#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:25:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181042 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/22/2212210.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212210_Fobs loop_ _publ_author_name 'Miyabayashi, Takayuki' 'Hara, Takeshi' 'Yamagata, Tsuneaki' 'Mashima, Kazushi' _publ_section_title ; Chlorido(6-diphenylphosphino-2-pyridonato-\k^2^P,N)(6-diphenylphosphino-2-hydroxypyridine-\k^2^P,N)hydridoiridium(III) chloroform 1.896-solvate ; _journal_coeditor_code HG2140 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m576 _journal_page_last m578 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.284 _cell_angle_gamma 90.000 _cell_length_a 11.2208 _cell_length_b 14.8301 _cell_length_c 23.1875 _exptl_crystal_F_000 1985.28 _reflns_d_resolution_high 0.7002 _cod_data_source_file hg2140Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n(#14) 120K40kV40mA rapid Fri Oct 14 09:20:24 2005' _shelx_refln_list_code 4 _shelx_f_calc_maximum 550.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 73777.16 76241.66 1221.91 o 4 0 0 51833.77 48961.17 705.24 o 6 0 0 56986.80 40783.23 10106.84 o 8 0 0 50586.29 48225.32 817.37 o 10 0 0 11317.93 11827.50 214.61 o 12 0 0 13149.81 12717.16 347.43 o 14 0 0 25707.70 25172.24 645.69 o 2 1 0 524.09 1047.94 10.50 o 3 1 0 328.88 398.41 9.95 o 4 1 0 2412.00 2706.62 28.75 o 5 1 0 7468.00 8732.24 80.13 o 6 1 0 2745.69 2991.65 33.99 o 7 1 0 1676.69 1778.85 45.14 o 8 1 0 824.31 777.99 24.25 o 9 1 0 3.92 76.75 16.10 o 10 1 0 566.43 605.82 27.19 o 11 1 0 632.04 531.58 30.88 o 12 1 0 1700.94 1774.17 74.68 o 13 1 0 0.78 59.82 29.05 o 14 1 0 1754.79 1634.47 69.69 o 15 1 0 11.33 40.87 34.50 o 1 2 0 3789.43 2966.39 15.13 o 2 2 0 142484.39 151699.80 2298.66 o 3 2 0 6959.04 6966.71 50.38 o 4 2 0 1004.25 1325.98 30.06 o 5 2 0 850.18 866.96 17.04 o 6 2 0 88648.46 88392.82 1206.80 o 7 2 0 0.35 39.55 11.45 o 8 2 0 50272.34 52427.26 637.21 o 9 2 0 274.63 281.06 22.10 o 10 2 0 16897.63 17103.64 195.01 o 11 2 0 850.08 960.69 56.48 o 12 2 0 6631.32 7509.69 123.83 o 13 2 0 0.18 25.91 23.89 o 14 2 0 11532.87 11835.89 234.95 o 15 2 0 318.41 257.78 47.38 o 1 3 0 2800.29 3269.09 22.18 o 2 3 0 14329.13 15178.71 98.86 o 3 3 0 19874.67 22176.50 160.95 o 4 3 0 825.17 933.59 17.24 o 5 3 0 3485.21 3440.14 65.65 o 6 3 0 4305.76 4427.75 38.58 o 7 3 0 1165.27 1372.12 44.26 o 8 3 0 28.00 62.94 19.02 o 