#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/20/2212063.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212063_Fobs loop_ _publ_author_name 'Rubin-Preminger, Janice M.' 'Englert, Ulli' _publ_section_title ; 3,4-Diaminopyridine ; _journal_coeditor_code BT2244 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o757 _journal_page_last o758 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.5815 _cell_length_b 7.3520 _cell_length_c 12.5790 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high .8142 _[local]_cod_data_source_file bt2244Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' diamin - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 89.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 327.22 315.64 7.58 o 4 0 0 .02 2.30 .96 o 6 0 0 47.17 44.96 7.10 o 1 1 0 2089.31 2090.44 28.49 o 2 1 0 .39 .56 .66 o 3 1 0 114.01 122.71 3.79 o 4 1 0 1.49 1.94 .70 o 5 1 0 1.48 1.25 2.02 o 6 1 0 5.53 6.80 2.79 o 0 2 0 7930.23 7757.69 131.99 o 1 2 0 4525.30 4434.62 64.25 o 2 2 0 48.52 45.43 2.11 o 3 2 0 26.80 31.48 2.12 o 4 2 0 13.93 17.93 1.66 o 5 2 0 1.69 3.79 1.51 o 6 2 0 10.57 9.74 2.47 o 1 3 0 161.04 140.85 3.77 o 2 3 0 68.32 81.37 3.07 o 3 3 0 34.64 39.75 2.66 o 4 3 0 11.59 12.87 1.54 o 5 3 0 .97 4.63 1.34 o 6 3 0 36.77 41.78 4.54 o 0 4 0 389.12 371.52 10.23 o 1 4 0 717.04 750.79 12.05 o 2 4 0 5.02 4.79 1.11 o 3 4 0 163.19 149.22 4.52 o 4 4 0 13.07 15.96 1.69 o 5 4 0 15.39 21.52 2.41 o 6 4 0 1.97 2.23 2.28 o 1 5 0 18.05 20.77 1.58 o 2 5 0 212.67 207.85 5.02 o 3 5 0 48.34 52.22 3.09 o 4 5 0 4.40 7.13 1.21 o 5 5 0 14.07 11.41 1.69 o 0 6 0 578.48 592.97 14.92 o 1 6 0 2.83 2.87 .62 o 2 6 0 .90 1.90 .68 o 3 6 0 218.27 211.03 5.93 o 4 6 0 21.07 20.12 1.86 o 5 6 0 21.33 27.93 2.67 o 1 7 0 16.71 18.33 2.99 o 2 7 0 54.79 55.58 4.93 o 3 7 0 136.38 122.18 7.07 o 4 7 0 10.77 8.11 3.62 o 0 8 0 141.38 110.17 10.20 o 1 8 0 31.68 38.79 4.41 o 2 8 0 .12 -.68 1.59 o 3 8 0 80.98 85.40 6.18 o 1 0 1 145.68 137.50 1.99 o 2 0 1 344.59 323.62 6.08 o 3 0 1 500.64 536.67 12.07 o 4 0 1 19.90 