#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/25/2212594.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212594_Fobs loop_ _publ_author_name 'Pruka\/la, Wies\/law' 'Marciniec, Bogdan' 'Kubicki, Maciej' _publ_section_title ; Tetra-n-butylammonium iodide: a space-group revision ; _journal_coeditor_code HG2184 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1464 _journal_page_last o1466 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.149 _cell_angle_gamma 90.000 _cell_length_a 14.2806 _cell_length_b 14.1864 _cell_length_c 19.5951 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.7188 _[local]_cod_data_source_file hg2184Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wp21_05 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 613.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15944.26 16772.15 66.57 o 4 0 0 43108.47 41439.54 578.31 o 6 0 0 77271.85 75348.63 468.73 o 8 0 0 42032.55 41479.80 293.31 o 10 0 0 19686.10 19742.56 185.50 o 12 0 0 12024.35 11549.44 143.58 o 14 0 0 904.18 907.81 106.93 o 16 0 0 0.80 17.01 141.35 o 1 1 0 152.98 204.08 88.08 o 3 1 0 30167.69 30628.17 181.02 o 5 1 0 9821.01 9733.96 79.96 o 7 1 0 34588.05 35207.77 107.62 o 9 1 0 31893.52 32021.95 191.96 o 11 1 0 29876.58 28814.82 211.09 o 13 1 0 27910.61 27677.23 163.64 o 15 1 0 16918.55 17011.93 361.27 o 17 1 0 10645.57 11182.75 190.03 o 0 2 0 8557.84 9888.02 51.04 o 2 2 0 145896.05 134943.45 967.37 o 4 2 0 91983.61 88407.61 192.35 o 6 2 0 80174.13 78269.16 708.90 o 8 2 0 43537.75 43052.83 228.69 o 10 2 0 7283.38 6864.53 74.09 o 12 2 0 287.08 291.44 31.41 o 14 2 0 3288.52 3304.42 71.14 o 16 2 0 1.78 10.11 12.19 o 1 3 0 3328.27 3748.10 69.81 o 3 3 0 11226.53 12206.33 93.96 o 5 3 0 28558.42 29048.34 103.45 o 7 3 0 25085.82 23655.99 113.31 o 9 3 0 33374.45 34120.25 206.00 o 11 3 0 42202.57 42250.62 325.38 o 13 3 0 19147.43 19066.42 242.17 o 15 3 0 17737.37 17661.02 151.55 o 17 3 0 18046.49 18344.85 237.50 o 0 4 0 323786.66 298385.34 16833.57 o 2 4 0 129619.51 121519.43 1092.66 o 4 4 0 39048.35 35143.07 125.38 o 6 4 0 29913.60 27799.73 260.84 o 8 4 0 51499.41 51529.87 579.14 o 10 4 0 8730.50 8507.58 83.44 o 12 4 0 14224.36 13674.85 129.77 o 14 4 0 688.74 644.92 53.40 o 16 4 0 259.26 220.57 60.90 o 1 5 0 458.85 535.38 119.02 o 3 5 0 10212.55 10615.38 94.46 o 5 5 0 7309.58 6719.75 70.31 o 7 5 0 33223.55 33092.93 154.62 o 9 5 0 25771.84 