#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:26:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181046 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212631.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212631_Fobs loop_ _publ_author_name 'Wu, Hui-Lu' 'Ma, Xing-Ke' 'Lv, Wei-Bing' 'Liu, Peng' 'Liu, Ji-Gang' _publ_section_title ; (4-Hydroxycinnamato)[tris(N-methylbenzimidazol-2-ylmethyl)amine]copper(II) perchlorate dimethylformamide hemisolvate ; _journal_coeditor_code LH2300 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m783 _journal_page_last m784 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.034 _cell_angle_gamma 90.000 _cell_length_a 15.1645 _cell_length_b 13.1277 _cell_length_c 19.6013 _exptl_crystal_F_000 1684.00 _reflns_d_resolution_high 0.7488 _cod_data_source_file lh2300Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 431.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 11518.49 7509.91 96.97 o 4 0 0 37625.11 43355.83 281.80 o 5 0 0 1877.83 1940.96 66.43 o 6 0 0 15.06 237.87 37.50 o 7 0 0 470.30 600.02 54.64 o 8 0 0 640.72 816.99 63.22 o 9 0 0 3592.39 3056.36 109.83 o 10 0 0 27.92 18.75 39.11 o 11 0 0 3685.70 3655.84 133.93 o 12 0 0 1679.12 1484.52 100.18 o 13 0 0 884.33 990.04 90.54 o 14 0 0 2.90 -47.14 47.14 o 15 0 0 230.93 343.41 81.43 o 16 0 0 370.94 509.48 88.40 o 17 0 0 57.88 30.08 46.52 o 18 0 0 180.93 159.14 55.29 o 19 0 0 4.13 -47.67 47.67 o 20 0 0 72.50 43.93 79.82 o 1 1 0 102769.65 72972.00 5129.38 o 3 1 0 5584.95 3438.30 49.06 o 4 1 0 3993.41 2740.77 50.76 o 5 1 0 7501.87 6565.53 113.31 o 6 1 0 2474.42 1978.36 118.40 o 7 1 0 107.85 92.15 24.41 o 8 1 0 1864.48 1451.53 160.72 o 9 1 0 119.08 216.25 33.90 o 10 1 0 2566.07 2472.29 76.31 o 11 1 0 94.86 103.30 36.18 o 12 1 0 2961.29 2751.77 90.50 o 13 1 0 131.95 99.79 41.27 o 14 1 0 885.53 912.06 66.10 o 15 1 0 354.91 367.39 45.05 o 16 1 0 292.94 238.39 43.90 o 17 1 0 450.18 481.81 53.69 o 18 1 0 0.87 7.45 30.56 o 19 1 0 89.64 65.67 38.82 o 20 1 0 12.61 -1.27 43.13 o 1 2 0 4378.13 3081.92 30.50 o 2 2 0 3452.23 5347.54 1049.60 o 3 2 0 116629.55 136753.69 3101.47 o 4 2 0 2976.91 3348.95 47.73 o 5 2 0 11420.06 13196.53 121.03 o 6 2 0 786.88 486.79 28.27 o 7 2 0 1797.24 1573.90 54.36 o 8 2 