#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212625.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212625_Fobs loop_ _publ_author_name 'Maldonado, Carmen R.' 'Quir\'os, Miguel' 'Salas, Juan M.' _publ_section_title ; 1,2,4-Triazolo[1,5-a]pyrimidin-3-ium chloride ; _journal_coeditor_code KP2087 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1509 _journal_page_last o1510 _journal_volume 63 _journal_year 2007 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.4813 _cell_length_b 9.8306 _cell_length_c 21.6230 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.7499 _[local]_cod_data_source_file kp2087Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (C5H5N4)Cl' _shelx_refln_list_code 4 _shelx_f_calc_maximum 436.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 190108.50 158408.64 4449.49 o 4 0 0 40389.13 41402.54 1149.13 o 6 0 0 8601.31 7947.86 236.99 o 8 0 0 1779.20 1675.46 49.61 o 0 2 0 5372.46 5689.06 113.82 o 2 2 0 2905.40 3094.06 39.81 o 4 2 0 742.45 722.33 14.08 o 6 2 0 164.10 180.85 25.56 o 8 2 0 34.26 33.40 6.30 o 0 4 0 6416.59 6699.90 135.64 o 2 4 0 4233.88 4125.56 60.30 o 4 4 0 1567.79 1476.16 25.28 o 6 4 0 439.21 412.66 14.53 o 0 6 0 2305.69 2539.30 56.18 o 2 6 0 1641.05 1621.16 37.28 o 4 6 0 695.20 764.77 24.27 o 6 6 0 208.06 245.86 17.62 o 0 8 0 3045.16 3120.74 69.87 o 2 8 0 2417.31 2443.47 47.66 o 4 8 0 1282.77 1225.46 29.54 o 6 8 0 486.21 488.15 22.43 o 0 10 0 264.27 269.86 19.52 o 2 10 0 211.67 206.36 10.98 o 4 10 0 109.73 126.46 12.61 o 0 12 0 94.55 137.16 17.72 o 2 12 0 79.86 113.32 11.50 o 1 1 1 703.85 653.35 6.78 o 3 1 1 79.55 107.84 3.16 o 5 1 1 0.84 2.94 1.36 o 7 1 1 0.16 0.94 2.03 o 0 2 1 15717.77 15347.55 246.76 o 2 2 1 8645.03 9131.32 83.94 o 4 2 1 2635.76 2712.20 29.28 o 6 2 1 752.95 716.10 13.62 o 8 2 1 181.46 183.33 10.57 o 1 3 1 5844.53 6034.20 60.72 o 3 3 1 2330.19 2400.16 24.27 o 5 3 1 740.26 716.83 13.93 o 7 3 1 197.16 203.12 12.39 o 0 4 1 1079.39 1041.20 17.34 o 2 4 1 681.40 666.79 8.68 o 4 4 1 249.79 240.69 5.57 o 6 4 1 78.07 74.38 4.71 o 1 5 1 69.72 55.39 2.50 o 3 5 1 57.31 58.54 3.19 o 5 5 1 36.19 38.17 4.20 o 7 5 1 14.41 20.62 5.46 o 0 6 1 2073.58 2116.71 33.87 o 2 6 1 1532.04 1495.93 27.98 o 4 6 1 719.64 657.96 15.43 o 6 6 1 243.82 245.19 21.56 o 1 7 1 384.41 338.08 10.34 o 3 7 1 280.54 246.71 6.90 o 5 7 1 144.46 138.97 7.34 o 0 8 1 413.44 403.15 12.42 o 2 8 1 297.30 311.48 7.89 o 4 8 1 128.05 137.23 6.52 o 6 8 1 41.75 36.74 4.94 o 1 9 1 275.53 272.84 7.46 o 3 9 1 182.99 180.21 7.21 o 5 9 1 90.27 91.20 8.16 o 0 10 1 458.87 452.79 18.51 o 2 10 1 373.33 367.40 9.87 o 4 10 1 207.35 222.31 9.98 o 1 11 1 232.71 193.40 9.78 o 3 11 1 