#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:24:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181040 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/20/2212068.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212068_Fobs loop_ _publ_author_name 'Kolev, T.' 'Spiteller, M.' 'van Almsick, T.' 'Mayer-Figge, H.' 'Sheldrick, W. S.' _publ_section_title ; Benzamidinium dihydrogenphosphate ; _journal_coeditor_code BT2254 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1016 _journal_page_last o1018 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.280 _cell_angle_gamma 90.000 _cell_length_a 12.2590 _cell_length_b 10.0669 _cell_length_c 8.0578 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8413 _cod_data_source_file bt2254Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 22-132 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4853.92 4770.12 44.20 o 3 0 0 8030.45 7328.33 394.50 o 4 0 0 1838.35 1728.43 213.67 o 5 0 0 2883.62 2956.36 313.78 o 6 0 0 110.15 154.94 23.63 o 7 0 0 661.66 748.96 127.15 o 8 0 0 238.86 238.33 49.49 o 9 0 0 18.45 8.74 18.90 o 10 0 0 343.73 341.28 42.55 o 11 0 0 225.84 234.83 17.99 o 12 0 0 63.14 70.81 9.44 o 13 0 0 108.53 112.02 15.69 o 14 0 0 74.32 76.39 11.08 o 1 1 0 240.52 328.81 5.82 o 2 1 0 6078.53 6269.11 39.46 o 3 1 0 2789.83 2629.12 42.57 o 4 1 0 416.15 402.09 34.62 o 5 1 0 157.91 154.32 13.88 o 6 1 0 725.91 750.29 57.60 o 7 1 0 0.69 4.69 7.41 o 8 1 0 0.96 0.00 7.18 o 9 1 0 246.59 236.03 11.23 o 10 1 0 256.90 272.02 11.57 o 11 1 0 87.18 72.31 9.12 o 12 1 0 207.58 272.68 15.17 o 13 1 0 0.68 5.52 9.19 o 14 1 0 0.22 21.24 9.31 o 0 2 0 22883.75 23722.26 87.05 o 1 2 0 511.57 552.37 9.75 o 2 2 0 1795.24 1787.38 26.38 o 3 2 0 1990.35 1843.71 44.18 o 4 2 0 21.80 15.64 5.11 o 5 2 0 328.63 370.18 35.35 o 6 2 0 100.63 90.23 14.23 o 7 2 0 209.00 214.24 17.11 o 8 2 0 98.14 101.57 20.32 o 9 2 0 432.13 406.99 12.68 o 10 2 0 3.83 6.13 8.64 o 11 2 0 427.57 432.95 38.38 o 12 2 0 46.68 45.00 12.08 o 13 2 0 20.58 38.99 9.72 o 14 2 0 26.33 18.49 10.71 o 1 3 0 1060.37 1004.79 18.13 o 2 3 0 424.38 553.74 11.60 o 3 3 0 264.88 302.49 8.50 o 4 3 0 491.92 582.49 44.78 o 5 3 0 33.86 36.87 6.00 o 6 3 0 79.50 58.71 6.93 o 7 3 0 130.01 131.84 15.65 o 8 3 0 154.94 149.80 9.48 o 9 3 