#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/21/2212158.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212158_Fobs loop_ _publ_author_name 'Rodr\'iguez de Barbar\'in, Cecilia' 'Bern\`es, Sylvain' 'N\'ajera, Blanca' 'Elizondo, Perla' 'Cerda, Patricia' _publ_section_title ; N,N'-Bis(2-aminobenzyl)ethane-1,2-diamine ; _journal_coeditor_code FL2086 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o549 _journal_page_last o550 _journal_volume 63 _journal_year 2007 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9737 _cell_length_b 22.7293 _cell_length_c 6.3837 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file fl2086Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PC31 in Pccn Final refinement without Abs. corrections' _shelx_refln_list_code 4 _shelx_f_calc_maximum 83.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 261.62 240.54 7.53 o 6 0 0 8.24 4.23 0.62 o 8 0 0 1.35 1.33 0.51 o 10 0 0 29.55 30.40 1.09 o 12 0 0 1.27 1.91 0.84 o 1 1 0 323.08 251.13 8.86 o 3 1 0 939.90 714.58 11.91 o 5 1 0 411.09 368.69 7.30 o 7 1 0 17.40 13.16 0.51 o 9 1 0 0.00 0.33 0.36 o 11 1 0 8.45 7.65 0.80 o 0 2 0 862.27 720.96 6.10 o 2 2 0 321.52 261.17 5.64 o 4 2 0 2327.28 2061.00 22.20 o 6 2 0 938.44 927.56 15.87 o 8 2 0 0.72 0.97 0.47 o 10 2 0 25.01 21.39 1.01 o 12 2 0 12.96 11.46 1.33 o 1 3 0 1755.47 1601.63 59.27 o 3 3 0 1944.75 1555.18 17.24 o 5 3 0 2001.53 1884.39 24.23 o 7 3 0 98.41 112.65 3.53 o 9 3 0 126.78 139.51 4.48 o 11 3 0 0.00 0.12 0.81 o 2 4 0 4.93 4.44 0.27 o 4 4 0 337.63 277.70 8.48 o 6 4 0 19.44 12.34 0.64 o 8 4 0 135.16 122.29 4.93 o 10 4 0 59.88 57.80 2.47 o 12 4 0 0.11 -1.12 1.12 o 1 5 0 0.33 0.47 0.13 o 3 5 0 1518.69 1281.43 16.61 o 5 5 0 97.31 81.62 3.01 o 7 5 0 126.63 118.91 5.06 o 9 5 0 0.81 -0.55 0.55 o 11 5 0 27.96 29.75 1.68 o 0 6 0 2266.98 1969.29 17.50 o 2 6 0 631.17 554.93 10.21 o 4 6 0 1494.35 1396.67 19.81 o 6 6 0 113.52 115.98 3.90 o 8 6 0 248.22 244.11 6.65 o 10 6 0 66.95 74.79 2.62 o 12 6 0 97.43 114.98 3.07 o 1 7 0 216.40 196.32 4.28 o 3 7 0 690.21 574.56 