153.33 152.53 9.50 o 0 12 1 408.46 394.28 18.92 o 2 12 1 333.46 361.73 15.05 o 0 0 2 556.75 543.36 12.57 o 2 0 2 338.05 311.33 11.20 o 4 0 2 89.14 83.85 6.68 o 6 0 2 17.34 23.44 5.07 o 8 0 2 3.11 3.45 4.12 o 1 1 2 6333.09 6320.54 58.11 o 3 1 2 1202.49 1442.59 16.42 o 5 1 2 97.25 107.81 4.74 o 7 1 2 7.96 9.73 2.47 o 0 2 2 2950.44 2930.95 48.96 o 2 2 2 1293.15 1294.83 14.27 o 4 2 2 243.89 244.02 4.82 o 6 2 2 43.48 45.95 3.72 o 8 2 2 6.28 3.89 3.37 o 1 3 2 6035.27 6358.51 63.95 o 3 3 2 2338.12 2484.78 25.07 o 5 3 2 714.66 677.00 12.27 o 7 3 2 193.90 172.20 9.48 o 0 4 2 2277.20 2669.54 40.12 o 2 4 2 1378.85 1540.02 17.61 o 4 4 2 423.33 422.22 7.83 o 6 4 2 102.83 100.00 5.57 o 8 4 2 22.55 17.30 9.65 o 1 5 2 1207.54 1060.68 13.94 o 3 5 2 818.40 732.09 11.26 o 5 5 2 410.75 373.74 11.26 o 7 5 2 140.05 150.80 16.00 o 0 6 2 1269.26 1350.55 23.19 o 2 6 2 821.06 818.49 12.29 o 4 6 2 275.86 257.24 8.92 o 6 6 2 66.01 63.60 9.10 o 1 7 2 108.67 107.53 4.07 o 3 7 2 67.96 61.65 4.29 o 5 7 2 34.17 36.32 4.72 o 0 8 2 1.74 1.38 2.36 o 2 8 2 1.85 2.40 1.46 o 4 8 2 1.74 0.57 3.12 o 6 8 2 1.18 6.90 3.33 o 1 9 2 1734.78 1730.12 28.32 o 3 9 2 1126.91 1118.50 19.41 o 5 9 2 487.30 490.43 13.94 o 0 10 2 112.11 117.78 10.39 o 2 10 2 85.05 82.46 6.00 o 4 10 2 38.90 39.97 4.80 o 1 11 2 6.62 2.92 3.41 o 3 11 2 3.01 1.47 2.82 o 0 12 2 0.01 -1.30 3.59 o 2 12 2 0.02 -0.44 3.54 o 1 1 3 1438.52 1325.93 11.86 o 3 1 3 209.36 223.59 4.08 o 5 1 3 16.54 15.38 2.10 o 7 1 3 1.97 -0.14 2.08 o 0 2 3 4551.29 5258.21 74.60 o 2 2 3 3100.30 3273.97 29.86 o 4 2 3 1351.21 1364.52 16.62 o 6 2 3 490.45 500.20 10.80 o 8 2 3 137.59 148.72 14.03 o 1 3 3 4973.86 5229.56 61.29 o 3 3 3 2040.75 2066.89 21.28 o 5 3 3 623.67 580.69 10.14 o 7 3 3 157.83 167.97 9.45 o 0 4 3 92.91 87.62 4.03 o 2 4 3 67.50 62.58 2.71 o 4 4 3 36.67 39.53 2.59 o 6 4 3 16.76 17.57 4.90 o 8 4 3 5.04 4.87 3.67 o 1 5 3 2725.85 3167.81 33.87 o 3 5 3 1291.30 1404.10 18.68 o 5 5 3 437.94 460.14 11.50 o 7 5 3 119.68 124.50 9.12 o 0 6 3 5330.26 5772.50 84.76 o 2 6 3 3825.63 4074.40 46.88 o 4 6 3 1665.24 1610.03 24.04 o 6 6 3 532.16 535.88 15.93 o 1 7 3 2940.24 2853.86 34.33 o 3 7 3 1676.97 1645.87 33.90 o 5 7 3 641.10 592.45 16.38 o 7 7 3 176.61 204.17 22.16 o 0 8 3 536.59 521.51 14.77 o 2 8 3 403.53 378.43 8.88 o 4 8 3 180.49 181.42 12.00 o 6 8 3 49.37 66.67 9.67 o 1 9 3 1086.76 1040.59 19.50 o 3 9 3 657.74 645.76 15.01 o 5 9 3 267.23 250.28 10.83 o 0 10 3 745.68 752.77 25.57 o 2 10 3 605.34 586.03 14.05 o 4 10 3 333.16 357.15 11.64 o 1 11 3 78.03 77.08 6.38 o 3 11 3 51.66 52.59 5.87 o 0 12 3 258.64 291.77 23.01 o 2 12 3 211.80 214.14 12.87 o 0 0 4 33564.80 35250.74 484.05 o 2 0 4 18741.15 