#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:25:05 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181041 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/21/2212152.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212152_Fobs loop_ _publ_author_name 'Bream, Richard' 'Hunter, Stuart J.' 'Fleet, George W. J.' 'Watkin, David J.' _publ_section_title ; 2-C-Hydroxymethyl-2,3-O-isopropylidene-D-mannono-1,5-lactam ; _journal_coeditor_code FL2067 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o621 _journal_page_last o623 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 06-08-29 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.3477(2) _cell_length_b 12.4398(3) _cell_length_c 14.1469(5) _cod_data_source_file fl20674sup2.hkl _cod_data_source_block 4 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 3298.20 3481.59 83.50 o 4 0 0 4.20 8.18 1.50 o 6 0 0 158.80 148.54 8.50 o 8 0 0 32.60 27.61 6.80 o 1 1 0 941.00 0.00 118.00 x 2 1 0 367.20 360.81 6.80 o 3 1 0 6422.80 6383.75 131.50 o 4 1 0 39.30 29.81 1.40 o 5 1 0 1348.90 1374.35 28.90 o 6 1 0 248.70 260.03 6.90 o 7 1 0 205.20 191.21 7.60 o 8 1 0 947.60 884.54 42.90 o 0 2 0 15.40 0.00 6.10 x 1 2 0 324.90 351.91 5.60 o 2 2 0 4237.60 4414.04 76.60 o 3 2 0 3875.50 3785.65 68.30 o 4 2 0 621.40 642.22 11.90 o 5 2 0 486.10 478.65 10.50 o 6 2 0 26.20 27.81 2.30 o 7 2 0 56.00 52.95 4.50 o 8 2 0 2.10 0.62 4.80 o 1 3 0 588.30 614.93 12.90 o 2 3 0 968.10 916.56 17.00 o 3 3 0 5.30 4.58 0.90 o 4 3 0 159.20 172.52 3.60 o 5 3 0 3.60 0.02 1.30 o 6 3 0 650.40 703.77 17.00 o 7 3 0 11.20 9.05 4.50 o 8 3 0 9.90 5.91 4.70 o 0 4 0 3772.20 3920.38 100.60 o 1 4 0 1138.00 1158.03 22.20 o 2 4 0 3.30 1.34 0.60 o 3 4 0 1231.50 1284.62 27.10 o 4 4 0 18.90 25.61 1.10 o 5 4 0 26.10 35.78 1.80 o 6 4 0 33.20 34.47 3.20 o 7 4 0 333.00 339.16 17.20 o 8 4 0 79.30 62.39 9.10 o 1 5 0 561.20 527.99 8.80 o 2 5 0 3184.70 3188.02 55.80 o 3 5 0 88.00 75.51 2.20 o 4 5 0 580.70 574.94 13.80 o 5 5 0 268.80 249.41 8.60 o 6 5 0 9.40 8.51 3.30 o 7 5 0 35.80 41.24 6.80 o 8 5 0 134.30 117.10 13.00 o 0 6 0 1288.90 1238.59 24.00 o 1 6 0 478.00 494.71 7.30 o 2 6 0 1517.00 1408.72 33.50 o 3 6 0 2.70 1.11 0.90 o 4 6 0 99.90 100.97 3.80 o 5 6 0 107.90 99.91 4.80 o 6 6 0 318.90 308.48 15.70 o 7 6 0 363.40 296.61 18.40 o 8 6 0 4.10 3.18 8.20 o 1 7 0 600.30 560.51 9.10 o 2 7 0 60.00 63.90 1.90 o 3 7 0 716.70 675.76 15.80 o 4 7 0 954.30 979.95 30.40 o 5 7 0 138.60 141.94 5.70 o 6 7 0 183.70 173.99 10.80 o 7 7 0 439.00 407.74 25.20 o 8 7 0 -8.60 0.17 7.80 o 0 8 0 1832.90 1890.15 39.70 o 1 8 0 2299.90 2302.28 33.90 o 2 8 0 87.40 75.25 1.80 o 3 8 0 825.10 885.37 27.80 o 4 8 0 0.90 2.62 2.47 o 5 8 0 476.40 513.87 20.60 o 6 8 0 410.90 427.65 23.10 o 7 8 0 45.80 49.34 6.60 o 1 9 0 140.80 135.58 2.80 o 2 9 0 1445.70 1473.73 27.60 o 3 9 0 1304.40 1387.10 37.50 o 4 9 0 1723.80 1800.49 57.90 o 5 9 0 516.40 475.24 21.20 o 6 9 0 45.10 56.15 6.00 o 7 9 0 16.50 9.75 5.70 o 0 10 0 530.40 532.20 14.90 o 1 10 0 3.00 1.51 0.80 o 2 10 0 248.70 278.17 6.40 o 3 10 0 4062.70 4231.23 85.50 o 4 10 0 74.10 79.84 3.00 o 5 10 0 207.10 204.26 10.60 o 6 10 0 150.90 141.98 10.40 o 7 10 0 77.30 93.34 10.00 o 1 11 0 79.60 91.52 2.50 o 2 11 0 0.10 0.02 0.82 o 3 11 0 1.80 0.70 0.50 o 4 11 0 284.80 295.84 9.20 o 5 11 0 388.90 368.25 