11.99 o 5 7 0 29.39 26.14 0.96 o 7 7 0 216.38 199.95 6.43 o 9 7 0 61.22 55.56 1.83 o 11 7 0 19.99 21.53 1.50 o 0 8 0 5675.21 5516.60 35.70 o 2 8 0 71.21 55.97 2.22 o 4 8 0 9.14 8.37 0.50 o 6 8 0 93.67 95.67 3.16 o 8 8 0 36.22 35.82 1.19 o 10 8 0 3.12 1.99 0.63 o 12 8 0 22.73 28.98 1.89 o 1 9 0 174.19 165.61 7.83 o 3 9 0 206.42 190.34 7.47 o 5 9 0 59.61 47.17 1.93 o 7 9 0 866.56 819.45 12.26 o 9 9 0 172.91 170.97 4.19 o 11 9 0 29.37 29.82 1.65 o 0 10 0 55.75 48.46 2.03 o 2 10 0 826.79 747.05 14.88 o 4 10 0 167.59 172.11 7.35 o 6 10 0 189.33 179.10 6.30 o 8 10 0 82.25 74.63 3.37 o 10 10 0 4.94 4.62 0.63 o 12 10 0 7.48 7.90 1.46 o 1 11 0 391.24 331.98 10.39 o 3 11 0 201.05 183.72 7.86 o 5 11 0 4.23 4.55 0.50 o 7 11 0 699.57 668.54 10.14 o 9 11 0 128.18 120.16 3.28 o 11 11 0 2.23 1.39 0.84 o 0 12 0 81.48 70.75 2.81 o 2 12 0 1591.09 1525.41 21.62 o 4 12 0 209.19 207.34 7.41 o 6 12 0 355.34 343.46 7.90 o 8 12 0 149.25 160.83 4.29 o 10 12 0 34.12 41.75 1.86 o 1 13 0 116.29 103.06 4.44 o 3 13 0 57.00 63.59 2.67 o 5 13 0 0.27 2.83 0.55 o 7 13 0 3.94 3.32 0.60 o 9 13 0 1.80 0.97 0.54 o 11 13 0 21.73 24.68 1.71 o 0 14 0 837.60 770.01 14.80 o 2 14 0 24.89 21.04 0.87 o 4 14 0 52.40 51.58 2.05 o 6 14 0 8.03 7.31 0.71 o 8 14 0 98.49 100.95 3.37 o 10 14 0 3.78 2.54 0.90 o 1 15 0 3.83 3.79 0.34 o 3 15 0 267.89 260.10 7.57 o 5 15 0 3.11 4.15 0.57 o 7 15 0 154.47 155.41 4.22 o 9 15 0 42.68 47.99 2.07 o 11 15 0 2.03 1.04 1.04 o 0 16 0 2.79 2.21 0.47 o 2 16 0 0.59 0.84 0.41 o 4 16 0 10.12 9.21 0.70 o 6 16 0 0.66 -0.25 0.47 o 8 16 0 6.22 1.77 0.57 o 10 16 0 15.31 18.12 1.56 o 1 17 0 23.11 24.28 0.73 o 3 17 0 45.49 45.28 1.70 o 5 17 0 23.28 21.82 1.01 o 7 17 0 0.97 0.00 0.50 o 9 17 0 7.43 6.78 1.22 o 0 18 0 7.95 6.29 0.63 o 2 18 0 89.00 85.62 4.20 o 4 18 0 264.68 253.03 6.05 o 6 18 0 13.05 9.54 0.78 o 8 18 0 23.25 18.48 1.38 o 10 18 0 2.16 1.06 1.72 o 1 19 0 63.68 62.50 2.43 o 3 19 0 0.36 0.68 0.47 o 5 19 0 49.01 42.78 1.43 o 7 19 0 4.72 2.82 0.56 o 9 19 0 8.73 7.23 1.19 o 0 20 0 1085.80 1114.24 12.73 o 2 20 0 164.45 163.76 4.74 