#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/25/2212583.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2212583_Fobs
loop_
_publ_author_name
'Amini, Mostafa M.'
'Alijani, Vajihe'
'Azadmeher, Amirreza'
'Ng, Seik Weng'
_publ_section_title
;
A hexagonal modification of
catena-poly[[ethyldiphenyltin(IV)]-\m-2-chloroacetato-\k^2^O:O']
;
_journal_coeditor_code HB2303
_journal_issue 3
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m913
_journal_page_last m914
_journal_volume 63
_journal_year 2007
_space_group_IT_number 169
_symmetry_space_group_name_Hall 'P 61'
_symmetry_space_group_name_H-M 'P 61'
_cell_angle_alpha 90.000
_cell_angle_beta 90.000
_cell_angle_gamma 120.000
_cell_length_a 10.8105
_cell_length_b 10.8105
_cell_length_c 25.8402
_exptl_crystal_F_000 1176.00
_reflns_d_resolution_high 0.8410
_[local]_cod_data_source_file hb2303Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' P61'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 216.41
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y, x-y, z+1/3'
'y, -x+y, z+5/6'
'-x+y, -x, z+2/3'
'x-y, x, z+1/6'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 0 -30 10086.56 9586.42 381.34 o
0 1 -30 260.09 243.01 32.57 o
-1 2 -30 1628.60 1607.34 51.35 o
0 2 -30 417.21 423.63 34.86 o
0 1 -29 1677.67 1918.58 53.33 o
-1 2 -29 1013.17 1014.45 40.79 o
0 2 -29 1556.97 1613.54 51.57 o
-2 3 -29 3147.04 2993.31 66.38 o
-1 3 -29 98.93 42.79 30.57 o
0 3 -29 2091.19 2075.80 55.61 o
-3 4 -29 1179.62 1190.40 46.26 o
-2 4 -29 427.31 513.56 35.27 o
-1 4 -29 265.63 227.54 33.25 o
0 1 -28 3795.59 3671.10 74.02 o
-1 2 -28 905.57 1006.68 41.49 o
0 2 -28 528.72 519.27 33.47 o
-2 3 -28 210.63 202.87 31.84 o
-1 3 -28 1647.42 1520.79 48.03 o
0 3 -28 521.16 563.88 34.42 o
-3 4 -28 1912.94 1737.13 52.02 o
-2 4 -28 2343.26 2295.30 57.63 o
-1 4 -28 2119.16 2251.62 58.06 o
0 4 -28 535.19 569.82 35.55 o
-4 5 -28 395.45 397.84 34.58 o
-3 5 -28 837.28 810.44 39.08 o
-2 5 -28 61.78 37.05 31.84 o
-1 5 -28 1143.47 1141.83 44.57 o
0 1 -27 358.46 448.47 32.54 o
-1 2 -27 3935.47 3885.67 74.38 o
0 2 -27 2149.60 2257.09 55.18 o
-2 3 -27 2.41 -0.86 28.31 o
-1 3 -27 2822.45 2926.33 63.96 o
0 3 -27 57.80 88.64 29.12 o
-3 4 -27 3115.50 2933.83 64.74 o
-2 4 -27 766.73 717.46 36.36 o
-1 4 -27 564.98 592.38 34.35 o
0 4 -27 5195.45 5261.98 93.99 o
-4 5 -27 229.35 162.11 30.48 o
-3 5 -27 2276.65 2025.82 54.61 o
-2 5 -27 137.29 65.46 30.30 o
-1 5 -27 685.34 707.33 36.86 o
0 5 -27 97.93 59.56 30.37 o
-4 6 -27 1163.67 1136.63 42.32 o
-3 6 -27 1767.06 1768.62 54.67 o
-2 6 -27 60.48 59.84 30.35 o
0 1 -26 1894.41 1867.46 49.86 o
-1 2 -26 912.34 957.10 38.56 o
0 2 -26 1898.23 2015.18 53.19 o
-2 3 -26 273.60 226.02 30.37 o
-1 3 -26 4054.76 3689.74 72.12 o