9 3 0 2932.92 3140.71 92.38 o 10 3 0 931.73 952.75 52.31 o 11 3 0 24.10 16.34 31.10 o 12 3 0 173.82 256.38 44.87 o 13 3 0 171.91 217.90 35.11 o 14 3 0 221.23 220.20 37.07 o 15 3 0 247.60 311.90 53.08 o 0 4 0 135327.89 147015.55 2954.37 o 1 4 0 7854.03 8503.60 49.07 o 2 4 0 25983.59 27521.61 197.30 o 3 4 0 69.63 111.61 8.56 o 4 4 0 56071.60 55825.27 577.72 o 5 4 0 27.42 95.13 9.40 o 6 4 0 49659.85 48748.77 521.64 o 7 4 0 0.32 25.55 10.75 o 8 4 0 72898.27 71848.80 900.95 o 9 4 0 0.06 35.63 15.19 o 10 4 0 18878.38 18723.94 233.21 o 11 4 0 312.82 291.93 28.53 o 12 4 0 7524.52 7538.88 118.78 o 13 4 0 82.05 78.31 27.14 o 14 4 0 12257.14 11894.37 226.07 o 15 4 0 33.52 22.19 34.41 o 1 5 0 12473.31 13321.37 82.17 o 2 5 0 27.56 82.56 6.67 o 3 5 0 1283.79 1405.58 18.43 o 4 5 0 260.90 191.03 11.79 o 5 5 0 125.49 226.46 13.92 o 6 5 0 331.86 328.02 14.45 o 7 5 0 5837.04 5803.01 62.37 o 8 5 0 163.44 205.74 17.46 o 9 5 0 177.49 213.25 22.72 o 10 5 0 572.10 578.19 34.03 o 11 5 0 81.39 55.42 20.64 o 12 5 0 39.63 79.94 26.73 o 13 5 0 44.61 132.48 37.52 o 14 5 0 1140.77 1047.63 105.81 o 15 5 0 402.36 256.39 59.32 o 0 6 0 87160.91 80195.74 1986.86 o 1 6 0 8845.39 9399.07 67.72 o 2 6 0 59444.29 57124.14 507.78 o 3 6 0 3601.11 3752.47 30.32 o 4 6 0 21619.15 21158.59 174.98 o 5 6 0 779.44 827.04 18.58 o 6 6 0 27596.42 26886.51 241.97 o 7 6 0 2704.75 2243.21 124.29 o 8 6 0 25018.59 25751.15 258.15 o 9 6 0 1037.61 1197.47 55.29 o 10 6 0 15017.31 15407.82 183.01 o 11 6 0 115.68 82.33 25.45 o 12 6 0 14510.46 14615.04 263.24 o 13 6 0 453.45 362.63 44.28 o 14 6 0 12375.49 12227.70 265.08 o 15 6 0 394.94 403.65 78.00 o 1 7 0 11907.60 12045.42 92.26 o 2 7 0 2610.90 3002.33 24.59 o 3 7 0 262.81 434.39 11.18 o 4 7 0 739.36 690.15 15.86 o 5 7 0 334.50 270.75 14.23 o 6 7 0 587.77 627.99 19.99 o 7 7 0 3309.57 3738.55 48.44 o 8 7 0 64.14 144.05 18.61 o 9 7 0 46.43 101.12 20.44 o 10 7 0 4.31 56.81 18.72 o 11 7 0 189.73 241.31 34.64 o 12 7 0 32.11 34.28 26.88 o 13 7 0 364.69 379.87 38.38 o 14 7 0 409.17 411.68 73.44 o 15 7 0 312.08 169.90 84.22 o 0 8 0 131003.90 133662.95 3113.74 o 1 8 0 266.93 245.50 13.49 o 2 8 0 56984.33 55995.62 521.42 o 3 8 0 1706.02 1608.64 20.59 o 4 8 0 37385.08 37130.52 331.08 o 5 8 0 68.49 77.66 11.42 o 6 8 0 34244.58 26771.99 2629.72 o 7 8 0 139.11 81.79 14.21 o 8 8 0 15114.06 15265.41 153.48 o 9 8 0 13.63 37.85 15.23 o 10 8 0 17494.31 18361.51 201.44 o 11 8 0 46.85 91.27 22.12 o 12 8 