#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:25:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181043 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/23/2212324.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212324_Fobs loop_ _publ_author_name 'Zhang, Tao' 'Davila, Alfonso' 'McLaughlin, Mark L.' 'Watkins, Steven F.' 'Fronczek, Frank R.' _publ_section_title ; 1,3,5-Trichloro-2,4,6-tripyrrol-1-ylbenzene ; _journal_coeditor_code OM2085 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o604 _journal_page_last o605 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.021 _cell_angle_beta 69.577 _cell_angle_gamma 65.190 _cell_length_a 11.1670 _cell_length_b 11.5340 _cell_length_c 15.7993 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.7570 _cod_data_source_file om2085Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tina in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 375.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 98.04 115.92 13.16 o 3 0 0 9.63 9.11 3.58 o 4 0 0 2.77 1.01 5.01 o 5 0 0 174.50 175.33 8.21 o 6 0 0 738.39 777.10 15.75 o 7 0 0 514.70 514.14 15.03 o 8 0 0 161.17 166.00 10.12 o 9 0 0 17.79 24.81 6.44 o 10 0 0 0.08 1.80 10.63 o 11 0 0 118.85 119.33 9.31 o 12 0 0 70.34 64.51 9.95 o -12 1 0 163.45 169.08 16.20 o -11 1 0 5.00 27.34 11.14 o -10 1 0 305.79 277.41 22.27 o -9 1 0 18.41 26.32 9.11 o -8 1 0 278.92 284.50 20.25 o -7 1 0 102.94 94.16 9.11 o -6 1 0 329.64 289.57 17.21 o -5 1 0 43.95 56.70 6.07 o -4 1 0 1242.20 1231.26 23.29 o -3 1 0 2024.88 2184.29 26.33 o -2 1 0 303.76 308.81 10.12 o -1 1 0 140.67 157.95 7.09 o 2 1 0 4361.99 4489.85 26.35 o 3 1 0 1173.48 1085.51 17.21 o 4 1 0 1846.36 1843.99 24.30 o 5 1 0 96.83 127.57 10.12 o 6 1 0 3466.65 3345.85 42.53 o 7 1 0 240.90 238.94 16.20 o 8 1 0 380.85 385.75 20.25 o 9 1 0 467.32 465.74 25.31 o 10 1 0 9.88 10.12 10.12 o 11 1 0 6.71 -8.10 16.20 o 12 1 0 478.50 522.43 28.35 o -11 2 0 11.95 -12.15 19.24 o -10 2 0 118.12 121.49 13.16 o -9 2 0 15.89 17.21 10.12 o -8 2 0 52.86 49.61 10.12 o -7 2 0 120.07 115.42 12.15 o -6 2 0 206.03 205.53 15.19 o -5 2 0 297.22 273.37 15.19 o -4 2 0 3659.39 3799.67 41.52 o -3 2 0 12.66 29.36 5.06 o -2 2 0 1769.04 1864.27 23.29 o -1 2 0 209.46 239.96 9.11 o 0 2 0 549.62 554.88 10.13 o 1 2 0 649.10 668.31 10.13 o 2 2 0 141293.19 125163.51 600.81 o 3 2 0 9299.36 9845.20 47.64 o 4 2 0 153.08 178.19 10.12 o 5 2 0 82.69 104.28 10.12 o 6 2 0 152.00 219.70 13.16 o 7 2 0 157.60 217.68 15.19 o 8 2 0 168.09 157.94 12.15 o 9 2 0 278.71 251.09 19.24 o 10 2 0 3.46 -10.12 10.12 o 11 2 0 0.84 -7.09 15.19 o 12 2 0 89.81 