0 3 -26 12.41 49.81 27.96 o
-3 4 -26 900.52 828.95 37.39 o
-2 4 -26 4617.21 4808.17 86.04 o
-1 4 -26 5215.67 5296.82 93.03 o
0 4 -26 95.96 72.96 29.09 o
-4 5 -26 1310.39 1196.78 42.02 o
-3 5 -26 1518.67 1474.90 49.31 o
-2 5 -26 72.93 63.91 29.43 o
-1 5 -26 1879.33 1916.51 53.40 o
0 5 -26 1525.81 1490.45 45.53 o
-5 6 -26 24.34 1.38 27.44 o
-4 6 -26 956.74 1072.59 40.56 o
-3 6 -26 1142.75 1093.56 41.56 o
-2 6 -26 38.43 124.89 30.54 o
-1 6 -26 569.92 600.22 32.51 o
0 1 -25 881.64 912.40 35.30 o
-1 2 -25 1001.92 1111.78 40.98 o
0 2 -25 3117.35 2930.86 61.50 o
-2 3 -25 3458.02 3550.30 68.42 o
-1 3 -25 169.32 171.96 28.66 o
0 3 -25 4980.37 4834.67 85.82 o
-3 4 -25 2467.03 2344.78 55.33 o
-2 4 -25 89.92 110.25 28.98 o
-1 4 -25 1402.86 1450.51 46.97 o
0 4 -25 263.86 225.47 29.47 o
-4 5 -25 3619.36 3451.21 66.68 o
-3 5 -25 1544.63 1639.04 46.96 o
-2 5 -25 1642.34 1762.85 50.27 o
-1 5 -25 1564.45 1486.97 47.72 o
0 5 -25 1717.86 1678.68 47.86 o
-5 6 -25 246.47 245.40 29.20 o
-4 6 -25 1160.37 1276.54 43.20 o
-3 6 -25 1809.56 1732.80 47.92 o
-2 6 -25 2539.95 2391.40 51.23 o
-1 6 -25 116.51 77.74 26.49 o
0 6 -25 469.58 478.52 40.19 o
-5 7 -25 128.57 90.37 30.42 o
-4 7 -25 852.37 761.60 36.85 o
-3 7 -25 359.41 378.35 32.04 o
-2 7 -25 1649.51 1680.58 46.19 o
0 0 -24 16146.86 16021.31 546.56 o
0 1 -24 547.74 609.03 30.83 o
-1 2 -24 989.31 943.07 36.68 o
0 2 -24 609.12 599.66 31.24 o
-2 3 -24 4461.40 4443.54 80.44 o
-1 3 -24 3225.79 3361.22 65.62 o
0 3 -24 3656.01 3484.60 68.40 o
-3 4 -24 207.18 207.58 28.32 o
-2 4 -24 1564.86 1491.25 46.56 o
-1 4 -24 529.75 521.80 31.55 o
0 4 -24 1970.61 1907.71 46.89 o
-4 5 -24 199.25 228.31 27.25 o
-3 5 -24 372.30 401.92 29.57 o
-2 5 -24 5343.15 5303.81 91.90 o
-1 5 -24 15.02 19.30 25.82 o
0 5 -24 244.38 297.11 28.19 o
-5 6 -24 6566.50 6322.96 99.63 o
-4 6 -24 500.12 533.33 32.48 o
-3 6 -24 146.82 143.97 28.85 o
-2 6 -24 1014.52 1071.85 35.69 o
-1 6 -24 2514.22 2450.59 55.39 o
0 6 -24 182.94 180.08 32.75 o
-6 7 -24 613.19 572.25 40.97 o
-5 7 -24 819.57 749.72 36.75 o
-4 7 -24 123.35 80.31 29.30 o
-3 7 -24 999.98 949.52 38.34 o
-2 7 -24 454.39 476.30 28.70 o
-1 7 -24 1037.60 1190.29 44.76 o
-4 8 -24 2373.73 2393.45 57.45 o
0 1 -23 3180.03 3181.53 62.03 o
-1 2 -23 3764.76 3869.18 70.66 o
0 2 -23 5076.53 5413.45 91.42 o
-2 3 -23 1885.52 1663.73 46.49 o
-1 3 -23 492.69 495.74 29.66 o
0 3 -23 3288.04 3328.06 61.50 o
-3 4 -23 3964.15 3863.17 64.53 o
-2 4 -23 90.54 88.27 26.15 o
-1 4 -23 1562.91 1631.79 43.73 o
0 4 -23 717.04 739.38 30.21 o
-4 5 -23 3524.01 3580.85 62.49 o
-3 5 -23 1362.70 1243.50 38.49 o
-2 5 -23 453.94 435.53 27.89 o
-1 5 -23 3001.94 2935.52 54.62 o
0 5 -23 1921.67 1765.87 43.91 o
-5 6 -23 2005.98 2102.36 48.94 o
-4 6 -23 1698.03 1683.10 44.83 o
-3 6 -23 3013.24 2812.94 53.20 o
