#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/23/2212352.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212352_Fobs loop_ _publ_author_name 'Tomyn, Stefaniya V.' 'Gumienna-Kontecka, El\'zbieta' 'Fritsky, Igor O.' 'Iskenderov, Turganbay S.' '\'Swiatek-Koz\/lowska, Jolanta' _publ_section_title ; \m-Oxalato-1\k^2^O,O':2\k^2^O'',O'''-bis(chloro{[1-(2-pyridyl-\kN)ethylidene]hydrazine-\kN}copper(II)) ; _journal_coeditor_code SA2033 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m438 _journal_page_last m440 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.420 _cell_angle_gamma 90.000 _cell_length_a 9.3780 _cell_length_b 9.2000 _cell_length_c 11.2500 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7476 _[local]_cod_data_source_file sa2033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' stza in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18966.17 18490.92 71.33 o 4 0 0 8832.83 8615.28 813.29 o 6 0 0 17959.24 17288.12 2545.93 o 8 0 0 7417.16 7457.79 978.71 o 10 0 0 1083.06 1182.94 52.43 o 12 0 0 883.33 1051.28 65.62 o 2 1 0 16.84 27.53 4.30 o 3 1 0 483.42 388.13 8.35 o 4 1 0 0.93 11.45 3.95 o 5 1 0 1208.40 1083.25 77.37 o 6 1 0 47.34 41.76 5.26 o 7 1 0 4254.43 4278.86 326.60 o 8 1 0 0.53 8.69 4.98 o 9 1 0 1143.68 1282.49 36.61 o 10 1 0 2.53 -1.61 11.69 o 11 1 0 41.51 43.07 16.19 o 12 1 0 65.25 51.16 24.65 o 0 2 0 8230.03 8852.67 510.76 o 1 2 0 92.07 84.31 7.30 o 2 2 0 29.05 18.46 3.77 o 3 2 0 96.98 81.94 4.64 o 4 2 0 507.35 688.81 12.29 o 5 2 0 1116.17 1207.77 16.82 o 6 2 0 1495.24 1671.08 45.93 o 7 2 0 967.59 997.46 68.74 o 8 2 0 274.95 309.36 16.19 o 9 2 0 340.40 345.75 53.68 o 10 2 0 107.48 125.23 19.51 o 11 2 0 175.95 154.51 34.47 o 1 3 0 11937.28 12565.33 277.67 o 2 3 0 1007.06 1042.11 53.67 o 3 3 0 2139.56 1997.73 88.77 o 4 3 0 1267.21 1376.67 62.96 o 5 3 0 1248.63 1241.71 26.44 o 6 3 0 1490.80 1674.45 27.50 o 7 3 0 5402.11 6102.32 78.18 o 8 3 0 303.21 341.90 17.21 o 9 3 0 851.78 945.58 88.68 o 10 3 0 212.59 202.58 34.02 o 11 3 0 1330.59 1427.71 68.61 o 0 4 0 768.48 887.81 68.67 o 1 4 0 576.17 645.31 13.56 o 2 4 0 147.99 134.97 5.98 o 3 4 0 8.50 16.92 3.41 o 4 4 0 1298.01 1354.56 56.86 o 5 4 0 416.62 394.04 17.00 o 6 4 0 655.34 694.00 16.67 o 7 4 0 358.98 360.20 14.41 o 8 4 0 114.14 113.77 14.60 o 9 4 0 36.59 32.21 24.35 o 10 4 0 6.88 21.11 22.76 o 11 4 0 102.65 123.13 32.41 o 1 5 0 897.37 877.56 11.12 o 2 5 0 127.54 134.54 9.09 o 3 5 0 3500.10 2886.77 374.26 o 4 5 0 