#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:25:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181043 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/23/2212338.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212338_Fobs loop_ _publ_author_name 'Song, Wen-Dong' 'Guo, Xian-Xia' 'Zhang, Chao-Hua' _publ_section_title ; Poly[aqua(\m~3~-3,5-dinitrosalicylato)calcium(II)] ; _journal_coeditor_code RZ2102 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m399 _journal_page_last m401 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.391 _cell_angle_gamma 90.000 _cell_length_a 12.6381 _cell_length_b 6.6650 _cell_length_c 12.4126 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7655 _cod_data_source_file rz2102Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4495.20 3193.06 57.26 o 2 0 0 4109.73 3558.76 30.59 o 3 0 0 621.57 773.75 7.77 o 4 0 0 3498.13 3761.29 38.58 o 5 0 0 2854.28 3002.67 27.21 o 6 0 0 117.59 167.27 3.33 o 7 0 0 133.30 96.79 2.75 o 8 0 0 89.23 92.13 2.77 o 9 0 0 41.68 60.72 3.80 o 10 0 0 625.45 649.84 9.40 o 11 0 0 4240.21 4210.19 40.20 o 12 0 0 449.27 404.36 16.75 o 13 0 0 13.53 11.56 4.33 o 14 0 0 2.45 -1.92 3.63 o 15 0 0 11.74 16.25 5.71 o 1 1 0 1072.45 1041.29 9.84 o 2 1 0 411.67 382.40 3.74 o 3 1 0 0.54 0.41 0.34 o 4 1 0 557.41 566.41 4.86 o 5 1 0 506.93 508.17 4.42 o 6 1 0 153.68 172.80 3.89 o 7 1 0 186.56 184.62 2.64 o 8 1 0 433.71 461.43 4.80 o 9 1 0 70.82 70.03 2.11 o 10 1 0 24.61 23.35 1.53 o 11 1 0 1.05 0.73 1.58 o 12 1 0 185.89 187.58 5.35 o 13 1 0 3.67 3.41 2.80 o 14 1 0 18.31 17.69 5.57 o 15 1 0 45.23 45.12 5.72 o 0 2 0 18018.65 16635.72 337.62 o 1 2 0 2726.06 2325.09 17.38 o 2 2 0 80.76 16.65 0.86 o 3 2 0 2149.91 2342.85 17.82 o 4 2 0 1200.20 1354.87 9.49 o 5 2 0 1971.19 1943.33 15.25 o 6 2 0 289.72 320.01 4.09 o 7 2 0 424.47 551.19 5.77 o 8 2 0 478.44 497.56 5.62 o 9 2 0 645.44 582.43 6.48 o 10 2 0 827.67 807.48 10.03 o 11 2 0 627.27 620.58 10.15 o 12 2 0 0.44 -1.16 1.41 o 13 2 0 1.26 1.60 1.78 o 14 2 0 137.15 123.83 9.80 o 15 2 0 2.38 3.22 5.41 o 1 3 0 932.29 1017.75 7.50 o 2 3 0 150.59 137.45 1.94 o 3 3 0 857.46 865.24 7.13 o 4 3 0 71.95 61.04 2.53 o 5 3 0 36.58 29.63 1.08 o 6 3 0 1681.29 1694.13 14.79 o 7 3 0 256.03 270.47 4.79 