22.32 1.88 o 5 0 1 158.87 160.86 8.35 o 6 0 1 5.64 9.34 4.69 o 0 1 1 48.79 49.23 1.16 o 1 1 1 1979.34 1997.16 16.84 o 2 1 1 466.52 481.32 5.43 o 3 1 1 21.37 19.96 1.15 o 4 1 1 7.35 10.11 .88 o 5 1 1 51.46 55.57 2.94 o 6 1 1 65.73 66.55 4.26 o 0 2 1 51.23 53.42 2.00 o 1 2 1 2382.26 2433.02 24.48 o 2 2 1 251.75 267.00 3.87 o 3 2 1 155.50 154.55 3.04 o 4 2 1 66.89 71.16 2.18 o 5 2 1 27.38 31.68 2.56 o 6 2 1 81.31 87.49 4.89 o 0 3 1 40.80 40.85 1.79 o 1 3 1 553.45 539.59 6.39 o 2 3 1 747.62 763.57 9.23 o 3 3 1 3.33 4.46 .82 o 4 3 1 48.09 50.63 2.08 o 5 3 1 3.86 6.58 1.26 o 6 3 1 2.30 .52 1.31 o 0 4 1 147.90 150.41 5.92 o 1 4 1 758.95 786.83 9.15 o 2 4 1 527.28 510.77 6.88 o 3 4 1 14.20 16.99 1.33 o 4 4 1 5.91 7.33 .95 o 5 4 1 20.87 24.05 2.08 o 6 4 1 55.87 57.49 3.70 o 0 5 1 1.41 2.96 .68 o 1 5 1 10.55 11.71 .83 o 2 5 1 410.65 408.53 5.83 o 3 5 1 125.73 121.41 3.23 o 4 5 1 17.33 17.73 1.21 o 5 5 1 37.20 35.98 2.53 o 0 6 1 51.61 53.67 4.05 o 1 6 1 90.78 87.16 2.47 o 2 6 1 118.10 118.89 3.00 o 3 6 1 28.55 29.42 1.66 o 4 6 1 50.12 47.61 2.49 o 5 6 1 9.90 13.11 2.41 o 0 7 1 .63 .86 1.23 o 1 7 1 65.06 66.19 3.17 o 2 7 1 34.55 36.02 2.26 o 3 7 1 117.65 113.27 4.84 o 4 7 1 40.52 40.16 3.20 o 0 8 1 2.67 2.04 2.97 o 1 8 1 31.27 30.93 2.71 o 2 8 1 3.51 5.84 1.40 o 3 8 1 2.22 1.07 1.21 o 0 9 1 .56 .05 2.20 o 0 0 2 443.61 446.58 7.56 o 1 0 2 169.71 155.03 3.54 o 2 0 2 1040.78 1045.13 17.76 o 3 0 2 4.83 6.12 .99 o 4 0 2 24.21 26.30 2.75 o 5 0 2 311.36 307.69 9.39 o 6 0 2 30.69 35.83 4.44 o 0 1 2 959.62 926.15 12.99 o 1 1 2 408.54 381.41 3.81 o 2 1 2 157.75 169.84 2.51 o 3 1 2 430.93 443.94 8.48 o 4 1 2 145.46 152.19 3.60 o 5 1 2 13.67 14.53 1.46 o 6 1 2 76.03 73.00 4.48 o 0 2 2 403.19 416.44 8.65 o 1 2 2 320.22 290.39 3.33 o 2 2 2 296.84 314.81 4.21 o 3 2 2 110.12 104.08 2.67 o 4 2 2 47.10 51.24 1.77 o 5 2 2 217.15 205.48 4.91 o 6 2 2 11.62 17.25 2.13 o 0 3 2 114.66 107.67 2.11 o 1 3 2 474.08 475.92 5.77 o 2 3 2 371.24 363.12 4.98 o 3 3 2 17.26 18.13 1.14 o 4 3 2 228.64 213.95 4.10 o 5 3 2 42.66 37.41 