0 287.93 384.26 38.93 o 9 2 0 247.50 291.87 37.45 o 10 2 0 97.92 63.88 31.43 o 11 2 0 1790.60 1978.34 75.19 o 12 2 0 203.20 226.22 36.14 o 13 2 0 51.50 102.13 33.22 o 14 2 0 47.40 62.15 31.16 o 15 2 0 26.37 -3.35 30.95 o 16 2 0 10.63 14.31 34.11 o 17 2 0 22.41 4.71 35.76 o 18 2 0 0.33 -35.83 35.86 o 19 2 0 4.78 -20.02 34.06 o 1 3 0 3762.64 5825.95 74.80 o 2 3 0 1549.94 1940.64 24.61 o 3 3 0 11362.46 13340.45 191.90 o 4 3 0 16767.21 15310.63 509.54 o 5 3 0 2894.13 3420.49 55.04 o 6 3 0 1670.01 1882.88 62.94 o 7 3 0 1005.88 1310.83 70.94 o 8 3 0 2.20 1.44 20.17 o 9 3 0 192.02 295.41 31.14 o 10 3 0 328.43 302.42 44.76 o 11 3 0 226.91 260.39 36.34 o 12 3 0 71.76 123.00 32.64 o 13 3 0 131.05 138.97 35.79 o 14 3 0 15.16 -18.86 27.83 o 15 3 0 5.16 -4.32 30.18 o 16 3 0 1.19 21.72 34.04 o 17 3 0 0.35 -11.09 36.83 o 18 3 0 45.44 88.60 44.00 o 19 3 0 14.69 41.91 42.93 o 0 4 0 75.84 36.53 12.94 o 1 4 0 85.58 46.45 11.88 o 2 4 0 6777.73 7162.29 49.72 o 3 4 0 605.08 756.55 20.02 o 4 4 0 4968.92 4221.89 117.76 o 5 4 0 7200.10 6589.17 78.94 o 6 4 0 1756.29 1855.58 48.12 o 7 4 0 1024.86 1163.09 42.80 o 8 4 0 6762.41 6531.57 194.19 o 9 4 0 1402.67 1250.87 47.88 o 10 4 0 0.49 -0.84 22.91 o 11 4 0 360.60 462.47 41.50 o 12 4 0 572.87 573.20 47.19 o 13 4 0 296.27 284.85 38.82 o 14 4 0 39.33 5.65 31.63 o 15 4 0 271.30 251.37 41.81 o 16 4 0 114.32 87.24 38.65 o 17 4 0 0.14 -3.22 35.43 o 18 4 0 68.08 73.42 44.03 o 19 4 0 1.68 -48.25 48.25 o 1 5 0 2669.98 3456.50 46.19 o 2 5 0 575.97 859.67 21.82 o 3 5 0 3657.27 3328.91 61.49 o 4 5 0 12027.12 11853.63 571.13 o 5 5 0 177.55 325.23 28.13 o 6 5 0 11624.27 13039.65 244.97 o 7 5 0 13323.07 14171.08 265.02 o 8 5 0 5152.01 5146.70 139.64 o 9 5 0 13.55 33.75 22.64 o 10 5 0 1236.78 1304.25 54.31 o 11 5 0 972.08 874.64 49.68 o 12 5 0 868.72 1021.06 54.11 o 13 5 0 1.70 0.80 28.27 o 14 5 0 171.40 139.59 36.56 o 15 5 0 57.06 105.82 38.77 o 16 5 0 60.54 26.14 35.92 o 17 5 0 187.02 172.71 44.22 o 18 5 0 1.83 -19.24 40.12 o 19 5 0 103.75 71.85 57.72 o 0 6 0 415.85 311.73 28.18 o 1 6 0 1678.38 1901.26 32.06 o 2 6 0 2324.55 1665.61 30.75 o 3 6 0 7280.50 7268.21 117.71 o 4 6 0 3989.46 4093.12 65.35 o 5 6 0 1695.71 1775.22 79.80 o 6 6 0 3926.67 2978.87 244.99 o 7 6 0 4961.03 4247.29 134.47 o 8 