o 8 3 0 353.38 331.53 5.62 o 9 3 0 119.88 106.76 3.84 o 10 3 0 7.43 8.11 1.89 o 11 3 0 146.37 151.28 4.95 o 12 3 0 5.86 6.32 1.99 o 13 3 0 10.55 7.02 2.10 o 14 3 0 32.39 41.20 5.19 o 0 4 0 2529.36 2692.51 22.64 o 1 4 0 3.63 2.16 0.61 o 2 4 0 269.89 179.14 2.37 o 3 4 0 1185.56 1294.80 9.27 o 4 4 0 1290.54 1409.61 13.24 o 5 4 0 1258.76 1249.95 11.72 o 6 4 0 835.19 811.38 8.79 o 7 4 0 1113.27 1188.86 12.82 o 8 4 0 563.69 566.25 9.15 o 9 4 0 131.23 154.08 6.33 o 10 4 0 170.26 179.82 5.40 o 11 4 0 268.24 235.92 6.41 o 12 4 0 5.30 1.42 2.14 o 13 4 0 2.30 6.77 2.78 o 1 5 0 73.30 77.86 2.36 o 2 5 0 24.61 25.69 1.57 o 3 5 0 256.96 237.39 4.71 o 4 5 0 23.57 22.73 2.00 o 5 5 0 166.35 181.95 6.39 o 6 5 0 82.84 84.47 4.17 o 7 5 0 153.47 138.61 5.40 o 8 5 0 219.18 238.69 13.11 o 9 5 0 320.42 331.42 11.00 o 10 5 0 109.25 113.24 6.92 o 11 5 0 380.80 395.80 18.65 o 12 5 0 72.65 79.02 9.40 o 0 6 0 1012.16 1014.65 15.43 o 1 6 0 1188.82 1202.19 13.89 o 2 6 0 543.79 517.39 7.95 o 3 6 0 2639.86 2627.28 28.49 o 4 6 0 857.00 883.54 17.04 o 5 6 0 70.04 68.42 7.28 o 6 6 0 1.60 2.98 2.87 o 7 6 0 491.66 489.63 13.69 o 8 6 0 116.31 117.46 6.95 o 9 6 0 0.39 3.69 3.69 o 10 6 0 1.98 4.55 4.45 o 11 6 0 1.36 1.68 3.23 o 1 7 0 19.74 20.75 4.25 o 2 7 0 169.85 170.34 8.92 o 3 7 0 21.49 28.68 3.19 o 4 7 0 0.41 1.93 2.53 o 5 7 0 0.17 1.18 3.04 o 6 7 0 71.63 64.72 5.55 o 7 7 0 14.71 17.67 5.83 o 8 7 0 47.91 59.50 8.82 o 9 7 0 8.19 5.49 3.91 o 0 8 0 260.04 223.08 13.42 o 1 8 0 270.26 278.57 10.62 o 2 8 0 237.14 263.13 15.09 o 3 8 0 125.26 161.26 12.20 o 4 8 0 172.73 161.28 12.52 o 5 8 0 40.78 42.59 7.73 o 6 8 0 88.86 85.27 9.72 o -15 1 1 115.77 112.98 7.53 o -14 1 1 390.58 371.09 19.30 o -13 1 1 114.87 105.64 5.64 o -12 1 1 509.60 489.95 7.04 o -11 1 1 556.48 596.94 7.75 o -10 1 1 5035.30 4888.28 34.24 o -9 1 1 455.15 383.22 4.62 o -8 1 1 1729.26 1630.70 11.39 o -7 1 1 1932.63 1979.28 13.06 o -6 1 1 1111.93 863.82 6.88 o -5 1 1 1575.39 1180.18 8.02 o -4 1 1 388.45 311.79 2.63 o -3 1 1 1203.48 1719.33 9.61 o -2 1 1 85.58 71.18 1.04 o -1 1 1 302.82 382.73 3.67 o 0 1 1 440.58 810.34 6.54 o 1 1 1 7179.06 6801.16 183.09 o 2 1 1 43.40 136.68 1.93 o 3 1 1 3176.03 2849.33 16.98 o 4 1 1 1677.40 1763.08 11.68 o 5 1 1 18.08 72.28 1.43 o 6 1 1 