#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/23/2212307.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212307_Fobs loop_ _publ_author_name 'Win, Yip Foo' 'Teoh, Siang Guan' 'Teh, Jeannie Bee-Jan' 'Fun, Hoong-Kun' 'Zakaria, Latiffah' _publ_section_title ; [4-(Diethylamino)benzoato-\kO]triphenyltin(IV) ; _journal_coeditor_code NG2192 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m323 _journal_page_last m325 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.632 _cell_angle_beta 82.117 _cell_angle_gamma 84.260 _cell_length_a 10.8876 _cell_length_b 13.0407 _cell_length_c 17.8896 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.5838 _[local]_cod_data_source_file ng2192Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yfw2_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8942.29 8978.23 133.79 o 3 0 0 151.73 118.76 7.09 o 4 0 0 12.98 1.94 3.65 o 5 0 0 1116.13 1139.19 38.78 o 6 0 0 10499.28 10733.07 207.16 o 7 0 0 718.89 705.62 30.42 o 8 0 0 6727.46 7059.94 152.09 o 9 0 0 5610.37 5513.07 72.13 o 10 0 0 5.80 19.92 3.79 o 11 0 0 288.71 312.87 17.94 o 12 0 0 11.00 15.97 5.25 o 13 0 0 146.44 147.83 19.00 o 14 0 0 2386.09 2502.98 58.33 o 15 0 0 154.39 173.34 15.44 o 16 0 0 11.34 21.51 9.64 o 17 0 0 422.99 461.92 41.61 o 18 0 0 287.89 327.56 57.56 o -18 1 0 135.20 110.37 38.94 o -17 1 0 178.68 179.04 18.16 o -16 1 0 463.26 534.87 27.17 o -15 1 0 2070.86 2186.70 45.03 o -14 1 0 171.05 213.34 23.92 o -13 1 0 320.25 317.47 13.76 o -12 1 0 25.48 34.67 7.62 o -11 1 0 16.63 17.12 4.57 o -10 1 0 1821.72 1744.36 26.65 o -9 1 0 2089.17 1996.77 29.18 o -8 1 0 1261.21 1182.31 20.27 o -7 1 0 12842.31 13117.15 164.18 o -6 1 0 4708.93 4724.82 60.79 o -5 1 0 4454.83 4795.47 70.75 o -4 1 0 5039.27 5418.86 78.88 o -3 1 0 3146.11 3283.74 46.63 o -2 1 0 25905.87 27077.36 390.94 o -1 1 0 48851.18 46166.98 1192.73 o 0 1 0 2061.89 -2.08 1.04 o 1 1 0 8454.42 5563.92 148.42 o 2 1 0 19811.22 20643.43 294.08 o 3 1 0 759.39 811.66 21.27 o 4 1 0 6456.50 6714.69 128.09 o 5 1 0 1.16 0.18 3.97 o 6 1 0 1758.29 1871.22 50.11 o 7 1 0 3623.92 3638.25 85.65 o 8 1 0 15413.22 15745.59 378.33 o 9 1 0 97.25 105.66 6.15 o 10 1 0 1058.02 1187.87 21.74 o 11 1 0 900.58 920.49 23.52 o 12 1 0 76.46 86.31 7.24 o 13 1 0 237.03 206.48 11.66 o 14 1 0 155.06 152.14 10.89 o 15 1 0 2.39 8.80 10.24 o 16 1 0 936.82 913.46 49.92 o 17 1 0 420.13 447.33 34.31 o -18 2 0 59.28 47.52 14.91 o -17 2 0 138.55 147.07 17.77 o -16 2 0 734.66 789.81 25.61 o -15 2 0 367.75 399.74 18.88 o -14 2 0 1636.76 1586.69 37.09 o -13 2 0 446.60 456.65 18.00 o -12 2 0 212.94 204.62 11.55 o -11 2 0 623.85 597.48 22.46 o -10 2 0 22.30 20.99 4.42 o -9 2 0 932.12 877.43 15.24 o -8 2 0 3982.22 3939.09 43.32 o -7 2 0 4042.23 