0 14505.31 14180.99 245.24 o 13 8 0 8.11 40.31 28.29 o 14 8 0 8968.70 9251.37 208.49 o 1 9 0 8600.44 8736.64 85.93 o 2 9 0 1150.02 970.06 23.16 o 3 9 0 1926.18 1977.17 30.35 o 4 9 0 2866.81 2711.01 34.76 o 5 9 0 537.47 633.23 36.86 o 6 9 0 2677.66 2739.84 43.60 o 7 9 0 2749.73 2652.17 40.75 o 8 9 0 2.73 33.38 16.96 o 9 9 0 1921.21 2026.52 52.02 o 10 9 0 127.91 82.02 20.77 o 11 9 0 1881.39 1957.85 63.91 o 12 9 0 20.99 44.78 25.14 o 13 9 0 1756.73 1767.06 79.84 o 14 9 0 11.10 8.94 45.06 o 0 10 0 21714.29 21769.46 304.66 o 1 10 0 418.14 359.86 11.37 o 2 10 0 30546.10 29075.47 262.40 o 3 10 0 5208.17 4903.93 42.83 o 4 10 0 43407.90 43830.64 433.01 o 5 10 0 3.24 14.98 11.01 o 6 10 0 38375.96 38045.96 389.45 o 7 10 0 1237.02 1092.14 33.66 o 8 10 0 17113.98 17214.24 176.65 o 9 10 0 81.41 61.35 20.58 o 10 10 0 15223.39 15178.18 203.26 o 11 10 0 35.31 84.14 25.69 o 12 10 0 9028.71 9314.48 177.13 o 13 10 0 2.56 135.86 56.37 o 14 10 0 4113.95 4239.44 147.59 o 1 11 0 601.81 607.82 58.48 o 2 11 0 120.56 200.26 13.37 o 3 11 0 1610.56 1562.67 40.65 o 4 11 0 188.68 249.19 15.44 o 5 11 0 219.04 242.90 18.95 o 6 11 0 288.94 359.05 20.35 o 7 11 0 2159.51 2121.69 43.83 o 8 11 0 1112.16 1191.58 40.93 o 9 11 0 516.01 736.53 36.43 o 10 11 0 406.24 429.26 34.63 o 11 11 0 1873.99 1859.04 66.37 o 12 11 0 3.07 56.16 34.08 o 13 11 0 37.13 155.61 69.28 o 0 12 0 1979.43 2021.58 66.80 o 1 12 0 1044.40 944.12 33.07 o 2 12 0 18113.87 17844.48 189.10 o 3 12 0 821.27 810.57 22.35 o 4 12 0 26188.21 26216.79 240.82 o 5 12 0 1786.50 1579.33 29.61 o 6 12 0 21916.71 21479.02 219.34 o 7 12 0 34.67 77.44 18.37 o 8 12 0 16293.41 16321.49 189.33 o 9 12 0 3007.94 3373.54 73.87 o 10 12 0 14130.61 14479.88 201.84 o 11 12 0 517.61 392.46 45.27 o 12 12 0 9089.84 9067.32 225.54 o 13 12 0 150.24 116.38 62.87 o 1 13 0 1871.67 2061.60 49.56 o 2 13 0 928.74 809.77 81.54 o 3 13 0 5438.74 5334.49 128.95 o 4 13 0 1727.29 1823.80 92.87 o 5 13 0 7493.31 7231.34 74.55 o 6 13 0 416.19 441.85 25.46 o 7 13 0 318.39 386.65 24.68 o 8 13 0 76.24 87.75 19.49 o 9 13 0 1199.78 1349.82 67.02 o 10 13 0 11.39 16.17 21.70 o 11 13 0 1723.56 2003.56 159.22 o 12 13 0 540.31 497.02 55.74 o 0 14 0 16626.67 16472.20 283.00 o 1 14 0 673.49 771.55 55.78 o 2 14 0 23719.47 22921.08 293.55 o 3 14 0 830.66 934.86 41.82 o 4 14 0 17181.34 17336.91 195.43 o 5 14 0 1862.94 2196.45 34.57 o 6 14 0 7257.40 7017.73 84.88 o 7 14 0 242.65 178.95 25.16 o 8 14 0 8655.34 