6 0 789.00 791.94 34.57 o 9 6 0 962.27 993.13 38.80 o 10 6 0 31.00 -2.76 25.49 o 11 6 0 5098.77 4616.12 189.85 o 12 6 0 62.22 74.83 33.01 o 13 6 0 54.16 101.71 34.98 o 14 6 0 34.78 -8.60 31.30 o 15 6 0 548.90 479.80 51.91 o 16 6 0 377.04 295.30 47.56 o 17 6 0 38.44 77.24 39.38 o 18 6 0 177.14 211.93 61.91 o 1 7 0 1826.91 1893.33 34.78 o 2 7 0 33.44 11.60 12.39 o 3 7 0 1254.99 1511.96 32.54 o 4 7 0 262.90 366.82 21.80 o 5 7 0 1142.64 1254.96 37.15 o 6 7 0 1027.91 1009.46 63.68 o 7 7 0 131.27 136.37 22.89 o 8 7 0 88.75 77.28 22.52 o 9 7 0 133.15 115.29 24.69 o 10 7 0 2542.94 2588.88 135.63 o 11 7 0 1401.58 1472.87 62.06 o 12 7 0 84.31 91.31 33.07 o 13 7 0 0.13 7.45 31.69 o 14 7 0 849.27 852.45 59.50 o 15 7 0 228.05 224.75 45.15 o 16 7 0 208.97 170.71 42.76 o 17 7 0 93.01 77.92 44.79 o 18 7 0 49.17 82.10 53.58 o 0 8 0 7734.30 8502.81 115.67 o 1 8 0 1798.40 1880.71 41.73 o 2 8 0 157.18 99.29 16.53 o 3 8 0 1264.93 1313.54 33.44 o 4 8 0 47.22 22.15 15.72 o 5 8 0 112.99 75.15 20.74 o 6 8 0 2.39 4.05 18.98 o 7 8 0 93.05 124.35 25.67 o 8 8 0 293.47 330.62 49.57 o 9 8 0 33.98 6.92 27.14 o 10 8 0 889.47 823.87 50.24 o 11 8 0 7.16 -26.32 26.32 o 12 8 0 14.05 -22.24 27.78 o 13 8 0 196.34 212.34 41.32 o 14 8 0 150.16 154.63 55.48 o 15 8 0 16.09 10.30 36.48 o 16 8 0 5.07 -5.23 37.94 o 17 8 0 9.12 -18.69 39.78 o 1 9 0 913.79 905.20 34.69 o 2 9 0 985.05 948.28 31.13 o 3 9 0 69.43 83.40 17.70 o 4 9 0 619.02 647.09 29.02 o 5 9 0 1179.21 1118.95 40.78 o 6 9 0 483.17 521.77 34.59 o 7 9 0 0.15 -2.31 24.98 o 8 9 0 329.98 236.01 35.05 o 9 9 0 503.84 435.80 159.17 o 10 9 0 408.91 432.96 45.40 o 11 9 0 267.14 346.18 43.02 o 12 9 0 34.08 37.85 32.88 o 13 9 0 3.49 -0.14 33.13 o 14 9 0 50.96 40.44 40.35 o 15 9 0 3.35 -20.75 35.34 o 16 9 0 1.08 -33.35 38.57 o 17 9 0 5.44 11.91 52.26 o 0 10 0 2222.10 2703.13 77.43 o 1 10 0 138.95 153.87 23.81 o 2 10 0 967.84 983.86 38.07 o 3 10 0 18.01 12.25 17.17 o 4 10 0 1395.60 1284.51 38.25 o 5 10 0 64.63 61.05 27.03 o 6 10 0 367.45 408.62 41.43 o 7 10 0 219.70 213.84 36.58 o 8 10 0 203.15 236.93 38.63 o 9 10 0 313.65 454.08 46.60 o 10 10 0 134.54 143.49 86.01 o 11 10 0 136.68 85.45 36.31 o 12 10 0 74.89 37.83 33.90 o 13 10 0 221.63 195.32 43.24 o 14 10 0 27.91 52.89 39.38 o 15 10 0 56.40 -11.95 