o 4 20 0 22.47 20.18 0.99 o 6 20 0 29.55 28.40 1.15 o 8 20 0 1.94 0.58 0.82 o 1 21 0 7.14 8.32 0.60 o 3 21 0 45.71 47.26 1.56 o 5 21 0 25.15 22.94 1.01 o 7 21 0 16.28 16.46 1.29 o 9 21 0 8.08 8.90 1.37 o 0 22 0 920.11 995.02 10.27 o 2 22 0 124.08 122.54 3.63 o 4 22 0 4.15 2.77 0.60 o 6 22 0 0.27 0.55 0.91 o 8 22 0 0.38 0.69 0.91 o 1 23 0 11.38 12.37 0.65 o 3 23 0 26.34 31.53 1.16 o 5 23 0 58.48 58.62 2.11 o 7 23 0 1.44 0.01 0.85 o 0 24 0 374.67 412.27 5.64 o 2 24 0 61.70 65.01 2.33 o 4 24 0 16.33 14.98 1.29 o 6 24 0 13.62 10.53 1.38 o 1 25 0 4.02 3.94 0.73 o 3 25 0 2.55 3.41 0.88 o 5 25 0 8.14 7.35 1.18 o 0 26 0 55.54 61.56 2.25 o 2 26 0 6.43 5.32 1.08 o 4 26 0 2.67 1.84 0.92 o 6 26 0 3.52 -0.01 1.04 o 1 27 0 2.09 1.17 0.66 o 3 27 0 3.82 4.04 0.98 o 5 27 0 0.11 -0.33 0.98 o 0 28 0 1.25 0.92 0.90 o 2 28 0 0.90 0.53 0.96 o 4 28 0 9.86 6.28 1.32 o 1 29 0 0.18 0.66 0.85 o 1 1 1 902.03 977.73 12.76 o 2 1 1 1934.80 1861.49 14.45 o 3 1 1 7046.84 5726.16 1514.48 o 4 1 1 370.47 310.11 8.30 o 5 1 1 800.38 731.19 24.64 o 6 1 1 0.13 0.07 0.18 o 7 1 1 193.23 171.93 6.20 o 8 1 1 8.92 5.42 0.42 o 9 1 1 15.61 19.16 0.78 o 10 1 1 6.98 4.34 0.63 o 11 1 1 12.37 9.04 0.56 o 12 1 1 4.21 4.24 0.79 o 1 2 1 5.53 5.17 0.13 o 2 2 1 324.22 270.69 4.51 o 3 2 1 978.68 879.47 20.47 o 4 2 1 1090.63 984.41 43.20 o 5 2 1 361.68 380.86 23.84 o 6 2 1 18.63 24.32 0.82 o 7 2 1 1.50 2.29 0.53 o 8 2 1 4.05 2.53 0.95 o 9 2 1 2.30 1.31 0.69 o 10 2 1 63.13 69.41 3.78 o 11 2 1 28.10 28.41 2.08 o 12 2 1 0.91 1.94 0.79 o 2 3 1 1013.32 876.66 8.59 o 3 3 1 47.14 38.28 2.20 o 4 3 1 14.24 10.06 0.57 o 5 3 1 320.02 292.63 14.92 o 6 3 1 2.14 1.50 0.82 o 7 3 1 34.78 32.90 1.06 o 8 3 1 111.71 102.07 3.84 o 9 3 1 62.85 64.97 1.54 o 10 3 1 35.00 34.61 1.60 o 11 3 1 10.46 12.45 0.86 o 12 3 1 0.36 -0.63 0.63 o 2 4 1 3606.12 3611.71 131.47 o 3 4 1 26.14 27.12 0.84 o 4 4 1 118.17 112.75 3.53 o 5 4 1 145.69 126.41 8.68 o 6 4 1 19.18 20.59 0.58 o 7 4 1 42.40 37.38 1.11 o 8 4 1 0.03 -0.01 0.49 o 9 4 1 7.11 7.54 0.54 o 10 4 1 0.59 0.19 0.36 o 11 4 1 3.00 5.19 0.82 