20020.24 279.74 o 4 0 4 5990.05 6300.42 130.70 o 6 0 4 1847.11 1809.85 47.16 o 8 0 4 493.60 476.01 23.07 o 1 1 4 653.16 602.77 6.79 o 3 1 4 128.28 121.01 2.82 o 5 1 4 9.00 8.06 1.70 o 7 1 4 0.17 2.28 2.53 o 0 2 4 48.96 56.96 2.05 o 2 2 4 9.19 9.64 0.83 o 4 2 4 1.38 1.84 1.06 o 6 2 4 4.77 6.70 1.95 o 8 2 4 3.08 6.16 3.34 o 1 3 4 686.06 771.67 10.28 o 3 3 4 230.82 233.81 4.30 o 5 3 4 44.80 49.93 3.19 o 7 3 4 9.56 18.55 3.89 o 0 4 4 2734.30 2513.80 44.31 o 2 4 4 2013.80 1851.66 22.60 o 4 4 4 929.16 889.96 12.55 o 6 4 4 307.27 294.51 9.37 o 8 4 4 71.62 87.14 7.52 o 1 5 4 662.23 877.47 11.28 o 3 5 4 240.17 259.79 9.64 o 5 5 4 46.98 54.44 5.06 o 7 5 4 8.31 9.95 3.66 o 0 6 4 1585.88 1683.46 27.96 o 2 6 4 1170.03 1183.67 20.78 o 4 6 4 541.53 545.77 13.81 o 6 6 4 177.03 174.08 11.32 o 1 7 4 556.86 547.04 10.18 o 3 7 4 288.09 288.41 7.57 o 5 7 4 92.73 94.10 12.78 o 7 7 4 19.62 24.69 9.39 o 0 8 4 2354.65 2250.55 101.08 o 2 8 4 1880.74 1967.97 28.31 o 4 8 4 1007.52 1034.65 20.48 o 6 8 4 382.55 384.46 15.46 o 1 9 4 32.70 38.62 4.40 o 3 9 4 16.66 19.86 3.25 o 5 9 4 5.11 7.79 3.44 o 0 10 4 381.62 423.69 21.69 o 2 10 4 309.11 330.24 11.43 o 4 10 4 164.29 190.99 9.46 o 1 11 4 1.62 1.84 2.73 o 3 11 4 1.53 9.84 3.66 o 0 12 4 72.73 65.09 12.66 o 2 12 4 60.78 66.38 9.01 o 1 1 5 6983.63 7692.51 67.97 o 3 1 5 2435.05 2566.01 27.70 o 5 1 5 630.25 590.67 15.53 o 7 1 5 136.05 153.49 8.99 o 0 2 5 121.64 127.60 3.09 o 2 2 5 133.28 126.60 2.33 o 4 2 5 124.43 130.93 3.65 o 6 2 5 69.55 73.94 8.47 o 8 2 5 22.22 26.51 5.18 o 1 3 5 9975.86 10359.71 118.97 o 3 3 5 4253.23 4264.53 39.37 o 5 3 5 1283.17 1259.38 15.76 o 7 3 5 315.76 297.01 10.22 o 0 4 5 2188.25 2372.12 36.58 o 2 4 5 1365.02 1464.59 18.61 o 4 4 5 493.05 505.41 8.75 o 6 4 5 151.92 143.12 7.48 o 8 4 5 37.17 26.58 10.55 o 1 5 5 0.50 3.79 0.90 o 3 5 5 5.04 4.29 1.36 o 5 5 5 9.33 14.22 2.54 o 7 5 5 4.46 3.97 3.53 o 0 6 5 0.35 9.39 1.69 o 2 6 5 0.68 2.88 1.23 o 4 6 5 4.13 2.15 1.78 o 6 6 5 3.14 6.98 3.12 o 1 7 5 1322.94 1295.20 19.52 o 3 7 5 832.63 806.31 16.25 o 5 7 5 353.22 337.11 11.99 o 7 7 5 101.00 107.93 17.30 o 0 8 5 224.96 220.30 9.17 o 2 8 5 161.76 173.57 6.98 o 4 8 5 68.35 84.51 6.23 o 6 8 5 20.83 26.32 4.55 o 1 9 5 374.32 346.87 13.03 o 3 9 5 241.21 229.76 9.25 o 5 9 5 110.56 116.02 8.71 o 0 10 5 251.77 222.67 14.41 o 2 10 5 203.08 198.51 9.90 o 4 10 5 108.99 100.61 7.17 o 1 11 5 354.01 348.17 13.99 o 3 11 5 234.73 251.69 13.05 o 0 12 5 264.55 263.30 24.69 o 2 12 5 218.90 235.97 21.10 o 0 0 6 3561.29 3785.78 62.68 o 2 0 6 2124.48 2209.81 38.58 o 4 0 6 672.50 643.43 15.52 o 6 0 6 182.55 192.46 8.33 o 8 0 6 44.53 58.25 8.95 o 1 1 6 13814.48 15273.55 127.37 o 3 1 