2.19 o 6 3 2 96.75 91.51 4.98 o 0 4 2 80.21 78.80 2.53 o 1 4 2 19.28 21.07 1.07 o 2 4 2 222.73 211.18 3.51 o 3 4 2 48.73 47.38 1.86 o 4 4 2 31.29 33.50 1.56 o 5 4 2 32.32 35.09 2.18 o 6 4 2 11.86 12.03 1.60 o 0 5 2 135.27 135.01 3.48 o 1 5 2 27.53 32.10 1.26 o 2 5 2 34.74 40.13 1.66 o 3 5 2 127.32 124.67 3.02 o 4 5 2 46.96 50.18 2.13 o 5 5 2 40.01 39.25 2.40 o 0 6 2 20.04 21.20 2.23 o 1 6 2 11.57 15.65 1.39 o 2 6 2 148.33 147.91 3.84 o 3 6 2 28.16 26.22 1.83 o 4 6 2 26.29 25.48 1.98 o 5 6 2 17.81 17.66 2.28 o 0 7 2 10.39 15.13 2.31 o 1 7 2 19.85 22.37 1.66 o 2 7 2 3.67 6.02 1.05 o 3 7 2 21.30 22.74 1.85 o 4 7 2 28.31 29.54 3.42 o 0 8 2 45.92 44.63 4.64 o 1 8 2 6.09 6.23 1.47 o 2 8 2 52.86 48.81 3.38 o 3 8 2 98.04 91.37 4.54 o 1 0 3 471.45 457.89 6.58 o 2 0 3 36.13 49.22 2.77 o 3 0 3 23.24 23.33 2.65 o 4 0 3 .70 4.31 1.43 o 5 0 3 47.07 44.29 4.14 o 6 0 3 129.49 126.53 8.89 o 0 1 3 92.45 86.22 1.81 o 1 1 3 55.36 50.62 1.17 o 2 1 3 36.49 38.14 .87 o 3 1 3 119.49 118.10 2.12 o 4 1 3 217.17 201.60 4.54 o 5 1 3 205.23 200.34 5.20 o 6 1 3 167.61 158.19 6.54 o 0 2 3 .05 .34 .93 o 1 2 3 269.59 273.58 3.57 o 2 2 3 81.13 85.32 1.84 o 3 2 3 13.80 13.94 .95 o 4 2 3 361.24 333.20 6.10 o 5 2 3 15.66 17.20 1.64 o 6 2 3 35.56 40.53 3.20 o 0 3 3 11.92 11.53 1.67 o 1 3 3 67.84 59.36 1.19 o 2 3 3 40.08 42.69 1.56 o 3 3 3 218.33 210.79 3.65 o 4 3 3 161.64 165.78 3.89 o 5 3 3 3.57 3.02 .90 o 6 3 3 78.15 79.19 4.57 o 0 4 3 19.96 25.10 2.66 o 1 4 3 67.43 74.20 1.71 o 2 4 3 22.15 25.86 1.31 o 3 4 3 133.07 126.96 2.80 o 4 4 3 295.54 280.42 5.51 o 5 4 3 93.73 89.62 3.86 o 6 4 3 19.51 25.97 3.17 o 0 5 3 42.95 42.15 1.98 o 1 5 3 27.96 27.77 1.54 o 2 5 3 16.68 18.90 1.06 o 3 5 3 163.57 159.26 4.23 o 4 5 3 1.31 2.11 .91 o 5 5 3 81.81 79.27 3.98 o 0 6 3 11.17 17.61 2.19 o 1 6 3 10.06 10.93 1.32 o 2 6 3 27.54 29.04 2.02 o 3 6 3 172.05 169.80 4.45 o 4 6 3 17.18 16.07 1.63 o 0 7 3 6.29 8.04 1.68 o 1 7 3 21.80 24.07 1.69 o 2 7 3 53.26 51.37 2.51 o 3 7 3 111.28 104.42 3.65 o 4 7 3 55.87 52.47 3.38 o 0 8 3 3.60 7.06 2.23 o 1 