35.17 22.77 5.21 o 5 5 0 2365.56 2502.67 76.76 o 6 5 0 210.44 219.07 12.88 o 7 5 0 682.99 732.05 34.67 o 8 5 0 434.45 470.30 26.53 o 9 5 0 1696.62 1792.02 69.46 o 10 5 0 208.77 242.41 40.14 o 0 6 0 9.19 18.53 8.30 o 1 6 0 91.11 90.91 8.67 o 2 6 0 311.39 269.61 17.82 o 3 6 0 0.34 7.23 4.91 o 4 6 0 102.08 106.86 10.72 o 5 6 0 1.89 7.68 5.32 o 6 6 0 354.58 392.10 18.85 o 7 6 0 3.02 7.66 9.95 o 8 6 0 578.12 593.03 32.68 o 9 6 0 292.97 240.59 35.65 o 10 6 0 98.63 83.29 29.65 o 1 7 0 1150.14 1151.86 32.96 o 2 7 0 20.76 30.82 8.89 o 3 7 0 847.74 886.96 29.72 o 4 7 0 252.35 273.94 15.90 o 5 7 0 649.61 704.44 23.89 o 6 7 0 110.69 111.15 16.75 o 7 7 0 1252.59 1347.62 59.62 o 8 7 0 11.67 20.37 12.18 o 9 7 0 179.42 150.30 40.39 o 0 8 0 2318.60 2527.79 188.40 o 1 8 0 4.19 11.18 6.60 o 2 8 0 8082.07 8510.07 330.63 o 3 8 0 8.78 14.35 6.64 o 4 8 0 4295.11 4687.76 169.44 o 5 8 0 206.19 215.22 23.71 o 6 8 0 3323.77 3618.03 61.05 o 7 8 0 32.58 35.84 16.52 o 8 8 0 2766.05 2967.78 109.58 o 1 9 0 1921.98 2098.11 74.69 o 2 9 0 123.12 112.76 15.42 o 3 9 0 2135.43 2438.76 201.86 o 4 9 0 0.08 8.11 13.66 o 5 9 0 1946.02 2166.04 58.63 o 6 9 0 19.10 24.65 17.32 o 7 9 0 1079.80 1149.64 43.34 o 8 9 0 184.19 162.47 23.39 o 0 10 0 286.47 267.19 35.99 o 1 10 0 0.91 18.83 9.62 o 2 10 0 265.07 245.67 20.57 o 3 10 0 1.67 16.44 15.99 o 4 10 0 334.34 376.20 32.13 o 5 10 0 154.61 113.88 42.83 o 6 10 0 63.16 43.02 18.26 o 1 11 0 1167.07 1090.87 48.97 o 2 11 0 168.94 113.48 40.78 o 3 11 0 507.18 470.89 61.87 o 4 11 0 131.10 106.57 23.85 o 0 12 0 986.87 1016.17 65.80 o 1 12 0 167.50 191.85 42.03 o -11 0 1 273.83 287.14 34.96 o -9 0 1 836.63 848.02 139.86 o -7 0 1 20.34 22.72 8.81 o -5 0 1 612.71 621.08 69.33 o -3 0 1 1364.95 1285.70 249.62 o 3 0 1 3058.51 3033.06 347.10 o 5 0 1 153.22 116.67 11.25 o 7 0 1 663.26 570.58 68.87 o 9 0 1 25.36 24.29 14.52 o 11 0 1 1261.74 1397.10 64.66 o -12 1 1 3.40 1.60 21.57 o -11 1 1 1679.26 1874.46 72.22 o -10 1 1 348.93 382.62 24.86 o -9 1 1 2432.24 2460.46 201.88 o -8 1 1 124.80 113.03 9.94 o -7 1 1 1845.37 1803.99 147.60 o -6 1 1 150.54 153.05 10.01 o -5 1 1 4492.46 4520.98 302.30 o -4 1 1 160.78 168.93 6.94 o -3 1 1 6094.28 6263.03 142.95 o -2 1 1 1599.99 1581.67 26.43 o -1 1 1 1123.18 1239.23 19.46 o 1 1 1 1886.76 1986.51 97.05 o 2 1 1 5877.99 6459.95 257.38 o 3 1 1 4362.35 4452.16 100.05 o 4 1 1 367.43 395.74 9.41 o 5 1 1 1948.05 1832.51 138.47 o 6 1 1 191.24 168.16 9.98 o 7 1 1 990.24 996.55 31.08 o 8 1 1 945.65 