4145.56 46.94 o -6 2 0 5585.34 5728.55 57.77 o -5 2 0 13717.10 13973.82 128.97 o -4 2 0 1431.05 1452.83 23.40 o -3 2 0 863.51 957.95 16.82 o -2 2 0 56.70 37.65 5.83 o -1 2 0 14943.38 15069.84 390.83 o 0 2 0 8253.25 8309.37 154.99 o 1 2 0 34042.74 35833.74 658.45 o 2 2 0 52050.34 55645.54 762.68 o 3 2 0 683.62 878.57 14.75 o 4 2 0 14658.24 15231.01 185.95 o 5 2 0 9.43 6.71 2.12 o 6 2 0 343.03 369.87 8.50 o 7 2 0 2486.79 2427.42 32.72 o 8 2 0 532.22 588.35 21.36 o 9 2 0 547.34 576.77 13.43 o 10 2 0 8409.63 8573.17 84.19 o 11 2 0 27.65 22.42 4.78 o 12 2 0 996.21 1017.55 22.59 o 13 2 0 185.60 188.09 11.23 o 14 2 0 100.51 101.50 20.48 o 15 2 0 455.37 436.21 17.45 o 16 2 0 1024.79 1031.00 38.05 o 17 2 0 54.17 62.01 15.21 o -18 3 0 61.70 66.84 24.85 o -17 3 0 8.73 8.26 15.20 o -16 3 0 28.35 29.34 13.33 o -15 3 0 1620.60 1679.23 41.07 o -14 3 0 731.19 742.84 25.34 o -13 3 0 132.48 140.43 13.65 o -12 3 0 1134.53 1113.38 32.13 o -11 3 0 324.72 309.09 13.11 o -10 3 0 23.46 12.23 4.74 o -9 3 0 51.38 55.48 7.03 o -8 3 0 2940.06 2902.17 41.97 o -7 3 0 985.25 963.13 16.91 o -6 3 0 6916.93 6790.01 85.88 o -5 3 0 3299.89 3353.92 41.34 o -4 3 0 6304.35 6613.74 71.64 o -3 3 0 16217.52 16702.71 207.38 o -2 3 0 102.75 80.43 8.38 o -1 3 0 4.92 5.21 3.06 o 0 3 0 1722.98 1699.52 39.28 o 1 3 0 1030.44 1034.82 24.09 o 2 3 0 8816.14 9916.21 269.25 o 3 3 0 20799.54 21647.11 314.01 o 4 3 0 5821.03 6324.42 71.90 o 5 3 0 5966.46 6414.31 65.35 o 6 3 0 1.39 12.00 4.24 o 7 3 0 368.68 386.39 8.81 o 8 3 0 9.77 14.39 2.68 o 9 3 0 11098.26 11051.29 113.08 o 10 3 0 2341.75 2363.37 35.67 o 11 3 0 1997.68 2011.65 35.22 o 12 3 0 1742.71 1742.56 33.05 o 13 3 0 0.53 -3.25 5.71 o 14 3 0 8.92 11.43 7.62 o 15 3 0 259.66 287.27 27.38 o 16 3 0 138.98 131.80 15.94 o 17 3 0 622.48 582.79 34.49 o 18 3 0 1162.82 1317.64 51.63 o -17 4 0 70.78 61.79 12.53 o -16 4 0 277.63 276.02 18.60 o -15 4 0 449.45 463.14 22.45 o -14 4 0 61.78 40.48 9.75 o -13 4 0 2317.10 2324.17 50.25 o -12 4 0 578.13 571.00 19.92 o -11 4 0 269.53 248.42 18.60 o -10 4 0 2336.40 2244.39 38.39 o -9 4 0 158.43 156.12 8.98 o -8 4 0 944.95 887.88 21.75 o -7 4 0 5413.12 5232.18 62.47 o -6 4 0 2800.25 2809.47 36.56 o -5 4 0 708.42 592.50 13.72 o -4 4 0 10958.82 10845.70 123.49 o -3 4 0 8866.85 9323.26 97.87 o -2 4 0 1425.05 1336.64 96.14 o -1 4 0 202.36 172.31 9.20 o 0 4 0 2284.01 2145.20 33.61 o 1 4 0 4059.94 4242.21 51.03 o 2 4 0 23381.35 24065.80 307.01 o 3 4 0 29444.05 32697.93 389.97 o 4 4 0 19116.34 19640.10 204.87 o 5 4 0 9546.16 9989.47 110.50 o 6 4 0 1393.27 1493.17 20.93 o 7 4 0 0.58 7.96 3.16 o 8 4 0 774.79 740.59 14.32 o 9 4 0 11.75 11.84 4.84 o 10 4 0 3196.70 3256.30 50.70 o 11 4 0 4139.46 4181.13 62.48 o 12 4 0 6.50 12.58 5.97 o 13 4 0 1520.72 