8 3 42.18 42.00 3.17 o 2 8 3 46.39 48.78 3.36 o 0 0 4 173.90 150.95 5.19 o 1 0 4 552.06 578.38 8.79 o 2 0 4 111.49 121.32 4.16 o 3 0 4 297.28 325.30 9.55 o 4 0 4 .22 2.36 1.98 o 5 0 4 201.19 195.61 7.42 o 6 0 4 7.03 9.26 2.52 o 0 1 4 1187.55 1120.09 16.14 o 1 1 4 182.77 190.26 2.61 o 2 1 4 309.45 328.64 3.96 o 3 1 4 96.34 103.32 2.62 o 4 1 4 64.80 72.82 3.37 o 5 1 4 55.74 53.99 3.00 o 6 1 4 .97 1.72 1.37 o 0 2 4 50.89 63.89 1.48 o 1 2 4 354.61 346.77 4.59 o 2 2 4 134.28 135.27 2.46 o 3 2 4 31.21 37.62 1.26 o 4 2 4 11.36 13.04 1.42 o 5 2 4 104.88 100.57 3.91 o 6 2 4 51.90 46.79 4.74 o 0 3 4 63.95 68.55 3.48 o 1 3 4 156.31 170.12 2.53 o 2 3 4 5.86 7.80 .69 o 3 3 4 133.09 126.33 2.59 o 4 3 4 149.71 150.12 4.30 o 5 3 4 32.96 27.09 2.28 o 6 3 4 3.77 7.85 1.37 o 0 4 4 369.27 336.39 17.52 o 1 4 4 109.72 104.49 2.29 o 2 4 4 33.41 34.36 1.38 o 3 4 4 86.43 80.91 2.23 o 4 4 4 24.97 21.30 1.63 o 5 4 4 11.52 9.65 1.26 o 0 5 4 3.92 5.01 1.47 o 1 5 4 39.33 38.43 2.17 o 2 5 4 6.63 6.62 1.07 o 3 5 4 129.20 129.53 3.48 o 4 5 4 94.20 86.94 4.23 o 5 5 4 13.77 15.88 1.83 o 0 6 4 87.93 86.01 4.50 o 1 6 4 13.52 12.85 1.59 o 2 6 4 248.92 249.30 6.38 o 3 6 4 44.77 40.90 2.28 o 4 6 4 25.90 23.32 3.01 o 0 7 4 4.02 4.25 1.93 o 1 7 4 2.72 3.37 1.03 o 2 7 4 11.96 16.29 1.39 o 3 7 4 29.26 31.48 1.95 o 0 8 4 18.90 25.91 2.95 o 1 8 4 47.00 52.55 3.03 o 2 8 4 80.94 90.70 4.00 o 1 0 5 .20 .79 .86 o 2 0 5 831.64 891.81 14.45 o 3 0 5 1.25 1.11 1.30 o 4 0 5 .75 .54 1.32 o 5 0 5 2.33 3.94 1.56 o 6 0 5 1.83 4.45 2.42 o 0 1 5 236.98 238.85 4.92 o 1 1 5 534.25 556.63 6.81 o 2 1 5 211.74 222.40 3.10 o 3 1 5 211.28 204.94 4.41 o 4 1 5 17.02 18.98 1.73 o 5 1 5 1.56 4.74 1.12 o 6 1 5 8.73 10.70 1.78 o 0 2 5 596.79 625.21 9.20 o 1 2 5 245.85 248.82 3.70 o 2 2 5 134.03 139.03 2.65 o 3 2 5 56.64 57.65 1.90 o 4 2 5 26.72 30.94 2.12 o 5 2 5 3.33 4.54 1.24 o 6 2 5 5.18 9.42 1.63 o 0 3 5 57.21 49.14 3.84 o 1 3 5 1.58 .83 .23 o 2 3 5 16.85 23.64 1.15 o 3 3 5 8.98 8.77 .65 o 4 3 5 12.73 12.71 1.37 o 5 3 5 10.94 12.02 1.38 o 6 3 5 1.86 2.96 2.39 