980.69 36.95 o 9 1 1 1253.62 1383.76 48.48 o 10 1 1 324.08 341.41 25.93 o 11 1 1 606.49 606.42 34.08 o 12 1 1 422.85 464.84 50.42 o -12 2 1 261.01 262.41 44.37 o -11 2 1 20.75 39.33 25.60 o -10 2 1 227.29 267.83 34.84 o -9 2 1 876.96 790.15 114.18 o -8 2 1 539.54 541.92 36.35 o -7 2 1 398.78 385.96 23.74 o -6 2 1 919.49 943.23 16.40 o -5 2 1 333.77 464.67 12.84 o -4 2 1 122.62 94.98 6.11 o -3 2 1 1807.20 2061.91 47.51 o -2 2 1 202.99 162.47 9.57 o -1 2 1 840.91 891.24 31.43 o 0 2 1 1551.35 1576.78 38.14 o 1 2 1 7318.49 7768.02 372.38 o 2 2 1 19.15 13.08 3.31 o 3 2 1 0.78 11.11 3.99 o 4 2 1 1923.67 2031.13 50.84 o 5 2 1 36.01 36.25 5.43 o 6 2 1 341.67 332.12 11.08 o 7 2 1 455.34 456.63 21.08 o 8 2 1 701.17 753.87 27.98 o 9 2 1 441.02 518.44 33.26 o 10 2 1 371.15 401.19 28.11 o 11 2 1 235.89 177.98 19.18 o -11 3 1 200.35 153.53 31.37 o -10 3 1 63.99 48.57 20.79 o -9 3 1 750.24 773.97 29.42 o -8 3 1 147.19 142.08 23.42 o -7 3 1 1970.48 2116.25 54.70 o -6 3 1 89.60 107.97 9.20 o -5 3 1 1913.97 1879.00 31.16 o -4 3 1 52.25 46.10 5.21 o -3 3 1 456.46 381.13 16.18 o -2 3 1 980.05 1023.15 65.04 o -1 3 1 4074.78 3925.76 121.10 o 0 3 1 3857.51 4479.28 110.20 o 1 3 1 6672.85 6654.21 258.76 o 2 3 1 81.89 79.35 5.80 o 3 3 1 1447.39 1400.95 56.78 o 4 3 1 12.36 20.56 5.98 o 5 3 1 951.18 993.88 17.10 o 6 3 1 0.89 10.46 5.21 o 7 3 1 2156.35 2358.44 28.65 o 8 3 1 410.68 471.13 25.68 o 9 3 1 652.19 708.78 30.57 o 10 3 1 44.11 43.44 17.19 o 11 3 1 24.75 20.39 26.83 o -11 4 1 34.57 25.66 24.17 o -10 4 1 1716.86 1973.29 70.50 o -9 4 1 72.36 63.56 22.68 o -8 4 1 4596.23 4925.40 78.93 o -7 4 1 167.93 180.52 13.56 o -6 4 1 10066.35 11014.81 271.92 o -5 4 1 32.66 32.77 6.95 o -4 4 1 9035.29 8376.37 408.58 o -3 4 1 543.18 566.70 24.25 o -2 4 1 12583.39 11564.05 579.18 o -1 4 1 3302.19 3828.97 86.39 o 0 4 1 28603.44 29924.74 483.87 o 1 4 1 728.82 868.38 28.09 o 2 4 1 23515.36 23071.93 1135.84 o 3 4 1 109.78 110.27 5.92 o 4 4 1 7830.82 7383.63 431.04 o 5 4 1 216.60 235.02 11.80 o 6 4 1 7106.54 7721.08 240.75 o 7 4 1 81.21 100.94 10.58 o 8 4 1 4577.87 4831.48 272.68 o 9 4 1 34.78 36.29 29.07 o 10 4 1 1482.99 1548.93 67.09 o -10 5 1 23.24 12.50 18.25 o -9 5 1 453.98 469.44 28.19 o -8 5 1 51.87 46.99 17.11 o -7 5 1 3116.10 3372.66 152.13 o -6 5 1 147.31 156.35 15.27 o -5 5 1 4125.36 4290.09 225.36 o -4 5 1 492.09 459.07 23.38 o -3 5 1 3478.29 3301.24 209.66 o -2 5 1 485.39 525.37 21.46 o -1 5 1 7754.29 8345.87 174.83 o 0 5 1 653.32 793.40 