0 600.45 597.94 15.83 o 10 3 0 26.70 28.97 20.15 o 11 3 0 0.77 11.92 8.41 o 12 3 0 59.44 55.84 10.22 o 13 3 0 21.62 22.82 10.01 o 14 3 0 0.03 0.00 9.98 o 0 4 0 2959.54 3506.84 65.53 o 1 4 0 641.37 758.25 14.01 o 2 4 0 357.81 397.34 9.85 o 3 4 0 9.34 11.36 5.74 o 4 4 0 2071.23 2228.42 204.71 o 5 4 0 126.35 130.98 20.62 o 6 4 0 328.56 286.88 19.21 o 7 4 0 178.45 168.80 21.95 o 8 4 0 4.32 0.00 8.34 o 9 4 0 1438.43 1307.73 105.55 o 10 4 0 189.33 190.89 10.74 o 11 4 0 255.58 229.49 12.05 o 12 4 0 6.25 0.00 9.47 o 13 4 0 5.06 0.00 10.74 o 1 5 0 0.56 0.43 6.15 o 2 5 0 656.46 758.55 16.07 o 3 5 0 219.01 306.95 14.65 o 4 5 0 882.26 981.48 61.70 o 5 5 0 19.99 13.54 7.68 o 6 5 0 83.94 83.61 10.91 o 7 5 0 0.01 4.09 8.44 o 8 5 0 3.87 0.00 8.84 o 9 5 0 116.69 114.73 10.52 o 10 5 0 30.64 27.26 9.49 o 11 5 0 0.96 0.00 14.81 o 12 5 0 1.31 17.18 9.35 o 13 5 0 1.69 26.55 9.65 o 0 6 0 34.24 37.39 10.50 o 1 6 0 247.31 247.76 9.56 o 2 6 0 325.06 361.98 16.35 o 3 6 0 130.30 128.84 9.12 o 4 6 0 467.53 437.02 27.96 o 5 6 0 1.38 0.00 8.82 o 6 6 0 11.04 10.82 9.62 o 7 6 0 154.42 133.60 18.72 o 8 6 0 64.09 70.31 9.69 o 9 6 0 86.40 82.88 10.00 o 10 6 0 43.77 40.94 16.02 o 11 6 0 22.39 31.97 9.77 o 12 6 0 12.17 8.17 16.38 o 1 7 0 252.16 259.76 11.28 o 2 7 0 268.01 291.84 20.40 o 3 7 0 42.22 35.09 8.71 o 4 7 0 157.83 162.27 10.70 o 5 7 0 292.20 296.13 25.76 o 6 7 0 0.10 8.80 10.21 o 7 7 0 193.63 159.43 10.81 o 8 7 0 118.92 99.60 13.37 o 9 7 0 32.27 25.56 14.25 o 10 7 0 113.02 125.74 11.34 o 11 7 0 45.73 24.90 16.53 o 0 8 0 228.35 194.13 16.22 o 1 8 0 0.03 2.97 9.12 o 2 8 0 51.82 62.28 9.48 o 3 8 0 195.87 206.40 27.96 o 4 8 0 3.08 0.00 9.51 o 5 8 0 418.19 400.34 40.94 o 6 8 0 227.79 192.48 13.52 o 7 8 0 49.89 46.26 11.63 o 8 8 0 217.84 165.97 12.74 o 9 8 0 111.21 87.04 11.63 o 10 8 0 1.85 0.00 10.54 o 1 9 0 900.41 843.32 20.63 o 2 9 0 856.40 886.75 21.08 o 3 9 0 57.96 34.14 15.31 o 4 9 0 100.61 104.72 10.93 o 5 9 0 275.78 253.82 19.13 o 6 9 0 0.04 0.00 9.66 o 7 9 0 91.25 88.69 17.31 o 8 9 0 10.32 0.47 10.38 o 9 9 0 58.88 43.83 16.62 o 0 10 0 97.65 115.68 15.84 o 1 10 0 17.36 15.40 11.73 o 2 10 0 36.85 23.63 10.91 o 3 10 0 280.71 262.09 13.32 o 4 10 0 0.18 15.37 9.58 o 5 10 0 257.72 256.81 58.88 o 6 10 0 108.70 94.53 11.75 o 7 10 0 31.96 17.73 10.73 o 8 