14.20 o 6 11 0 70.40 77.22 8.20 o 0 12 0 1624.50 1731.70 66.30 o 1 12 0 175.30 180.85 5.00 o 2 12 0 146.80 146.08 5.90 o 3 12 0 2.00 2.05 2.40 o 4 12 0 45.20 42.63 2.40 o 5 12 0 12.40 18.60 3.20 o 6 12 0 84.70 87.52 5.90 o 1 13 0 279.50 291.64 8.70 o 2 13 0 127.40 138.61 5.90 o 3 13 0 193.50 191.58 8.70 o 4 13 0 2.60 0.87 2.30 o 5 13 0 47.80 55.71 4.70 o 0 14 0 243.30 241.53 12.30 o 1 14 0 127.90 122.77 6.40 o 2 14 0 9.70 9.96 2.30 o 3 14 0 95.20 90.22 5.60 o 4 14 0 68.60 70.40 5.10 o 5 14 0 49.00 49.60 4.60 o 1 15 0 31.10 25.93 4.70 o 2 15 0 1.70 1.42 2.40 o 3 15 0 109.00 111.37 7.60 o 4 15 0 39.50 39.84 4.40 o 0 16 0 51.10 63.68 7.20 o 1 16 0 50.20 52.20 7.80 o 2 16 0 31.50 25.51 7.50 o 3 16 0 433.70 420.01 29.90 o 1 17 0 20.80 25.24 6.80 o 2 17 0 137.50 126.11 13.30 o 1 0 1 340.40 0.00 30.90 x 2 0 1 923.90 956.96 16.10 o 3 0 1 315.60 314.70 5.80 o 4 0 1 14.10 14.54 1.10 o 5 0 1 51.30 56.80 2.00 o 6 0 1 206.40 227.51 7.30 o 7 0 1 11.30 9.67 2.90 o 8 0 1 89.70 98.00 7.70 o 0 1 1 -0.10 0.00 0.06 x 1 1 1 319.90 0.00 25.42 x 2 1 1 1827.35 1935.94 34.24 o 3 1 1 1477.35 1443.39 26.25 o 4 1 1 276.50 316.74 6.06 o 5 1 1 148.80 150.62 4.00 o 6 1 1 369.50 391.07 10.92 o 7 1 1 40.10 40.43 3.60 o 8 1 1 51.65 47.83 6.70 o 0 2 1 126.40 0.00 6.70 x 1 2 1 223.45 242.58 4.20 o 2 2 1 1322.45 1351.47 25.04 o 3 2 1 531.20 495.54 9.20 o 4 2 1 998.40 996.92 19.35 o 5 2 1 234.45 257.10 5.60 o 6 2 1 70.10 72.07 3.20 o 7 2 1 151.05 163.64 7.88 o 8 2 1 7.15 1.83 4.04 o 0 3 1 3868.60 4243.63 71.40 o 1 3 1 2048.05 2287.39 37.99 o 2 3 1 1044.25 1050.86 18.30 o 3 3 1 1029.75 982.05 19.28 o 4 3 1 296.40 301.55 6.82 o 5 3 1 603.90 643.22 17.01 o 6 3 1 896.05 971.26 28.17 o 7 3 1 143.55 156.92 8.22 o 8 3 1 106.95 92.82 10.87 o 0 4 1 2245.80 2362.14 34.90 o 1 4 1 1705.15 1705.86 30.79 o 2 4 1 1483.45 1326.27 24.49 o 3 4 1 188.75 178.83 4.27 o 4 4 1 151.45 160.65 3.97 o 5 4 1 155.85 152.69 5.36 o 6 4 1 193.55 186.52 7.30 o 7 4 1 305.35 271.33 14.80 o 8 4 1 78.90 88.00 9.33 o 0 5 1 326.10 323.57 4.60 o 1 5 1 1386.60 1337.43 19.90 o 2 5 1 3163.60 3107.84 58.29 o 3 5 1 38.60 34.33 1.41 o 4 5 1 902.35 864.03 20.75 o 5 5 1 842.45 786.57 24.41 o 6 5 1 147.40 160.60 6.91 o 7 5 1 204.80 219.86 12.21 o 8 5 1 510.90 471.34 33.33 o 0 6 1 5231.80 4891.33 80.80 o 1 6 1 1808.25 1752.86 28.03 o 2 6 1 355.55 368.09 7.43 o 3 6 1 1307.15 1245.32 26.47 o 4 6 1 550.35 553.30 16.65 o 5 6 1 145.75 142.37 5.80 o 6 6 1 43.50 36.92 5.12 o 7 6 1 231.85 208.18 13.55 o 8 6 1 19.00 20.45 6.20 o 0 7 1 249.00 243.46 3.40 o 1 7 1 879.30 805.13 13.58 o 2 7 1 842.00 782.56 15.54 o 3 7 1 1064.40 1056.27 22.60 o 4 7 1 133.05 130.97 5.10 o 5 7 1 279.00 262.31 10.76 o 6 7 1 45.40 46.99 4.87 o 7 7 1 139.40 143.51 9.83 o 8 7 1 147.55 137.68 11.85 o 0 8 1 472.30 441.84 7.60 o 1 8 1 9.25 6.32 0.71 o 2 8 1 369.05 371.66 6.55 o 3 8 1 171.90 178.28 5.52 o 4 8 1 25.30 25.95 2.10 o 5 8 1 78.95 85.91 5.41 o 6 8 1 6.95 8.71 3.80 o 7 8 1 184.75 172.67 13.85 o 0 9 1 584.00 552.33 11.00 o 1 9 1 186.60 172.45 3.60 o 2 9 1 78.35 71.25 2.39 o 3 9 1 287.55 265.84 7.20 o 4 9 1 111.25 108.38 4.65 o 5 9 1 129.70 129.43 8.02 o 6 9 1 9.00 5.01 4.92 o 7 9 1 149.40 129.66 12.49 o 0 10 1 1463.10 1427.60 29.70 o 1 10 1 434.35 441.10 8.46 o 2 10 1 154.05 161.08 4.18 o 3 10 1 79.70 78.97 2.47 o 4 10 1 159.55 166.44 