39.93 o 16 10 0 79.87 78.61 46.43 o 1 11 0 259.77 264.95 27.25 o 2 11 0 164.36 141.64 25.18 o 3 11 0 519.64 555.18 37.35 o 4 11 0 223.92 143.98 25.76 o 5 11 0 328.34 422.86 43.30 o 6 11 0 858.45 869.96 64.29 o 7 11 0 261.81 307.95 40.67 o 8 11 0 566.56 676.69 53.63 o 9 11 0 2.58 -3.64 31.39 o 10 11 0 359.47 383.97 47.55 o 11 11 0 12.84 -26.06 27.94 o 12 11 0 286.65 274.71 47.20 o 13 11 0 143.54 122.55 42.72 o 14 11 0 37.85 49.77 41.50 o 15 11 0 57.44 90.96 40.19 o 0 12 0 432.31 459.12 84.11 o 1 12 0 51.56 52.09 37.28 o 2 12 0 152.62 130.81 43.39 o 3 12 0 3.91 -33.86 33.86 o 4 12 0 355.30 327.35 51.58 o 5 12 0 777.11 917.28 68.49 o 6 12 0 407.10 413.20 57.66 o 7 12 0 909.40 980.22 71.07 o 8 12 0 53.89 48.97 41.85 o 9 12 0 53.42 -23.63 41.79 o 10 12 0 105.74 102.27 47.73 o 11 12 0 171.92 174.15 53.62 o 12 12 0 23.00 62.03 51.04 o 13 12 0 22.73 53.53 52.08 o 14 12 0 22.35 -26.40 48.97 o 1 13 0 76.15 79.66 40.72 o 2 13 0 99.86 110.45 42.03 o 3 13 0 27.93 -11.79 37.88 o 4 13 0 10.87 -2.51 38.52 o 5 13 0 42.05 101.33 56.25 o 6 13 0 224.50 246.81 53.73 o 7 13 0 145.97 125.10 47.45 o 8 13 0 147.19 125.53 49.57 o 9 13 0 0.16 -24.56 42.18 o 10 13 0 4.34 15.46 46.90 o 11 13 0 17.59 17.31 47.19 o 12 13 0 48.26 42.14 51.94 o 13 13 0 1.10 -14.05 50.34 o 0 14 0 0.32 25.18 61.61 o 1 14 0 101.19 117.33 47.92 o 2 14 0 44.08 3.45 38.74 o 3 14 0 88.13 11.79 42.59 o 4 14 0 0.29 -10.02 41.09 o 5 14 0 57.59 92.26 46.96 o 6 14 0 5.48 -39.74 39.74 o 7 14 0 2.61 0.57 41.54 o 8 14 0 13.08 29.96 57.06 o 9 14 0 0.36 -15.25 46.40 o 10 14 0 2.53 -39.04 46.00 o 11 14 0 24.62 37.00 50.72 o 12 14 0 21.98 24.60 54.06 o 1 15 0 112.90 157.17 53.98 o 2 15 0 27.20 27.77 43.98 o 3 15 0 102.84 122.97 50.69 o 4 15 0 26.84 5.61 43.75 o 5 15 0 10.30 -2.30 45.38 o 6 15 0 0.84 -40.40 40.40 o 7 15 0 83.34 68.14 49.81 o 8 15 0 194.95 140.08 68.57 o 9 15 0 0.26 -50.09 50.09 o 10 15 0 1.62 -38.59 52.26 o 0 16 0 189.12 78.22 73.40 o 1 16 0 0.43 -42.25 46.91 o 2 16 0 157.71 184.89 56.81 o 3 16 0 0.51 -6.35 45.59 o 4 16 0 13.57 54.79 48.62 o 5 16 0 5.40 55.63 48.13 o 6 16 0 18.42 47.80 48.80 o 7 16 0 70.19 63.59 52.06 o 8 16 0 5.94 17.91 54.11 o 1 17 0 61.07 46.48 53.04 o 2 17 0 16.19 -25.68 48.65 o 3 17 0 113.57 147.07 57.87 o 4 17 0 0.35 41.23 53.22 