10 0 117.20 102.84 12.64 o 1 11 0 541.36 478.96 16.79 o 2 11 0 476.27 400.00 15.54 o 3 11 0 0.54 0.00 10.69 o 4 11 0 172.15 171.53 12.86 o 5 11 0 45.79 32.40 11.30 o -14 1 1 1.48 0.00 13.71 o -13 1 1 6.49 38.95 12.17 o -12 1 1 3.20 15.98 12.03 o -11 1 1 0.00 7.17 11.80 o -10 1 1 0.03 0.00 12.06 o -9 1 1 46.03 30.74 12.03 o -8 1 1 16.87 12.81 10.57 o -7 1 1 46.29 34.62 9.56 o -6 1 1 30.34 39.89 8.33 o -5 1 1 312.88 338.63 12.11 o -4 1 1 185.96 209.37 9.83 o -3 1 1 3.33 0.00 6.39 o -2 1 1 144.04 126.35 6.69 o -1 1 1 474.68 470.19 10.57 o 0 1 1 1595.96 1682.18 28.94 o 1 1 1 0.03 0.00 3.70 o 2 1 1 761.65 829.60 18.09 o 3 1 1 4293.95 4042.52 58.40 o 4 1 1 170.86 180.28 9.42 o 5 1 1 345.08 297.91 11.67 o 6 1 1 483.77 415.59 14.73 o 7 1 1 6.59 9.19 9.30 o 8 1 1 2.18 0.00 10.64 o 9 1 1 39.05 34.21 12.10 o 10 1 1 11.98 17.74 12.06 o 11 1 1 0.83 0.00 12.14 o 12 1 1 13.48 2.54 13.03 o 13 1 1 40.79 54.45 13.86 o 14 1 1 4.33 1.87 13.41 o -14 2 1 28.57 20.73 14.42 o -13 2 1 83.77 119.19 15.24 o -12 2 1 86.59 89.38 14.38 o -11 2 1 6.56 10.94 11.61 o -10 2 1 6.25 2.46 11.80 o -9 2 1 193.46 191.99 15.06 o -8 2 1 113.24 112.10 12.22 o -7 2 1 29.55 27.30 9.82 o -6 2 1 129.65 118.28 9.86 o -5 2 1 38.71 54.27 7.88 o -4 2 1 7.36 16.92 7.10 o -3 2 1 69.36 68.10 8.07 o -2 2 1 17.34 7.28 6.72 o -1 2 1 239.79 228.35 9.46 o 0 2 1 17.71 11.91 5.75 o 1 2 1 3812.01 4373.16 57.85 o 2 2 1 380.54 526.57 14.67 o 3 2 1 1938.73 1972.23 46.08 o 4 2 1 4859.46 4549.99 71.31 o 5 2 1 274.63 254.47 11.70 o 6 2 1 1151.33 1008.82 27.23 o 7 2 1 965.73 861.14 25.30 o 8 2 1 86.15 70.07 12.51 o 9 2 1 50.47 30.81 12.85 o 10 2 1 49.41 48.03 13.37 o 11 2 1 3.76 0.00 12.47 o 12 2 1 0.23 0.00 13.37 o 13 2 1 3.17 0.00 13.82 o 14 2 1 2.50 12.17 13.63 o -14 3 1 15.48 19.38 15.05 o -13 3 1 11.22 0.00 13.37 o -12 3 1 20.35 5.79 13.26 o -11 3 1 50.17 68.61 13.41 o -10 3 1 74.88 81.16 12.89 o -9 3 1 307.62 276.41 16.52 o -8 3 1 223.63 213.16 14.65 o -7 3 1 35.86 26.59 10.76 o -6 3 1 704.66 735.74 20.88 o -5 3 1 812.69 809.60 21.93 o -4 3 1 276.04 309.87 12.33 o -3 3 1 638.34 623.23 17.56 o -2 3 1 0.47 0.00 7.32 o -1 3 1 133.88 117.19 8.82 o 0 3 1 685.42 711.55 20.42 o 1 3 1 81.56 77.45 8.70 o 2 3 1 3255.04 3480.59 62.83 o 3 3 1 4123.09 4293.79 72.60 o 4 3 1 1.78 12.32 7.39 o 5 3 