66.61 43.84 2.04 o 7 1 1 21.24 10.95 0.83 o 8 1 1 42.57 55.57 1.63 o 9 1 1 82.95 82.07 2.23 o 10 1 1 536.68 530.65 8.77 o 11 1 1 28.79 26.61 2.42 o 12 1 1 201.98 214.60 7.31 o 13 1 1 194.48 187.71 8.66 o 14 1 1 180.16 194.88 9.31 o 15 1 1 136.86 137.13 8.47 o -15 2 1 4.38 4.81 3.51 o -14 2 1 55.92 67.64 4.71 o -13 2 1 1.27 -0.18 1.70 o -12 2 1 47.63 45.34 3.10 o -11 2 1 153.92 140.50 3.59 o -10 2 1 1.58 3.12 1.00 o -9 2 1 39.30 52.62 1.91 o -8 2 1 3.27 1.20 0.76 o -7 2 1 102.39 100.19 2.46 o -6 2 1 1005.81 1065.86 8.26 o -5 2 1 3279.09 3758.94 28.32 o -4 2 1 1370.15 1619.02 12.09 o -3 2 1 479.01 578.43 4.81 o -2 2 1 1068.66 1165.88 8.24 o -1 2 1 532.04 498.94 4.68 o 0 2 1 63.51 76.36 1.33 o 1 2 1 1512.35 1442.51 10.69 o 2 2 1 670.31 786.74 6.53 o 3 2 1 595.85 554.65 4.95 o 4 2 1 1139.26 1309.17 9.85 o 5 2 1 11.24 6.03 0.84 o 6 2 1 2269.73 2584.03 18.52 o 7 2 1 369.39 406.70 4.66 o 8 2 1 171.11 157.88 3.67 o 9 2 1 154.76 151.22 6.31 o 10 2 1 52.92 51.81 3.32 o 11 2 1 0.05 0.64 1.54 o 12 2 1 11.85 10.02 2.11 o 13 2 1 57.28 53.51 4.27 o 14 2 1 4.70 7.36 3.54 o -14 3 1 74.38 58.67 5.20 o -13 3 1 283.98 284.04 9.05 o -12 3 1 65.43 73.68 4.48 o -11 3 1 83.50 98.17 4.12 o -10 3 1 754.94 748.65 12.72 o -9 3 1 299.22 261.20 4.61 o -8 3 1 1214.60 1141.80 12.39 o -7 3 1 2437.25 2540.59 21.01 o -6 3 1 4310.43 4239.25 32.41 o -5 3 1 4380.98 4218.44 30.02 o -4 3 1 1047.06 1041.32 8.27 o -3 3 1 5201.27 5817.51 34.66 o -2 3 1 4758.19 5254.89 32.72 o -1 3 1 1670.97 1896.33 13.76 o 0 3 1 152.55 233.83 3.47 o 1 3 1 353.44 378.01 3.80 o 2 3 1 75.24 36.50 1.27 o 3 3 1 207.58 172.96 2.60 o 4 3 1 138.97 134.40 2.38 o 5 3 1 260.50 332.98 3.84 o 6 3 1 382.48 410.72 7.30 o 7 3 1 1136.98 1100.98 13.45 o 8 3 1 6.43 4.68 1.37 o 9 3 1 273.18 304.87 6.52 o 10 3 1 565.93 548.16 11.13 o 11 3 1 408.04 428.99 8.61 o 12 3 1 152.48 142.39 5.17 o 13 3 1 12.14 10.77 2.92 o 14 3 1 59.57 70.32 6.61 o -14 4 1 0.95 -1.94 2.01 o -13 4 1 8.93 5.58 2.70 o -12 4 1 3.82 3.08 1.85 o -11 4 1 0.87 0.81 2.50 o -10 4 1 530.65 501.50 10.71 o -9 4 1 80.56 75.04 3.45 o -8 4 1 9.70 5.17 1.17 o -7 4 1 221.05 206.04 4.02 o -6 4 1 55.09 54.21 2.08 o -5 4 1 96.21 115.63 2.49 o -4 4 1 54.86 75.36 1.84 o -3 4 1 58.85 71.49 1.56 o -2 4 1 32.04 49.18 1.36 o -1 4 1 2.33 1.11 0.66 o 0 4 1 5.36 7.70 0.89 o 1 4 1 2731.84 2717.57 19.46 o 2 4 1 3.63 0.37 0.73 o 3 4 1 3.75 3.16 0.89 o 4 4 1 75.10 75.16 2.48 o 5 4 1 25.06 28.63 1.57 o 6 4 1 328.81 342.50 6.67 o 7 4 1 45.01 37.00 2.47 o 8 4 1 122.14 118.72 4.14 o 9 4 1 1.45 -0.18 1.44 o 10 4 1 29.31 29.60 2.81 o 11 4 1 24.35 22.92 2.71 o 12 4 1 338.01 353.68 9.73 o 13 4 1 14.79 18.77 3.61 o -13 5 1 129.97 106.42 10.58 o -12 5 1 316.87 340.23 17.55 o -11 5 1 301.12 276.28 15.33 o -10 5 1 243.53 232.05 9.31 o -9 5 1 9.90 11.67 6.00 o -8 5 1 50.73 48.33 7.08 o -7 5 1 3178.62 3169.30 33.53 o -6 5 1 1208.84 1176.00 15.28 o -5 5 1 451.43 443.00 7.87 o -4 5 1 269.44 282.83 5.94 o -3 5 1 72.30 76.07 4.85 o -2 5 1 225.53 241.25 4.65 o -1 5 1 321.43 338.22 5.39 o 0 5 1 42.89 61.67 2.16 o 1 5 1 0.81 1.75 0.95 o 2 5 1 16.16 24.05 1.55 o 3 5 1 62.72 50.62 2.30 o 4 5 1 2894.12 2822.88 29.54 o 5 5 1 2.26 4.96 1.89 o 6 5 1 33.23 37.00 6.41 o 7 5 1 0.85 0.44 2.15 o 8 5 1 79.63 97.25 6.22 o 9 5 1 93.33 94.00 6.29 o 10 5 1 128.45 144.18 13.79 o 11 5 1 83.18 101.27 9.96 o 12 5 1 134.50 118.56 10.78 o -11 6 1 1.19 -1.30 2.26 o -10 6 1 3.73 6.29 4.81 o -9 6 1 0.19 2.74 3.61 o -8 6 1 88.89 82.64 5.97 o -7 6 1 4.68 4.61 2.60 o -6 6 1 30.42 25.92 3.69 o -5 6 1 11.24 9.46 2.01 o -4 6 1 61.50 68.33 3.37 o -3 6 1 264.26 274.75 6.30 o -2 6 1 564.60 540.92 9.11 o -1 6 1 297.03 302.50 7.14 o 0 6 1 595.84 617.13 8.50 o 1 6 1 502.46 470.71 8.29 o 2 6 1 286.76 274.36 6.21 o 3 6 1 1573.41 1569.99 19.07 o 4 6 1 241.60 233.25 11.03 o 5 6 1 263.50 251.34 9.25 o 6 6 1 74.38 60.33 5.22 o 7 6 1 83.38 93.80 6.38 o 8 6 1 15.55 6.88 2.69 o 9 6 1 283.46 282.69 15.57 o 10 6 1 32.44 31.98 6.43 o -9 7 1 99.48 110.65 10.54 o -8 7 1 372.71 395.56 19.01 o -7 7 1 397.65 323.24 16.77 o -6 7 1 268.42 278.72 13.05 o -5 7 1 2.54 4.36 2.87 o -4 7 1 53.95 59.45 4.32 o -3 7 1 117.13 114.25 8.34 o -2 7 1 79.68 99.01 5.85 o -1 7 1 15.88 20.65 3.61 o 0 7 1 9.34 7.63 2.73 o 1 7 1 3.41 8.40 2.79 o 2 7 1 34.26 34.54 4.10 o 3 7 1 277.12 289.29 15.09 o 4 7 1 293.19 268.14 10.04 o 5 7 1 13.12 9.78 3.41 o 6 7 1 21.37 14.91 3.44 o 7 7 1 18.46 21.76 6.03 o 8 7 1 24.14 18.25 5.73 o -6 8 1 78.70 71.74 8.94 o -5 8 1 111.60 100.19 10.44 o -4 8 1 25.12 13.28 5.67 o -3 8 1 4.69 3.09 