o 12 4 1 28.35 34.37 3.84 o 1 5 1 547.67 534.35 6.53 o 2 5 1 340.52 292.86 7.93 o 3 5 1 80.40 63.14 1.63 o 4 5 1 295.95 256.00 9.04 o 5 5 1 27.48 29.37 0.88 o 6 5 1 0.45 0.31 0.46 o 7 5 1 68.46 57.55 1.44 o 8 5 1 70.09 71.63 6.61 o 9 5 1 46.07 48.83 1.16 o 10 5 1 16.41 15.12 0.88 o 11 5 1 1.08 -0.71 0.71 o 12 5 1 2.09 4.35 0.91 o 1 6 1 2080.22 2096.30 42.86 o 2 6 1 48.68 35.96 1.02 o 3 6 1 591.14 522.46 39.16 o 4 6 1 62.69 65.32 3.75 o 5 6 1 3.54 2.96 0.54 o 6 6 1 587.80 544.87 21.68 o 7 6 1 66.56 65.05 1.67 o 8 6 1 531.74 508.08 23.95 o 9 6 1 36.03 33.41 1.26 o 10 6 1 52.10 51.59 2.07 o 11 6 1 8.33 7.12 0.76 o 12 6 1 1.62 0.40 1.39 o 1 7 1 427.39 466.25 9.13 o 2 7 1 0.31 0.63 0.18 o 3 7 1 1023.12 980.75 46.88 o 4 7 1 368.06 317.31 7.04 o 5 7 1 21.32 23.65 1.89 o 6 7 1 89.02 85.20 4.30 o 7 7 1 246.51 226.55 8.70 o 8 7 1 7.12 5.56 1.85 o 9 7 1 193.26 196.41 8.23 o 10 7 1 14.32 11.64 2.53 o 11 7 1 7.58 9.32 0.85 o 12 7 1 0.54 -0.92 1.08 o 1 8 1 139.34 139.19 2.87 o 2 8 1 2.08 4.20 1.27 o 3 8 1 81.98 88.25 5.47 o 4 8 1 441.89 415.70 24.06 o 5 8 1 85.10 63.32 2.39 o 6 8 1 121.43 97.65 3.08 o 7 8 1 227.57 204.42 6.84 o 8 8 1 75.23 66.80 4.53 o 9 8 1 42.50 43.83 2.09 o 10 8 1 2.20 1.08 0.96 o 11 8 1 1.22 1.43 0.71 o 12 8 1 7.22 5.05 2.99 o 1 9 1 203.73 214.93 5.85 o 2 9 1 202.58 186.70 9.83 o 3 9 1 2019.59 2106.40 94.86 o 4 9 1 28.37 31.22 1.88 o 5 9 1 0.33 0.91 0.36 o 6 9 1 79.93 74.26 4.35 o 7 9 1 55.20 50.11 2.38 o 8 9 1 4.46 4.75 1.90 o 9 9 1 0.27 -0.07 0.36 o 10 9 1 4.93 4.66 1.59 o 11 9 1 2.28 4.43 0.79 o 12 9 1 12.03 13.11 2.95 o 1 10 1 1815.62 1764.18 36.80 o 2 10 1 106.66 111.06 11.20 o 3 10 1 492.36 423.16 14.19 o 4 10 1 737.59 686.86 47.18 o 5 10 1 0.31 0.57 0.28 o 6 10 1 166.30 162.08 4.20 o 7 10 1 73.03 75.92 2.21 o 8 10 1 131.86 131.00 3.04 o 9 10 1 0.01 -0.28 0.35 o 10 10 1 20.42 23.64 1.08 o 11 10 1 32.65 42.83 3.69 o 12 10 1 2.98 1.89 1.94 o 1 11 1 48.32 57.12 1.17 o 2 11 1 86.18 67.68 6.52 o 3 11 1 284.21 265.66 10.85 o 4 11 1 0.24 0.33 0.29 o 5 11 1 8.80 8.72 1.13 o 6 11 1 0.83 -0.05 0.35 o 