25271.45 149.43 o 11 5 0 12853.93 12642.62 134.51 o 13 5 0 36030.93 35088.92 248.43 o 15 5 0 13689.75 13805.60 406.30 o 17 5 0 6020.56 6438.11 127.33 o 0 6 0 111303.38 105381.55 697.46 o 2 6 0 76739.77 73659.97 1280.11 o 4 6 0 59225.57 55800.61 384.51 o 6 6 0 107425.74 106060.30 270.08 o 8 6 0 24911.25 24095.27 164.47 o 10 6 0 6732.67 6453.65 98.81 o 12 6 0 1369.73 1389.40 51.63 o 14 6 0 4087.97 4307.48 155.02 o 16 6 0 34.73 88.84 70.96 o 1 7 0 981.06 1140.24 42.81 o 3 7 0 2183.82 1975.77 40.03 o 5 7 0 20460.26 20357.00 165.83 o 7 7 0 22879.95 23067.69 110.57 o 9 7 0 23112.51 22543.63 225.19 o 11 7 0 28408.05 28494.18 225.42 o 13 7 0 15406.51 15348.09 197.40 o 15 7 0 18841.64 18842.20 238.20 o 0 8 0 82053.35 83204.71 299.19 o 2 8 0 62343.98 59805.66 659.57 o 4 8 0 44452.66 43189.04 388.87 o 6 8 0 26255.73 25426.54 372.66 o 8 8 0 13357.60 13052.99 145.56 o 10 8 0 11583.99 11703.03 161.60 o 12 8 0 8347.88 8329.80 212.62 o 14 8 0 64.10 155.85 73.41 o 16 8 0 15.36 6.75 29.86 o 1 9 0 1640.21 1552.76 43.30 o 3 9 0 1392.94 1334.44 48.76 o 5 9 0 20404.39 20013.62 118.39 o 7 9 0 13712.10 13650.83 163.87 o 9 9 0 18395.73 18261.06 179.33 o 11 9 0 17321.35 17414.75 226.01 o 13 9 0 15993.51 15940.65 181.92 o 15 9 0 17000.13 17186.48 233.54 o 0 10 0 52510.04 50231.62 352.29 o 2 10 0 56327.15 55004.57 400.75 o 4 10 0 35242.06 35417.90 374.18 o 6 10 0 63059.94 60427.59 499.82 o 8 10 0 17209.20 17346.78 198.67 o 10 10 0 4872.24 4895.39 127.80 o 12 10 0 1118.90 1012.09 65.18 o 14 10 0 3985.90 3816.07 107.79 o 1 11 0 90.02 209.21 31.23 o 3 11 0 2676.10 2680.86 59.88 o 5 11 0 7350.05 6975.39 99.02 o 7 11 0 19595.04 19348.50 402.64 o 9 11 0 13628.25 14191.65 356.72 o 11 11 0 7827.27 7686.62 198.91 o 13 11 0 18919.14 18548.47 249.88 o 0 12 0 48038.68 47558.62 381.65 o 2 12 0 38012.05 36295.28 202.63 o 4 12 0 25610.36 24601.87 214.77 o 6 12 0 12862.21 12352.43 175.58 o 8 12 0 15913.54 15920.23 204.40 o 10 12 0 2365.01 2406.88 144.42 o 12 12 0 8301.15 8375.08 173.52 o 1 13 0 1072.22 1052.62 61.61 o 3 13 0 2164.43 2003.96 62.35 o 5 13 0 8011.52 7976.29 113.42 o 7 13 0 8904.37 9159.60 161.18 o 9 13 0 10081.19 10185.13 181.94 o 11 13 0 17161.63 17306.81 347.31 o 13 13 0 10759.34 11517.42 313.34 o 0 14 0 18258.33 17841.92 260.80 o 2 14 0 33019.30 32414.14 210.69 o 4 14 0 18695.69 18666.76 173.50 o 6 14 0 24824.40 24082.34 241.62 o 8 14 0 10537.93 10542.82 186.60 o 10 14 