o 0 4 5 12.59 14.83 2.10 o 1 4 5 383.45 385.72 6.36 o 2 4 5 59.10 59.62 1.70 o 3 4 5 4.40 5.23 .68 o 4 4 5 20.60 24.24 1.66 o 5 4 5 13.47 14.28 1.39 o 0 5 5 158.59 140.63 5.68 o 1 5 5 36.16 39.84 2.37 o 2 5 5 36.62 35.59 2.17 o 3 5 5 34.05 38.54 2.12 o 4 5 5 10.46 10.34 1.66 o 5 5 5 3.39 5.73 1.37 o 0 6 5 90.05 91.23 4.86 o 1 6 5 186.07 187.14 4.70 o 2 6 5 135.52 133.63 4.22 o 3 6 5 .22 1.77 1.29 o 4 6 5 6.02 4.31 1.53 o 0 7 5 157.98 147.71 6.16 o 1 7 5 37.10 41.04 2.49 o 2 7 5 78.59 78.41 3.53 o 3 7 5 9.72 17.55 2.02 o 0 8 5 76.41 73.61 5.35 o 1 8 5 106.38 112.08 4.61 o 2 8 5 81.58 77.34 3.94 o 0 0 6 398.26 404.34 11.74 o 1 0 6 123.19 119.49 3.65 o 2 0 6 36.05 33.85 1.60 o 3 0 6 49.73 43.72 3.87 o 4 0 6 2.79 3.29 1.60 o 5 0 6 2.58 5.71 1.72 o 6 0 6 17.04 16.31 2.44 o 0 1 6 110.41 111.90 3.23 o 1 1 6 57.59 59.03 1.72 o 2 1 6 205.00 202.51 3.59 o 3 1 6 64.81 66.38 2.78 o 4 1 6 135.10 139.12 4.62 o 5 1 6 65.15 59.84 3.31 o 6 1 6 9.55 12.53 1.62 o 0 2 6 293.21 281.07 6.16 o 1 2 6 78.40 86.67 2.87 o 2 2 6 13.97 14.44 .94 o 3 2 6 148.13 141.82 3.75 o 4 2 6 13.85 11.16 1.43 o 5 2 6 2.32 2.66 1.16 o 6 2 6 1.30 2.88 1.36 o 0 3 6 536.83 580.00 10.36 o 1 3 6 160.05 156.71 3.06 o 2 3 6 410.49 400.85 5.73 o 3 3 6 103.11 102.35 2.76 o 4 3 6 .11 1.69 .83 o 5 3 6 35.51 41.06 2.49 o 0 4 6 62.70 61.48 4.00 o 1 4 6 11.72 13.39 1.44 o 2 4 6 50.72 53.69 2.16 o 3 4 6 103.40 102.49 3.47 o 4 4 6 19.68 20.89 2.08 o 5 4 6 2.01 3.86 1.40 o 0 5 6 181.09 176.48 6.46 o 1 5 6 219.42 212.02 4.85 o 2 5 6 67.94 66.38 2.94 o 3 5 6 42.78 45.48 2.88 o 4 5 6 27.67 28.96 2.88 o 5 5 6 4.08 1.35 2.03 o 0 6 6 4.76 4.55 1.70 o 1 6 6 19.19 23.61 2.01 o 2 6 6 58.41 64.42 3.06 o 3 6 6 3.37 5.93 1.28 o 4 6 6 2.05 .58 1.57 o 0 7 6 35.33 41.16 3.48 o 1 7 6 144.06 147.29 4.78 o 2 7 6 .77 3.01 .97 o 3 7 6 8.67 8.58 1.99 o 0 8 6 32.26 32.10 3.39 o 1 8 6 57.93 61.67 3.55 o 1 0 7 472.60 486.95 10.03 o 2 0 7 27.14 28.80 2.06 o 3 0 7 111.91 110.69 5.32 o 4 0 7 262.07 256.28 12.61 o 5 0 7 12.04 14.48 2.43 o 6 0 7 1.32 3.81 1.57 o 0 1 7 24.76 