8.01 o 5 10 1 96.60 85.75 6.76 o 6 10 1 289.95 263.30 16.57 o 7 10 1 33.95 19.53 6.85 o 0 11 1 -0.60 0.58 1.39 o 1 11 1 296.60 283.33 6.80 o 2 11 1 558.95 595.16 13.74 o 3 11 1 477.60 485.14 13.27 o 4 11 1 9.95 7.83 1.93 o 5 11 1 84.75 80.24 5.50 o 6 11 1 62.05 51.47 7.14 o 0 12 1 301.00 329.60 8.80 o 1 12 1 704.40 714.93 14.95 o 2 12 1 65.25 76.78 3.45 o 3 12 1 127.05 128.24 4.69 o 4 12 1 40.20 39.27 2.98 o 5 12 1 64.85 71.75 4.60 o 6 12 1 104.25 95.72 7.35 o 0 13 1 1.80 0.45 0.80 o 1 13 1 4.55 1.31 2.25 o 2 13 1 61.95 63.16 3.35 o 3 13 1 187.25 184.31 7.80 o 4 13 1 10.40 14.90 3.00 o 5 13 1 197.65 192.62 10.45 o 0 14 1 67.30 80.81 5.10 o 1 14 1 444.65 438.29 14.26 o 2 14 1 147.35 147.44 8.02 o 3 14 1 21.95 24.91 2.90 o 4 14 1 130.35 129.41 7.25 o 5 14 1 12.30 15.26 6.42 o 0 15 1 113.30 116.01 7.00 o 1 15 1 47.55 58.50 4.26 o 2 15 1 17.20 11.97 5.41 o 3 15 1 44.45 53.43 6.86 o 4 15 1 415.05 404.44 22.84 o 0 16 1 17.40 18.52 5.00 o 1 16 1 66.75 66.31 7.28 o 2 16 1 81.40 84.02 9.70 o 3 16 1 199.65 194.57 12.52 o 0 17 1 9.80 0.00 5.30 o 1 17 1 75.20 74.55 9.97 o 2 17 1 0.25 7.41 9.35 o 2 0 2 2875.70 2886.07 55.10 o 3 0 2 157.30 148.71 3.00 o 4 0 2 197.50 190.32 4.20 o 5 0 2 35.70 44.17 1.90 o 6 0 2 432.20 437.56 12.80 o 7 0 2 92.40 90.51 6.50 o 8 0 2 7.00 4.95 7.10 o 0 1 2 -0.50 0.00 0.57 x 1 1 2 1403.90 1583.33 41.18 o 2 1 2 8656.60 9294.24 294.03 o 3 1 2 585.65 601.02 11.91 o 4 1 2 179.00 168.64 3.80 o 5 1 2 134.00 137.03 3.65 o 6 1 2 732.65 740.07 22.79 o 7 1 2 25.50 27.31 4.97 o 8 1 2 131.10 130.26 10.26 o 0 2 2 747.20 1199.87 35.60 x 1 2 2 4428.20 4881.13 98.04 o 2 2 2 472.55 461.37 9.53 o 3 2 2 3070.40 2972.87 57.24 o 4 2 2 419.15 393.13 9.33 o 5 2 2 228.00 240.81 6.27 o 6 2 2 43.60 52.02 3.04 o 7 2 2 121.85 129.17 6.88 o 8 2 2 222.90 209.19 15.13 o 0 3 2 2439.30 2522.39 35.40 o 2 3 2 2933.40 2912.61 56.42 o 3 3 2 1228.90 1217.69 22.77 o 4 3 2 240.55 221.50 5.68 o 5 3 2 79.85 106.34 3.42 o 6 3 2 66.15 70.02 3.48 o 7 3 2 72.65 73.15 5.96 o 8 3 2 33.20 34.74 6.16 o 0 4 2 4202.10 4407.11 59.60 o 1 4 2 359.80 356.39 6.36 o 2 4 2 336.85 343.15 6.30 o 3 4 2 629.80 592.88 11.81 o 4 4 2 672.90 651.56 14.42 o 5 4 2 86.00 85.84 3.66 o 6 4 2 630.75 601.97 20.13 o 7 4 2 115.80 115.45 7.51 o 8 4 2 98.60 103.77 10.20 o 0 5 2 639.10 664.68 8.50 o 1 5 2 1877.50 1913.35 30.14 o 2 5 2 22.15 29.49 0.91 o 3 5 2 54.25 50.75 1.65 o 4 5 2 827.15 838.71 17.95 o 5 5 2 165.70 156.52 5.64 o 6 5 2 5.65 4.28 2.16 o 7 5 2 26.75 26.52 4.18 o 8 5 2 58.00 65.75 8.80 o 0 6 2 1887.80 1886.99 24.90 o 1 6 2 163.60 150.33 2.97 o 2 6 2 347.95 331.50 8.37 o 3 6 2 61.15 61.44 1.77 o 4 6 2 244.30 254.38 7.88 o 5 6 2 542.35 571.44 17.34 o 6 6 2 20.65 24.40 4.61 o 7 6 2 1.10 5.46 5.98 o 8 6 2 160.70 174.01 12.70 o 0 7 2 1566.80 1462.51 22.70 o 1 7 2 578.35 568.25 9.87 o 2 7 2 618.35 634.43 11.34 o 3 7 2 113.25 105.92 3.00 o 4 7 2 1457.75 1462.62 47.38 o 5 7 2 131.00 126.33 5.55 o 6 7 2 58.70 59.07 5.18 o 7 7 2 219.30 208.80 13.17 o 8 7 2 -0.80 3.36 9.48 o 0 8 2 825.20 807.85 16.40 o 1 8 2 1669.30 1680.83 27.17 o 2 8 2 996.15 1006.89 18.32 o 3 8 2 28.75 29.37 1.90 o 4 8 2 677.90 711.02 23.81 o 5 8 2 174.30 162.12 9.47 o 6 8 2 346.45 333.75 17.05 o 7 8 2 204.15 205.77 13.01 o 0 9 2 41.00 45.08 1.60 o 1 9 2 1433.70 1432.89 25.72 o 2 9 2 441.85 465.37 8.64 o 3 