1 1051.58 876.94 25.13 o 6 3 1 1101.05 940.32 25.91 o 7 3 1 6.66 0.00 11.02 o 8 3 1 37.83 32.34 11.99 o 9 3 1 27.49 10.98 12.96 o 10 3 1 91.52 81.65 14.23 o 11 3 1 12.90 1.49 12.92 o 12 3 1 7.74 15.20 12.88 o 13 3 1 68.99 89.27 15.28 o -13 4 1 56.94 64.84 15.09 o -12 4 1 22.45 24.99 13.15 o -11 4 1 36.47 34.81 13.41 o -10 4 1 120.05 128.12 14.49 o -9 4 1 322.72 349.12 17.53 o -8 4 1 782.12 775.12 26.52 o -7 4 1 799.92 842.07 25.55 o -6 4 1 191.74 193.95 12.85 o -5 4 1 947.77 1015.39 28.11 o -4 4 1 750.55 692.11 21.48 o -3 4 1 125.59 126.61 9.68 o -2 4 1 17.68 6.16 7.99 o -1 4 1 581.39 568.30 16.65 o 0 4 1 167.32 164.16 10.39 o 1 4 1 132.18 127.97 9.23 o 2 4 1 31.16 29.66 8.18 o 3 4 1 198.32 183.37 10.91 o 4 4 1 2719.59 2602.40 54.59 o 5 4 1 13.80 16.69 9.97 o 6 4 1 684.59 607.78 20.53 o 7 4 1 1030.54 965.26 30.09 o 8 4 1 24.01 28.01 11.99 o 9 4 1 76.72 50.46 14.12 o 10 4 1 70.92 58.64 12.92 o 11 4 1 113.74 112.39 15.39 o 12 4 1 71.65 95.80 15.35 o 13 4 1 18.63 29.47 15.42 o -13 5 1 0.06 0.00 14.27 o -12 5 1 42.40 37.12 15.24 o -11 5 1 185.46 200.30 16.62 o -10 5 1 112.05 92.26 14.83 o -9 5 1 364.25 351.04 17.71 o -8 5 1 409.52 372.47 18.01 o -7 5 1 16.42 0.00 13.03 o -6 5 1 2492.23 2381.89 59.46 o -5 5 1 786.83 843.91 24.65 o -4 5 1 56.89 59.39 10.27 o -3 5 1 1376.79 1493.40 37.89 o -2 5 1 39.92 48.89 9.56 o -1 5 1 42.91 62.26 9.23 o 0 5 1 86.55 105.04 10.27 o 1 5 1 70.21 69.70 9.56 o 2 5 1 541.03 594.45 19.45 o 3 5 1 20.31 25.47 10.01 o 4 5 1 468.19 525.68 19.03 o 5 5 1 517.11 440.67 17.87 o 6 5 1 493.44 500.20 18.73 o 7 5 1 46.11 55.09 12.77 o 8 5 1 231.31 222.19 16.51 o 9 5 1 547.81 513.12 21.87 o 10 5 1 42.98 26.78 14.12 o 11 5 1 76.67 76.87 15.16 o 12 5 1 33.84 19.98 16.02 o 13 5 1 1.99 14.53 14.04 o -12 6 1 0.70 0.00 14.04 o -11 6 1 53.89 34.77 15.28 o -10 6 1 118.22 125.21 14.87 o -9 6 1 42.89 15.69 14.45 o -8 6 1 1056.98 1044.79 31.69 o -7 6 1 1223.26 1214.35 35.22 o -6 6 1 31.90 3.92 12.92 o -5 6 1 1460.67 1514.62 40.42 o -4 6 1 985.45 980.60 29.83 o -3 6 1 32.82 37.87 11.43 o -2 6 1 135.10 130.42 12.44 o -1 6 1 17.32 32.49 10.12 o 0 6 1 1.45 0.00 10.64 o 1 6 1 0.10 0.00 10.64 o 2 6 1 0.29 0.00 10.91 o 3 6 1 25.13 45.79 11.06 o 4 6 1 346.67 352.77 16.82 o 5 6 1 1.79 32.57 11.73 o 6 6 1 139.26 133.77 14.05 o 7 6 