23.53 o 1 5 1 10047.24 11284.91 228.59 o 2 5 1 273.90 327.24 14.89 o 3 5 1 7058.13 7307.22 240.02 o 4 5 1 217.44 188.40 9.85 o 5 5 1 2129.76 2233.13 50.61 o 6 5 1 77.47 74.59 8.82 o 7 5 1 1752.61 1907.74 44.73 o 8 5 1 65.68 81.48 15.71 o 9 5 1 1193.60 1215.73 60.37 o 10 5 1 36.11 69.11 30.13 o -10 6 1 135.00 133.08 33.13 o -9 6 1 1.77 11.56 14.87 o -8 6 1 376.81 422.57 26.46 o -7 6 1 216.53 204.39 20.38 o -6 6 1 990.21 1020.72 53.07 o -5 6 1 68.98 47.29 10.63 o -4 6 1 837.03 893.86 40.87 o -3 6 1 285.53 336.57 18.21 o -2 6 1 14.29 40.41 9.03 o -1 6 1 0.79 11.25 5.87 o 0 6 1 1145.38 1192.12 35.85 o 1 6 1 93.86 103.67 7.66 o 2 6 1 2687.87 3031.79 85.97 o 3 6 1 937.36 910.70 36.97 o 4 6 1 280.80 257.16 14.45 o 5 6 1 816.33 823.23 36.32 o 6 6 1 69.86 76.88 10.88 o 7 6 1 160.77 153.11 13.24 o 8 6 1 97.41 90.65 19.43 o 9 6 1 151.53 131.47 35.58 o -9 7 1 383.94 421.49 65.14 o -8 7 1 492.69 523.09 24.98 o -7 7 1 4243.09 4557.63 193.96 o -6 7 1 982.41 1156.30 36.90 o -5 7 1 1897.35 1994.21 69.81 o -4 7 1 219.76 221.44 19.16 o -3 7 1 348.27 344.48 24.32 o -2 7 1 341.27 327.29 15.50 o -1 7 1 3053.44 3177.64 102.37 o 0 7 1 22.29 20.43 7.31 o 1 7 1 5374.36 5706.53 187.49 o 2 7 1 200.07 217.09 16.62 o 3 7 1 1581.33 1611.12 83.82 o 4 7 1 1578.70 1606.81 59.03 o 5 7 1 625.01 615.28 19.36 o 6 7 1 542.74 488.48 46.85 o 7 7 1 1207.27 1221.43 70.73 o 8 7 1 441.35 444.82 42.71 o 9 7 1 1420.14 1297.67 66.53 o -9 8 1 47.98 56.59 32.60 o -8 8 1 356.08 370.41 29.12 o -7 8 1 156.40 142.55 22.94 o -6 8 1 614.24 657.43 33.12 o -5 8 1 37.47 55.86 16.76 o -4 8 1 147.54 118.75 18.45 o -3 8 1 0.12 13.33 7.76 o -2 8 1 99.64 89.02 12.35 o -1 8 1 0.45 10.83 6.41 o 0 8 1 1961.10 2050.12 76.51 o 1 8 1 19.27 11.39 7.22 o 2 8 1 1936.26 1978.88 97.41 o 3 8 1 619.35 615.66 28.81 o 4 8 1 9.13 32.96 10.58 o 5 8 1 255.63 228.82 31.16 o 6 8 1 642.30 650.69 38.07 o 7 8 1 181.12 150.99 18.03 o 8 8 1 1199.34 1255.30 138.32 o -8 9 1 17.69 31.39 17.63 o -7 9 1 269.28 253.75 30.10 o -6 9 1 3.58 19.96 16.78 o -5 9 1 704.88 723.07 33.73 o -4 9 1 23.52 25.34 13.56 o -3 9 1 2506.77 2503.86 75.53 o -2 9 1 15.44 14.81 10.09 o -1 9 1 1626.07 1589.62 79.56 o 0 9 1 162.40 139.71 13.61 o 1 9 1 575.38 587.30 19.91 o 2 9 1 0.70 11.26 8.10 o 3 9 1 758.03 695.95 49.86 o 4 9 1 182.78 174.30 22.41 o 5 9 1 990.05 1086.53 45.19 o 6 9 1 244.50 259.34 24.55 o 7 9 1 577.05 610.25 35.33 o 8 9 1 139.59 126.37 33.99 o -6 10 1 72.85 81.61 23.70 o -5 10 1 340.01 317.44 37.50 o -4 10 