9 2 539.55 550.53 13.31 o 4 9 2 137.05 147.52 5.55 o 5 9 2 488.45 497.91 22.93 o 6 9 2 154.60 157.22 9.91 o 7 9 2 49.55 52.54 8.67 o 0 10 2 559.80 578.51 10.90 o 1 10 2 901.00 906.97 17.70 o 2 10 2 1091.75 1137.30 24.31 o 3 10 2 1470.95 1495.12 36.60 o 4 10 2 173.20 170.21 6.55 o 5 10 2 60.55 59.50 5.56 o 6 10 2 51.05 45.92 6.35 o 7 10 2 108.80 98.80 10.71 o 0 11 2 79.60 87.37 3.10 o 1 11 2 274.55 297.21 6.10 o 2 11 2 110.35 109.72 3.18 o 3 11 2 93.05 101.35 3.75 o 4 11 2 7.65 6.61 1.33 o 5 11 2 168.10 157.98 9.23 o 6 11 2 62.80 61.67 7.30 o 0 12 2 115.70 129.98 3.60 o 1 12 2 21.70 21.91 1.51 o 2 12 2 31.15 35.06 2.25 o 3 12 2 28.40 35.99 2.88 o 4 12 2 1.70 4.38 2.56 o 5 12 2 96.35 96.20 6.47 o 6 12 2 177.95 170.21 10.01 o 0 13 2 5.60 6.45 1.30 o 1 13 2 309.85 307.78 9.45 o 2 13 2 21.55 25.01 3.05 o 3 13 2 342.10 331.11 13.26 o 4 13 2 170.20 173.68 7.98 o 5 13 2 36.90 36.82 4.30 o 0 14 2 115.60 112.94 4.50 o 1 14 2 43.50 48.73 3.91 o 2 14 2 46.75 46.51 5.29 o 3 14 2 3.65 6.08 3.40 o 4 14 2 39.70 31.25 6.08 o 5 14 2 18.50 10.16 3.80 o 0 15 2 -1.60 0.33 3.50 o 1 15 2 101.35 98.73 5.66 o 2 15 2 113.15 114.23 8.94 o 3 15 2 31.15 34.37 5.42 o 4 15 2 23.30 27.18 5.70 o 0 16 2 89.90 93.16 7.10 o 1 16 2 36.15 43.17 6.46 o 2 16 2 238.80 214.18 14.89 o 3 16 2 36.50 30.56 7.19 o 0 17 2 98.90 129.62 12.50 o 1 17 2 53.80 57.70 8.70 o 1 0 3 4163.30 4415.78 80.20 o 2 0 3 721.30 626.33 14.40 o 3 0 3 282.80 300.54 6.30 o 4 0 3 30.20 36.02 1.60 o 5 0 3 248.80 265.54 7.10 o 6 0 3 1019.60 1020.48 41.50 o 7 0 3 30.70 40.68 4.50 o 8 0 3 347.50 344.91 25.60 o 0 1 3 1740.00 1834.92 57.10 o 1 1 3 459.15 488.42 10.20 o 2 1 3 1467.20 1482.09 27.04 o 3 1 3 86.60 86.08 2.45 o 4 1 3 339.70 326.79 7.85 o 5 1 3 195.50 194.62 5.95 o 6 1 3 84.25 103.83 4.82 o 7 1 3 80.25 65.44 6.91 o 8 1 3 26.90 27.57 6.46 o 1 2 3 993.85 1035.98 19.85 o 2 2 3 2936.95 2947.18 62.87 o 3 2 3 1107.35 1136.59 20.82 o 4 2 3 156.00 139.08 3.87 o 5 2 3 130.60 144.18 4.59 o 6 2 3 124.20 126.65 6.59 o 7 2 3 37.55 38.06 5.90 o 8 2 3 33.60 34.42 6.00 o 0 3 3 2559.00 2606.03 42.00 o 1 3 3 1231.90 1177.57 23.31 o 2 3 3 131.10 129.68 3.34 o 3 3 3 428.50 391.66 8.44 o 4 3 3 816.30 807.77 16.70 o 5 3 3 196.95 207.26 8.38 o 6 3 3 54.15 66.51 4.06 o 7 3 3 186.95 173.93 11.55 o 8 3 3 126.85 127.44 10.99 o 0 4 3 4815.60 4802.42 75.50 o 1 4 3 2486.50 2470.06 48.45 o 2 4 3 1696.75 1590.12 37.74 o 3 4 3 524.85 490.39 9.75 o 4 4 3 773.50 765.86 18.75 o 5 4 3 832.95 781.83 23.30 o 6 4 3 142.10 163.31 5.54 o 7 4 3 194.40 180.76 12.53 o 8 4 3 142.50 131.53 12.50 o 0 5 3 483.90 516.75 7.30 o 1 5 3 164.00 138.84 2.92 o 2 5 3 1248.85 1286.00 21.63 o 3 5 3 1879.50 1861.65 35.44 o 4 5 3 244.75 237.74 5.65 o 5 5 3 602.85 625.48 18.78 o 6 5 3 191.40 198.00 8.96 o 7 5 3 97.65 96.31 7.99 o 8 5 3 146.80 158.45 11.70 o 0 6 3 7.90 6.87 0.50 o 1 6 3 1444.05 1348.91 24.92 o 2 6 3 300.25 309.81 6.08 o 3 6 3 433.80 412.26 8.71 o 4 6 3 77.20 87.05 2.82 o 5 6 3 138.70 156.09 5.25 o 6 6 3 95.25 90.89 5.85 o 7 6 3 1.10 3.51 4.10 o 8 6 3 95.50 115.11 10.30 o 0 7 3 77.10 71.50 1.80 o 1 7 3 121.50 114.16 2.76 o 2 7 3 358.35 335.95 8.02 o 3 7 3 189.85 201.09 5.01 o 4 7 3 200.55 186.07 6.41 o 5 7 3 82.95 87.57 3.86 o 6 7 3 331.45 341.03 16.10 o 7 7 3 193.10 151.89 13.80 o 0 8 3 92.00 92.07 2.20 o 1 8 3 487.60 474.61 8.88 