6 5024.86 5280.00 48.60 o 5 1 6 1303.66 1245.64 16.48 o 7 1 6 275.98 291.29 13.28 o 0 2 6 77.63 58.93 2.15 o 2 2 6 37.64 35.06 1.33 o 4 2 6 6.45 7.41 1.18 o 6 2 6 1.09 3.32 1.86 o 8 2 6 0.42 5.33 6.54 o 1 3 6 825.91 819.97 11.42 o 3 3 6 500.62 496.91 8.46 o 5 3 6 248.31 241.23 6.30 o 7 3 6 90.54 91.87 6.54 o 0 4 6 7152.94 8182.32 116.79 o 2 4 6 4601.00 5066.81 56.42 o 4 4 6 1663.44 1641.51 21.91 o 6 4 6 483.19 455.57 12.16 o 1 5 6 2794.73 2713.51 32.04 o 3 5 6 1610.89 1562.48 20.71 o 5 5 6 659.89 661.67 16.76 o 7 5 6 197.46 196.59 11.03 o 0 6 6 116.67 94.56 5.71 o 2 6 6 93.62 89.82 3.86 o 4 6 6 50.60 53.24 4.32 o 6 6 6 19.32 31.50 4.71 o 1 7 6 14.12 12.39 1.92 o 3 7 6 8.67 6.88 2.11 o 5 7 6 2.59 5.78 3.03 o 0 8 6 181.13 158.55 8.06 o 2 8 6 149.37 127.44 8.74 o 4 8 6 86.17 88.45 6.12 o 6 8 6 36.06 40.15 5.58 o 1 9 6 772.62 750.25 17.80 o 3 9 6 508.49 494.74 14.65 o 5 9 6 225.29 217.43 11.72 o 0 10 6 17.98 17.07 4.89 o 2 10 6 14.59 19.44 3.91 o 4 10 6 7.64 11.39 3.32 o 1 11 6 1.45 -2.64 2.76 o 3 11 6 1.03 2.27 2.99 o 0 12 6 0.11 6.01 6.75 o 2 12 6 0.04 9.81 7.28 o 1 1 7 2010.70 2046.05 18.46 o 3 1 7 758.21 740.76 8.96 o 5 1 7 204.30 198.05 6.18 o 7 1 7 47.48 48.88 7.38 o 0 2 7 4477.12 4758.26 61.17 o 2 2 7 3096.81 3193.36 29.99 o 4 2 7 1443.17 1429.27 16.48 o 6 2 7 555.34 522.05 11.63 o 1 3 7 1380.20 1369.88 15.54 o 3 3 7 634.09 591.66 8.82 o 5 3 7 207.41 197.17 6.13 o 7 3 7 54.64 48.90 5.07 o 0 4 7 328.24 392.63 8.88 o 2 4 7 167.09 185.74 4.67 o 4 4 7 24.04 24.00 2.51 o 6 4 7 0.77 2.48 2.29 o 1 5 7 1537.97 1835.81 22.92 o 3 5 7 804.51 874.39 18.49 o 5 5 7 304.22 291.56 9.09 o 7 5 7 92.57 83.96 7.49 o 0 6 7 1687.27 1802.59 35.21 o 2 6 7 1326.05 1347.32 20.36 o 4 6 7 694.16 692.83 15.01 o 6 6 7 264.75 258.55 12.09 o 1 7 7 160.47 153.59 5.21 o 3 7 7 118.61 106.22 6.01 o 5 7 7 64.02 70.15 5.70 o 0 8 7 3.64 2.89 2.12 o 2 8 7 1.07 3.52 1.83 o 4 8 7 0.20 1.53 2.36 o 6 8 7 0.43 10.58 4.50 o 1 9 7 32.50 34.16 5.63 o 3 9 7 15.87 18.04 4.69 o 5 9 7 4.00 8.12 3.43 o 0 10 7 1283.41 1169.26 69.88 o 2 10 7 1029.44 923.66 22.05 o 4 10 7 543.45 503.90 16.13 o 1 11 7 45.49 50.64 6.48 o 3 11 7 29.02 36.52 5.23 o 0 12 7 83.62 105.08 16.88 o 0 0 8 5748.40 5810.27 95.20 o 2 0 8 3867.17 3774.06 50.74 o 4 0 8 1692.80 1662.25 25.27 o 6 0 8 636.21 580.81 17.43 o 1 1 8 212.99 197.17 2.97 o 3 1 8 96.81 84.20 2.55 o 5 1 8 37.64 36.65 2.87 o 7 1 8 10.45 13.34 3.68 o 0 2 8 3.55 9.48 1.35 o 2 2 8 0.17 2.29 0.59 o 4 2 8 3.24 2.01 1.28 o 6 2 8 5.58 3.92 1.88 o 1 3 8 1012.59 1103.83 11.72 o 3 3 8 405.75 433.24 7.99 o 5 3 8 120.12 128.64 5.82 o 7 3 8 33.62 28.53 4.58 o 0 4 8 4036.77 4126.94 61.30 o 2 4 8 2829.04 2780.65 32.73 o 4 