0 3760.78 3727.23 136.44 o 12 14 0 263.04 239.67 78.76 o 1 15 0 11.85 16.97 46.36 o 3 15 0 2207.27 1944.48 68.42 o 5 15 0 4977.98 4812.26 85.17 o 7 15 0 6152.34 6326.73 384.33 o 9 15 0 9768.71 9663.51 192.41 o 11 15 0 5862.43 5844.78 233.44 o 0 16 0 62265.78 61759.57 519.04 o 2 16 0 9535.07 9511.39 154.04 o 4 16 0 13630.39 13402.92 181.54 o 6 16 0 13056.89 13115.87 140.55 o 8 16 0 7384.38 7781.44 174.52 o 1 17 0 497.26 452.22 63.26 o 3 17 0 2747.63 2706.71 94.70 o 5 17 0 1286.60 1211.67 60.42 o 7 17 0 6811.50 6776.07 169.95 o 0 18 0 8226.46 8183.57 214.26 o 2 18 0 14439.24 14679.39 199.90 o 4 18 0 9615.71 9687.89 239.16 o 6 18 0 8163.57 8029.96 221.54 o 3 19 0 1267.78 1124.00 120.47 o 5 19 0 2682.24 2429.16 142.16 o -17 1 1 82.62 29.62 26.31 o -15 1 1 27.17 93.41 62.70 o -13 1 1 2313.34 2273.66 58.47 o -11 1 1 128.50 92.49 25.40 o -9 1 1 127.81 92.46 21.40 o -7 1 1 277.25 338.66 14.40 o -5 1 1 360.76 438.62 16.67 o -3 1 1 6738.46 7151.05 54.66 o 1 1 1 66.93 243.50 91.80 o 3 1 1 36241.08 39293.24 245.93 o 5 1 1 5413.16 6453.66 35.48 o 7 1 1 14.53 13.50 9.54 o 9 1 1 126.41 157.68 19.01 o 11 1 1 333.56 318.08 31.42 o 13 1 1 1595.51 1674.11 61.48 o 15 1 1 306.18 243.44 69.99 o 17 1 1 172.92 211.79 70.99 o -18 2 1 10.21 57.31 86.57 o -16 2 1 0.34 1.59 23.99 o -14 2 1 59.44 79.82 28.71 o -12 2 1 308.16 231.71 36.01 o -10 2 1 108.08 95.83 25.38 o -8 2 1 268.05 235.11 23.09 o -6 2 1 10.88 38.81 12.75 o -4 2 1 2342.06 2751.59 35.87 o -2 2 1 0.93 156.25 11.96 o 0 2 1 0.40 56.73 7.39 o 2 2 1 90.19 237.40 10.68 o 4 2 1 5376.78 6120.59 58.50 o 6 2 1 801.15 908.16 18.77 o 8 2 1 18.01 63.32 24.72 o 10 2 1 28.47 27.77 26.22 o 12 2 1 282.04 218.27 31.61 o 14 2 1 55.17 80.66 46.35 o 16 2 1 105.08 91.42 58.34 o -17 3 1 211.53 152.16 76.72 o -15 3 1 340.01 320.80 47.24 o -13 3 1 386.78 364.26 40.13 o -11 3 1 50.20 77.16 22.90 o -9 3 1 362.14 329.03 27.61 o -7 3 1 53.61 79.70 17.71 o -5 3 1 24.21 112.66 14.75 o -3 3 1 0.31 71.97 21.90 o -1 3 1 5816.73 6376.59 79.33 o 1 3 1 28671.00 30938.47 446.51 o 3 3 1 25.28 46.04 10.77 o 5 3 1 584.78 609.11 23.11 o 7 3 1 636.03 627.78 27.73 o 9 3 1 1.84 -4.10 18.19 o 11 3 1 143.74 176.17 33.44 o 13 3 1 12.33 7.20 19.44 o 15 3 1 40.23 71.54 43.04 o 17 3 1 52.15 43.53 58.06 o -16 4 1 383.02 357.48 46.20 o -14 4 1 1242.47 1195.04 60.55 o -12 4 1 133.16 121.72 28.60 o -10 4 1 5.23 3.21 19.48 o -8 4 1 729.58 950.82 31.16 o -6 4 