1597.27 33.53 o 14 4 0 211.54 219.65 14.28 o 15 4 0 1.68 23.33 8.48 o 16 4 0 105.98 118.46 36.05 o 17 4 0 795.86 814.38 43.32 o 18 4 0 82.76 105.25 20.69 o -17 5 0 120.89 100.30 21.61 o -16 5 0 57.18 45.71 12.36 o -15 5 0 6.83 10.32 9.53 o -14 5 0 1895.10 1955.43 48.21 o -13 5 0 392.85 441.69 21.72 o -12 5 0 265.32 254.29 19.26 o -11 5 0 3206.45 3262.78 70.98 o -10 5 0 31.03 36.06 7.25 o -9 5 0 41.78 18.54 6.10 o -8 5 0 660.37 605.83 16.64 o -7 5 0 1633.11 1537.40 26.97 o -6 5 0 2615.54 2577.79 40.20 o -5 5 0 11304.14 10657.93 135.88 o -4 5 0 4464.32 4402.92 53.90 o -3 5 0 1928.56 1780.11 32.95 o -2 5 0 17704.28 18639.30 233.32 o -1 5 0 6653.90 6938.09 110.42 o 0 5 0 5527.90 5908.44 71.56 o 1 5 0 393.15 334.53 8.86 o 2 5 0 1974.14 2068.48 27.35 o 3 5 0 9447.83 9384.14 103.18 o 4 5 0 12825.48 12832.29 122.25 o 5 5 0 2278.43 2575.39 33.78 o 6 5 0 2624.86 2690.19 36.15 o 7 5 0 696.96 817.21 16.53 o 8 5 0 105.94 98.41 7.45 o 9 5 0 1997.84 2050.47 37.04 o 10 5 0 2001.00 2070.61 37.94 o 11 5 0 64.82 58.90 11.03 o 12 5 0 2009.60 2104.65 40.49 o 13 5 0 2125.49 2172.81 42.44 o 14 5 0 2.00 9.46 7.05 o 15 5 0 39.39 42.43 9.29 o 16 5 0 115.27 119.63 14.22 o 17 5 0 13.38 22.62 10.51 o 18 5 0 61.78 69.06 20.77 o -17 6 0 9.73 -0.49 12.04 o -16 6 0 79.29 99.02 14.88 o -15 6 0 443.96 444.99 24.93 o -14 6 0 82.54 93.25 13.84 o -13 6 0 108.27 125.86 16.97 o -12 6 0 2812.26 2873.03 55.14 o -11 6 0 1264.31 1186.70 31.45 o -10 6 0 794.40 815.39 23.32 o -9 6 0 3431.36 3349.26 66.08 o -8 6 0 207.66 209.95 10.06 o -7 6 0 30.34 20.65 4.52 o -6 6 0 4115.55 3957.31 49.17 o -5 6 0 2000.02 1938.98 25.12 o -4 6 0 4138.53 4080.05 47.31 o -3 6 0 8429.56 7899.54 94.81 o -2 6 0 1290.09 1295.04 26.30 o -1 6 0 5.62 33.16 8.35 o 0 6 0 4304.53 4665.91 54.61 o 1 6 0 260.88 333.19 8.91 o 2 6 0 80.05 77.86 6.49 o 3 6 0 3524.08 3389.98 43.73 o 4 6 0 2.58 5.93 3.70 o 5 6 0 4706.35 4521.85 52.81 o 6 6 0 4763.51 4898.16 57.20 o 7 6 0 626.70 707.67 15.34 o 8 6 0 136.41 160.90 10.19 o 9 6 0 96.81 100.20 9.39 o 10 6 0 7.55 -2.02 5.62 o 11 6 0 791.28 838.65 24.09 o 12 6 0 3232.36 3201.85 67.90 o 13 6 0 302.58 330.02 16.69 o 14 6 0 1263.06 1304.00 36.07 o 15 6 0 445.15 466.40 27.94 o 16 6 0 41.34 56.12 11.46 o 17 6 0 7.93 34.65 11.65 o 18 6 0 225.51 188.77 27.37 o -16 7 0 452.90 426.06 29.67 o -15 7 0 58.62 59.09 16.37 o -14 7 0 30.52 31.30 10.41 o -13 7 0 549.37 614.43 25.79 o -12 7 0 610.39 593.46 19.33 o -11 7 0 969.70 956.10 34.02 o -10 7 0 5164.71 5054.68 64.54 o -9 7 0 1228.36 1146.78 23.78 o -8 7 0 670.28 589.23 19.26 o -7 7 0 1446.54 1287.24 22.88 o -6 7 0 1.20 5.01 3.13 o -5 7 0 303.43 307.61 13.92 o -4 7 0 10950.93 10382.27 118.79 o -3 7 0 943.54 926.02 16.56 o -2 7 0 8218.65 8436.26 93.87 o -1 7 0 8133.46 