o 2 8 3 1026.95 1008.93 20.20 o 3 8 3 495.90 539.79 12.57 o 4 8 3 1.20 0.94 1.27 o 5 8 3 180.30 170.80 9.65 o 6 8 3 28.35 30.78 4.80 o 7 8 3 88.80 87.02 9.40 o 0 9 3 72.60 93.16 2.20 o 1 9 3 103.20 101.05 2.82 o 2 9 3 64.50 59.05 2.26 o 3 9 3 266.50 254.99 10.88 o 4 9 3 190.15 194.20 7.70 o 5 9 3 17.55 28.23 4.76 o 6 9 3 63.75 68.18 6.10 o 7 9 3 35.60 48.42 8.90 o 0 10 3 18.80 16.81 1.50 o 1 10 3 254.50 253.66 6.13 o 2 10 3 28.50 23.85 1.85 o 3 10 3 419.80 399.05 11.47 o 4 10 3 64.00 61.84 3.30 o 5 10 3 112.20 101.66 7.57 o 6 10 3 -5.70 1.10 4.10 o 7 10 3 -0.70 6.58 8.20 o 0 11 3 36.90 41.93 1.90 o 1 11 3 30.70 27.71 1.65 o 2 11 3 125.75 130.74 3.72 o 3 11 3 21.35 22.92 2.40 o 4 11 3 0.35 1.63 3.58 o 5 11 3 24.35 24.42 4.87 o 6 11 3 113.00 109.72 10.70 o 0 12 3 321.10 331.32 8.50 o 1 12 3 73.55 74.37 2.75 o 2 12 3 104.65 97.68 4.16 o 3 12 3 5.45 5.46 2.16 o 4 12 3 127.90 118.65 5.95 o 5 12 3 266.10 259.03 13.51 o 6 12 3 99.50 99.16 7.10 o 0 13 3 122.00 116.38 4.50 o 1 13 3 453.00 440.77 13.39 o 2 13 3 103.55 112.03 4.72 o 3 13 3 402.55 361.27 16.07 o 4 13 3 55.60 55.14 5.69 o 5 13 3 126.85 139.75 8.00 o 0 14 3 911.00 898.35 25.20 o 1 14 3 31.65 30.23 2.63 o 2 14 3 182.65 179.15 8.55 o 3 14 3 149.40 145.03 9.28 o 4 14 3 244.30 238.25 14.28 o 5 14 3 169.80 163.64 9.30 o 0 15 3 220.30 211.70 8.00 o 1 15 3 22.90 21.98 3.44 o 2 15 3 17.35 20.27 5.16 o 3 15 3 101.10 107.73 8.13 o 4 15 3 43.30 50.76 5.10 o 0 16 3 1.20 0.09 5.70 o 1 16 3 21.80 24.09 7.21 o 2 16 3 109.30 106.58 8.67 o 3 16 3 70.40 70.91 5.70 o 0 17 3 89.10 63.09 10.50 o 1 17 3 100.85 116.68 11.06 o 0 0 4 58.70 55.40 2.60 o 1 0 4 609.40 618.04 11.00 o 2 0 4 2697.50 2773.46 54.60 o 3 0 4 2102.40 2011.77 41.20 o 4 0 4 2045.50 2034.12 44.60 o 5 0 4 31.90 27.83 2.10 o 6 0 4 7.40 1.48 2.70 o 7 0 4 64.20 77.25 6.00 o 8 0 4 -0.60 1.67 7.59 o 0 1 4 7198.90 7617.48 272.20 o 1 1 4 3365.35 3637.31 66.02 o 2 1 4 603.00 554.06 13.34 o 3 1 4 19.55 16.93 1.25 o 4 1 4 209.90 195.10 5.30 o 5 1 4 1048.45 1037.64 30.62 o 6 1 4 267.05 280.82 11.19 o 7 1 4 56.15 55.14 5.98 o 8 1 4 40.80 41.80 7.03 o 0 2 4 3386.30 3490.58 79.70 o 1 2 4 628.40 668.16 12.30 o 2 2 4 1491.55 1420.13 31.74 o 3 2 4 214.35 204.01 4.60 o 4 2 4 1712.15 1675.82 37.43 o 5 2 4 268.85 269.67 8.85 o 6 2 4 48.60 53.31 4.01 o 7 2 4 81.15 82.37 6.26 o 8 2 4 21.25 27.22 7.20 o 0 3 4 6666.60 6869.93 155.00 o 1 3 4 2701.80 2709.06 56.35 o 2 3 4 720.25 731.91 15.25 o 3 3 4 624.95 599.26 12.45 o 4 3 4 586.00 552.49 12.78 o 5 3 4 179.75 170.33 6.45 o 6 3 4 7.90 13.69 3.14 o 7 3 4 18.85 14.43 4.73 o 8 3 4 18.20 27.79 6.42 o 0 4 4 1157.10 1095.76 19.50 o 1 4 4 164.65 145.18 3.20 o 2 4 4 179.00 137.25 3.82 o 3 4 4 731.95 707.40 14.93 o 4 4 4 284.40 277.34 6.95 o 5 4 4 412.25 380.10 13.45 o 6 4 4 34.60 35.63 3.49 o 7 4 4 11.95 9.54 5.36 o 8 4 4 9.10 4.20 5.90 o 0 5 4 34.80 23.63 1.30 o 1 5 4 1010.90 988.89 16.16 o 2 5 4 1241.85 1185.80 24.15 o 3 5 4 169.55 163.53 4.15 o 4 5 4 244.85 218.35 7.55 o 5 5 4 609.85 580.90 20.90 o 6 5 4 12.85 10.17 4.34 o 7 5 4 75.90 74.55 7.80 o 8 5 4 23.60 22.65 7.00 o 0 6 4 475.00 389.09 8.80 o 1 6 4 2859.50 2745.56 49.36 o 2 6 4 19.80 20.13 1.41 o 3 6 4 627.85 635.20 13.95 o 4 6 4 497.65 494.92 15.35 o 5 6 4 38.15 52.79 2.95 o 6 6 4 57.50 55.40 5.83 o 7 6 4 18.80 28.14 5.10 o 8 6 4 42.30 49.91 