-2 6 -23 2975.96 2853.19 53.22 o
-1 6 -23 49.05 30.79 22.56 o
0 6 -23 1336.04 1371.32 49.05 o
-6 7 -23 404.64 422.40 36.84 o
-5 7 -23 142.42 112.87 28.03 o
-4 7 -23 749.31 809.37 33.14 o
-3 7 -23 191.19 156.98 25.92 o
-2 7 -23 1424.32 1246.23 37.14 o
-1 7 -23 1541.44 1563.43 49.74 o
0 7 -23 318.72 248.34 36.29 o
-6 8 -23 526.53 617.46 40.47 o
-5 8 -23 1864.27 1767.71 48.73 o
-4 8 -23 282.24 331.69 36.37 o
-3 8 -23 128.63 197.38 28.44 o
-2 8 -23 800.78 875.77 40.22 o
0 1 -22 4939.14 4709.96 74.98 o
-1 2 -22 1319.28 1350.50 38.74 o
0 2 -22 2843.39 2751.97 54.75 o
-2 3 -22 734.37 787.17 28.86 o
-1 3 -22 4058.46 4370.44 70.81 o
0 3 -22 71.53 79.86 20.83 o
-3 4 -22 4918.35 4728.87 70.24 o
-2 4 -22 5412.69 5432.20 77.52 o
-1 4 -22 4186.62 3913.17 61.29 o
0 4 -22 1529.24 1446.37 34.45 o
-4 5 -22 515.70 507.45 25.19 o
-3 5 -22 1413.98 1422.53 38.00 o
-2 5 -22 39.03 15.80 20.82 o
-1 5 -22 4204.19 4103.03 56.14 o
0 5 -22 718.42 709.73 26.73 o
-5 6 -22 42.20 35.09 19.83 o
-4 6 -22 2949.79 2809.71 51.79 o
-3 6 -22 2477.36 2546.84 46.87 o
-2 6 -22 589.21 476.12 25.19 o
-1 6 -22 1250.67 1293.46 32.97 o
0 6 -22 1660.08 1566.25 50.92 o
-6 7 -22 1726.67 1985.71 56.59 o
-5 7 -22 2756.36 2504.04 54.26 o
-4 7 -22 544.86 571.59 29.45 o
-3 7 -22 1270.98 1276.11 36.53 o
-2 7 -22 837.65 826.94 31.73 o
-1 7 -22 1241.37 1207.90 42.17 o
0 7 -22 571.95 576.06 38.73 o
-7 8 -22 34.81 29.77 34.86 o
-6 8 -22 283.93 242.86 36.29 o
-5 8 -22 767.47 781.64 36.88 o
-4 8 -22 108.16 77.40 26.98 o
-3 8 -22 3361.80 3235.41 56.17 o
-2 8 -22 77.63 79.87 32.09 o
-1 8 -22 746.84 730.23 39.62 o
0 1 -21 147.48 192.78 15.72 o
-1 2 -21 7625.24 7569.72 90.96 o
0 2 -21 1126.30 1228.18 31.20 o
-2 3 -21 21.62 26.60 18.75 o
-1 3 -21 4137.03 4044.80 57.26 o
0 3 -21 260.57 296.72 20.36 o
-3 4 -21 4346.69 4526.76 63.00 o
-2 4 -21 2516.17 2525.32 40.85 o
-1 4 -21 240.46 282.14 20.59 o
0 4 -21 11843.41 11333.46 128.89 o
-4 5 -21 629.40 726.12 28.18 o
-3 5 -21 3143.27 3246.39 50.36 o
-2 5 -21 63.48 44.19 18.33 o
-1 5 -21 265.81 222.73 18.88 o
0 5 -21 8.27 4.59 16.98 o
-5 6 -21 8.66 -11.39 22.08 o
-4 6 -21 832.78 877.21 31.33 o
-3 6 -21 3102.53 3040.59 50.44 o
-2 6 -21 132.65 125.49 19.84 o
-1 6 -21 5979.82 5822.48 85.85 o
0 6 -21 7.88 21.68 29.34 o
-6 7 -21 395.15 444.35 33.59 o
-5 7 -21 1045.81 1132.83 36.66 o
-4 7 -21 1176.91 1239.88 40.67 o
-3 7 -21 4811.24 4757.94 68.69 o
-2 7 -21 172.40 174.02 23.13 o
-1 7 -21 30.40 18.09 30.16 o
0 7 -21 1946.29 1799.37 51.12 o
-7 8 -21 2.62 -16.50 34.15 o
-6 8 -21 1691.96 1601.60 50.91 o
-5 8 -21 535.50 512.93 34.22 o
-4 8 -21 72.48 49.80 26.39 o
-3 8 -21 318.32 331.63 25.75 o
-2 8 -21 98.78 73.33 30.40 o
-1 8 -21 109.98 107.08 33.17 o
0 8 -21 1321.39 1336.74 47.75 o
-6 9 -21 2441.29 2498.17 57.59 o