2.93 o -2 8 1 78.00 73.31 6.05 o -1 8 1 306.71 302.40 16.73 o 0 8 1 240.31 254.00 12.37 o 1 8 1 167.39 163.42 11.70 o 2 8 1 352.92 416.32 19.25 o 3 8 1 367.96 369.02 18.25 o 4 8 1 184.86 197.16 13.60 o 5 8 1 185.16 149.86 12.04 o -16 0 2 89.65 98.73 10.64 o -15 0 2 30.26 34.68 7.15 o -14 0 2 366.72 371.92 9.44 o -13 0 2 702.06 720.49 12.37 o -12 0 2 156.58 143.66 4.56 o -11 0 2 2520.87 2448.30 25.63 o -10 0 2 0.37 0.00 0.97 o -9 0 2 124.52 137.79 3.26 o -8 0 2 1433.74 1435.78 13.74 o -7 0 2 623.91 669.90 8.34 o -6 0 2 5.72 7.35 1.02 o -5 0 2 960.52 656.35 19.44 o -4 0 2 36.44 23.42 0.92 o -3 0 2 11180.31 10266.65 146.47 o -2 0 2 2950.39 3548.82 30.47 o -1 0 2 26.07 6.50 0.81 o 1 0 2 10174.62 9048.64 129.78 o 2 0 2 16119.67 15759.37 155.92 o 3 0 2 6197.88 5725.84 56.65 o 4 0 2 21702.92 19471.71 248.03 o 5 0 2 4344.20 4625.32 47.21 o 6 0 2 1293.08 1559.97 18.45 o 7 0 2 704.21 693.40 12.28 o 8 0 2 120.80 127.06 3.30 o 9 0 2 2902.47 3009.61 70.86 o 10 0 2 272.21 261.81 15.61 o 11 0 2 5.07 6.41 3.65 o 12 0 2 292.65 278.08 14.42 o 13 0 2 803.86 819.49 27.39 o 14 0 2 243.59 284.81 15.87 o -16 1 2 11.88 9.49 9.53 o -15 1 2 88.72 91.76 7.60 o -14 1 2 64.33 60.67 3.70 o -13 1 2 196.67 200.46 4.67 o -12 1 2 97.10 100.16 3.13 o -11 1 2 0.49 -0.62 0.84 o -10 1 2 1011.19 994.53 8.94 o -9 1 2 26.99 24.97 1.51 o -8 1 2 123.02 108.95 2.03 o -7 1 2 133.03 140.26 1.98 o -6 1 2 1367.57 1525.99 9.40 o -5 1 2 1022.71 1124.43 7.04 o -4 1 2 327.47 334.46 2.94 o -3 1 2 13.08 12.81 0.43 o -2 1 2 3347.23 3543.49 20.50 o -1 1 2 218.47 269.87 3.08 o 0 1 2 443.50 465.37 5.21 o 1 1 2 6258.85 6291.75 53.31 o 2 1 2 2505.85 2643.29 21.02 o 3 1 2 95.00 98.02 1.36 o 4 1 2 1497.12 1507.61 10.95 o 5 1 2 1602.68 1802.48 13.12 o 6 1 2 52.33 47.08 1.46 o 7 1 2 151.60 155.01 4.29 o 8 1 2 62.68 63.89 2.39 o 9 1 2 231.54 247.92 4.81 o 10 1 2 22.23 24.47 3.54 o 11 1 2 84.11 96.69 5.90 o 12 1 2 18.14 14.28 2.72 o 13 1 2 34.53 37.54 6.36 o 14 1 2 1.39 5.34 8.73 o -15 2 2 383.24 434.16 11.10 o -14 2 2 249.28 251.12 7.93 o -13 2 2 836.52 819.30 12.66 o -12 2 2 63.41 62.05 3.33 o -11 2 2 160.68 159.93 3.47 o -10 2 2 25.09 35.67 2.07 o -9 2 2 212.92 191.39 3.45 o -8 2 2 416.37 447.57 5.32 o -7 2 2 194.77 172.56 2.94 o -6 2 2 30.66 40.96 1.61 