1 138.55 124.65 14.49 o 8 6 1 0.41 3.73 12.55 o 9 6 1 24.94 17.67 14.23 o 10 6 1 45.52 48.70 14.23 o 11 6 1 19.94 2.35 14.64 o 12 6 1 107.94 115.64 17.14 o -11 7 1 30.50 18.79 14.83 o -10 7 1 12.23 0.00 14.08 o -9 7 1 62.13 64.73 13.22 o -8 7 1 96.98 102.01 15.31 o -7 7 1 26.80 46.91 12.44 o -6 7 1 377.07 337.98 18.46 o -5 7 1 154.75 143.86 14.94 o -4 7 1 138.83 126.79 15.28 o -3 7 1 344.61 372.82 16.48 o -2 7 1 71.01 93.38 12.81 o -1 7 1 19.57 26.40 12.70 o 0 7 1 73.51 82.96 13.33 o 1 7 1 152.63 129.93 14.23 o 2 7 1 0.08 0.00 12.14 o 3 7 1 26.19 35.44 12.81 o 4 7 1 70.79 64.99 13.48 o 5 7 1 346.52 328.14 17.64 o 6 7 1 185.59 184.40 15.84 o 7 7 1 28.95 42.95 13.07 o 8 7 1 246.32 234.44 15.69 o 9 7 1 110.26 93.64 15.20 o 10 7 1 0.42 0.00 14.30 o 11 7 1 24.98 8.37 14.27 o -10 8 1 7.14 0.00 14.90 o -9 8 1 0.51 0.00 13.59 o -8 8 1 0.91 17.85 12.70 o -7 8 1 111.20 106.68 14.46 o -6 8 1 33.56 40.34 13.59 o -5 8 1 107.62 115.79 15.46 o -4 8 1 29.68 54.27 13.59 o -3 8 1 15.28 0.00 13.00 o -2 8 1 61.63 82.88 14.04 o -1 8 1 49.26 61.40 13.07 o 0 8 1 103.21 84.19 15.35 o 1 8 1 354.81 338.50 17.98 o 2 8 1 573.39 591.80 22.95 o 3 8 1 127.67 99.96 14.87 o 4 8 1 271.40 205.80 16.66 o 5 8 1 78.75 67.83 14.23 o 6 8 1 13.84 22.93 13.11 o 7 8 1 2.76 0.00 14.34 o 8 8 1 1.79 18.26 12.74 o 9 8 1 0.10 0.00 14.42 o 10 8 1 0.00 7.17 14.90 o -9 9 1 36.91 63.60 14.75 o -8 9 1 2.52 0.00 14.15 o -7 9 1 1.58 10.01 13.52 o -6 9 1 85.80 44.86 15.13 o -5 9 1 6.71 12.36 13.15 o -4 9 1 0.13 0.00 13.03 o -3 9 1 8.47 0.00 13.26 o -2 9 1 58.17 55.05 13.26 o -1 9 1 66.37 67.23 14.57 o 0 9 1 278.95 243.68 17.86 o 1 9 1 6.74 9.34 13.07 o 2 9 1 19.17 13.00 13.07 o 3 9 1 157.89 135.23 15.39 o 4 9 1 60.19 68.13 14.53 o 5 9 1 17.05 27.94 14.15 o 6 9 1 34.07 45.71 14.79 o 7 9 1 12.45 0.00 13.97 o 8 9 1 3.19 13.26 14.12 o 9 9 1 51.68 27.41 15.72 o -7 10 1 78.27 79.41 15.61 o -6 10 1 0.79 0.00 14.42 o -5 10 1 21.93 27.97 15.57 o -4 10 1 168.26 135.49 17.33 o -3 10 1 36.45 47.17 14.12 o -2 10 1 13.01 22.03 13.89 o -1 10 1 35.09 35.29 13.63 o 0 10 1 39.17 43.66 14.27 o 1 10 1 39.98 12.96 14.79 o 2 10 1 157.32 145.16 16.10 o 3 10 1 3.15 16.84 13.71 o 4 10 1 44.51 38.13 15.05 o 5 10 1 3.78 33.84 13.37 o 6 10 1 1.11 15.31 13.30 o 7 10 1 29.10 0.00 15.24 o -5 11 1 19.30 