8598.29 132.60 o 9 14 0 1476.25 1292.38 57.25 o 10 14 0 8169.66 8373.56 172.59 o 11 14 0 532.46 1184.49 273.26 o 1 15 0 3701.72 3548.07 77.92 o 2 15 0 35.82 73.29 30.22 o 3 15 0 10217.13 10279.55 197.65 o 4 15 0 671.50 521.72 24.77 o 5 15 0 2978.02 2808.66 63.59 o 6 15 0 156.76 252.04 27.52 o 7 15 0 64.27 118.66 26.28 o 8 15 0 353.10 358.19 33.80 o 9 15 0 344.33 369.98 38.74 o 10 15 0 1.59 7.56 37.68 o 11 15 0 3563.71 3958.73 138.68 o 0 16 0 8358.96 8230.34 187.12 o 1 16 0 4840.66 5049.99 122.63 o 2 16 0 14815.18 15231.04 231.80 o 3 16 0 1704.39 1841.18 83.60 o 4 16 0 13776.58 13677.95 200.63 o 5 16 0 329.47 260.59 47.52 o 6 16 0 14567.49 14614.57 249.28 o 7 16 0 6.48 13.38 29.20 o 8 16 0 7707.03 7485.80 160.84 o 9 16 0 985.44 887.80 64.53 o 10 16 0 5521.17 5824.09 177.66 o 1 17 0 1235.65 1283.60 59.95 o 2 17 0 100.18 130.07 33.34 o 3 17 0 5247.83 5059.38 124.52 o 4 17 0 177.09 183.40 43.47 o 5 17 0 4967.37 4945.37 139.56 o 6 17 0 5.20 -2.60 31.90 o 7 17 0 868.01 700.12 130.30 o 8 17 0 217.12 257.84 65.40 o 9 17 0 1211.38 1332.87 121.81 o 0 18 0 6711.73 6404.61 196.96 o 1 18 0 614.52 714.64 53.84 o 2 18 0 8650.27 8365.25 166.63 o 3 18 0 257.59 327.69 40.76 o 4 18 0 11439.33 11539.49 229.54 o 5 18 0 744.52 685.16 55.12 o 6 18 0 12636.62 12855.11 273.89 o 7 18 0 60.44 53.40 40.52 o 8 18 0 7948.48 8613.06 349.93 o 1 19 0 560.00 579.10 70.73 o 2 19 0 44.74 112.18 45.29 o 3 19 0 3951.67 3997.10 116.51 o 4 19 0 11.33 78.62 44.61 o 5 19 0 4340.38 3941.16 154.49 o 6 19 0 266.62 165.43 43.10 o 7 19 0 327.72 418.80 118.46 o 0 20 0 8879.33 8598.91 317.05 o 1 20 0 83.61 115.08 53.32 o 2 20 0 7777.42 7554.32 207.22 o 3 20 0 6.26 42.17 44.81 o 4 20 0 7231.75 8008.99 202.91 o 5 20 0 11.18 76.70 40.17 o 1 21 0 1385.71 1353.04 88.85 o -15 0 1 773.47 910.12 115.17 o -13 0 1 1305.78 1593.88 234.25 o -11 0 1 3832.06 3702.79 113.90 o -9 0 1 21742.39 23084.85 353.68 o -7 0 1 3249.38 2936.73 51.29 o -5 0 1 4017.85 4334.87 74.00 o -3 0 1 58846.36 61603.41 957.00 o 3 0 1 924.76 1235.86 23.11 o 5 0 1 13122.46 13944.85 164.62 o 7 0 1 13872.16 15920.71 218.55 o 9 0 1 590.24 570.54 30.02 o 11 0 1 8933.58 9541.98 178.20 o 13 0 1 21299.86 21005.99 576.47 o 15 0 1 5105.00 5108.93 242.74 o -15 1 1 11421.99 10952.62 243.32 o -14 1 1 0.73 33.09 26.47 o -13 1 1 16378.08 15995.50 254.54 o -12 1 1 253.81 368.37 39.63 o -11 1 1 9009.43 9101.57 140.57 o -10 1 1 2401.19 2426.52 59.48 o -9 1 1 21874.46 21893.18 