7 11 1 4.41 4.39 1.27 o 8 11 1 0.04 -0.11 0.55 o 9 11 1 2.03 1.80 1.33 o 10 11 1 1.92 1.70 1.71 o 11 11 1 0.42 -0.08 0.80 o 1 12 1 179.46 180.79 6.72 o 2 12 1 1.87 1.33 1.07 o 3 12 1 56.53 54.40 6.26 o 4 12 1 394.16 368.70 23.68 o 5 12 1 2.69 2.10 0.73 o 6 12 1 3.24 1.29 0.37 o 7 12 1 2.90 1.56 0.41 o 8 12 1 0.14 0.33 0.45 o 9 12 1 0.36 0.83 0.54 o 10 12 1 14.48 12.97 1.66 o 11 12 1 5.20 4.73 1.08 o 1 13 1 65.82 84.84 2.07 o 2 13 1 155.99 144.67 4.55 o 3 13 1 767.66 762.16 32.52 o 4 13 1 3.99 4.03 0.38 o 5 13 1 6.70 7.18 0.46 o 6 13 1 20.87 17.73 1.78 o 7 13 1 1.97 3.42 0.74 o 8 13 1 11.47 8.68 2.34 o 9 13 1 51.60 62.83 3.12 o 10 13 1 7.41 5.80 1.79 o 11 13 1 6.08 6.69 2.01 o 1 14 1 41.92 48.24 2.55 o 2 14 1 31.87 31.36 2.73 o 3 14 1 105.08 110.41 3.29 o 4 14 1 3.37 2.45 1.42 o 5 14 1 8.42 8.14 0.82 o 6 14 1 231.88 211.54 8.95 o 7 14 1 61.03 62.29 3.08 o 8 14 1 166.39 165.57 2.64 o 9 14 1 0.21 0.41 0.63 o 10 14 1 9.91 7.89 1.74 o 11 14 1 15.14 20.48 1.64 o 1 15 1 105.54 101.54 2.33 o 2 15 1 5.61 5.12 1.21 o 3 15 1 12.63 12.46 1.03 o 4 15 1 96.45 89.90 3.33 o 5 15 1 41.39 40.83 1.47 o 6 15 1 44.98 40.19 1.55 o 7 15 1 68.11 76.86 2.50 o 8 15 1 0.74 0.79 0.43 o 9 15 1 65.61 66.36 3.83 o 10 15 1 2.04 0.69 0.61 o 11 15 1 0.62 -0.45 0.91 o 1 16 1 34.15 31.12 1.26 o 2 16 1 13.54 15.19 1.09 o 3 16 1 17.24 16.52 0.61 o 4 16 1 82.29 79.76 3.58 o 5 16 1 1.66 2.25 0.88 o 6 16 1 14.95 13.15 1.92 o 7 16 1 34.71 35.18 0.99 o 8 16 1 22.43 20.67 2.26 o 9 16 1 16.58 17.65 0.98 o 10 16 1 5.87 3.79 1.96 o 1 17 1 454.34 451.71 14.98 o 2 17 1 0.67 0.56 0.34 o 3 17 1 34.45 33.41 2.36 o 4 17 1 0.36 0.84 0.44 o 5 17 1 1.85 2.57 0.38 o 6 17 1 1.35 0.97 0.42 o 7 17 1 12.24 12.50 1.50 o 8 17 1 0.33 -0.71 0.71 o 9 17 1 4.68 7.10 2.62 o 10 17 1 0.05 -0.41 0.62 o 1 18 1 416.45 413.14 9.26 o 2 18 1 70.15 69.52 3.63 o 3 18 1 69.58 70.78 1.61 o 4 18 1 49.57 46.59 1.71 o 5 18 1 0.01 0.10 0.33 o 6 18 1 29.92 23.49 1.92 o 7 18 1 12.28 10.99 1.88 o 8 18 1 35.13 35.59 5.25 o 9 18 1 7.36 7.71 3.69 o 10 18 1 18.83 23.71 1.28 o 1 19 1 132.27 134.21 