0 9010.95 8566.00 434.20 o 10 7 0 10815.73 10572.67 268.78 o 11 7 0 3628.79 3620.35 175.73 o 12 7 0 3719.91 3652.48 182.93 o 13 7 0 629.92 852.55 261.99 o 14 7 0 18009.38 17715.45 655.50 o 15 7 0 2692.64 2654.75 337.08 o 16 7 0 3.02 -208.61 233.39 o 17 7 0 469.52 -191.18 244.09 o 18 7 0 827.67 435.58 353.91 o 19 7 0 3070.87 3179.34 408.05 o 0 8 0 13507.31 13979.32 289.06 o 1 8 0 11502.46 12290.35 178.03 o 2 8 0 1988.86 1908.63 170.82 o 3 8 0 15563.24 15508.51 701.85 o 4 8 0 17986.47 15943.71 357.42 o 5 8 0 27490.90 26252.21 495.73 o 6 8 0 3098.10 3441.97 153.25 o 7 8 0 23589.49 23025.76 563.74 o 8 8 0 666.34 561.52 150.95 o 9 8 0 5940.45 5212.91 180.16 o 10 8 0 428.24 450.67 289.52 o 11 8 0 102.94 -92.50 92.50 o 12 8 0 28268.64 26908.73 851.88 o 13 8 0 27.66 -97.88 193.01 o 14 8 0 32.49 286.00 233.69 o 15 8 0 2438.84 1989.76 306.80 o 16 8 0 7653.09 7489.82 461.58 o 17 8 0 1441.02 958.63 294.87 o 18 8 0 111.77 -248.68 248.68 o 19 8 0 343.12 -35.79 287.22 o 1 9 0 77.70 3.88 47.71 o 2 9 0 37740.08 37802.63 528.59 o 3 9 0 23142.60 24414.59 482.28 o 4 9 0 973.22 1284.88 105.72 o 5 9 0 2127.72 2354.93 186.13 o 6 9 0 13350.31 12459.09 259.81 o 7 9 0 90.41 -246.68 419.82 o 8 9 0 1950.91 2066.36 192.86 o 9 9 0 66.33 -275.60 275.60 o 10 9 0 2555.95 3057.90 260.00 o 11 9 0 5607.07 5354.46 333.41 o 12 9 0 7171.25 6763.05 400.40 o 13 9 0 1044.19 1300.92 267.95 o 14 9 0 36043.84 35792.14 1119.53 o 15 9 0 121.33 -184.75 219.93 o 16 9 0 1812.30 1832.84 322.71 o 17 9 0 483.44 -4.89 257.25 o 18 9 0 678.45 227.88 275.60 o 19 9 0 217.33 -59.95 316.28 o 0 10 0 11729.54 12156.60 259.00 o 1 10 0 167.53 211.07 150.29 o 2 10 0 119.11 368.30 122.34 o 3 10 0 389.49 340.63 160.28 o 4 10 0 49865.71 48251.91 912.60 o 5 10 0 2971.93 2717.36 169.92 o 6 10 0 3109.85 2794.84 200.05 o 7 10 0 113.17 -106.75 106.75 o 8 10 0 287.90 -96.96 131.53 o 9 10 0 7092.32 7084.53 339.22 o 10 10 0 3892.52 3726.25 329.43 o 11 10 0 473.49 368.59 217.18 o 12 10 0 14685.67 15301.74 605.03 o 13 10 0 4510.83 5114.96 410.80 o 14 10 0 792.31 732.28 277.13 o 15 10 0 8.27 -216.26 248.38 o 16 10 0 15170.89 16166.16 700.16 o 17 10 0 131.67 -248.07 248.07 o 18 10 0 1990.36 2141.17 391.22 o 1 11 0 570.19 622.39 75.96 o 2 11 0 76150.29 79716.88 1027.09 o 3 11 0 30520.96 32937.81 642.91 o 4 11 0 1059.04 1079.97 104.79 o 5 11 0 7405.83 7095.93 227.27 o 6 11 0 3224.79 2942.28 212.89 o 7 11 0 5151.06 4639.61 287.22 o 8 11 0 465.85 86.56 170.07 o 9 11 0 263.26 277.13 181.69 o 10 11 0 1533.00 1632.19 260.61 o 11 11 0 9050.17 8639.63 425.79 o 12 11 0 4575.54 4684.58 372.26 o 13 11 0 914.95 1075.17 288.45 o 14 11 0 19065.35 19141.17 715.15 o 15 11 0 2660.11 2438.18 364.92 o 16 11 0 1367.81 1316.52 353.91 o 17 11 0 182.82 -262.45 262.45 o 18 11 0 1415.05 1012.77 369.81 o 0 12 0 11572.73 12717.21 282.64 o 1 12 0 3308.76 3239.40 127.99 o 2 12 0 2735.05 2952.21 237.04 o 3 12 0 8795.90 9112.14 196.87 o 4 12 0 15715.93 16654.03 373.17 o 5 12 0 59114.33 60428.88 1652.53 o 6 12 0 21.78 -143.15 143.15 o 7 12 0 