-5 9 -21 84.63 52.81 27.16 o
-4 9 -21 417.15 348.40 33.02 o
-3 9 -21 1039.06 1164.78 42.09 o
0 1 -20 8607.53 9138.15 89.09 o
-1 2 -20 1638.21 1697.82 30.03 o
0 2 -20 3112.11 3345.88 39.90 o
-2 3 -20 3275.18 3202.04 40.75 o
-1 3 -20 2126.45 2204.13 35.02 o
0 3 -20 1570.06 1533.72 32.51 o
-3 4 -20 3319.86 3447.15 47.57 o
-2 4 -20 4299.96 4554.81 60.91 o
-1 4 -20 3872.19 3547.91 46.30 o
0 4 -20 2471.97 2559.99 41.46 o
-4 5 -20 1827.36 1672.62 33.89 o
-3 5 -20 3335.81 3303.30 48.46 o
-2 5 -20 111.82 130.59 18.72 o
-1 5 -20 2675.71 2565.13 40.14 o
0 5 -20 2030.34 1900.13 33.98 o
-5 6 -20 36.09 62.89 26.79 o
-4 6 -20 2095.34 2340.51 45.77 o
-3 6 -20 919.20 962.17 30.17 o
-2 6 -20 2112.53 2166.36 38.98 o
-1 6 -20 218.01 175.67 26.19 o
0 6 -20 3917.52 3922.68 62.56 o
-6 7 -20 2933.59 2661.02 59.36 o
-5 7 -20 2272.54 2225.14 42.65 o
-4 7 -20 2426.86 2390.03 45.20 o
-3 7 -20 1453.23 1399.94 38.52 o
-2 7 -20 1165.04 1047.92 33.79 o
-1 7 -20 814.76 847.09 34.38 o
0 7 -20 943.35 1010.04 40.26 o
-7 8 -20 513.26 483.84 35.27 o
-6 8 -20 985.14 1071.87 40.24 o
-5 8 -20 944.12 853.39 37.77 o
-4 8 -20 239.67 263.93 26.40 o
-3 8 -20 2246.75 2454.95 63.31 o
-2 8 -20 208.78 143.75 29.53 o
-1 8 -20 376.43 374.37 35.87 o
0 8 -20 428.34 472.68 36.91 o
-7 9 -20 154.44 92.80 33.78 o
-6 9 -20 80.26 56.55 24.91 o
-5 9 -20 541.80 614.56 32.11 o
-4 9 -20 1096.70 1086.93 41.36 o
-3 9 -20 2247.65 2300.14 57.44 o
-2 9 -20 75.38 84.91 31.71 o
0 1 -19 7255.00 7664.49 75.78 o
-1 2 -19 5720.44 6270.13 61.96 o
0 2 -19 8459.36 8692.66 83.60 o
-2 3 -19 2139.81 2272.32 33.95 o
-1 3 -19 2775.09 2822.33 38.70 o
0 3 -19 2874.95 2606.82 38.31 o
-3 4 -19 2531.72 2324.88 37.16 o
-2 4 -19 825.19 841.45 21.17 o
-1 4 -19 2989.20 2885.35 39.34 o
0 4 -19 407.90 369.79 20.15 o
-4 5 -19 3494.28 3350.16 48.61 o
-3 5 -19 1697.34 1713.45 31.94 o
-2 5 -19 2316.38 2246.98 36.64 o
-1 5 -19 3728.00 3516.65 49.01 o
0 5 -19 5962.14 6118.67 82.08 o
-5 6 -19 417.40 452.01 28.52 o
-4 6 -19 2690.67 2683.81 42.76 o
-3 6 -19 2678.76 2729.96 41.68 o
-2 6 -19 2404.30 2352.05 40.26 o
-1 6 -19 435.68 409.24 26.24 o
0 6 -19 3267.51 3159.45 55.01 o
-6 7 -19 267.42 227.42 29.64 o
-5 7 -19 423.62 499.67 24.70 o
-4 7 -19 2290.99 2020.53 41.82 o
-3 7 -19 614.89 580.75 26.57 o
-2 7 -19 1274.98 1311.98 32.64 o
-1 7 -19 3742.22 3837.71 62.34 o
0 7 -19 609.93 688.72 32.10 o
-7 8 -19 2514.99 2333.09 54.66 o
-6 8 -19 1691.56 1643.02 50.34 o
-5 8 -19 2186.46 2222.94 48.57 o
-4 8 -19 812.10 807.46 30.08 o
-3 8 -19 23.17 32.76 24.04 o
-2 8 -19 1968.91 1964.17 48.98 o
-1 8 -19 2727.17 2818.18 58.83 o
0 8 -19 566.43 670.90 38.27 o
-8 9 -19 1332.87 1238.18 47.46 o
-7 9 -19 1468.92 1661.19 52.79 o
-6 9 -19 245.71 162.57 25.88 o
-5 9 -19 1793.39 1762.16 45.95 o
-4 9 -19 222.20 289.14 27.05 o