8000.47 97.19 o 0 7 0 1322.71 1427.30 22.96 o 1 7 0 1429.73 1365.18 31.41 o 2 7 0 3194.52 3394.94 36.92 o 3 7 0 327.84 304.43 7.57 o 4 7 0 8590.20 8936.73 81.65 o 5 7 0 5613.56 5601.86 57.54 o 6 7 0 1152.67 1187.64 23.76 o 7 7 0 1347.38 1319.92 23.29 o 8 7 0 1631.82 1594.90 26.23 o 9 7 0 60.94 45.66 9.62 o 10 7 0 23.22 34.36 7.55 o 11 7 0 1095.24 1008.64 27.89 o 12 7 0 118.90 119.28 11.72 o 13 7 0 1242.68 1334.85 37.52 o 14 7 0 2228.89 2267.05 52.67 o 15 7 0 38.95 33.09 10.41 o 16 7 0 195.22 175.03 25.21 o 17 7 0 8.22 20.38 11.34 o -16 8 0 227.26 210.44 23.52 o -15 8 0 137.50 116.26 13.33 o -14 8 0 19.54 4.50 14.59 o -13 8 0 650.92 707.77 23.64 o -12 8 0 0.90 9.50 6.82 o -11 8 0 3120.65 3168.84 48.37 o -10 8 0 1370.65 1343.45 27.72 o -9 8 0 630.40 630.81 17.45 o -8 8 0 3527.18 3365.69 47.34 o -7 8 0 488.77 476.39 14.49 o -6 8 0 891.49 733.89 14.34 o -5 8 0 2286.97 1994.14 27.32 o -4 8 0 2134.90 2078.46 26.16 o -3 8 0 3587.95 3649.88 42.88 o -2 8 0 9792.17 9499.40 98.68 o -1 8 0 684.46 618.83 15.70 o 0 8 0 3947.78 4081.59 50.95 o 1 8 0 1242.08 1165.23 19.10 o 2 8 0 279.32 353.56 9.42 o 3 8 0 1277.35 1380.91 18.12 o 4 8 0 6772.91 6725.04 65.18 o 5 8 0 38.52 46.88 6.22 o 6 8 0 3619.03 3609.15 40.79 o 7 8 0 5362.43 5230.67 65.28 o 8 8 0 6.38 7.29 4.20 o 9 8 0 379.70 352.44 13.51 o 10 8 0 32.50 26.89 8.60 o 11 8 0 14.30 25.79 7.86 o 12 8 0 1376.03 1378.71 39.28 o 13 8 0 1400.93 1446.86 41.22 o 14 8 0 67.04 43.93 10.87 o 15 8 0 474.71 520.03 26.00 o 16 8 0 660.38 682.32 37.85 o 17 8 0 35.08 44.88 17.63 o -16 9 0 73.38 83.17 23.31 o -15 9 0 839.16 808.26 40.14 o -14 9 0 96.65 93.67 12.59 o -13 9 0 233.39 234.82 15.82 o -12 9 0 204.80 194.39 13.97 o -11 9 0 612.79 619.77 21.81 o -10 9 0 879.09 833.79 23.52 o -9 9 0 3965.67 4001.30 56.46 o -8 9 0 1008.85 941.51 26.35 o -7 9 0 1730.79 1574.04 28.19 o -6 9 0 315.22 248.63 13.50 o -5 9 0 6.54 2.65 3.70 o -4 9 0 339.14 305.76 10.15 o -3 9 0 6876.97 6611.56 62.05 o -2 9 0 1623.07 1603.43 30.04 o -1 9 0 3938.69 3957.81 54.13 o 0 9 0 8487.90 8620.34 92.57 o 1 9 0 1470.63 1468.21 25.28 o 2 9 0 122.93 150.92 7.94 o 3 9 0 689.73 647.61 13.85 o 4 9 0 888.68 923.04 16.48 o 5 9 0 2617.66 2546.48 33.66 o 6 9 0 11213.02 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0 501.40 492.34 16.64 o 9 11 0 1990.12 1993.35 34.04 o 10 11 0 1611.83 1642.94 42.18 o 11 11 0 31.82 11.08 8.44 o 12 11 0 353.65 384.23 20.47 o 13 11 0 123.77 135.50 14.47 o 14 11 0 14.02 19.49 10.03 o 15 11 0 577.77 591.55 32.36 o 16 11 0 358.47 341.07 34.78 o -14 12 0 442.60 439.88 34.06 o -13 12 0 122.71 141.98 17.35 o -12 12 0 187.49 199.65 23.87 o -11 12 0 5.15 8.17 9.51 o -10 12 0 115.95 116.27 18.36 o -9 12 0 326.34 276.03 33.89 o -8 12 0 622.49 627.69 25.23 o -7 