7.30 o 0 7 4 218.10 202.42 3.80 o 1 7 4 748.05 734.43 13.75 o 2 7 4 1753.20 1646.18 38.55 o 3 7 4 713.30 731.11 23.03 o 4 7 4 167.10 170.24 5.60 o 5 7 4 273.60 276.71 9.75 o 6 7 4 257.70 233.50 16.70 o 7 7 4 275.50 266.79 18.30 o 0 8 4 12.90 11.27 0.40 o 1 8 4 520.20 493.85 9.97 o 2 8 4 1063.10 1113.11 21.92 o 3 8 4 155.85 161.01 5.25 o 4 8 4 367.30 358.06 16.81 o 5 8 4 222.80 223.39 12.50 o 6 8 4 15.40 16.18 4.20 o 7 8 4 92.30 88.64 7.90 o 0 9 4 241.20 249.68 5.20 o 1 9 4 167.75 181.29 4.01 o 2 9 4 48.20 42.18 2.15 o 3 9 4 103.25 105.02 5.37 o 4 9 4 340.35 349.51 13.94 o 5 9 4 233.90 232.08 12.90 o 6 9 4 8.70 2.39 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39.20 4.40 o 4 15 4 3.50 2.10 3.60 o 0 16 4 129.30 138.35 13.50 o 1 16 4 93.55 93.27 6.62 o 2 16 4 132.70 128.54 7.80 o 3 16 4 88.40 89.10 6.20 o 0 17 4 21.80 23.74 8.50 o 1 17 4 29.40 34.88 8.72 o 1 0 5 3002.30 3116.03 51.40 o 2 0 5 458.30 455.23 9.60 o 3 0 5 420.40 411.31 7.70 o 4 0 5 46.10 50.58 2.10 o 5 0 5 731.30 747.50 24.50 o 6 0 5 596.90 597.14 26.10 o 7 0 5 54.40 60.32 5.00 o 8 0 5 259.30 239.27 17.90 o 0 1 5 1351.50 1349.29 32.10 o 1 1 5 545.60 521.61 10.95 o 2 1 5 1460.65 1347.92 29.81 o 3 1 5 877.10 830.39 17.21 o 4 1 5 719.10 702.53 15.47 o 5 1 5 262.45 276.17 11.29 o 6 1 5 122.20 126.11 8.00 o 7 1 5 41.65 48.66 5.46 o 8 1 5 19.70 17.49 6.00 o 0 2 5 1970.20 1974.10 38.10 o 1 2 5 815.80 830.99 15.95 o 2 2 5 1104.25 1031.65 22.79 o 3 2 5 599.55 553.88 12.07 o 4 2 5 804.45 806.44 17.02 o 5 2 5 340.35 361.74 11.67 o 6 2 5 239.20 251.39 8.90 o 7 2 5 74.60 73.31 6.98 o 8 2 5 115.45 116.22 10.71 o 0 3 5 14.10 14.45 0.70 o 1 3 5 275.45 261.72 5.55 o 2 3 5 4427.80 4434.68 81.42 o 3 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7.75 o 5 7 5 3.20 2.06 2.72 o 6 7 5 186.10 185.52 12.10 o 7 7 5 248.60 252.63 18.10 o 0 8 5 87.40 94.80 1.90 o 1 8 5 479.05 483.11 10.27 o 2 8 5 1261.85 1256.57 26.78 o 3 8 5 29.70 25.42 1.66 o 4 8 5 95.70 101.15 3.70 o 5 8 5 97.40 116.39 7.50 o 6 8 5 141.90 145.06 8.80 o 7 8 5 9.10 3.66 7.90 o 0 9 5 211.50 200.49 5.90 o 1 9 5 697.05 699.75 15.14 o 2 9 5 12.45 15.77 1.40 o 3 9 5 223.35 220.21 8.81 o 4 9 5 17.60 17.24 2.73 o 5 9 5 19.50 21.10 4.00 o 6 9 5 1.20 1.84 4.30 o 7 9 5 64.10 55.54 8.60 o 0 10 5 182.30 193.05 5.30 o 1 10 5 27.35 25.21 1.61 o 2 10 5 563.60 583.27 14.01 o 3 10 5 734.35 741.58 20.98 o 4 10 5 25.15 19.95 3.77 o 5 10 5 137.45 123.24 8.95 o 6 10 5 11.70 2.63 4.80 o 0 11 5 396.30 413.75 10.50 o 1 11 5 348.00 355.25 9.56 o 2 11 5 125.15 136.17 4.89 o 3 11 5 192.80 173.93 8.59 o 4 11 5 112.75 106.04 5.60 o 5 11 5 63.40 62.15 7.50 o 6 11 5 82.20 74.97 9.80 o 0 12 5 92.00 81.68 4.50 o 1 12 5 697.00 733.32 20.53 o 2 12 5 438.40 409.76 13.44 o 3 12 5 118.65 116.87 5.37 o 4 12 5 51.65 48.45 4.16 o 5 12 5 71.00 65.87 6.68 o 6 12 5 9.40 10.86 4.70 o 0 13 5 168.10 163.69 7.20 o 1 13 5 90.35 83.60 4.41 o 2 13 5 201.70 183.15 7.48 o 3 13 5 178.65 164.21 7.85 o 4 13 5 99.20 101.07 6.98 o 5 13 5 30.90 27.73 5.26 o 0 14 5 4.00 2.34 1.80 o 1 14 5 44.70 42.46 3.30 o 2 14 5 18.60 17.41 2.63 o 3 14 5 102.30 93.44 7.16 o 4 14 5 234.20 232.12 11.40 o 0 15 5 5.80 4.06 2.80 o 1 15 5 41.05 38.65 4.01 o 2 15 5 129.75 125.00 10.00 o 3 15 5 77.70 69.66 6.40 o 4 15 5 1.20 1.68 4.10 o 0 16 5 13.80 12.91 9.60 o 1 16 5 90.40 69.91 