4 8 1175.57 1133.97 18.26 o 6 4 8 347.78 330.32 9.22 o 1 5 8 147.74 116.41 6.20 o 3 5 8 85.22 75.10 4.15 o 5 5 8 30.76 33.57 3.70 o 7 5 8 6.19 9.55 3.76 o 0 6 8 624.40 617.81 15.57 o 2 6 8 477.05 459.02 13.88 o 4 6 8 231.58 234.57 10.48 o 6 6 8 77.58 67.79 6.56 o 1 7 8 34.97 33.20 2.95 o 3 7 8 20.24 25.56 2.87 o 5 7 8 8.43 18.11 3.33 o 0 8 8 1147.27 1138.03 26.16 o 2 8 8 933.90 945.99 16.90 o 4 8 8 516.00 494.23 13.24 o 6 8 8 197.95 226.93 22.90 o 1 9 8 223.43 214.30 8.15 o 3 9 8 143.51 153.15 8.08 o 5 9 8 60.61 68.37 6.87 o 0 10 8 287.15 305.82 19.16 o 2 10 8 232.24 225.83 10.71 o 4 10 8 123.58 132.87 9.33 o 1 11 8 15.90 19.52 4.74 o 3 11 8 11.22 16.50 4.14 o 2 12 8 15.11 15.09 8.33 o 1 1 9 713.57 738.93 8.31 o 3 1 9 383.62 365.44 7.15 o 5 1 9 138.71 136.73 5.94 o 7 1 9 34.10 40.62 4.23 o 0 2 9 1326.67 1448.95 20.72 o 2 2 9 809.73 820.90 10.15 o 4 2 9 253.65 230.73 5.78 o 6 2 9 59.70 60.94 4.93 o 1 3 9 4397.77 4475.80 41.49 o 3 3 9 2262.70 2230.59 27.53 o 5 3 9 815.70 822.49 19.26 o 7 3 9 223.51 227.39 11.38 o 0 4 9 246.01 279.84 12.42 o 2 4 9 183.90 190.53 5.28 o 4 4 9 89.90 95.33 4.87 o 6 4 9 34.89 42.39 4.02 o 1 5 9 44.41 35.43 3.91 o 3 5 9 37.69 35.66 2.94 o 5 5 9 22.45 28.98 3.29 o 7 5 9 7.83 12.04 4.35 o 0 6 9 291.60 283.33 8.35 o 2 6 9 199.64 179.71 5.75 o 4 6 9 69.68 74.10 6.05 o 6 6 9 12.66 20.09 4.28 o 1 7 9 2501.19 2478.89 34.13 o 3 7 9 1528.55 1536.68 24.02 o 5 7 9 616.35 633.41 17.39 o 0 8 9 1146.10 1082.75 32.15 o 2 8 9 856.27 812.81 15.42 o 4 8 9 378.20 366.19 11.28 o 6 8 9 107.01 139.69 19.52 o 1 9 9 614.80 522.04 14.71 o 3 9 9 383.62 321.53 11.96 o 5 9 9 161.76 140.72 9.79 o 0 10 9 21.02 25.90 6.04 o 2 10 9 14.68 11.48 5.77 o 4 10 9 5.28 12.83 3.68 o 1 11 9 515.84 579.87 19.89 o 3 11 9 343.36 393.04 28.71 o 2 12 9 73.92 99.70 17.30 o 0 0 10 12466.74 13476.04 217.54 o 2 0 10 7858.99 8422.73 89.55 o 4 0 10 2690.74 2555.01 37.06 o 6 0 10 732.14 676.67 19.73 o 1 1 10 5.83 2.22 0.67 o 3 1 10 35.34 33.51 1.99 o 5 1 10 37.71 41.99 3.51 o 7 1 10 15.43 20.84 4.22 o 0 2 10 95.07 92.24 4.60 o 2 2 10 56.58 68.21 2.47 o 4 2 10 22.71 32.54 2.58 o 6 2 10 9.69 11.67 2.51 o 1 3 10 688.69 691.61 9.00 o 3 3 10 431.25 396.36 7.74 o 5 3 10 203.48 200.44 6.78 o 7 3 10 72.73 76.23 7.25 o 0 4 10 2208.46 2523.12 39.59 o 2 4 10 1610.69 1581.55 45.58 o 4 4 10 743.27 690.00 13.08 o 6 4 10 263.15 261.51 11.16 o 1 5 10 2207.48 2229.98 30.08 o 3 5 10 1387.24 1355.82 25.85 o 5 5 10 615.21 640.44 13.47 o 7 5 10 193.91 204.39 23.21 o 0 6 10 246.51 249.23 9.60 o 2 6 10 196.68 189.67 7.60 o 4 6 10 106.14 118.46 5.93 o 6 6 10 40.37 53.13 13.26 o 1 7 10 38.95 47.98 3.58 o 3 7 10 20.93 19.81 3.23 o 5 7 10 6.47 7.36 