o -20 1 1 61.41 48.41 38.80 o -19 1 1 19.96 27.26 37.39 o -18 1 1 103.41 57.85 39.02 o -17 1 1 5.11 -24.62 34.87 o -16 1 1 129.00 177.75 52.34 o -15 1 1 501.11 549.77 63.25 o -14 1 1 6.57 13.10 36.92 o -13 1 1 1.50 -43.39 53.31 o -12 1 1 245.67 300.06 76.88 o -11 1 1 5163.21 5442.98 187.24 o -10 1 1 6.76 -6.84 27.24 o -9 1 1 39.15 48.23 27.58 o -8 1 1 1194.03 1494.70 56.25 o -7 1 1 5600.38 5707.70 131.79 o -6 1 1 3814.33 3148.39 66.29 o -5 1 1 3268.57 3132.41 61.37 o -4 1 1 7700.23 9290.54 109.29 o -3 1 1 7252.75 5777.96 65.53 o -2 1 1 8582.99 8125.52 390.68 o 0 1 1 2814.86 1648.86 105.43 o 1 1 1 6692.92 3373.71 846.75 o 2 1 1 7993.69 5677.54 2216.39 o 3 1 1 3621.26 1788.20 587.06 o 4 1 1 984.59 809.85 198.04 o 5 1 1 118.20 295.32 29.47 o 6 1 1 1600.91 1186.96 48.48 o 7 1 1 8158.64 7406.55 99.79 o 8 1 1 216.62 244.92 33.34 o 9 1 1 3293.22 3407.47 81.06 o 10 1 1 13.93 11.49 26.70 o 11 1 1 766.23 630.57 52.47 o 12 1 1 1.70 -8.75 25.20 o 13 1 1 23.23 27.13 27.89 o 14 1 1 638.29 758.12 54.17 o 15 1 1 1.48 -15.07 31.04 o 16 1 1 22.94 22.05 29.06 o 17 1 1 1.31 -9.91 29.63 o 18 1 1 176.46 177.39 39.50 o 19 1 1 2.39 -9.86 39.42 o -20 2 1 5.77 -29.24 35.54 o -19 2 1 84.16 29.63 42.62 o -18 2 1 88.05 24.10 38.56 o -17 2 1 519.89 552.96 56.09 o -16 2 1 179.02 181.02 42.23 o -15 2 1 68.00 69.53 33.66 o -14 2 1 223.39 212.80 48.07 o -13 2 1 111.97 146.85 42.14 o -12 2 1 1601.69 1808.42 77.84 o -11 2 1 10.17 -0.54 31.82 o -10 2 1 3837.84 3691.48 94.70 o -9 2 1 92.30 166.71 33.28 o -8 2 1 5488.74 6063.60 181.35 o -7 2 1 95.27 248.01 32.31 o -6 2 1 90.81 371.33 33.33 o -5 2 1 15440.56 17905.35 285.01 o -4 2 1 34998.86 36714.06 5455.91 o -3 2 1 46134.52 49096.52 3564.50 o -2 2 1 3896.45 2393.71 34.56 o -1 2 1 9395.46 10304.45 1519.29 o 0 2 1 10792.25 14750.82 198.11 o 3 2 1 11806.18 11613.68 312.01 o 4 2 1 41969.71 50278.75 931.18 o 5 2 1 8644.88 9806.19 89.50 o 6 2 1 1762.93 2441.14 57.66 o 7 2 1 1375.13 1001.91 37.38 o 8 2 1 23779.31 25579.63 863.83 o 9 2 1 113.30 62.36 22.61 o 10 2 1 785.62 738.81 67.55 o 11 2 1 13.48 1.47 23.92 o 12 2 1 385.21 444.94 40.78 o 13 2 1 688.87 687.18 49.47 o 14 2 1 47.82 30.90 29.64 o 15 2 1 168.79 146.96 36.89 o 16 2 1 208.01 233.01 41.97 o 17 2 1 312.33 358.17 50.16 o 18 2 1 0.51 -8.66 32.73 o 19 2 1 64.13 72.94 45.15 o -19 3 1 31.68 -5.42 42.60 o -18 3 1 164.24 91.78 43.68 o -17 3 1 121.83 131.38 43.77 o -16 3 1 165.25 183.03 42.60 o -15 3 1 554.71 679.24 55.98 o -14 3 1 24.26 4.67 36.46 o -13 3 1 456.02 489.58 63.54 o -12 3 1 121.87 169.42 35.58 o -11 3 1 2990.65 2826.63 72.98 o -10 3 1 181.85 240.94 40.91 o -9 3 1 3559.76 3669.30 90.90 o -8 3 1 3655.78 3389.92 83.34 o -7 3 1 2849.23 2393.95 68.00 o -6 3 1 7825.14 7953.80 109.48 o -5 3 1 285.93 434.88 26.50 o -4 3 1 15542.58 18630.48 1195.22 o -2 3 1 5824.34 5215.36 765.78 o -1 3 1 15451.00 18062.60 457.76 o 0 3 1 6065.52 5655.75 84.27 o 1 3 1 2178.42 1427.70 28.53 o 2 3 1 1843.38 2545.04 56.37 o 3 3 1 10284.64 8159.87 60.15 o 4 3 1 14417.00 15510.60 141.16 o 5 3 1 4141.46 3021.45 152.81 o 6 3 1 251.68 344.08 28.19 o 7 3 1 12047.97 11897.42 240.97 o 8 3 1 107.99 98.23 22.58 o 9 3 1 6702.88 6400.47 134.59 o 10 3 1 93.38 36.23 24.69 o 11 3 1 2510.14 2416.18 67.53 o 12 3 1 2222.05 2148.30 67.59 o 13 3 1 32.92 14.18 28.61 o 14 3 1 193.51 192.69 39.18 o 15 3 1 646.62 697.16 56.23 o 16 3 1 412.91 497.02 51.86 o 17 3 1 5.32 7.15 35.37 o 18 3 1 44.18 12.86 44.75 o 19 3 1 27.47 56.08 41.69 o -19 4 1 80.49 102.39 46.91 o -18 4 1 11.09 -32.21 39.55 o -17 4 1 177.64 196.18 45.09 o -16 4 1 17.57 -12.44 35.01 o -15 4 1 106.46 112.19 37.35 o -14 4 1 838.47 801.05 53.59 o -13 4 1 0.28 -1.40 26.99 o -12 4 1 197.61 271.11 38.19 o -11 4 1 1.02 -13.24 26.03 o -10 4 1 955.98 959.26 56.01 o -9 4 1 2381.70 2385.19 61.78 o -8 4 1 2045.47 2082.65 103.36 o -7 4 1 17657.80 16847.55 783.86 o -6 4 1 19214.41 19213.49 171.11 o -5 4 1 2161.01 2353.85 63.23 o -4 4 1 955.80 747.88 20.38 o -3 4 1 674.47 570.25 99.42 o -2 4 1 1709.11 2330.25 28.91 o -1 4 1 150.61 244.59 13.91 o 0 4 1 1797.31 2474.94 29.62 o 1 4 1 2865.87 2488.61 42.98 o 2 4 1 6563.78 6824.48 99.67 o 3 4 1 8.59 21.53 11.94 o 4 4 1 5803.02 7801.41 76.46 o 5 4 1 10292.38 8249.75 185.49 o 6 4 1 3972.15 3244.07 60.50 o 7 4 1 7573.15 8066.66 261.86 o 8 4 1 6215.85 5925.80 108.48 o 9 4 1 2.76 -16.85 21.71 o 10 4 1 3004.15 2742.93 69.78 o 11 4 1 650.80 633.19 44.42 o 12 4 1 196.63 171.32 39.93 o 13 4 1 2.42 9.11 29.74 o 14 4 1 452.11 477.67 47.03 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