99.22 14.17 o 13 2 0 195.19 276.40 23.29 o -11 3 0 714.86 763.41 38.47 o -10 3 0 397.80 361.45 27.34 o -9 3 0 25.26 17.21 11.14 o -8 3 0 0.12 -2.02 13.16 o -7 3 0 2.60 -12.15 12.15 o -6 3 0 1130.61 1070.22 29.36 o -5 3 0 1578.17 1518.80 32.40 o -4 3 0 2784.88 2589.28 37.47 o -3 3 0 736.47 790.77 20.25 o -2 3 0 500.94 506.25 14.17 o -1 3 0 109.56 136.68 9.11 o 0 3 0 703.49 846.48 14.18 o 1 3 0 577.86 564.99 11.14 o 2 3 0 379.76 384.75 11.14 o 3 3 0 411.63 407.02 12.15 o 4 3 0 10419.49 10936.73 58.78 o 5 3 0 1910.09 1855.08 27.34 o 6 3 0 1200.10 1240.35 25.31 o 7 3 0 25.91 34.42 7.09 o 8 3 0 4026.08 4147.81 53.67 o 9 3 0 76.49 86.06 10.12 o 10 3 0 515.71 448.52 25.31 o 11 3 0 12.01 0.00 16.20 o 12 3 0 298.59 288.55 24.30 o 13 3 0 26.67 25.31 13.16 o -10 4 0 3.15 -10.12 19.24 o -9 4 0 12.50 17.21 12.15 o -8 4 0 102.75 98.21 11.14 o -7 4 0 13.69 21.26 9.11 o -6 4 0 469.09 467.76 23.29 o -5 4 0 1311.31 1283.87 32.40 o -4 4 0 0.29 -3.04 10.12 o -3 4 0 785.46 740.14 21.26 o -2 4 0 371.62 463.71 15.19 o -1 4 0 0.69 5.06 5.06 o 0 4 0 5060.84 5335.12 38.49 o 1 4 0 704.23 739.14 15.19 o 2 4 0 3044.97 3044.38 27.34 o 3 4 0 0.14 14.17 5.06 o 4 4 0 9339.11 9531.56 55.73 o 5 4 0 3280.40 3587.96 38.48 o 6 4 0 410.32 418.15 17.21 o 7 4 0 3.40 -2.02 7.09 o 8 4 0 91.44 99.22 10.12 o 9 4 0 4.45 -5.06 12.15 o 10 4 0 23.56 13.16 10.12 o 11 4 0 8.72 8.10 10.12 o 12 4 0 0.43 -5.06 16.20 o 13 4 0 0.52 -13.16 13.16 o -9 5 0 744.39 736.07 37.46 o -8 5 0 509.82 438.40 26.32 o -7 5 0 126.79 119.47 12.15 o -6 5 0 46.40 26.32 10.12 o -5 5 0 56.59 72.90 9.11 o -4 5 0 1299.91 1199.83 30.38 o -3 5 0 1221.79 1173.51 27.34 o -2 5 0 4444.99 4486.38 47.60 o -1 5 0 345.95 388.79 15.19 o 0 5 0 524.51 578.13 16.20 o 1 5 0 575.91 600.41 15.19 o 2 5 0 5.70 27.34 5.06 o 3 5 0 611.31 459.68 14.18 o 4 5 0 53.06 76.95 6.07 o 5 5 0 525.76 505.23 17.21 o 6 5 0 6154.69 6550.95 58.74 o 7 5 0 193.62 226.79 15.19 o 8 5 0 8.21 4.05 8.10 o 9 5 0 2.90 -1.01 12.15 o 10 5 0 1827.15 1831.66 42.53 o 11 5 0 48.04 48.60 12.15 o 12 5 0 30.61 15.19 12.15 o 13 5 0 39.48 49.61 13.16 o -9 6 0 0.04 -12.15 12.15 o -8 6 0 197.24 235.90 19.24 o -7 6 0 59.06 83.02 12.15 o -6 6 0 53.51 65.81 10.12 o -5 6 0 7.24 21.26 9.11 o -4 6 0 233.04 226.79 17.21 o -3 6 0 2356.81 2315.74 40.50 o -2 6 0 10.63 -3.04 7.09 o -1 6 0 510.67 502.19 18.22 o 0 6 0 4828.48 5171.16 47.60 o 1 6 0 442.78 413.09 15.19 o 2 6 0 2755.52 2629.84 31.39 o 3 6 0 61.82 106.31 9.11 o 4 6 0 9067.63 9015.22 60.78 o 5 6 0 870.89 913.28 22.28 o 6 6 0 1198.95 1278.81 28.35 o 7 6 0 764.38 773.54 24.30 o 8 6 0 1198.24 1199.82 31.39 o 9 6 0 31.53 52.65 9.11 