11239.64 10052.80 418.14 o 8 12 0 803.77 17.74 173.13 o 9 12 0 7399.95 7246.95 382.66 o 10 12 0 659.73 493.39 235.83 o 11 12 0 2487.23 2485.29 313.53 o 12 12 0 8390.83 9073.37 481.46 o 13 12 0 8966.81 8790.74 469.22 o 14 12 0 1870.51 2257.41 337.69 o 15 12 0 766.94 899.29 313.53 o 16 12 0 6945.95 7418.86 509.29 o 17 12 0 762.32 851.27 363.08 o 18 12 0 432.46 -11.01 298.54 o 1 13 0 4728.13 4949.46 259.52 o 2 13 0 15180.65 14924.54 279.68 o 3 13 0 41529.57 41751.33 1057.45 o 4 13 0 511.74 935.43 239.81 o 5 13 0 28767.29 30717.23 627.39 o 6 13 0 1203.41 1267.97 581.79 o 7 13 0 19764.33 20018.43 654.59 o 8 13 0 871.36 810.59 212.59 o 9 13 0 8529.32 8127.58 399.18 o 10 13 0 1915.86 1448.35 263.98 o 11 13 0 6219.20 6977.77 436.80 o 12 13 0 615.96 957.41 260.31 o 13 13 0 226.96 418.14 274.99 o 14 13 0 4519.99 4903.59 427.32 o 15 13 0 7640.11 8297.65 544.47 o 16 13 0 41.01 616.35 318.42 o 17 13 0 214.55 157.53 326.38 o 0 14 0 113.93 349.26 99.59 o 1 14 0 15931.22 17007.60 332.02 o 2 14 0 5243.46 5691.20 157.57 o 3 14 0 6842.46 7242.48 359.65 o 4 14 0 1553.84 1655.98 273.38 o 5 14 0 65895.66 69145.49 1508.00 o 6 14 0 3520.78 3293.94 307.26 o 7 14 0 15544.52 15151.85 562.82 o 8 14 0 91.86 253.27 196.99 o 9 14 0 9630.68 9470.10 456.99 o 10 14 0 29.31 -168.54 168.54 o 11 14 0 10312.10 10339.11 490.02 o 12 14 0 488.67 601.67 261.53 o 13 14 0 7184.76 7331.99 474.42 o 14 14 0 657.16 166.40 299.46 o 15 14 0 60.12 -187.20 256.02 o 16 14 0 326.78 -193.32 311.69 o 17 14 0 5435.58 4738.11 492.47 o 1 15 0 1201.30 1352.51 199.23 o 2 15 0 10107.50 9772.46 217.01 o 3 15 0 19117.01 19787.09 359.47 o 4 15 0 124.65 209.27 99.19 o 5 15 0 493.42 415.26 212.74 o 6 15 0 19933.72 18989.65 1155.77 o 7 15 0 31360.34 32213.33 964.75 o 8 15 0 29.72 361.55 203.72 o 9 15 0 16669.35 16650.67 616.66 o 10 15 0 823.31 310.47 216.56 o 11 15 0 2104.00 2505.78 375.93 o 12 15 0 6107.95 6140.27 447.51 o 13 15 0 687.00 731.06 317.51 o 14 15 0 518.08 794.37 303.13 o 15 15 0 3788.72 4007.05 421.20 o 16 15 0 374.60 -287.22 287.22 o 0 16 0 11404.29 11838.85 464.63 o 1 16 0 1707.86 1455.24 478.40 o 2 16 0 299.41 -44.82 264.63 o 3 16 0 1155.82 1123.08 115.75 o 4 16 0 11576.79 12441.90 270.63 o 5 16 0 26670.80 27294.69 533.68 o 6 16 0 101.58 227.96 292.88 o 7 16 0 573.37 665.60 223.91 o 8 16 0 8978.27 9406.17 479.62 o 9 16 0 9455.57 10880.83 503.79 o 10 16 0 165.54 3.98 251.13 o 11 16 0 13670.53 14920.30 628.28 o 12 16 0 2779.08 2790.87 412.33 o 13 16 0 7.10 50.47 274.38 o 14 16 0 1266.46 1185.29 343.81 o 15 16 0 314.62 116.54 305.58 o 16 16 0 2798.30 2502.42 434.96 o 1 17 0 1738.90 1176.59 168.09 o 2 17 0 14793.04 13804.24 360.22 o 3 17 0 106.22 286.95 132.94 o 4 17 0 2.66 140.36 331.66 o 5 17 0 25.80 64.29 197.32 o 6 17 0 9269.85 9652.68 552.05 o 7 17 0 7345.77 7849.23 430.07 o 8 17 0 663.70 616.05 260.61 o 9 17 0 12477.44 12198.87 550.89 o 10 17 0 16321.05 17175.26 696.19 o 11 17 0 8.95 85.95 252.66 o 12 17 0 18.32 71.27 283.25 o 13 17 0 380.58 784.89 305.27 o 14 17 0 3403.53 3027.31 