2.95 o 0 8 10 544.66 478.91 24.92 o 2 8 10 439.69 413.43 12.27 o 4 8 10 238.96 231.67 9.80 o 1 9 10 661.65 693.68 24.77 o 3 9 10 442.72 475.29 13.26 o 5 9 10 200.02 239.29 17.27 o 0 10 10 16.61 25.29 7.86 o 2 10 10 13.62 19.19 5.32 o 4 10 10 7.24 26.79 6.23 o 1 11 10 4.02 4.65 3.35 o 1 1 11 58.04 58.21 1.90 o 3 1 11 35.75 38.14 2.20 o 5 1 11 16.75 19.15 2.68 o 7 1 11 6.21 10.30 2.81 o 0 2 11 7350.72 7930.24 90.86 o 2 2 11 5242.72 5552.59 57.90 o 4 2 11 2316.31 2266.43 28.70 o 6 2 11 764.95 689.72 14.37 o 1 3 11 227.32 252.72 4.64 o 3 3 11 76.42 75.88 3.96 o 5 3 11 12.13 9.44 2.10 o 7 3 11 1.08 0.25 3.15 o 0 4 11 479.26 456.16 9.04 o 2 4 11 345.22 323.52 8.97 o 4 4 11 149.41 152.67 7.01 o 6 4 11 47.04 49.10 4.43 o 1 5 11 27.89 37.38 2.90 o 3 5 11 21.45 22.16 2.53 o 5 5 11 14.89 18.14 2.89 o 7 5 11 9.69 14.14 8.12 o 0 6 11 1982.28 1938.28 39.39 o 2 6 11 1570.05 1450.34 34.26 o 4 6 11 820.96 761.17 14.94 o 6 6 11 296.87 301.09 11.49 o 1 7 11 4.13 5.33 1.87 o 3 7 11 0.02 2.58 2.00 o 5 7 11 2.25 3.56 2.87 o 0 8 11 135.30 164.81 24.80 o 2 8 11 108.70 129.28 9.22 o 4 8 11 56.14 60.29 5.35 o 1 9 11 250.78 235.05 10.33 o 3 9 11 143.82 131.60 7.80 o 5 9 11 51.31 37.26 5.91 o 0 10 11 342.50 302.13 21.64 o 2 10 11 279.23 248.81 14.76 o 4 10 11 153.22 179.85 21.00 o 1 11 11 58.18 60.66 7.21 o 0 0 12 12600.84 13158.66 213.24 o 2 0 12 8594.35 8890.06 102.46 o 4 0 12 3487.02 3448.74 48.52 o 6 0 12 1078.02 967.23 25.19 o 1 1 12 98.93 129.68 2.65 o 3 1 12 11.24 14.11 1.52 o 5 1 12 1.94 7.09 2.07 o 7 1 12 4.17 7.10 2.54 o 0 2 12 1317.74 1429.69 18.65 o 2 2 12 883.63 915.10 11.49 o 4 2 12 335.84 344.59 7.85 o 6 2 12 96.06 94.75 5.84 o 1 3 12 501.22 444.09 6.83 o 3 3 12 259.00 231.37 9.13 o 5 3 12 83.45 91.96 5.84 o 7 3 12 15.90 16.84 4.09 o 0 4 12 164.67 123.52 5.24 o 2 4 12 139.83 134.87 6.84 o 4 4 12 78.56 73.33 4.71 o 6 4 12 24.52 32.71 3.86 o 1 5 12 0.21 1.66 1.26 o 3 5 12 1.50 4.00 1.70 o 5 5 12 2.29 4.43 2.22 o 7 5 12 0.71 -0.21 6.43 o 0 6 12 162.36 157.65 8.80 o 2 6 12 129.50 115.67 5.45 o 4 6 12 67.79 76.05 5.06 o 6 6 12 24.00 30.82 5.06 o 1 7 12 14.90 16.80 3.66 o 3 7 12 7.85 11.54 2.41 o 5 7 12 2.16 8.00 3.12 o 0 8 12 552.02 531.48 54.80 o 2 8 12 447.69 422.72 15.11 o 4 8 12 242.38 231.63 12.70 o 1 9 12 312.03 317.44 11.54 o 3 9 12 207.42 205.88 10.91 o 5 9 12 92.14 81.26 10.54 o 0 10 12 66.99 78.68 10.17 o 2 10 12 55.51 56.38 14.88 o 1 11 12 17.52 11.17 5.87 o 1 1 13 100.43 76.58 2.25 o 3 1 13 97.36 87.88 3.54 o 5 1 13 60.67 72.93 4.39 o 7 1 13 21.17 37.84 4.07 o 0 2 13 342.90 334.49 8.54 o 2 2 13 230.06 232.81 5.01 o 4 2 13 85.49 90.36 4.58 o 6 2 13 21.08 22.86 3.37 o 1 3 13 2374.42 2210.68 26.57 o 3 