28.42 2.16 o 1 1 7 88.56 82.64 2.37 o 2 1 7 18.09 23.00 1.32 o 3 1 7 141.18 139.53 3.89 o 4 1 7 36.57 37.31 2.56 o 5 1 7 25.29 27.65 2.32 o 6 1 7 21.59 22.80 2.16 o 0 2 7 223.17 219.61 5.43 o 1 2 7 97.24 103.92 3.86 o 2 2 7 246.59 235.72 3.91 o 3 2 7 336.55 316.68 6.47 o 4 2 7 96.01 99.15 3.77 o 5 2 7 14.19 15.48 1.62 o 0 3 7 15.34 21.11 1.80 o 1 3 7 4.10 2.77 .56 o 2 3 7 88.22 86.54 2.10 o 3 3 7 94.24 90.30 3.33 o 4 3 7 45.22 46.97 2.68 o 5 3 7 113.62 109.76 4.10 o 0 4 7 19.88 19.64 2.61 o 1 4 7 48.97 45.07 2.51 o 2 4 7 240.84 226.14 4.87 o 3 4 7 230.44 212.37 6.71 o 4 4 7 .78 .92 1.34 o 5 4 7 .38 1.64 1.43 o 0 5 7 16.11 17.20 2.72 o 1 5 7 66.39 68.86 3.28 o 2 5 7 71.30 69.31 3.04 o 3 5 7 .69 4.54 1.50 o 4 5 7 3.84 3.41 1.48 o 0 6 7 6.30 6.28 2.10 o 1 6 7 31.51 37.89 2.48 o 2 6 7 49.19 49.32 2.65 o 3 6 7 44.10 41.07 4.11 o 4 6 7 33.46 42.33 3.36 o 0 7 7 118.34 117.36 6.53 o 1 7 7 70.37 69.20 3.44 o 2 7 7 4.66 5.70 1.23 o 3 7 7 23.73 23.12 2.99 o 0 8 7 .16 2.95 1.62 o 0 0 8 .75 -.76 1.56 o 1 0 8 .90 .53 .97 o 2 0 8 12.48 12.02 1.52 o 3 0 8 88.33 88.62 5.11 o 4 0 8 714.03 683.45 16.78 o 5 0 8 .35 1.19 1.90 o 0 1 8 1.33 .13 .91 o 1 1 8 73.16 76.77 2.30 o 2 1 8 2.26 2.08 .68 o 3 1 8 44.41 46.40 2.66 o 4 1 8 65.84 71.55 3.55 o 5 1 8 132.55 126.02 5.49 o 0 2 8 10.36 13.80 1.35 o 1 2 8 5.94 7.41 .75 o 2 2 8 11.57 15.41 .96 o 3 2 8 126.50 123.55 3.75 o 4 2 8 184.56 173.97 4.87 o 5 2 8 199.37 201.64 6.23 o 0 3 8 6.91 5.67 1.77 o 1 3 8 22.77 24.00 1.44 o 2 3 8 78.33 84.81 2.53 o 3 3 8 10.72 12.08 1.29 o 4 3 8 11.23 14.37 1.86 o 5 3 8 40.41 44.70 3.29 o 0 4 8 7.99 7.85 1.81 o 1 4 8 40.45 40.89 2.52 o 2 4 8 1.69 1.68 1.01 o 3 4 8 34.16 36.99 3.19 o 4 4 8 77.98 74.34 4.70 o 5 4 8 67.50 75.73 4.75 o 0 5 8 3.88 2.33 1.85 o 1 5 8 31.01 35.38 2.49 o 2 5 8 143.87 143.55 4.97 o 3 5 8 23.79 29.90 2.83 o 4 5 8 17.87 18.04 2.23 o 0 6 8 28.52 29.46 3.41 o 1 6 8 58.88 56.60 3.12 o 2 6 8 7.97 9.02 1.44 o 3 6 8 16.67 15.64 2.16 o 0 7 8 .58 1.20 1.56 o 1 7 8 56.32 55.17 3.14 o 2 7 8 24.41 24.92 2.09 o 1 0 9 577.98 