1 141.76 189.17 16.95 o -4 4 1 13.09 188.07 20.12 o -2 4 1 5890.87 7006.81 128.33 o 0 4 1 2.71 10.09 14.24 o 2 4 1 151.44 203.14 15.11 o 4 4 1 107.32 114.93 26.23 o 6 4 1 7410.80 8250.18 64.65 o 8 4 1 0.87 0.24 2.86 o 10 4 1 123.62 87.46 34.71 o 12 4 1 1.57 18.75 25.35 o 14 4 1 957.64 1017.07 47.03 o 16 4 1 74.74 -2.55 12.43 o -17 5 1 673.46 605.19 67.80 o -15 5 1 440.17 406.71 57.64 o -13 5 1 222.31 268.09 36.86 o -11 5 1 1098.48 1147.68 44.79 o -9 5 1 93.31 72.89 21.06 o -7 5 1 1951.89 2037.53 43.86 o -5 5 1 205.49 236.33 23.15 o -3 5 1 0.65 37.98 18.14 o -1 5 1 13.47 64.31 19.78 o 1 5 1 1449.03 1555.25 38.58 o 3 5 1 10.74 17.58 17.50 o 5 5 1 334.71 357.62 20.91 o 7 5 1 603.93 559.41 29.82 o 9 5 1 2452.73 2503.32 50.21 o 11 5 1 858.03 963.52 40.39 o 13 5 1 17.87 26.39 24.69 o 15 5 1 306.00 204.11 54.62 o 17 5 1 357.85 204.37 141.03 o -16 6 1 3.17 -31.89 44.80 o -14 6 1 35.08 36.68 34.08 o -12 6 1 1.29 -12.85 13.50 o -10 6 1 22.92 48.37 26.64 o -8 6 1 0.01 7.01 18.24 o -6 6 1 158.09 166.44 25.68 o -4 6 1 1427.87 1422.53 32.00 o -2 6 1 397.08 373.47 30.45 o 0 6 1 0.05 0.12 8.09 o 2 6 1 428.49 491.24 55.41 o 4 6 1 8116.17 9370.29 78.26 o 6 6 1 38.21 42.51 18.12 o 8 6 1 5.52 -0.55 8.73 o 10 6 1 41.86 -6.02 28.80 o 12 6 1 501.26 380.09 43.29 o 14 6 1 193.18 136.70 56.57 o 16 6 1 711.47 620.93 68.82 o -15 7 1 38.77 36.13 28.11 o -13 7 1 510.53 495.00 51.43 o -11 7 1 0.08 2.77 34.97 o -9 7 1 138.21 129.31 31.65 o -7 7 1 38.92 54.08 34.05 o -5 7 1 3952.46 3905.95 50.97 o -3 7 1 105.32 174.37 34.45 o -1 7 1 138.35 175.83 24.05 o 1 7 1 53.98 102.75 30.60 o 3 7 1 1.97 0.70 8.00 o 5 7 1 1728.31 1914.68 39.65 o 7 7 1 255.44 267.85 26.57 o 9 7 1 1.53 -17.83 17.83 o 11 7 1 0.64 39.01 24.38 o 13 7 1 27.01 33.22 27.91 o 15 7 1 100.10 163.22 57.69 o -16 8 1 1.94 -22.47 46.38 o -14 8 1 123.22 34.48 90.64 o -12 8 1 9.63 13.47 36.80 o -10 8 1 0.12 -4.22 8.85 o -8 8 1 23.33 9.62 15.64 o -6 8 1 345.20 292.72 33.08 o -4 8 1 486.74 538.45 37.44 o -2 8 1 53.32 230.74 29.39 o 0 8 1 0.14 15.62 15.91 o 2 8 1 94.26 151.19 30.69 o 4 8 1 338.38 438.76 31.60 o 6 8 1 806.00 697.55 39.00 o 8 8 1 14.94 5.48 27.58 o 10 8 1 0.06 -18.61 18.61 o 12 8 1 144.57 22.94 66.48 o 14 8 1 3.52 -18.64 18.64 o -15 9 1 61.14 66.16 85.31 o -13 9 1 557.07 490.67 61.06 o -11 9 1 185.73 207.32 39.30 o -9 9 1 0.18 -15.86 15.86 o -7 9 1 1.02 -7.08 12.74 o -5 9 1 1982.27 2082.11 57.20 o -3 9 1 