o 10 6 0 43.99 42.52 11.14 o 11 6 0 154.02 168.07 16.20 o 12 6 0 2.12 -5.06 11.14 o 13 6 0 0.35 8.10 12.15 o -8 7 0 12.59 10.12 12.15 o -7 7 0 884.06 938.57 37.46 o -6 7 0 232.21 185.28 16.20 o -5 7 0 5.51 4.05 14.17 o -4 7 0 683.33 682.41 27.34 o -3 7 0 1.94 -6.07 12.15 o -2 7 0 155.82 144.78 13.16 o -1 7 0 77.03 62.77 8.10 o 0 7 0 1982.66 1969.43 33.41 o 1 7 0 3.14 13.16 7.09 o 2 7 0 67.07 74.92 9.11 o 3 7 0 552.07 512.32 17.21 o 4 7 0 411.13 494.09 17.21 o 5 7 0 288.70 274.38 14.17 o 6 7 0 18.33 12.15 8.10 o 7 7 0 262.47 286.53 17.21 o 8 7 0 281.49 293.61 19.24 o 9 7 0 2.25 -7.09 12.15 o 10 7 0 43.02 39.49 10.12 o 11 7 0 39.96 52.65 10.12 o 12 7 0 142.52 137.69 14.17 o 13 7 0 29.56 7.09 14.17 o -7 8 0 10.37 -4.05 19.24 o -6 8 0 336.23 453.58 28.35 o -5 8 0 307.91 289.56 23.29 o -4 8 0 910.27 993.25 33.41 o -3 8 0 298.22 292.60 20.25 o -2 8 0 0.20 -3.04 8.10 o -1 8 0 3135.12 3221.07 48.60 o 0 8 0 141.60 152.88 10.12 o 1 8 0 716.71 725.95 23.29 o 2 8 0 1432.49 1453.99 29.36 o 3 8 0 68.39 70.87 8.10 o 4 8 0 1711.55 1604.88 30.38 o 5 8 0 42.94 35.44 8.10 o 6 8 0 1638.62 1668.65 33.41 o 7 8 0 357.29 371.58 20.25 o 8 8 0 10.77 8.10 9.11 o 9 8 0 281.50 281.46 20.25 o 10 8 0 268.51 268.30 22.27 o 11 8 0 55.37 63.78 11.14 o 12 8 0 73.86 73.91 13.16 o 13 8 0 210.01 248.05 24.30 o -6 9 0 7.75 -8.10 12.15 o -5 9 0 1038.92 1046.91 39.49 o -4 9 0 83.15 97.20 13.16 o -3 9 0 34.85 41.51 11.14 o -2 9 0 1218.95 1253.47 35.44 o -1 9 0 695.19 667.22 26.32 o 0 9 0 241.41 274.38 19.24 o 1 9 0 219.58 235.90 17.21 o 2 9 0 43.43 30.37 8.10 o 3 9 0 0.92 -1.01 11.14 o 4 9 0 988.89 940.61 26.32 o 5 9 0 481.86 471.81 20.25 o 6 9 0 157.60 146.81 13.16 o 7 9 0 141.16 134.66 13.16 o 8 9 0 16.50 30.37 10.12 o 9 9 0 90.49 85.05 12.15 o 10 9 0 130.12 151.87 13.16 o 11 9 0 32.74 33.41 11.14 o 12 9 0 420.84 428.27 28.35 o 13 9 0 42.80 49.61 14.17 o -5 10 0 34.90 34.42 13.16 o -4 10 0 262.95 280.45 27.34 o -3 10 0 62.67 52.65 12.15 o -2 10 0 976.14 975.03 34.42 o -1 10 0 36.95 22.27 10.12 o 0 10 0 60.47 67.83 11.14 o 1 10 0 2975.39 2868.63 47.59 o 2 10 0 3.65 6.07 13.16 o 3 10 0 452.90 441.44 21.26 o 4 10 0 0.24 2.02 11.14 o 5 10 0 66.95 84.03 10.12 o 6 10 0 6.95 14.17 9.11 o 7 10 0 0.74 -4.05 12.15 o 8 10 0 0.20 1.01 13.16 o 9 10 0 1.09 -10.12 14.17 o 10 10 0 4.80 1.01 15.19 o 11 10 0 124.83 109.35 13.16 o 12 10 0 116.82 131.62 14.17 o 13 10 0 0.32 -8.10 18.22 o -4 11 0 34.69 44.55 12.15 o -3 11 0 497.08 494.08 29.36 o -2 11 0 483.27 539.65 29.36 o -1 11 0 83.51 101.25 12.15 o 0 11 0 1284.65 1315.24 37.46 o 1 11 0 381.07 352.34 21.26 o 2 11 0 297.89 299.69 21.26 o 3 11 0 50.25 