0.00 16.21 o -4 11 1 2.27 0.00 14.64 o -3 11 1 20.90 18.82 15.72 o -2 11 1 38.64 26.22 15.57 o -1 11 1 4.00 0.00 15.24 o 0 11 1 11.28 20.28 14.68 o 1 11 1 11.81 18.49 14.90 o 2 11 1 44.31 48.85 15.42 o 3 11 1 2.06 20.24 14.71 o 4 11 1 33.01 8.66 16.43 o 5 11 1 137.94 142.46 18.30 o -14 0 2 166.25 207.73 18.08 o -13 0 2 5.28 0.00 12.96 o -12 0 2 91.54 139.73 14.94 o -11 0 2 177.06 179.54 15.91 o -10 0 2 22.92 58.64 12.92 o -9 0 2 434.47 486.62 19.47 o -8 0 2 19.67 12.10 10.72 o -7 0 2 16.79 2.24 9.11 o -6 0 2 258.12 319.64 12.93 o -5 0 2 3331.23 3866.26 69.23 o -4 0 2 0.04 7.17 6.35 o -3 0 2 2750.27 2526.63 49.22 o -2 0 2 4379.06 3993.87 55.41 o -1 0 2 2552.67 2362.74 40.90 o 0 0 2 822.43 717.89 20.90 o 1 0 2 929.16 816.99 25.15 o 2 0 2 7843.39 6845.79 75.32 o 3 0 2 2300.36 2126.57 46.29 o 4 0 2 100.36 77.26 7.55 o 5 0 2 861.90 754.55 21.27 o 6 0 2 1876.60 1692.87 38.17 o 7 0 2 1219.43 1049.08 27.53 o 8 0 2 1039.34 989.51 29.01 o 9 0 2 0.28 0.00 11.84 o 10 0 2 217.84 216.47 15.84 o 11 0 2 152.84 175.42 15.20 o 12 0 2 35.32 53.52 13.15 o 13 0 2 55.06 71.78 14.72 o 14 0 2 0.17 24.54 13.52 o -14 1 2 30.79 33.46 13.97 o -13 1 2 276.84 302.10 19.80 o -12 1 2 181.84 193.28 16.59 o -11 1 2 389.60 392.01 18.57 o -10 1 2 345.96 352.42 16.89 o -9 1 2 0.45 0.00 11.76 o -8 1 2 3.69 8.07 10.83 o -7 1 2 21.52 14.15 9.64 o -6 1 2 169.60 206.24 10.84 o -5 1 2 0.35 1.72 7.17 o -4 1 2 568.76 726.80 19.91 o -3 1 2 336.40 307.92 11.44 o -2 1 2 7609.05 7506.01 78.75 o -1 1 2 591.49 577.30 14.61 o 2 1 2 484.63 492.15 16.32 o 3 1 2 126.94 107.24 8.29 o 4 1 2 983.58 903.71 22.07 o 5 1 2 1264.52 1119.87 29.73 o 6 1 2 8.11 11.32 8.25 o 7 1 2 784.60 696.16 22.71 o 8 1 2 121.51 114.23 13.15 o 9 1 2 791.33 686.66 24.50 o 10 1 2 105.78 87.59 13.82 o 11 1 2 32.19 31.37 12.89 o 12 1 2 51.71 50.87 13.97 o 13 1 2 37.26 66.52 13.33 o 14 1 2 1.06 17.55 14.04 o -14 2 2 105.29 138.09 17.97 o -13 2 2 5.79 0.00 14.57 o -12 2 2 53.76 64.58 13.89 o -11 2 2 140.30 163.35 15.28 o -10 2 2 7.51 9.75 11.88 o -9 2 2 11.02 0.00 12.29 o -8 2 2 78.98 89.98 11.95 o -7 2 2 36.14 41.31 9.97 o -6 2 2 16.04 11.54 8.74 o -5 2 2 559.05 595.49 17.32 o -4 2 2 357.11 345.51 13.12 o -3 2 2 3328.15 3559.24 62.13 o -2 2 2 135.81 141.92 8.56 o -1 2 2 1843.53 2100.31 37.50 o 0 2 2 617.84 