251.32 o -8 1 1 1278.28 899.88 32.28 o -7 1 1 68874.94 69794.16 878.29 o -6 1 1 389.71 505.40 19.40 o -5 1 1 30946.00 29264.40 255.79 o -4 1 1 10955.72 11242.57 83.66 o -3 1 1 18424.27 17426.16 123.88 o -2 1 1 1897.92 2016.83 14.98 o 2 1 1 10362.44 10614.34 65.44 o 3 1 1 25224.86 24527.90 187.95 o 4 1 1 3096.95 3552.47 31.23 o 5 1 1 13819.36 12986.05 100.08 o 6 1 1 3734.27 3973.85 38.13 o 7 1 1 25506.36 25906.24 245.77 o 8 1 1 1206.26 864.92 25.07 o 9 1 1 18497.05 18724.84 198.01 o 10 1 1 38.52 57.23 22.89 o 11 1 1 12112.29 12452.44 171.35 o 12 1 1 133.48 141.41 23.31 o 13 1 1 8613.41 8877.99 156.60 o 14 1 1 574.55 629.13 49.34 o 15 1 1 10058.00 9667.39 217.82 o -15 2 1 2530.82 2374.02 164.31 o -14 2 1 1740.16 1792.30 72.06 o -13 2 1 211.25 166.64 32.88 o -12 2 1 3.39 -9.68 19.89 o -11 2 1 6173.06 6156.65 109.10 o -10 2 1 158.61 166.10 25.32 o -9 2 1 9574.46 9459.56 113.31 o -8 2 1 31.91 124.24 16.26 o -7 2 1 6046.22 5739.60 66.63 o -6 2 1 164.18 222.61 21.35 o -5 2 1 11075.68 9771.05 76.58 o -4 2 1 14093.03 14026.72 116.84 o -3 2 1 33104.30 36343.10 326.91 o -2 2 1 7786.04 9389.53 62.97 o -1 2 1 25684.09 30688.42 237.63 o 1 2 1 10037.71 9551.32 50.05 o 2 2 1 25831.67 27412.93 203.93 o 3 2 1 32457.11 31828.86 270.69 o 4 2 1 665.25 628.07 14.32 o 5 2 1 9684.83 8888.22 68.60 o 6 2 1 556.42 601.10 52.95 o 7 2 1 9190.73 8816.58 86.39 o 8 2 1 1221.94 1329.87 32.57 o 9 2 1 612.08 749.92 27.95 o 10 2 1 1787.71 1898.44 41.59 o 11 2 1 3518.16 3148.21 69.63 o 12 2 1 1036.23 1209.73 54.52 o 13 2 1 4078.27 3876.11 97.59 o 14 2 1 33.58 89.37 32.73 o 15 2 1 3726.16 3215.58 232.51 o -15 3 1 9339.08 9360.63 182.86 o -14 3 1 331.37 362.83 41.75 o -13 3 1 11090.64 11503.82 168.73 o -12 3 1 85.15 123.15 28.98 o -11 3 1 5942.61 5838.88 89.22 o -10 3 1 404.72 431.06 23.73 o -9 3 1 31451.20 31900.55 362.92 o -8 3 1 38.12 109.06 25.32 o -7 3 1 65573.29 65224.72 831.00 o -6 3 1 4308.15 4580.14 52.07 o -5 3 1 30136.26 14043.82 4948.25 o -4 3 1 651.35 777.07 22.76 o -3 3 1 1086.59 1156.79 21.04 o -2 3 1 356.92 786.74 10.32 o -1 3 1 31197.72 31919.51 214.94 o 0 3 1 1988.24 2648.33 28.02 o 1 3 1 160268.17 175587.80 2591.43 o 2 3 1 2017.19 2444.55 23.05 o 3 3 1 65315.85 65117.71 729.11 o 4 3 1 25569.99 25503.11 203.80 o 5 3 1 28851.19 27008.41 255.41 o 6 3 1 715.94 787.32 22.24 o 7 3 1 46546.36 45902.39 510.07 o 8 3 1 2259.75 2377.63 38.49 o 9 3 1 34150.88 33343.33 377.07 o 10 3 1 1640.57 1760.48 