1 305.07 280.02 28.28 o -3 10 1 83.91 85.15 17.80 o -2 10 1 798.93 756.54 32.16 o -1 10 1 1.27 7.06 12.58 o 0 10 1 172.03 149.25 18.14 o 1 10 1 60.15 73.63 14.44 o 2 10 1 123.05 119.51 15.93 o 3 10 1 0.74 17.94 16.66 o 4 10 1 89.89 118.03 24.76 o 5 10 1 51.14 60.06 18.63 o 6 10 1 313.84 302.12 33.86 o -4 11 1 1.60 8.16 18.65 o -3 11 1 256.62 212.13 30.39 o -2 11 1 403.98 405.48 33.16 o -1 11 1 67.63 61.37 16.32 o 0 11 1 10.58 25.55 13.43 o 1 11 1 67.30 44.45 13.32 o 2 11 1 1.42 17.74 14.62 o 3 11 1 15.34 19.76 16.83 o 4 11 1 2.00 18.98 28.69 o -1 12 1 14.64 9.78 24.98 o 0 12 1 1854.46 1798.61 54.61 o 1 12 1 2.52 12.81 14.95 o -10 0 2 410.63 387.89 58.19 o -8 0 2 7053.10 7106.13 1136.03 o -6 0 2 12386.32 11962.99 2036.23 o -4 0 2 17249.91 15461.25 2906.02 o -2 0 2 19754.70 16030.04 2855.09 o 2 0 2 59080.84 56520.75 4174.53 o 4 0 2 14158.88 12901.60 490.14 o 6 0 2 5983.71 6344.83 87.58 o 8 0 2 7108.20 7898.44 113.09 o 10 0 2 3347.05 3490.09 88.51 o -11 1 2 1041.20 1093.96 55.00 o -10 1 2 83.34 64.97 13.10 o -9 1 2 312.73 301.81 19.43 o -8 1 2 4.62 11.69 7.06 o -7 1 2 4485.79 4447.98 349.27 o -6 1 2 140.86 149.59 13.23 o -5 1 2 9659.59 9973.86 672.60 o -4 1 2 431.14 488.64 23.81 o -3 1 2 4736.07 4597.47 164.01 o -2 1 2 149.15 143.54 5.48 o -1 1 2 1879.26 1612.32 29.80 o 0 1 2 2212.99 2228.64 284.14 o 1 1 2 15449.64 15730.73 1033.82 o 2 1 2 12194.68 13160.14 622.32 o 3 1 2 6345.46 7012.21 253.55 o 4 1 2 0.58 5.86 2.64 o 5 1 2 2556.18 2565.07 168.93 o 6 1 2 511.23 552.63 17.51 o 7 1 2 636.48 686.99 26.49 o 8 1 2 203.70 203.52 18.04 o 9 1 2 1076.07 1089.96 36.36 o 10 1 2 55.05 41.02 15.50 o 11 1 2 466.38 439.54 36.40 o -12 2 2 172.13 161.29 35.72 o -11 2 2 314.20 289.85 36.77 o -10 2 2 222.08 150.58 48.04 o -9 2 2 773.38 733.00 62.85 o -8 2 2 771.67 788.39 45.71 o -7 2 2 5.77 14.35 6.40 o -6 2 2 1400.66 1595.37 51.68 o -5 2 2 872.13 960.69 18.63 o -4 2 2 4168.46 4476.19 95.96 o -3 2 2 438.07 476.25 14.97 o -2 2 2 255.59 202.00 13.02 o -1 2 2 0.52 5.51 2.72 o 0 2 2 1808.13 2132.96 103.54 o 1 2 2 2513.64 2789.92 129.06 o 2 2 2 4546.34 4533.51 203.93 o 3 2 2 114.57 115.15 6.50 o 4 2 2 1677.62 1711.11 45.47 o 5 2 2 472.30 484.54 12.56 o 6 2 2 94.94 131.06 9.45 o 7 2 2 607.72 569.77 18.77 o 8 2 2 283.98 307.89 22.34 o 9 2 2 282.81 327.35 27.38 o 10 2 2 182.64 180.55 24.10 o 11 2 2 167.55 165.02 21.60 o -11 3 2 519.76 499.13 42.45 o -10 3 2 233.67 208.55 26.52 o -9 3 2 1752.61 1671.74 125.78 o -8 3 2 9.09 14.52 11.22 o -7 3 2 1900.45 1950.18 77.21 o -6 3 2 476.72 561.49 14.33 o -5 3 2 5756.49 6096.09 69.12 o -4 3 2 447.46 512.07 17.01 o -3 3 2 1573.52 1353.27 46.00 o -2 3 2 59.50 49.03 5.58 o -1 3 2 3118.47 3183.09 64.38 o 0 3 2 494.03 535.87 19.99 o 1 3 2 731.73 665.15 25.87 o 2 3 2 1083.95 1134.25 45.42 o 3 3 2 6824.66 6738.55 346.41 o 4 3 2 143.56 115.97 7.31 o 5 3 2 3529.04 3606.37 113.46 o 6 3 2 1398.88 1475.13 49.01 o 7 3 2 1086.08 1121.26 51.18 o 8 3 2 918.76 911.11 32.14 o 9 3 2 2119.58 2311.04 123.77 o 10 3 2 413.97 446.63 30.12 o 11 3 2 668.93 686.37 37.84 o -11 4 2 22.17 50.96 31.75 o -10 4 2 157.88 99.61 17.87 o -9 4 2 52.32 43.12 15.62 o -8 4 2 435.26 454.24 25.22 o -7 4 2 35.63 53.17 10.47 o -6 4 2 291.35 269.12 14.58 o -5 4 2 6.53 14.99 4.26 o -4 4 2 78.62 81.82 4.99 o -3 4 2 182.40 206.71 9.17 o -2 4 2 15.59 32.01 6.03 o -1 4 2 182.97 157.18 7.87 o 0 4 2 535.28 583.81 12.61 o 1 4 2 651.36 644.22 20.81 o 2 4 2 8.30 12.40 4.07 o 3 4 2 56.44 44.24 5.38 o 4 4 2 500.74 538.97 23.39 o 5 4 2 261.45 270.06 12.05 o 6 4 2 253.19 282.23 13.77 o 7 4 2 569.87 576.22 24.22 o 8 4 2 501.77 507.31 27.29 o 9 4 2 577.38 589.31 35.42 o 10 4 2 1.60 10.32 16.11 o -11 5 2 1360.56 1479.69 68.64 o -10 5 2 77.90 83.87 21.87 o -9 5 2 493.29 512.43 29.76 o -8 5 2 18.98 17.31 7.72 o -7 5 2 1357.54 1318.74 56.27 o -6 5 2 51.76 60.32 8.93 o -5 5 2 3125.24 3076.98 189.87 o -4 5 2 73.27 48.64 8.12 o -3 5 2 4062.81 4125.08 183.08 o -2 5 2 244.07 279.97 11.73 o -1 5 2 2360.20 2346.81 74.41 o 0 5 2 90.29 70.70 7.22 o 1 5 2 5834.41 6392.71 185.94 o 2 5 2 8.18 15.19 5.08 o 3 5 2 1932.97 1969.99 85.66 o 4 5 2 261.24 272.88 11.17 o 5 5 2 396.71 415.43 15.00 o 6 5 2 63.53 53.98 8.55 o 7 5 2 819.97 886.40 31.59 o 8 5 2 724.04 731.89 46.25 o 9 5 2 296.59 288.02 28.65 o 10 5 2 310.48 249.63 46.25 o -10 6 2 219.06 212.57 28.44 o -9 6 2 6.50 39.31 19.08 o -8 6 2 95.11 83.60 15.13 o -7 6 2 344.68 349.77 18.97 o -6 6 2 1195.41 1288.52 28.52 o -5 6 2 101.47 88.82 13.80 o -4 6 2 264.80 277.71 19.25 o -3 6 2 0.48 9.76 5.89 o -2 6 2 139.67 147.09 9.14 o -1 6 2 5.11 11.52 5.00 o 0 6 2 2158.96 2353.58 61.86 o 1 6 2 957.98 1067.99 33.29 o 2 6 2 911.31 1037.68 22.66 o 3 6 2 823.38 777.02 37.85 o 4 6 2 29.91 30.62 7.64 o 5 6 2 50.95 48.00 9.11 o 6 6 2 48.66 51.77 9.06 o 7 6 2 447.37 458.75 34.49 o 8 6 2 356.59 346.53 21.54 o 9 6 2 439.43 406.95 49.03 o -10 7 2 11.78 12.91 21.86 o -9 7 2 51.50 68.65 31.49 o -8 7 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