81.83 91.56 33.37 o -1 9 1 83.98 108.63 23.48 o 1 9 1 0.73 11.00 18.80 o 3 9 1 528.98 565.61 32.56 o 5 9 1 497.36 395.97 36.57 o 7 9 1 0.08 -1.91 21.04 o 9 9 1 20.69 20.94 16.98 o 11 9 1 38.33 -38.19 57.92 o 13 9 1 124.48 66.43 40.39 o 15 9 1 486.72 492.34 78.07 o -14 10 1 1.61 -9.75 34.07 o -12 10 1 16.33 34.42 69.73 o -10 10 1 1.45 10.90 27.29 o -8 10 1 2.01 -6.10 36.52 o -6 10 1 851.67 826.02 40.55 o -4 10 1 440.12 489.77 36.34 o -2 10 1 74.65 89.71 25.30 o 0 10 1 0.68 15.07 15.24 o 2 10 1 19.49 37.48 30.65 o 4 10 1 60.74 36.73 26.04 o 6 10 1 36.91 13.55 29.86 o 8 10 1 179.21 140.76 45.96 o 10 10 1 53.71 -0.60 50.62 o 12 10 1 1.14 -3.75 12.39 o 14 10 1 589.16 554.94 70.38 o -13 11 1 1199.63 1077.36 92.03 o -11 11 1 41.80 41.68 95.50 o -9 11 1 597.72 531.28 55.61 o -7 11 1 2607.57 2680.15 90.94 o -5 11 1 558.24 504.28 36.78 o -3 11 1 75.53 76.86 33.83 o -1 11 1 9.31 37.90 31.66 o 1 11 1 288.37 300.71 40.08 o 3 11 1 43.47 31.96 50.35 o 5 11 1 49.34 78.10 42.71 o 7 11 1 268.60 256.25 58.93 o 9 11 1 205.99 134.99 53.37 o 11 11 1 32.15 51.41 51.16 o 13 11 1 46.06 117.97 81.35 o -14 12 1 46.15 60.62 70.29 o -12 12 1 240.45 171.37 132.72 o -10 12 1 0.13 -2.77 35.40 o -8 12 1 209.92 215.88 61.14 o -6 12 1 349.20 330.40 42.72 o -4 12 1 3.46 30.82 30.39 o -2 12 1 1213.56 1121.44 48.67 o 0 12 1 2.19 0.16 4.74 o 2 12 1 9.01 2.26 10.07 o 4 12 1 9.64 5.11 33.32 o 6 12 1 107.23 36.06 57.56 o 8 12 1 33.86 11.27 20.68 o 10 12 1 83.21 26.86 70.58 o 12 12 1 39.40 26.67 48.48 o -13 13 1 10.31 8.53 25.38 o -11 13 1 271.00 285.64 69.16 o -9 13 1 1665.43 1603.52 91.03 o -7 13 1 554.62 480.26 72.38 o -5 13 1 78.55 78.03 35.80 o -3 13 1 5.42 5.35 27.02 o -1 13 1 37.48 60.91 47.60 o 1 13 1 1397.40 1420.65 54.04 o 3 13 1 6.39 -11.84 11.84 o 5 13 1 4.71 -4.24 30.39 o 7 13 1 551.92 570.43 74.49 o 9 13 1 606.66 666.57 78.77 o 11 13 1 0.56 35.43 45.27 o -12 14 1 208.25 206.20 82.17 o -10 14 1 248.75 229.20 77.62 o -8 14 1 36.28 31.65 49.52 o -6 14 1 4.34 60.84 33.43 o -4 14 1 1.22 41.82 29.91 o -2 14 1 762.30 852.84 52.09 o 0 14 1 1.65 -22.40 22.40 o 2 14 1 126.47 140.08 39.06 o 4 14 1 2334.35 2281.70 71.75 o 6 14 1 85.60 77.81 37.51 o 8 14 1 0.50 -34.72 120.19 o 10 14 1 396.37 448.12 82.56 o -11 15 1 4.75 -16.21 92.53 o -9 15 1 32.95 37.64 113.78 o -7 15 1 260.93 212.13 77.08 o -5 15 1 551.47 463.14 45.81 o -3 15 1 54.73 64.85 44.36 o -1 15 1 4.11 -7.04 39.20 o 1 15 1 