57.71 10.12 o 4 11 0 6.26 17.21 9.11 o 5 11 0 54.91 52.65 9.11 o 6 11 0 1621.19 1564.34 38.48 o 7 11 0 299.42 297.66 21.26 o 8 11 0 0.03 3.04 13.16 o 9 11 0 4.82 -2.02 14.17 o 10 11 0 4.71 -6.07 15.19 o 11 11 0 2.67 -7.09 12.15 o 12 11 0 22.85 56.70 11.14 o -3 12 0 115.41 107.32 15.19 o -2 12 0 58.25 52.65 14.17 o -1 12 0 11.86 -11.14 13.16 o 0 12 0 86.92 65.81 12.15 o 1 12 0 0.07 7.09 11.14 o 2 12 0 447.56 429.29 25.31 o 3 12 0 798.76 791.76 30.37 o 4 12 0 626.54 638.87 28.35 o 5 12 0 0.54 -8.10 10.12 o 6 12 0 41.50 44.55 10.12 o 7 12 0 95.32 89.10 12.15 o 8 12 0 723.67 633.81 29.36 o 9 12 0 30.12 51.64 11.14 o 10 12 0 1.43 -12.15 18.22 o 11 12 0 1.43 -4.05 18.22 o 12 12 0 63.04 77.96 14.17 o -1 13 0 57.29 52.65 14.17 o 0 13 0 82.19 99.22 14.17 o 1 13 0 11.07 -4.05 11.14 o 2 13 0 590.23 606.47 31.39 o 3 13 0 65.83 61.76 12.15 o 4 13 0 41.04 39.49 12.15 o 5 13 0 1.41 -12.15 12.15 o 6 13 0 5.08 3.04 15.19 o 7 13 0 16.96 24.30 10.12 o 8 13 0 572.00 535.60 31.39 o 9 13 0 221.86 249.06 24.30 o 10 13 0 0.12 -10.12 18.22 o 11 13 0 3.22 5.06 12.15 o 1 14 0 45.12 62.77 13.16 o 2 14 0 31.76 43.54 14.17 o 3 14 0 0.81 -13.16 13.16 o 4 14 0 574.95 632.79 30.37 o 5 14 0 269.57 289.56 23.29 o 6 14 0 195.32 211.60 19.24 o 7 14 0 2.79 -11.14 18.22 o 9 14 0 40.61 46.57 13.16 o 10 14 0 249.82 242.99 22.27 o 4 15 0 7.03 25.31 13.16 o 5 15 0 188.37 262.23 26.32 o 6 15 0 30.03 37.46 14.17 o 7 15 0 14.60 34.42 13.16 o -7 -15 1 45.37 64.80 14.17 o -6 -15 1 537.13 610.52 33.41 o -5 -15 1 356.45 379.67 28.35 o -4 -15 1 327.21 325.00 27.34 o -9 -14 1 437.58 495.10 30.37 o -8 -14 1 46.92 54.67 13.16 o -7 -14 1 94.44 107.32 14.17 o -6 -14 1 24.20 24.30 12.15 o -5 -14 1 7.02 7.09 11.14 o -4 -14 1 41.84 60.75 13.16 o -3 -14 1 19.05 12.15 13.16 o -2 -14 1 4.41 -12.15 13.16 o -1 -14 1 305.23 311.84 27.34 o -11 -13 1 20.58 34.42 13.16 o -10 -13 1 3.25 -12.15 12.15 o -9 -13 1 44.14 42.52 13.16 o -8 -13 1 93.91 106.31 14.17 o -7 -13 1 46.68 26.32 12.15 o -6 -13 1 98.28 82.01 13.16 o -5 -13 1 111.36 134.66 15.19 o -4 -13 1 345.02 347.27 23.29 o -3 -13 1 1371.68 1392.19 40.50 o -2 -13 1 265.41 285.51 23.29 o -1 -13 1 3.90 2.02 18.22 o 0 -13 1 124.61 118.46 15.19 o 1 -13 1 0.18 5.06 13.16 o -11 -12 1 72.93 65.81 14.17 o -10 -12 1 128.93 129.59 14.17 o -9 -12 1 80.85 108.33 13.16 o -8 -12 1 23.06 18.22 11.14 o -7 -12 1 663.44 682.41 29.36 o -6 -12 1 8.76 -10.12 10.12 o -5 -12 1 19.19 25.31 10.12 o -4 -12 1 264.29 254.13 21.26 o -3 -12 1 137.80 131.62 13.16 o -2 -12 1 520.85 478.90 25.31 o -1 -12 1 9.24 20.25 10.12 o 0 -12 1 86.04 78.97 13.16 o 1 -12 1 907.81 899.08 38.47 o 2 -12 1 