2.54 o 2 19 1 1.30 0.63 0.37 o 3 19 1 75.50 71.85 2.81 o 4 19 1 20.53 19.85 3.65 o 5 19 1 0.05 0.34 0.34 o 6 19 1 0.02 0.00 0.64 o 7 19 1 28.90 31.75 1.88 o 8 19 1 24.06 28.12 3.17 o 9 19 1 9.26 8.88 2.22 o 1 20 1 87.55 92.57 4.11 o 2 20 1 0.29 0.45 0.34 o 3 20 1 4.19 4.12 1.53 o 4 20 1 23.33 25.39 1.81 o 5 20 1 16.06 14.87 0.63 o 6 20 1 13.42 11.32 2.18 o 7 20 1 0.41 0.57 0.68 o 8 20 1 3.47 2.28 1.04 o 9 20 1 0.14 -0.43 0.68 o 1 21 1 96.98 108.88 2.77 o 2 21 1 42.24 39.40 4.57 o 3 21 1 139.46 132.44 4.70 o 4 21 1 5.58 5.04 1.92 o 5 21 1 59.19 52.58 1.57 o 6 21 1 0.97 1.15 0.82 o 7 21 1 11.89 12.84 1.34 o 8 21 1 0.00 0.19 0.58 o 1 22 1 3.61 1.65 0.86 o 2 22 1 2.98 1.07 0.43 o 3 22 1 14.94 15.78 2.47 o 4 22 1 8.90 6.69 1.07 o 5 22 1 4.65 5.11 2.14 o 6 22 1 0.03 0.83 0.58 o 7 22 1 0.00 1.00 0.57 o 8 22 1 0.13 1.24 0.88 o 1 23 1 21.96 20.92 1.25 o 2 23 1 1.13 0.82 0.36 o 3 23 1 16.54 18.30 1.25 o 4 23 1 0.04 0.22 0.31 o 5 23 1 0.19 1.01 0.63 o 6 23 1 0.02 0.15 0.56 o 7 23 1 0.01 0.14 0.55 o 1 24 1 10.17 10.20 1.52 o 2 24 1 27.93 29.72 2.01 o 3 24 1 11.81 10.98 0.83 o 4 24 1 1.35 1.34 0.67 o 5 24 1 2.07 2.00 0.68 o 6 24 1 0.68 2.52 0.90 o 7 24 1 0.33 0.87 0.73 o 1 25 1 50.73 53.30 2.03 o 2 25 1 23.74 22.98 4.93 o 3 25 1 7.90 7.98 1.92 o 4 25 1 6.69 4.25 2.39 o 5 25 1 10.91 10.59 1.61 o 6 25 1 0.15 -0.58 0.64 o 1 26 1 13.53 11.65 2.07 o 2 26 1 5.33 6.44 0.87 o 3 26 1 2.47 0.85 0.76 o 4 26 1 1.24 1.37 0.74 o 5 26 1 3.79 1.99 1.33 o 1 27 1 12.93 14.78 2.49 o 2 27 1 0.05 -0.07 0.78 o 3 27 1 7.93 7.86 2.10 o 4 27 1 1.72 2.58 1.43 o 5 27 1 0.74 1.03 1.84 o 1 28 1 32.93 34.84 1.03 o 2 28 1 2.93 3.29 0.79 o 3 28 1 3.42 1.22 0.88 o 1 29 1 8.89 6.98 1.08 o 0 0 2 5193.57 6112.62 277.47 o 1 0 2 541.73 606.38 19.71 o 2 0 2 4.64 6.51 0.64 o 3 0 2 576.92 612.37 8.68 o 4 0 2 42.30 38.63 1.21 o 5 0 2 55.55 57.43 1.64 o 6 0 2 426.54 421.63 10.28 o 7 0 2 34.35 30.50 0.86 o 8 0 2 73.65 84.24 1.86 o 9 0 2 88.25 99.70 2.56 o 10 0 2 76.12 77.11 1.79 o 11 0 2 5.21 5.83 3.35 o 12 0 2 13.21 16.81 4.59 o 0 1 2 3458.08 3948.47 88.79 