o -5 2 2 1430.68 1827.83 12.18 o -4 2 2 1892.89 1727.84 12.12 o -3 2 2 51.33 32.30 0.98 o -2 2 2 1137.81 932.61 6.90 o -1 2 2 3468.06 3782.77 26.13 o 0 2 2 652.55 443.42 4.11 o 1 2 2 144.79 70.19 1.47 o 2 2 2 180.86 133.21 2.61 o 3 2 2 72.24 25.90 1.04 o 4 2 2 5252.38 4866.67 32.29 o 5 2 2 1175.40 1265.33 9.95 o 6 2 2 759.68 870.85 9.05 o 7 2 2 11.45 4.91 1.04 o 8 2 2 449.43 435.00 7.50 o 9 2 2 926.43 990.44 13.18 o 10 2 2 732.98 747.15 11.41 o 11 2 2 547.11 550.82 12.93 o 12 2 2 294.98 311.25 10.13 o 13 2 2 483.25 514.02 11.93 o 14 2 2 211.26 238.35 10.55 o -15 3 2 75.84 85.91 5.54 o -14 3 2 7.30 5.25 2.12 o -13 3 2 120.38 113.35 4.72 o -12 3 2 1.14 4.24 2.08 o -11 3 2 7.11 9.23 1.79 o -10 3 2 0.30 -0.94 0.94 o -9 3 2 53.99 57.87 2.57 o -8 3 2 18.90 17.13 1.44 o -7 3 2 400.43 361.60 5.10 o -6 3 2 16.42 35.55 1.48 o -5 3 2 1.48 0.37 0.61 o -4 3 2 2555.25 2710.79 18.49 o -3 3 2 747.39 839.08 6.22 o -2 3 2 4201.74 4556.29 30.94 o -1 3 2 359.84 325.57 3.95 o 0 3 2 76.60 73.09 1.79 o 1 3 2 4.02 8.85 0.85 o 2 3 2 2.69 1.67 0.75 o 3 3 2 523.76 527.15 6.18 o 4 3 2 59.33 48.21 2.68 o 5 3 2 382.08 442.41 5.90 o 6 3 2 29.47 40.65 2.28 o 7 3 2 708.00 718.32 10.23 o 8 3 2 134.40 117.64 3.96 o 9 3 2 28.34 28.14 2.49 o 10 3 2 486.63 475.59 8.95 o 11 3 2 24.63 27.31 2.91 o 12 3 2 0.06 0.80 1.83 o 13 3 2 0.70 1.41 2.92 o -14 4 2 306.53 285.50 12.18 o -13 4 2 241.08 262.31 10.21 o -12 4 2 139.37 168.12 7.87 o -11 4 2 153.73 151.74 5.05 o -10 4 2 0.51 3.23 1.64 o -9 4 2 5.38 2.88 1.17 o -8 4 2 59.41 53.31 2.26 o -7 4 2 60.76 72.30 2.43 o -6 4 2 95.75 117.38 2.89 o -5 4 2 119.71 155.81 3.20 o -4 4 2 0.05 0.87 0.65 o -3 4 2 16.26 21.43 1.07 o -2 4 2 390.63 506.12 5.26 o -1 4 2 314.90 365.91 4.68 o 0 4 2 638.68 541.59 6.31 o 1 4 2 383.59 364.26 5.21 o 2 4 2 182.34 171.00 3.42 o 3 4 2 2.71 7.85 1.29 o 4 4 2 350.72 281.24 4.58 o 5 4 2 18.93 21.87 2.35 o 6 4 2 382.06 410.94 8.64 o 7 4 2 58.51 57.35 3.63 o 8 4 2 412.75 423.21 9.48 o 9 4 2 1440.11 1365.24 20.44 o 10 4 2 515.31 507.36 11.33 o 11 4 2 522.89 594.92 12.85 o 12 4 2 379.27 411.53 13.80 o 13 4 2 246.72 220.40 14.69 o -13 5 2 1.40 3.05 3.27 o -12 5 2 2.26 4.39 3.83 o -11 5 2 30.39 29.78 4.97 o -10 5 2 26.21 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