8.39 o 2 16 5 35.90 34.05 6.81 o 0 0 6 2666.00 2789.71 90.90 o 1 0 6 1767.00 1744.51 38.40 o 2 0 6 78.30 76.45 2.10 o 3 0 6 211.40 254.78 4.20 o 4 0 6 3287.00 3211.28 65.60 o 5 0 6 65.30 61.02 2.90 o 6 0 6 13.50 15.74 3.50 o 7 0 6 4.80 6.46 4.10 o 8 0 6 24.30 24.84 6.10 o 0 1 6 513.10 582.40 12.30 o 1 1 6 1101.45 1082.00 20.32 o 2 1 6 1096.55 1081.51 22.31 o 3 1 6 288.95 286.39 5.76 o 4 1 6 990.50 992.01 22.03 o 5 1 6 620.55 640.73 18.46 o 6 1 6 5.15 1.42 4.08 o 7 1 6 50.80 55.50 6.11 o 8 1 6 52.75 49.39 7.87 o 0 2 6 1207.70 1282.04 24.10 o 1 2 6 73.20 71.60 2.10 o 2 2 6 4979.15 4876.01 96.40 o 3 2 6 342.15 337.69 8.06 o 4 2 6 81.85 82.03 2.91 o 5 2 6 767.90 769.43 23.16 o 6 2 6 68.05 82.22 4.88 o 7 2 6 22.55 20.25 4.63 o 8 2 6 28.15 30.46 6.07 o 0 3 6 1.60 0.13 1.10 o 1 3 6 1657.55 1571.66 37.71 o 2 3 6 3088.90 3022.83 60.09 o 3 3 6 40.90 42.73 1.98 o 4 3 6 680.10 671.52 16.95 o 5 3 6 116.45 130.04 4.90 o 6 3 6 365.05 397.16 18.44 o 7 3 6 13.35 15.46 4.38 o 8 3 6 11.20 5.86 5.90 o 0 4 6 2.40 2.51 0.60 o 1 4 6 714.70 729.55 15.23 o 2 4 6 174.05 154.16 3.75 o 3 4 6 30.20 22.03 1.76 o 4 4 6 1683.00 1682.41 46.61 o 5 4 6 189.15 198.88 7.00 o 6 4 6 94.15 85.70 7.06 o 7 4 6 -1.20 5.60 4.45 o 8 4 6 24.70 21.04 6.70 o 0 5 6 102.40 105.71 2.50 o 1 5 6 1814.05 1709.03 32.62 o 2 5 6 733.90 716.55 14.26 o 3 5 6 241.70 241.81 6.28 o 4 5 6 183.35 174.67 6.30 o 5 5 6 450.95 450.95 15.63 o 6 5 6 79.45 93.45 6.37 o 7 5 6 30.90 40.56 5.40 o 8 5 6 35.40 24.65 7.50 o 0 6 6 28.80 29.57 1.30 o 1 6 6 398.45 399.92 7.23 o 2 6 6 515.00 517.03 11.36 o 3 6 6 629.90 627.39 16.12 o 4 6 6 307.60 302.58 10.15 o 5 6 6 433.85 479.33 15.56 o 6 6 6 -0.50 2.05 5.37 o 7 6 6 34.30 24.92 5.50 o 0 7 6 1.00 2.16 1.20 o 1 7 6 466.85 472.18 9.49 o 2 7 6 1034.75 1007.81 21.66 o 3 7 6 328.85 303.11 10.21 o 4 7 6 277.90 287.93 9.75 o 5 7 6 54.70 52.92 4.75 o 6 7 6 101.30 89.31 7.10 o 7 7 6 36.30 41.40 6.80 o 0 8 6 38.40 31.39 1.20 o 1 8 6 709.10 719.01 14.54 o 2 8 6 76.10 74.20 2.47 o 3 8 6 10.50 13.41 1.37 o 4 8 6 419.70 398.46 12.81 o 5 8 6 231.30 218.58 14.10 o 6 8 6 100.30 97.76 7.40 o 7 8 6 51.70 55.34 7.80 o 0 9 6 523.30 541.70 9.80 o 1 9 6 494.40 539.02 12.86 o 2 9 6 303.25 293.45 7.72 o 3 9 6 26.60 29.06 2.66 o 4 9 6 71.00 76.81 4.85 o 5 9 6 104.10 105.57 7.18 o 6 9 6 13.40 8.24 4.60 o 7 9 6 165.20 164.14 12.90 o 0 10 6 26.10 32.68 1.90 o 1 10 6 670.10 689.05 15.98 o 2 10 6 151.10 142.21 5.25 o 3 10 6 292.05 321.89 10.07 o 4 10 6 12.15 15.43 3.21 o 5 10 6 116.00 99.26 9.30 o 6 10 6 227.00 212.04 15.80 o 0 11 6 4.00 1.14 2.10 o 1 11 6 401.85 410.72 10.50 o 2 11 6 226.00 235.45 7.48 o 3 11 6 279.45 243.81 9.95 o 4 11 6 12.10 12.57 2.76 o 5 11 6 42.90 52.60 5.60 o 6 11 6 3.10 2.24 4.90 o 0 12 6 22.10 23.29 2.90 o 1 12 6 325.40 331.70 11.21 o 2 12 6 160.30 158.01 6.01 o 3 12 6 13.90 13.43 3.00 o 4 12 6 73.25 76.95 5.52 o 5 12 6 134.20 143.07 10.04 o 0 13 6 18.70 20.78 2.90 o 1 13 6 102.20 97.42 5.46 o 2 13 6 140.35 142.91 5.94 o 3 13 6 81.65 85.61 6.01 o 4 13 6 14.80 14.39 4.82 o 5 13 6 53.95 59.48 6.15 o 0 14 6 69.60 60.10 4.70 o 1 14 6 113.80 102.95 6.15 o 2 14 6 106.20 101.32 6.27 o 3 14 6 0.20 1.55 4.90 o 4 14 6 85.35 74.76 7.54 o 0 15 6 249.90 218.77 12.50 o 1 15 6 329.60 315.16 15.01 o 2 15 6 45.70 48.59 4.29 o 3 15 6 27.10 29.01 4.40 o 0 16 6 512.60 