o 1 1 2 54.21 53.58 1.14 o 2 1 2 296.27 294.93 11.03 o 3 1 2 357.91 341.45 5.23 o 4 1 2 218.63 239.81 4.63 o 5 1 2 66.98 73.51 1.46 o 6 1 2 0.71 1.77 0.49 o 7 1 2 23.64 23.00 0.53 o 8 1 2 54.93 63.93 1.01 o 9 1 2 229.57 233.06 2.57 o 10 1 2 4.55 5.68 1.25 o 11 1 2 23.43 20.83 2.34 o 12 1 2 2.01 2.86 0.56 o 0 2 2 5932.86 7096.07 184.87 o 1 2 2 83.47 97.68 4.18 o 2 2 2 534.85 520.87 21.51 o 3 2 2 992.70 1032.20 28.36 o 4 2 2 243.20 239.45 6.25 o 5 2 2 366.48 337.25 7.09 o 6 2 2 116.55 115.93 6.82 o 7 2 2 3.18 4.16 0.43 o 8 2 2 66.91 59.76 2.14 o 9 2 2 16.59 15.47 1.94 o 10 2 2 24.79 20.67 3.82 o 11 2 2 0.04 0.47 0.59 o 12 2 2 1.64 0.30 0.74 o 0 3 2 549.81 577.93 22.32 o 1 3 2 2740.42 3093.08 20.22 o 2 3 2 6.26 8.25 0.49 o 3 3 2 169.23 162.91 6.20 o 4 3 2 337.85 290.94 6.86 o 5 3 2 48.83 50.03 1.44 o 6 3 2 307.77 274.88 11.50 o 7 3 2 17.52 13.18 0.56 o 8 3 2 258.71 271.79 7.33 o 9 3 2 260.09 263.07 12.03 o 10 3 2 39.20 43.44 3.39 o 11 3 2 15.41 15.41 3.67 o 12 3 2 2.18 0.23 1.80 o 0 4 2 3690.17 4350.78 64.44 o 1 4 2 668.45 696.57 20.32 o 2 4 2 479.48 514.95 11.46 o 3 4 2 622.66 649.64 31.49 o 4 4 2 50.93 53.12 2.25 o 5 4 2 3.01 3.61 0.71 o 6 4 2 54.21 55.02 1.49 o 7 4 2 10.64 9.07 0.60 o 8 4 2 0.11 0.35 0.37 o 9 4 2 0.52 0.51 0.45 o 10 4 2 19.90 17.74 2.81 o 11 4 2 0.53 -0.56 0.96 o 12 4 2 0.40 0.59 1.13 o 0 5 2 728.67 735.01 10.56 o 1 5 2 2370.27 2691.85 39.91 o 2 5 2 280.94 291.58 6.54 o 3 5 2 11.66 11.68 0.57 o 4 5 2 1066.17 1092.76 37.84 o 5 5 2 243.76 238.47 7.36 o 6 5 2 61.52 65.80 1.71 o 7 5 2 2.80 1.15 0.40 o 8 5 2 0.97 0.19 0.36 o 9 5 2 0.07 0.13 0.68 o 10 5 2 3.15 4.23 0.76 o 11 5 2 0.03 -0.79 0.79 o 12 5 2 0.67 0.08 0.75 o 0 6 2 3.96 14.59 10.70 o 1 6 2 189.35 213.31 3.78 o 2 6 2 803.02 764.02 10.21 o 3 6 2 35.91 44.51 1.40 o 4 6 2 141.51 144.44 4.95 o 5 6 2 186.80 190.79 7.24 o 6 6 2 337.24 325.23 24.76 o 7 6 2 18.28 17.94 1.75 o 8 6 2 18.04 14.94 1.64 o 9 6 2 40.31 38.86 3.06 o 10 6 2 0.58 -0.01 0.33 o 11 6 2 0.04 0.65 1.33 o 12 6 2 3.04 2.50 3.26 o 0 7 2 55.16 60.84 1.66 o 1 7 2 1717.29 1835.53 