3 13 1518.01 1430.86 20.07 o 5 3 13 687.24 664.12 13.80 o 7 3 13 215.11 261.41 18.18 o 0 4 13 162.98 161.51 5.98 o 2 4 13 121.73 122.44 5.51 o 4 4 13 58.46 50.66 4.34 o 6 4 13 22.79 20.85 3.87 o 1 5 13 1097.60 1114.29 18.02 o 3 5 13 660.51 662.29 13.01 o 5 5 13 269.81 270.36 9.61 o 0 6 13 405.22 396.25 16.53 o 2 6 13 313.61 273.99 8.54 o 4 6 13 160.59 158.37 7.15 o 6 6 13 63.31 69.61 8.55 o 1 7 13 269.04 241.50 9.36 o 3 7 13 196.65 207.82 9.71 o 5 7 13 99.97 109.97 7.42 o 0 8 13 1.48 10.36 3.84 o 2 8 13 0.90 3.36 2.48 o 4 8 13 0.18 2.12 2.59 o 1 9 13 0.27 0.93 2.81 o 3 9 13 0.49 0.00 2.99 o 0 10 13 1.45 5.43 5.33 o 2 10 13 1.07 0.14 2.94 o 1 11 13 349.26 374.89 27.02 o 0 0 14 8112.79 8421.67 138.92 o 2 0 14 5697.22 5903.07 77.01 o 4 0 14 2329.26 2286.42 39.16 o 6 0 14 680.71 624.59 19.59 o 1 1 14 573.27 509.75 6.30 o 3 1 14 356.58 328.66 6.70 o 5 1 14 151.82 156.84 6.05 o 7 1 14 44.93 52.99 4.75 o 0 2 14 37.65 36.30 3.21 o 2 2 14 23.00 27.63 1.89 o 4 2 14 4.84 7.31 1.91 o 6 2 14 0.06 3.83 2.48 o 1 3 14 2950.76 3054.71 34.03 o 3 3 14 1690.82 1669.74 27.15 o 5 3 14 669.14 651.47 14.20 o 7 3 14 200.31 224.44 23.64 o 0 4 14 1053.96 998.51 27.42 o 2 4 14 824.38 812.21 13.19 o 4 4 14 424.57 419.00 11.28 o 6 4 14 160.52 170.94 9.18 o 1 5 14 2670.35 2631.49 35.86 o 3 5 14 1616.56 1570.77 24.31 o 5 5 14 663.23 641.83 15.72 o 0 6 14 1554.43 1493.84 33.06 o 2 6 14 1204.61 1187.91 21.98 o 4 6 14 592.75 600.27 13.31 o 6 6 14 198.91 220.56 13.70 o 1 7 14 0.96 3.02 1.93 o 3 7 14 0.30 1.57 2.31 o 5 7 14 0.02 2.19 2.98 o 0 8 14 398.80 391.47 18.13 o 2 8 14 326.52 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99.63 92.91 18.57 o 2 4 19 82.70 81.28 5.75 o 4 4 19 46.81 48.63 5.83 o 1 5 19 273.46 232.83 13.39 o 3 5 19 174.50 175.24 17.35 o 5 5 19 76.67 89.87 7.96 o 0 6 19 517.94 499.63 33.95 o 2 6 19 422.66 458.26 14.61 o 4 6 19 230.51 261.71 12.71 o 1 7 19 64.71 63.32 5.54 o 3 7 19 37.54 45.11 5.56 o 0 8 19 92.37 102.69 11.37 o 2 8 19 79.12 83.73 7.40 o 1 9 19 3.70 4.62 3.57 o 0 0 20 57.51 59.05 6.75 o 2 0 20 53.56 58.28 6.07 o 4 0 20 36.89 45.99 4.92 o 1 1 20 2554.04 2479.94 34.73 o 3 1 20 1602.39 1534.41 24.72 o 5 1 20 676.22 660.90 17.64 o 0 2 20 197.55 178.68 9.68 o 2 2 20 148.37 123.86 9.01 o 4 2 20 66.64 61.40 5.70 o 6 2 20 19.37 36.41 12.03 o 1 3 20 12.61 13.94 2.54 o 3 3 20 5.58 6.37 2.71 o 5 3 20 1.30 3.10 3.27 o 0 4 20 5.03 6.14 3.70 o 2 4 20 3.72 3.90 2.58 o 4 4 20 1.17 0.27 3.17 o 1 5 20 648.92 611.39 14.82 o 3 5 20 411.25 399.76 13.80 o 5 5 20 169.93 179.27 22.37 o 0 6 20 37.94 39.57 5.84 o 2 6 20 31.10 29.32 4.72 o 4 6 20 17.30 24.09 5.36 o 1 7 20 14.79 15.96 4.14 o 3 7 20 11.71 12.93 3.82 o 