-3 9 -19 179.74 181.06 25.93 o
-2 9 -19 244.10 119.15 32.50 o
-1 9 -19 593.83 581.92 37.20 o
-6 10 -19 509.53 475.05 31.78 o
-5 10 -19 67.44 35.28 28.35 o
-4 10 -19 1080.26 1044.16 38.95 o
0 0 -18 32250.79 30978.36 631.17 o
0 1 -18 1324.06 1555.62 24.85 o
-1 2 -18 4104.17 4454.24 47.79 o
0 2 -18 574.08 533.48 16.01 o
-2 3 -18 8935.86 9033.94 88.31 o
-1 3 -18 1331.19 1448.76 26.43 o
0 3 -18 8490.08 8626.20 92.08 o
-3 4 -18 1466.82 1329.21 28.28 o
-2 4 -18 4240.62 3881.08 44.31 o
-1 4 -18 827.47 858.86 21.44 o
0 4 -18 4298.16 3933.57 50.22 o
-4 5 -18 1027.01 1162.53 28.98 o
-3 5 -18 1297.42 1195.67 27.19 o
-2 5 -18 4978.72 4999.36 61.41 o
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-5 6 -18 9524.17 9683.11 126.48 o
-4 6 -18 247.34 268.65 19.47 o
-3 6 -18 235.56 251.94 20.78 o
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0 6 -18 686.01 831.45 30.92 o
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-4 7 -18 407.01 372.79 22.13 o
-3 7 -18 2367.10 2473.28 42.74 o
-2 7 -18 194.45 235.76 19.20 o
-1 7 -18 899.53 908.73 33.10 o
0 7 -18 1336.55 1196.64 37.38 o
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-6 8 -18 388.92 320.27 31.74 o
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-1 8 -18 553.97 504.51 31.27 o
0 8 -18 494.20 571.64 33.23 o
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-7 9 -18 1002.90 1142.49 44.47 o
-6 9 -18 1025.90 973.60 41.82 o
-5 9 -18 444.79 424.02 30.39 o
-4 9 -18 830.46 837.31 31.52 o
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0 1 -17 4849.76 5141.58 50.90 o
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-2 3 -17 5614.40 5574.85 58.43 o
-1 3 -17 1223.79 1081.26 23.28 o
0 3 -17 5867.26 5328.80 61.49 o
-3 4 -17 4908.57 4780.19 53.76 o
-2 4 -17 326.89 350.85 16.06 o
-1 4 -17 2360.54 2370.19 33.70 o
0 4 -17 207.45 281.59 14.79 o
-4 5 -17 4048.81 4002.95 49.54 o
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-2 5 -17 1680.57 1582.02 29.75 o
-1 5 -17 3741.93 3478.70 42.97 o
0 5 -17 1856.40 1759.65 42.82 o
-5 6 -17 1952.17 1958.22 43.61 o
-4 6 -17 2180.29 2053.63 37.29 o
-3 6 -17 3426.19 3553.04 48.08 o
-2 6 -17 6870.75 7207.06 79.71 o
-1 6 -17 48.60 42.62 23.59 o
0 6 -17 766.14 863.88 30.47 o
-6 7 -17 622.93 585.10 30.22 o
-5 7 -17 717.62 762.18 27.03 o
-4 7 -17 1038.71 1063.37 29.45 o
-3 7 -17 497.46 459.52 21.63 o
-2 7 -17 1550.30 1536.23 33.00 o
-1 7 -17 2449.94 2318.81 47.56 o
0 7 -17 126.67 107.85 26.94 o
-7 8 -17 2820.82 2902.43 56.29 o
-6 8 -17 558.32 655.78 26.56 o
-5 8 -17 3032.58 2855.60 49.91 o
-4 8 -17 2494.23 2571.33 51.23 o
-3 8 -17 15.10 16.25 23.88 o
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0 8 -17 1231.37 1165.38 38.38 o
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