12 0 697.92 624.71 18.83 o -6 12 0 2941.15 2933.30 43.60 o -5 12 0 176.54 152.49 10.91 o -4 12 0 331.78 351.93 14.67 o -3 12 0 474.34 451.76 16.95 o -2 12 0 71.01 56.27 7.68 o -1 12 0 1217.79 1196.05 26.19 o 0 12 0 7760.03 8089.36 90.10 o 1 12 0 61.13 79.11 8.89 o 2 12 0 5900.71 5821.68 69.68 o 3 12 0 2002.94 2156.35 34.53 o 4 12 0 394.44 354.62 12.90 o 5 12 0 102.54 73.74 9.36 o 6 12 0 1120.01 1090.20 20.19 o 7 12 0 150.85 146.70 8.65 o 8 12 0 1428.66 1417.23 24.16 o 9 12 0 1615.27 1628.78 67.06 o 10 12 0 37.28 34.69 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12.32 o 8 8 28 73.43 32.83 22.55 o -1 9 28 297.13 251.08 31.69 o 0 9 28 6.64 34.05 26.41 o 1 9 28 129.52 163.63 37.16 o 2 9 28 2.43 30.71 23.07 o 3 9 28 0.97 22.70 22.55 o 4 9 28 402.65 498.23 47.40 o 5 9 28 515.42 489.92 61.42 o 6 9 28 2.51 12.35 15.11 o 7 9 28 525.46 478.37 72.51 o 0 10 28 568.85 475.76 54.30 o 1 10 28 332.41 308.42 46.14 o 2 10 28 10.62 -14.54 20.69 o 3 10 28 49.10 63.27 26.26 o 4 10 28 399.74 343.21 42.35 o 5 10 28 66.18 55.11 23.29 o 6 10 28 392.87 361.03 66.65 o 1 -5 29 196.67 216.12 31.72 o 2 -5 29 20.95 31.23 17.67 o 3 -5 29 0.03 2.75 14.88 o -1 -4 29 17.55 20.22 16.49 o 0 -4 29 676.28 682.58 48.63 o 1 -4 29 112.99 149.77 27.46 o 2 -4 29 5.99 5.46 15.33 o 3 -4 29 2.23 17.03 26.15 o 4 -4 29 28.82 22.40 17.13 o 5 -4 29 63.98 33.14 17.80 o -2 -3 29 40.89 44.63 28.89 o -1 -3 29 1118.84 1214.85 48.80 o 0 -3 29 517.54 547.00 43.97 o 1 -3 29 15.48 11.13 17.26 o 2 -3 29 387.86 451.83 39.73 o 3 -3 29 3.46 16.56 17.11 o 4 -3 29 2.64 19.68 16.62 o 5 -3 29 43.08 35.91 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291.75 34.33 o -1 1 29 11.01 7.14 14.42 o 0 1 29 13.72 17.36 18.84 o 1 1 29 405.81 427.45 38.41 o 2 1 29 247.32 273.46 55.48 o 3 1 29 148.89 111.13 30.04 o 4 1 29 345.61 335.64 35.49 o 5 1 29 507.50 535.66 37.94 o 6 1 29 112.05 105.63 19.85 o 7 1 29 3.42 25.09 18.07 o 8 1 29 35.65 34.78 18.37 o -3 2 29 771.96 667.94 60.53 o -2 2 29 413.32 386.52 49.85 o -1 2 29 9.37 35.48 15.74 o 0 2 29 12.35 40.94 19.72 o 1 2 29 164.10 168.91 27.91 o 2 2 29 16.65 -7.69 13.79 o 3 2 29 842.36 884.15 48.68 o 4 2 29 594.79 649.19 56.85 o 5 2 29 313.26 270.39 29.17 o 6 2 29 326.64 374.49 38.35 o 7 2 29 42.26 31.56 10.77 o 8 2 29 0.57 41.72 18.58 o -3 3 29 381.58 340.02 46.51 o -2 3 29 8.88 1.41 23.81 o -1 3 29 296.34 356.02 34.84 o 0 3 29 83.21 68.17 22.65 o 1 3 29 6.87 4.78 16.04 o 2 3 29 113.92 147.54 32.97 o 3 3 29 227.60 197.38 75.06 o 4 3 29 318.41 253.91 29.60 o 5 3 29 948.20 1112.82 50.67 o 6 3 29 219.91 191.49 35.60 o 7 3 29 87.80 64.41 12.77 o 8 3 29 11.28 34.44 18.32 o -3 4 29 18.94 26.48 25.89 o 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33.62 o 4 6 30 12.00 9.45 15.45 o