22.57 o 2 7 2 36.13 51.29 1.65 o 3 7 2 922.30 915.63 12.02 o 4 7 2 174.80 164.39 5.02 o 5 7 2 20.97 16.89 0.55 o 6 7 2 8.63 8.01 1.29 o 7 7 2 96.59 92.90 6.27 o 8 7 2 0.16 0.36 0.37 o 9 7 2 0.10 -0.07 0.37 o 10 7 2 11.05 10.99 4.37 o 11 7 2 11.00 12.40 1.37 o 12 7 2 2.16 1.35 0.93 o 0 8 2 1110.30 1374.08 41.80 o 1 8 2 25.73 18.77 0.57 o 2 8 2 2118.98 2326.00 30.86 o 3 8 2 43.06 42.87 1.30 o 4 8 2 2.74 4.06 0.43 o 5 8 2 5.59 4.09 0.86 o 6 8 2 311.87 295.32 5.55 o 7 8 2 0.04 1.08 0.40 o 8 8 2 1.94 1.39 1.41 o 9 8 2 0.26 0.40 0.35 o 10 8 2 2.68 1.89 0.90 o 11 8 2 7.82 9.36 2.10 o 12 8 2 0.01 0.33 0.75 o 0 9 2 1043.74 1181.39 15.50 o 1 9 2 771.06 825.88 9.83 o 2 9 2 1222.43 1379.55 49.61 o 3 9 2 48.53 44.52 1.30 o 4 9 2 592.12 603.24 23.26 o 5 9 2 28.46 29.92 0.84 o 6 9 2 106.26 94.58 5.91 o 7 9 2 183.58 189.62 4.09 o 8 9 2 28.39 31.85 4.42 o 9 9 2 0.52 0.43 0.56 o 10 9 2 2.14 0.84 1.86 o 11 9 2 0.67 -0.70 0.70 o 0 10 2 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7 33.44 32.01 0.98 o 2 8 7 0.17 0.26 0.79 o 3 8 7 4.96 3.79 2.81 o 4 8 7 4.35 3.06 2.56 o 5 8 7 2.58 1.46 0.98 o 6 8 7 1.40 -1.30 1.30 o 1 9 7 9.46 5.99 0.70 o 2 9 7 3.05 1.26 1.05 o 3 9 7 3.67 3.85 1.69 o 4 9 7 3.02 -0.36 0.94 o 5 9 7 3.05 1.46 0.85 o 1 10 7 1.27 1.22 0.64 o 2 10 7 10.51 8.92 1.08 o 3 10 7 7.89 4.64 0.96 o 4 10 7 2.96 1.46 0.90 o 5 10 7 15.31 10.79 2.22 o 1 11 7 0.47 1.18 0.75 o 2 11 7 0.84 0.32 0.89 o 3 11 7 1.60 0.97 0.86 o 4 11 7 0.39 0.05 0.75 o 5 11 7 0.00 0.22 1.54 o 1 12 7 3.30 3.09 1.04 o 2 12 7 0.80 0.24 1.30 o 3 12 7 1.61 0.32 0.84 o 4 12 7 5.37 2.42 0.98 o 1 13 7 3.62 3.06 1.16 o 2 13 7 0.20 -0.78 1.03 o 3 13 7 4.28 2.09 1.77 o 1 14 7 21.00 21.75 1.33 o 2 14 7 0.92 -0.54 1.56 o 3 14 7 7.91 3.26 1.01 o 1 15 7 4.00 3.30 1.71 o 2 15 7 0.02 -0.14 0.93 o 0 0 8 0.68 1.61 0.70 o 1 0 8 0.82 0.25 0.57 o 2 0 8 0.76 -0.79 0.79 o 3 0 8 5.07 2.39 1.83 o 0 1 8 3.68 3.56 1.24 o 1 1 8 0.00 -0.38 0.38 o 2 1 8 4.64 1.77 0.75 o 3 1 8 0.65 0.51 0.68 o 0 2 8 0.73 -0.21 0.74 o 1 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