406.52 o 15 17 0 33.09 14.99 331.88 o 0 18 0 14884.88 15038.37 547.83 o 1 18 0 378.55 636.59 397.03 o 2 18 0 360.44 530.80 147.28 o 3 18 0 2.47 262.08 134.55 o 4 18 0 985.49 1103.71 229.87 o 5 18 0 782.06 1399.15 309.25 o 6 18 0 7.61 161.11 586.17 o 7 18 0 49.47 -134.27 154.38 o 8 18 0 14284.87 14596.07 599.53 o 9 18 0 0.49 390.61 272.54 o 10 18 0 47.93 210.14 245.32 o 11 18 0 1596.86 233.08 260.92 o 12 18 0 6538.40 7309.66 522.75 o 13 18 0 813.66 243.18 337.69 o 14 18 0 757.73 -268.26 324.85 o 1 19 0 42.16 354.38 184.63 o 2 19 0 11896.19 12214.97 703.07 o 3 19 0 102.38 151.60 199.74 o 4 19 0 6709.52 5946.44 253.59 o 5 19 0 47.75 12.05 194.69 o 6 19 0 1874.47 2205.54 250.06 o 7 19 0 49.50 752.48 692.21 o 8 19 0 824.86 342.28 284.78 o 9 19 0 70.58 -145.91 265.81 o 10 19 0 12636.33 12990.19 646.63 o 11 19 0 203.87 276.52 310.16 o 12 19 0 529.74 -282.63 282.63 o 13 19 0 1.51 -297.01 297.01 o 0 20 0 19569.47 19214.88 691.90 o 1 20 0 634.70 37.41 595.09 o 2 20 0 4528.13 4854.79 262.13 o 3 20 0 2688.22 1992.02 483.75 o 4 20 0 509.12 451.29 192.71 o 5 20 0 93.61 407.13 301.60 o 6 20 0 4.10 -15.32 171.54 o 7 20 0 3034.63 3082.85 355.89 o 8 20 0 942.42 1735.27 370.12 o 9 20 0 5382.79 5419.61 493.39 o 10 20 0 312.48 -288.75 288.75 o 11 20 0 1049.63 700.47 389.39 o 12 20 0 3814.46 4334.04 546.30 o 13 20 0 405.87 -156.92 396.12 o 1 21 0 3330.12 4487.16 857.69 o 2 21 0 3959.41 4476.14 258.12 o 3 21 0 115.74 559.25 187.35 o 4 21 0 2192.67 1876.72 205.91 o 5 21 0 1255.80 1673.20 391.83 o 6 21 0 1063.06 662.53 197.00 o 7 21 0 1931.20 1663.41 337.39 o 8 21 0 318.86 963.53 322.09 o 9 21 0 4583.99 6017.92 486.35 o 11 21 0 214.74 -290.59 290.59 o 0 22 0 2686.24 2982.65 333.72 o 1 22 0 2431.61 2923.19 826.03 o 2 22 0 2253.71 1946.26 767.30 o 3 22 0 1130.15 1340.25 587.45 o 4 22 0 161.84 812.46 535.45 o 5 22 0 1195.91 1107.61 345.03 o 6 22 0 524.70 602.05 237.11 o 7 22 0 2260.36 2637.98 262.12 o 8 22 0 2303.59 2377.92 370.73 o 9 22 0 2470.85 2110.58 368.59 o 10 22 0 871.47 2095.90 398.26 o 1 23 0 2319.13 2851.62 328.52 o 2 23 0 21.51 154.84 197.58 o 3 23 0 2057.56 1773.69 226.29 o 4 23 0 1444.18 1810.41 977.14 o 5 23 0 958.25 1471.30 702.15 o 6 23 0 1791.57 1681.28 426.40 o 7 23 0 943.79 360.72 527.95 o 8 23 0 151.59 213.81 323.01 o 9 23 0 1218.82 1589.36 373.18 o 0 24 0 278.35 370.73 322.71 o 1 24 0 2459.87 2686.85 282.58 o 2 24 0 449.19 848.68 1049.94 o 3 24 0 571.27 600.83 222.76 o 4 24 0 1222.47 1549.10 1227.50 o 5 24 0 1246.98 1230.75 234.38 o 6 24 0 952.96 1088.24 245.66 o 7 24 0 2213.68 2426.87 379.60 o 1 25 0 87.46 336.72 358.49 o 2 25 0 4151.88 3602.29 801.41 o 3 25 0 2903.49 4207.23 676.15 o 4 25 0 157.15 961.76 977.75 o 5 25 0 1384.92 2409.72 415.69 o -19 0 1 1275.77 1138.80 314.45 o -17 0 1 9984.08 8353.02 442.31 o -15 0 1 6186.96 6894.58 392.14 o -13 0 1 18671.40 18968.04 623.69 o -11 0 1 693.35 417.83 176.80 o -9 0 1 143.16 298.23 133.67 o -7 0 1 70807.88 66020.00 1716.30 o -5 0 1 44310.77 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