44.92 o 11 3 1 4360.16 4734.62 102.26 o 12 3 1 558.18 437.31 45.20 o 13 3 1 4593.43 4643.21 96.51 o 14 3 1 42.74 106.94 32.85 o 15 3 1 8735.95 8636.80 223.97 o -15 4 1 2767.57 3047.55 108.19 o -14 4 1 19.15 85.00 36.62 o -13 4 1 666.62 676.60 44.49 o -12 4 1 30.28 53.72 22.76 o -11 4 1 741.73 909.23 39.00 o -10 4 1 159.82 161.90 19.42 o -9 4 1 3550.97 3955.34 58.11 o -8 4 1 5113.58 5201.12 65.91 o -7 4 1 1147.31 1036.97 30.98 o -6 4 1 6.46 60.13 11.84 o -5 4 1 1785.66 1605.46 24.54 o -4 4 1 229.59 506.53 12.88 o -3 4 1 18146.62 17283.56 115.44 o -2 4 1 406.61 304.42 8.38 o -1 4 1 13439.26 13450.33 75.98 o 0 4 1 30080.84 31727.25 252.51 o 1 4 1 12913.65 12525.87 71.84 o 2 4 1 7630.85 8437.42 52.09 o 3 4 1 28464.84 28672.95 225.52 o 4 4 1 3299.38 3732.51 34.73 o 5 4 1 21931.10 22311.72 182.48 o 6 4 1 6025.84 5665.53 55.30 o 7 4 1 15182.35 15238.29 130.38 o 8 4 1 1043.91 1257.70 79.30 o 9 4 1 11097.44 11499.34 123.47 o 10 4 1 284.47 252.45 25.97 o 11 4 1 6072.08 6266.95 90.60 o 12 4 1 2.31 41.77 23.01 o 13 4 1 3305.58 3154.43 87.44 o 14 4 1 589.29 422.29 46.83 o 15 4 1 2274.17 2379.23 108.59 o -15 5 1 10655.42 10225.95 201.18 o -14 5 1 47.67 59.84 33.66 o -13 5 1 17398.51 16966.31 285.84 o -12 5 1 380.78 383.72 30.87 o -11 5 1 9203.15 9266.63 128.97 o -10 5 1 29.87 51.58 18.00 o -9 5 1 24735.21 26093.50 279.50 o -8 5 1 493.46 501.60 23.73 o -7 5 1 66593.84 66138.06 802.37 o -6 5 1 213.50 392.68 16.79 o -5 5 1 26965.49 27579.50 235.39 o -4 5 1 10671.17 11397.26 83.55 o -3 5 1 29841.22 32330.93 326.30 o -2 5 1 5259.38 5171.09 35.00 o -1 5 1 31026.22 29933.66 263.07 o 0 5 1 13593.13 13700.54 88.67 o 1 5 1 116037.79 118356.20 1412.38 o 2 5 1 807.28 959.49 13.58 o 3 5 1 51458.59 50504.01 460.27 o 4 5 1 2363.78 2850.63 29.69 o 5 5 1 33901.79 34313.24 316.94 o 6 5 1 938.34 1049.15 21.88 o 7 5 1 30035.04 29846.72 282.90 o 8 5 1 629.25 612.14 24.94 o 9 5 1 36018.57 35836.79 414.19 o 10 5 1 4003.64 4288.06 66.30 o 11 5 1 10468.34 10618.94 148.45 o 12 5 1 434.97 472.02 35.70 o 13 5 1 6318.02 6341.84 117.45 o 14 5 1 34.92 75.62 34.22 o 15 5 1 7418.65 7773.66 267.99 o -15 6 1 1256.27 1018.85 128.92 o -14 6 1 29.97 52.96 40.38 o -13 6 1 1379.77 1423.92 68.81 o -12 6 1 604.87 535.00 42.07 o -11 6 1 2485.10 2462.72 55.76 o -10 6 1 29.77 48.67 19.11 o -9 6 1 6159.16 6338.98 80.24 o -8 6 1 8601.22 8571.70 94.10 o -7 6 1 10263.00 9767.08 94.36 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