505.69 22.00 o 1 16 6 82.25 80.10 8.32 o 2 16 6 98.50 85.03 9.87 o 1 0 7 320.20 264.61 7.00 o 2 0 7 60.30 57.93 1.90 o 3 0 7 711.50 711.96 15.10 o 4 0 7 2973.50 2926.19 65.40 o 5 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7 56.30 57.72 5.28 o 7 4 7 88.40 99.18 8.80 o 8 4 7 51.50 54.60 8.60 o 0 5 7 817.90 869.24 14.40 o 1 5 7 149.50 135.41 3.71 o 2 5 7 121.75 130.20 3.31 o 3 5 7 149.50 141.12 5.18 o 4 5 7 168.90 174.32 6.10 o 5 5 7 251.95 249.57 9.85 o 6 5 7 70.70 69.83 6.16 o 7 5 7 17.90 21.06 6.90 o 0 6 7 0.10 0.08 0.38 o 1 6 7 24.00 24.02 1.53 o 2 6 7 77.00 88.61 2.70 o 3 6 7 332.80 345.82 10.15 o 4 6 7 958.75 982.96 31.90 o 5 6 7 52.75 51.88 4.61 o 6 6 7 109.70 98.45 9.10 o 7 6 7 1.50 1.17 5.00 o 0 7 7 601.70 612.90 13.40 o 1 7 7 206.70 207.29 5.09 o 2 7 7 249.25 242.00 7.10 o 3 7 7 852.50 907.07 25.70 o 4 7 7 462.95 497.15 14.78 o 5 7 7 8.60 5.73 3.90 o 6 7 7 73.90 74.67 7.60 o 7 7 7 192.30 182.59 14.60 o 0 8 7 976.40 936.95 17.90 o 1 8 7 559.45 588.46 12.29 o 2 8 7 257.00 261.50 6.32 o 3 8 7 235.65 239.43 10.08 o 4 8 7 352.35 369.39 15.14 o 5 8 7 151.50 158.82 9.41 o 6 8 7 24.00 31.09 5.70 o 7 8 7 95.30 97.39 10.40 o 0 9 7 1919.60 1974.96 35.00 o 1 9 7 773.80 769.78 17.75 o 2 9 7 110.10 119.80 4.00 o 3 9 7 202.25 208.98 7.45 o 4 9 7 18.05 24.66 3.32 o 5 9 7 30.10 27.22 6.60 o 6 9 7 71.40 70.70 7.30 o 0 10 7 18.60 23.31 2.00 o 1 10 7 438.05 473.97 11.61 o 2 10 7 647.65 659.87 17.20 o 3 10 7 201.60 204.39 8.10 o 4 10 7 9.10 8.99 3.47 o 5 10 7 213.80 200.25 13.70 o 6 10 7 73.70 64.75 8.60 o 0 11 7 321.60 311.81 10.60 o 1 11 7 525.45 534.23 12.85 o 2 11 7 194.00 225.40 6.52 o 3 11 7 279.05 263.39 10.91 o 4 11 7 -1.30 2.84 3.21 o 5 11 7 124.20 118.71 10.45 o 6 11 7 2.90 11.20 5.70 o 0 12 7 2.10 0.58 2.30 o 1 12 7 233.90 236.44 9.36 o 2 12 7 203.30 199.83 7.30 o 3 12 7 40.40 41.02 5.16 o 4 12 7 10.95 9.27 4.67 o 5 12 7 14.55 18.82 5.94 o 0 13 7 2.00 0.94 3.40 o 1 13 7 195.35 192.86 7.91 o 2 13 7 5.80 4.79 3.26 o 3 13 7 110.50 105.03 7.68 o 4 13 7 10.95 12.82 4.10 o 5 13 7 53.80 60.34 7.84 o 0 14 7 135.60 136.28 6.90 o 1 14 7 6.45 12.48 3.00 o 2 14 7 51.00 42.34 4.55 o 3 14 7 199.30 198.51 13.98 o 4 14 7 70.65 76.60 6.65 o 0 15 7 243.30 258.29 12.70 o 1 15 7 50.00 54.93 4.70 o 2 15 7 116.55 108.72 7.30 o 3 15 7 5.90 7.14 4.60 o 0 16 7 3.70 4.83 3.90 o 1 16 7 358.95 327.46 20.40 o 0 0 8 935.50 941.67 30.60 o 1 0 8 18.20 16.11 1.30 o 2 0 8 108.90 93.71 2.90 o 3 0 8 1122.60 1108.86 25.20 o 4 0 8 372.40 391.41 10.00 o 5 0 8 292.70 305.69 9.40 o 6 0 8 22.40 12.84 4.20 o 7 0 8 4.30 2.86 4.30 o 0 1 8 3940.50 3773.08 84.10 o 1 1 8 343.00 336.59 7.25 o 2 1 8 647.55 657.83 13.36 o 3 1 8 186.90 165.99 4.95 o 4 1 8 958.35 976.94 23.14 o 5 1 8 438.20 451.66 13.84 o 6 1 8 182.65 171.41 10.20 o 7 1 8 23.00 19.79 6.08 o 8 1 8 14.30 10.34 6.15 o 0 2 8 318.80 352.48 7.00 o 1 2 8 811.90 756.42 23.50 o 2 2 8 934.20 898.05 19.21 o 3 2 8 74.65 65.17 2.45 o 4 2 8 19.25 19.41 1.80 o 5 2 8 100.00 109.09 4.71 o 6 2 8 90.05 91.49 7.34 o 7 2 8 33.40 25.55 6.20 o 8 2 8 82.90 78.03 9.70 o 0 3 8 398.30 389.63 8.80 o 1 3 8 846.50 792.71 23.12 o 2 3 8 885.25 851.35 19.05 o 3 3 8 139.95 132.63 3.75 o 4 3 8 226.00 244.02 6.86 o 5 3 8 80.25 85.09 4.25 o 6 3 8 79.05 86.29 6.41 o 7 3 8 98.10 95.03 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