116.20 114.41 15.19 o 3 -12 1 113.05 148.83 16.20 o -12 -11 1 2.18 3.04 18.22 o -11 -11 1 515.75 538.63 30.37 o -10 -11 1 332.10 328.04 24.30 o -9 -11 1 20.63 28.35 11.14 o -8 -11 1 28.52 23.29 10.12 o -7 -11 1 5.87 -4.05 14.17 o -6 -11 1 32.16 37.46 10.12 o -5 -11 1 39.88 30.37 9.11 o -4 -11 1 28.41 19.24 10.12 o -3 -11 1 249.53 209.58 18.22 o -2 -11 1 1.46 -14.17 14.17 o -1 -11 1 1735.68 1588.64 39.49 o 0 -11 1 0.13 -14.17 14.17 o 1 -11 1 10.57 0.00 10.12 o 2 -11 1 4.62 -7.09 17.21 o 3 -11 1 172.36 225.78 22.27 o 4 -11 1 45.79 50.62 13.16 o -12 -10 1 161.74 171.11 15.19 o -11 -10 1 566.73 517.37 29.36 o -10 -10 1 1.68 -9.11 16.20 o -9 -10 1 378.79 351.33 24.30 o -8 -10 1 382.99 439.41 23.29 o -7 -10 1 261.38 280.45 19.24 o -6 -10 1 52.94 54.67 10.12 o -5 -10 1 195.02 188.32 17.21 o -4 -10 1 130.79 147.82 12.15 o -3 -10 1 292.61 312.85 18.22 o -2 -10 1 626.76 637.86 24.30 o -1 -10 1 1045.11 946.68 29.36 o 0 -10 1 2596.38 2619.48 48.60 o 1 -10 1 7.57 -1.01 10.12 o 2 -10 1 217.19 225.78 19.24 o 3 -10 1 916.05 925.41 35.44 o 4 -10 1 2.60 -17.21 17.21 o 5 -10 1 162.20 169.08 18.22 o -13 -9 1 68.44 88.08 14.17 o -12 -9 1 4.13 -3.04 12.15 o -11 -9 1 108.88 98.21 13.16 o -10 -9 1 387.79 326.01 26.32 o -9 -9 1 798.17 831.25 31.39 o -8 -9 1 445.02 442.45 23.29 o -7 -9 1 90.84 91.12 10.12 o -6 -9 1 2.27 -11.14 11.14 o -5 -9 1 0.25 -5.06 11.14 o -4 -9 1 250.93 224.77 16.20 o -3 -9 1 73.06 78.97 9.11 o -2 -9 1 14.45 15.19 8.10 o -1 -9 1 27.71 -8.10 13.16 o 0 -9 1 615.82 622.67 24.30 o 1 -9 1 240.87 265.26 19.24 o 2 -9 1 660.67 685.45 26.32 o 3 -9 1 5.20 0.00 13.16 o 4 -9 1 252.94 275.39 22.27 o 5 -9 1 43.14 58.72 13.16 o 6 -9 1 6.21 -4.05 16.20 o -13 -8 1 177.01 241.98 24.30 o -12 -8 1 282.36 252.10 25.31 o -11 -8 1 44.45 39.49 11.14 o -10 -8 1 185.29 202.49 19.24 o -9 -8 1 545.65 522.44 25.31 o -8 -8 1 502.24 434.35 23.29 o -7 -8 1 725.28 705.70 25.31 o -6 -8 1 693.87 711.78 24.30 o -5 -8 1 633.23 643.94 21.26 o -4 -8 1 32.56 18.22 7.09 o -3 -8 1 39.16 22.27 8.10 o -2 -8 1 1941.63 1960.30 33.41 o -1 -8 1 284.88 231.85 16.20 o 0 -8 1 346.00 373.60 17.21 o 1 -8 1 1533.14 1453.98 34.43 o 2 -8 1 2451.48 2384.58 43.54 o 3 -8 1 476.78 452.57 24.30 o 4 -8 1 4.17 3.04 13.16 o 5 -8 1 1109.10 1070.20 36.45 o 6 -8 1 294.96 310.83 25.31 o 7 -8 1 468.13 500.16 30.37 o -13 -7 1 172.61 155.92 19.24 o -12 -7 1 91.92 84.03 14.17 o -11 -7 1 110.84 113.39 13.16 o -10 -7 1 34.66 41.51 11.14 o -9 -7 1 93.76 94.16 11.14 o -8 -7 1 3579.16 3470.22 52.66 o -7 -7 1 1305.42 1368.92 32.40 o -6 -7 1 1644.86 1755.74 33.41 o -5 -7 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