0 8 20 86.47 80.87 8.34 o 2 8 20 69.55 82.07 10.44 o 1 9 20 370.25 422.29 28.81 o 1 1 21 161.77 167.56 7.52 o 3 1 21 113.32 104.92 9.34 o 5 1 21 56.04 74.08 4.88 o 0 2 21 10.54 10.76 3.30 o 2 2 21 10.35 11.18 2.99 o 4 2 21 8.06 10.96 3.37 o 1 3 21 648.82 595.05 18.31 o 3 3 21 449.09 408.66 14.53 o 5 3 21 217.52 239.64 24.38 o 0 4 21 1.82 0.53 3.43 o 2 4 21 1.54 4.60 2.57 o 4 4 21 1.04 6.43 3.44 o 1 5 21 136.51 129.98 7.45 o 3 5 21 93.49 87.90 7.98 o 0 6 21 13.79 10.73 5.22 o 2 6 21 8.82 7.17 3.67 o 1 7 21 199.20 180.98 10.38 o 3 7 21 132.38 130.98 13.25 o 0 8 21 1.12 -0.24 3.64 o 2 8 21 0.53 -4.64 5.70 o 0 0 22 17.76 25.00 7.17 o 2 0 22 16.08 25.30 5.71 o 4 0 22 10.07 5.89 5.23 o 1 1 22 48.02 49.40 6.82 o 3 1 22 34.69 32.14 6.35 o 5 1 22 18.57 28.76 6.45 o 0 2 22 18.02 15.69 4.55 o 2 2 22 15.19 14.32 3.25 o 4 2 22 9.54 15.92 3.52 o 1 3 22 11.38 15.85 3.14 o 3 3 22 10.02 8.05 3.03 o 5 3 22 6.86 20.04 9.49 o 0 4 22 312.59 271.52 28.81 o 2 4 22 256.96 236.97 11.35 o 4 4 22 141.65 142.00 9.78 o 1 5 22 44.78 48.01 5.83 o 3 5 22 33.07 42.73 5.65 o 0 6 22 108.37 129.56 13.01 o 2 6 22 91.77 115.28 8.73 o 1 7 22 0.21 1.44 3.16 o 1 1 23 206.72 188.77 8.55 o 3 1 23 133.20 140.05 9.25 o 0 2 23 592.58 623.20 23.54 o 2 2 23 466.86 487.39 13.28 o 4 2 23 230.95 244.66 12.46 o 1 3 23 54.14 69.26 8.07 o 3 3 23 38.85 45.46 4.98 o 0 4 23 146.26 138.55 12.75 o 2 4 23 116.36 140.62 9.50 o 4 4 23 60.02 50.71 8.47 o 1 5 23 171.37 189.71 12.78 o 3 5 23 105.38 122.61 9.23 o 0 6 23 245.96 261.06 38.04 o 2 6 23 198.38 213.37 13.81 o 0 0 24 101.33 74.49 12.34 o 2 0 24 80.14 69.86 12.66 o 4 0 24 39.84 29.16 7.23 o 1 1 24 407.92 417.50 11.93 o 3 1 24 291.66 304.11 13.61 o 0 2 24 16.19 17.83 7.17 o 2 2 24 12.50 20.10 4.48 o 4 2 24 5.81 16.88 9.28 o 1 3 24 403.23 392.86 15.79 o 3 3 24 258.74 264.49 11.29 o 0 4 24 5.25 16.34 5.96 o 2 4 24 3.86 7.82 4.70 o 4 4 24 1.47 15.61 9.07 o 1 5 24 391.78 389.20 16.37 o 0 6 24 9.12 16.10 6.49 o 1 1 25 216.00 227.94 14.09 o 3 1 25 145.59 154.94 11.16 o 0 2 25 142.89 152.47 19.10 o 2 2 25 112.72 109.70 7.40 o 1 3 25 164.74 160.13 15.95 o 3 3 25 118.75 118.98 10.14 o 0 4 25 66.11 64.36 13.19 o 2 4 25 51.84 48.04 8.26 o 1 5 25 169.12 188.42 15.74 o 0 6 25 58.28 70.47 13.93 o 2 0 26 280.53 350.28 23.53 o 1 1 26 23.44 17.54 4.93 o 3 1 26 14.74 16.91 4.98 o 0 2 26 40.88 30.49 10.34 o 2 2 26 30.10 38.16 5.08 o 1 3 26 57.92 58.58 11.02 o 3 3 26 37.23 50.43 12.03 o 0 4 26 40.44 52.12 12.87 o 2 4 26 33.43 34.92 11.39 o 1 1 27 5.10 2.52 3.94 o 0 2 27 78.37 115.42 17.20 o 2 2 27 63.34 66.28 9.58 o 1 3 27 96.30 147.33 13.95 o 2 0 28 19.30 25.53 9.60 o 1 1 28 336.51 351.87 28.07 o 0 2 28 1.87 23.42 8.76 o