619.95 17.00 o 1 2 2 474.77 522.51 15.31 o 2 2 2 663.37 791.07 19.88 o 3 2 2 22.05 21.70 7.62 o 4 2 2 90.32 94.06 8.59 o 5 2 2 13.07 14.30 8.22 o 6 2 2 261.27 257.00 12.67 o 7 2 2 345.28 358.16 15.21 o 8 2 2 405.85 388.16 16.78 o 9 2 2 3.29 0.00 12.25 o 10 2 2 388.75 396.02 19.10 o 11 2 2 18.07 10.31 12.85 o 12 2 2 9.28 2.73 12.88 o 13 2 2 12.40 0.00 13.86 o -13 3 2 8.06 4.18 13.33 o -12 3 2 18.26 44.59 13.33 o -11 3 2 13.15 0.00 12.92 o -10 3 2 248.65 255.18 15.73 o -9 3 2 177.12 160.94 15.62 o -8 3 2 985.41 892.73 27.02 o -7 3 2 26.84 20.17 10.94 o -6 3 2 10.58 15.20 9.78 o -5 3 2 1445.02 1427.68 34.94 o -4 3 2 1911.24 2018.47 45.17 o -3 3 2 266.44 285.79 11.29 o -2 3 2 6960.57 7721.57 95.70 o -1 3 2 1917.47 2254.94 43.29 o 0 3 2 724.05 840.79 20.15 o 1 3 2 3.88 9.97 7.36 o 2 3 2 133.80 153.34 9.23 o 3 3 2 38.90 41.57 8.25 o 4 3 2 16.44 7.62 8.48 o 5 3 2 288.87 287.93 13.19 o 6 3 2 26.99 27.45 10.16 o 7 3 2 70.55 68.91 12.03 o 8 3 2 25.34 17.59 12.62 o 9 3 2 62.66 46.61 13.33 o 10 3 2 133.66 139.89 14.05 o 11 3 2 20.10 31.67 13.67 o 12 3 2 95.30 71.12 16.25 o 13 3 2 15.12 44.78 13.78 o -13 4 2 18.59 28.12 13.67 o -12 4 2 9.39 16.54 13.44 o -11 4 2 73.54 66.26 13.93 o -10 4 2 0.05 0.00 12.73 o -9 4 2 219.56 248.78 15.54 o -8 4 2 203.01 192.74 15.21 o -7 4 2 112.81 100.78 13.22 o -6 4 2 42.58 64.43 11.17 o -5 4 2 5.19 6.42 9.93 o -4 4 2 357.77 446.70 16.75 o -3 4 2 663.33 695.76 21.18 o -2 4 2 913.94 1077.48 27.37 o -1 4 2 809.54 963.48 25.94 o 0 4 2 515.45 542.61 17.66 o 1 4 2 203.90 219.54 10.80 o 2 4 2 23.79 16.84 8.96 o 3 4 2 1012.72 1068.74 26.63 o 4 4 2 386.66 452.07 16.30 o 5 4 2 1034.82 1083.86 28.79 o 6 4 2 1.27 0.00 11.35 o 7 4 2 3.66 2.17 12.10 o 8 4 2 10.07 21.29 12.29 o 9 4 2 40.66 34.21 13.18 o 10 4 2 259.75 264.03 17.56 o 11 4 2 46.07 41.42 14.27 o 12 4 2 1.70 4.18 13.41 o 13 4 2 5.69 22.93 14.00 o -12 5 2 6.85 6.05 12.85 o -11 5 2 0.17 11.13 12.21 o -10 5 2 0.44 0.00 12.77 o -9 5 2 163.74 160.97 14.87 o -8 5 2 670.56 610.17 23.82 o -7 5 2 66.72 56.18 13.63 o -6 5 2 27.25 14.86 11.91 o -5 5 2 70.18 74.93 11.65 o -4 5 2 724.46 706.60 23.68 o -3 5 2 757.17 809.24 23.31 o -2 5 2 379.61 448.66 16.71 o -1 5 2 386.71 512.64 17.94 o 0 5 2 86.09 92.27 10.65 o 1 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