552.09 20.03 o 2 0 9 22.68 25.18 2.10 o 3 0 9 1.23 2.92 1.56 o 4 0 9 71.01 69.59 5.02 o 5 0 9 .93 2.68 1.74 o 0 1 9 49.25 47.38 3.24 o 1 1 9 55.24 55.46 2.25 o 2 1 9 215.76 218.86 4.32 o 3 1 9 61.29 60.64 3.11 o 4 1 9 20.38 29.03 2.40 o 5 1 9 13.69 12.93 1.60 o 0 2 9 156.67 157.98 4.70 o 1 2 9 117.60 118.87 2.76 o 2 2 9 107.59 102.37 2.76 o 3 2 9 184.43 173.81 5.26 o 4 2 9 30.36 29.43 2.10 o 5 2 9 30.96 32.66 2.30 o 0 3 9 195.98 190.21 6.63 o 1 3 9 18.08 21.09 1.73 o 2 3 9 89.33 87.61 3.18 o 3 3 9 20.81 25.59 2.27 o 4 3 9 5.31 6.63 1.68 o 5 3 9 21.85 21.14 2.45 o 0 4 9 5.01 5.58 2.45 o 1 4 9 40.07 38.07 2.48 o 2 4 9 70.11 67.80 3.19 o 3 4 9 199.55 166.21 6.59 o 4 4 9 71.44 64.00 4.35 o 0 5 9 90.50 92.08 5.60 o 1 5 9 24.31 24.99 2.06 o 2 5 9 13.58 14.21 1.68 o 3 5 9 36.50 39.51 3.36 o 4 5 9 25.67 24.01 2.63 o 0 6 9 42.92 43.21 4.03 o 1 6 9 24.22 26.76 2.10 o 2 6 9 10.10 8.15 1.45 o 3 6 9 38.36 36.93 3.29 o 0 7 9 .71 1.60 1.83 o 1 7 9 17.04 17.12 1.68 o 0 0 10 18.18 24.45 3.56 o 1 0 10 103.66 104.40 4.65 o 2 0 10 488.01 455.47 11.95 o 3 0 10 2.66 3.76 1.69 o 4 0 10 .16 4.08 1.52 o 5 0 10 .00 -1.24 2.46 o 0 1 10 185.58 189.23 5.73 o 1 1 10 308.29 304.11 5.54 o 2 1 10 80.58 82.68 3.37 o 3 1 10 27.86 28.01 2.15 o 4 1 10 30.62 26.95 2.12 o 5 1 10 39.33 39.37 2.60 o 0 2 10 26.27 34.40 2.75 o 1 2 10 147.02 147.27 3.61 o 2 2 10 221.88 215.90 5.17 o 3 2 10 68.23 72.84 3.43 o 4 2 10 2.80 4.56 1.07 o 5 2 10 .10 3.29 4.09 o 0 3 10 152.25 160.98 6.47 o 1 3 10 .28 -.15 .93 o 2 3 10 130.56 123.14 5.58 o 3 3 10 93.37 89.79 5.00 o 4 3 10 9.32 8.49 1.81 o 0 4 10 14.64 16.40 2.67 o 1 4 10 173.70 157.40 4.70 o 2 4 10 8.34 7.12 1.76 o 3 4 10 56.83 55.42 4.06 o 4 4 10 5.15 4.34 2.17 o 0 5 10 5.76 8.84 2.03 o 1 5 10 84.99 87.43 3.89 o 2 5 10 .48 4.50 1.69 o 3 5 10 47.15 44.04 3.64 o 0 6 10 3.27 5.87 1.80 o 1 6 10 74.65 69.53 3.39 o 2 6 10 86.09 79.27 5.04 o 1 0 11 29.28 32.03 2.78 o 2 0 11 3.76 3.48 1.92 o 3 0 11 13.27 14.83 2.64 o 4 0 11 7.41 7.97 1.85 o 0 1 11 250.77 238.53 6.84 o 1 1 11 294.58 291.01 6.58 