1032.33 974.65 62.99 o 3 15 1 986.01 865.28 55.34 o 5 15 1 472.22 431.55 44.04 o 7 15 1 96.34 157.97 68.69 o 9 15 1 27.43 -27.20 27.20 o -10 16 1 20.49 38.22 216.42 o -8 16 1 25.76 16.98 29.32 o -6 16 1 112.78 121.73 38.49 o -4 16 1 726.86 768.03 56.43 o -2 16 1 1946.33 1938.55 83.36 o 0 16 1 2.62 40.03 33.11 o 2 16 1 420.82 400.26 61.20 o 4 16 1 251.88 227.15 47.50 o 6 16 1 0.12 12.76 20.38 o 8 16 1 63.18 -20.80 94.35 o -7 17 1 508.08 497.63 64.96 o -5 17 1 3.60 5.25 9.43 o -3 17 1 154.82 155.91 104.28 o -1 17 1 1.00 2.25 23.99 o 1 17 1 380.55 360.70 54.84 o 3 17 1 1131.59 1260.41 108.73 o 5 17 1 356.79 307.97 57.02 o 7 17 1 29.97 128.42 69.47 o -6 18 1 29.24 -9.04 29.26 o -4 18 1 224.90 212.26 55.27 o -2 18 1 665.24 720.55 99.23 o 0 18 1 0.91 28.77 60.56 o 2 18 1 100.84 160.60 80.97 o 4 18 1 463.82 481.74 66.46 o 6 18 1 101.80 100.59 94.48 o -1 19 1 277.47 335.57 91.87 o 1 19 1 284.09 243.31 83.49 o 3 19 1 9.80 -7.28 24.69 o -18 0 2 1048.34 971.85 127.68 o -16 0 2 4933.38 4830.25 184.30 o -14 0 2 7605.05 7560.28 133.88 o -12 0 2 31573.40 31518.31 587.56 o -10 0 2 39703.12 37735.94 229.68 o -8 0 2 44937.11 42710.46 166.18 o -6 0 2 111282.97 106362.80 1291.16 o -4 0 2 319760.66 270296.84 1835.23 o -2 0 2 14413.30 15357.69 308.85 o 2 0 2 51652.49 52540.89 178.71 o 4 0 2 74536.83 75068.34 239.40 o 6 0 2 28427.23 28790.69 213.16 o 8 0 2 3946.15 3522.81 50.03 o 10 0 2 32.17 51.05 33.97 o 12 0 2 26.33 47.76 43.58 o 14 0 2 2949.87 3004.57 137.09 o 16 0 2 920.23 931.16 114.61 o -17 1 2 12685.85 12760.40 199.01 o -15 1 2 18984.53 19010.47 185.35 o -13 1 2 16118.84 15830.29 217.64 o -11 1 2 14449.85 13943.21 93.67 o -9 1 2 16190.77 15816.59 86.98 o -7 1 2 8892.49 10225.82 117.00 o -5 1 2 76.23 234.83 17.32 o -3 1 2 6069.68 6582.67 44.77 o -1 1 2 3648.91 4536.23 266.19 o 1 1 2 18003.93 19085.58 242.08 o 3 1 2 67831.34 68763.84 291.71 o 5 1 2 48458.42 47769.46 147.21 o 7 1 2 48191.84 47320.08 124.28 o 9 1 2 45810.84 45645.95 237.82 o 11 1 2 31800.14 31493.56 205.99 o 13 1 2 27927.28 28077.81 246.74 o 15 1 2 12986.44 13058.86 151.93 o 17 1 2 8359.06 8825.22 174.28 o -18 2 2 469.28 368.53 72.57 o -16 2 2 2858.08 2675.34 85.28 o -14 2 2 8351.15 7968.51 99.17 o -12 2 2 14102.26 14451.15 160.07 o -10 2 2 40463.05 38857.30 404.17 o -8 2 2 59483.16 56896.54 316.72 o -6 2 2 78119.52 74250.73 295.22 o -4 2 2 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