o 2 1 11 31.71 37.93 2.34 o 3 1 11 24.68 24.15 1.95 o 4 1 11 3.34 5.55 1.86 o 0 2 11 289.56 281.69 9.94 o 1 2 11 46.57 48.70 2.45 o 2 2 11 18.21 20.62 1.90 o 3 2 11 26.88 28.42 2.64 o 4 2 11 3.17 3.49 1.61 o 0 3 11 703.89 697.86 16.73 o 1 3 11 47.45 44.81 2.69 o 2 3 11 39.90 40.45 3.33 o 3 3 11 46.21 44.32 3.47 o 4 3 11 2.35 3.21 1.45 o 0 4 11 184.31 174.39 8.18 o 1 4 11 81.21 85.78 3.53 o 2 4 11 23.87 25.44 2.72 o 3 4 11 34.13 29.40 2.91 o 0 5 11 152.43 145.48 6.92 o 1 5 11 105.24 99.28 4.55 o 2 5 11 14.40 12.98 2.22 o 0 6 11 9.42 10.73 2.67 o 1 6 11 24.92 27.12 2.26 o 0 0 12 5.46 3.78 2.04 o 1 0 12 166.64 161.21 5.71 o 2 0 12 17.49 16.84 2.70 o 3 0 12 .03 1.86 1.44 o 4 0 12 2.36 8.71 2.40 o 0 1 12 17.79 27.14 2.42 o 1 1 12 47.77 52.82 2.35 o 2 1 12 75.86 79.91 3.16 o 3 1 12 12.65 9.03 1.40 o 4 1 12 4.02 4.15 1.27 o 0 2 12 .01 3.15 2.45 o 1 2 12 39.93 39.02 2.75 o 2 2 12 48.89 46.17 3.83 o 3 2 12 21.19 19.77 2.58 o 4 2 12 6.10 4.62 1.59 o 0 3 12 1.89 .80 2.41 o 1 3 12 23.31 21.84 2.02 o 2 3 12 13.76 15.11 2.13 o 3 3 12 19.82 19.67 2.56 o 0 4 12 4.43 9.15 2.13 o 1 4 12 43.65 48.31 2.97 o 2 4 12 .76 2.70 1.52 o 3 4 12 48.53 48.85 3.75 o 0 5 12 1.39 2.36 1.58 o 1 5 12 41.52 44.74 2.81 o 2 5 12 6.47 4.03 1.66 o 1 0 13 2.47 .91 1.37 o 2 0 13 116.32 120.50 6.09 o 3 0 13 19.10 22.40 2.39 o 0 1 13 4.69 3.88 1.73 o 1 1 13 37.03 35.73 2.65 o 2 1 13 13.00 15.29 1.64 o 3 1 13 .10 2.27 1.33 o 0 2 13 18.34 20.22 3.00 o 1 2 13 2.56 2.03 1.52 o 2 2 13 40.63 42.97 3.78 o 3 2 13 28.26 27.03 2.84 o 0 3 13 .25 3.84 1.68 o 1 3 13 7.05 6.51 1.83 o 2 3 13 21.34 24.93 2.67 o 0 4 13 15.52 13.14 2.19 o 1 4 13 .39 3.61 1.55 o 2 4 13 11.04 14.31 2.30 o 0 0 14 .12 .65 1.74 o 1 0 14 14.42 18.09 2.31 o 2 0 14 1.87 1.92 1.41 o 0 1 14 13.28 17.83 3.01 o 1 1 14 8.40 10.11 1.86 o 2 1 14 9.52 14.74 1.89 o 0 2 14 4.37 8.31 4.15 o 1 2 14 20.33 25.53 2.85 o 2 2 14 3.69 4.70 1.59 o 0 3 14 3.47 1.86 1.92 o 1 3 14 2.63 3.91 2.17 o 1 0 15 .06 3.16 2.22 o 0 1 15 12.01 13.56 3.04 o 1 1 15 12.78 16.50 2.07 o 0 2 15 17.13 13.25 2.85 o